#------------------------------------------------------------------------------ #$Date: 2013-10-24 17:51:33 +0300 (Thu, 24 Oct 2013) $ #$Revision: 89414 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/85/2238518.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238518_Fobs loop_ _publ_author_name 'Zukerman-Schpector, Julio' 'Hino, Camila Lury' 'Moran, Paulo J. S.' 'de Paula, Bruno R. S.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; Ethyl (2Z)-3-oxo-2-(3,4,5-trimethoxybenzylidene)butanoate ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1474 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 61.130 _cell_angle_beta 77.450 _cell_angle_gamma 82.534 _cell_length_a 8.3432 _cell_length_b 10.2446 _cell_length_c 10.4543 _exptl_crystal_F_000 328.00 _reflns_d_resolution_high 0.7945 _[local]_cod_data_source_file kj2231Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' b in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 74.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 100.39 102.31 1.96 o 2 0 0 1418.84 1368.55 6.26 o 3 0 0 846.67 748.53 6.02 o 4 0 0 33.76 32.72 1.47 o 5 0 0 532.47 518.82 6.59 o 6 0 0 9.20 11.08 1.08 o 7 0 0 67.20 66.82 2.57 o 8 0 0 89.70 100.68 2.27 o 9 0 0 2.64 1.70 0.29 o 10 0 0 125.40 112.61 2.05 o -10 1 0 1.26 1.10 0.21 o -9 1 0 195.96 193.03 2.77 o -8 1 0 20.58 20.73 1.58 o -7 1 0 30.16 32.29 1.98 o -6 1 0 34.70 32.24 1.91 o -5 1 0 125.55 118.95 3.36 o -4 1 0 31.99 27.24 1.29 o -3 1 0 14.91 25.87 1.04 o -2 1 0 109.39 93.52 1.55 o 1 1 0 371.90 353.37 1.52 o 2 1 0 58.71 51.59 1.07 o 3 1 0 342.64 348.02 2.56 o 4 1 0 125.67 132.72 2.84 o 5 1 0 22.93 27.25 1.47 o 6 1 0 29.48 34.62 1.83 o 7 1 0 31.42 35.11 1.93 o 8 1 0 0.10 0.23 0.25 o 9 1 0 132.00 131.81 2.25 o 10 1 0 86.68 76.04 1.67 o -9 2 0 155.06 155.85 3.87 o -8 2 0 161.10 164.13 4.34 o -7 2 0 22.19 23.65 1.72 o -6 2 0 135.21 132.89 2.74 o -5 2 0 17.53 13.15 1.07 o -4 2 0 190.50 180.63 3.33 o -3 2 0 310.62 316.86 3.67 o -2 2 0 114.93 139.71 2.04 o -1 2 0 145.42 133.36 0.85 o 0 2 0 377.94 328.07 2.55 o 1 2 0 284.47 255.82 2.41 o 2 2 0 90.09 81.22 1.07 o 3 2 0 22.75 22.11 0.68 o 4 2 0 192.96 196.06 2.26 o 5 2 0 136.29 122.87 3.09 o 6 2 0 108.72 122.48 2.42 o 7 2 0 0.46 0.75 0.40 o 8 2 0 2.80 3.99 0.69 o 9 2 0 4.13 6.02 0.49 o -9 3 0 23.31 22.24 0.88 o -8 3 0 4.53 4.03 0.50 o -7 3 0 32.36 34.86 2.10 o -6 3 0 6.52 7.30 0.71 o -5 3 0 39.82 46.30 2.05 o -4 3 0 513.77 551.34 5.99 o -3 3 0 20.58 27.81 1.18 o -2 3 0 1324.50 1314.48 7.18 o -1 3 0 23.11 15.08 0.42 o 0 3 0 602.01 579.84 9.08 o 1 3 0 164.87 156.56 2.34 o 2 3 0 988.91 902.94 4.11 o 3 3 0 61.74 57.36 1.15 o 4 3 0 76.16 79.38 1.52 o 5 3 0 167.46 179.20 3.86 o 6 3 0 2.75 3.35 0.43 o 7 3 0 32.41 40.90 2.20 o 8 3 0 58.00 60.63 2.53 o 9 3 0 59.42 59.39 2.03 o -9 4 0 0.08 0.02 0.18 o -8 4 0 0.19 0.28 0.20 o -7 4 0 2.74 2.38 0.61 o -6 4 0 148.22 149.27 4.28 o -5 4 0 214.52 239.04 9.25 o -4 4 0 39.83 42.52 1.79 o -3 4 0 219.03 244.76 3.88 o -2 4 0 2157.78 2151.51 10.52 o -1 4 0 170.13 174.88 2.88 o 0 4 0 718.40 721.57 5.75 o 1 4 0 113.32 120.78 2.45 o 2 4 0 4.34 8.61 2.69 o 3 4 0 191.14 207.91 2.42 o 4 4 0 505.09 520.95 6.41 o 5 4 0 0.01 0.89 0.34 o 6 4 0 1.78 2.01 0.55 o 7 4 0 68.13 74.55 2.97 o 8 4 0 15.07 15.43 1.27 o 9 4 0 1.70 2.20 0.41 o -9 5 0 83.72 77.19 1.53 o -8 5 0 89.39 91.61 2.59 o -7 5 0 7.78 7.20 0.88 o -6 5 0 3.89 4.68 0.76 o -5 5 0 7.51 10.53 0.83 o -4 5 0 37.95 42.86 1.93 o -3 5 0 6.26 3.68 0.56 o -2 5 0 543.74 544.45 5.99 o -1 5 0 112.34 139.57 2.95 o 0 5 0 876.41 900.79 7.38 o 1 5 0 414.12 440.96 5.26 o 2 5 0 335.63 342.67 3.30 o 3 5 0 107.27 112.29 1.97 o 4 5 0 96.05 83.87 2.80 o 5 5 0 1.78 1.81 0.28 o 6 5 0 3.98 5.71 0.59 o 7 5 0 189.45 202.68 4.73 o 8 5 0 63.58 70.92 2.47 o 9 5 0 23.18 23.31 1.03 o -8 6 0 129.63 122.57 1.93 o -7 6 0 0.26 0.16 0.22 o -6 6 0 0.58 1.00 0.38 o -5 6 0 5.91 6.82 0.58 o -4 6 0 86.99 92.78 3.29 o -3 6 0 17.61 19.27 0.95 o -2 6 0 365.26 362.98 5.40 o -1 6 0 246.27 282.63 4.72 o 0 6 0 227.19 246.15 4.35 o 1 6 0 224.01 223.46 4.20 o 2 6 0 225.64 217.58 2.91 o 3 6 0 10.09 10.93 1.05 o 4 6 0 35.45 34.60 1.08 o 5 6 0 645.95 634.26 5.93 o 6 6 0 304.42 303.62 4.06 o 7 6 0 52.15 53.22 2.23 o 8 6 0 8.89 8.99 0.80 o -7 7 0 41.93 40.19 1.68 o -6 7 0 58.02 57.75 2.43 o -5 7 0 5.29 5.72 0.74 o -4 7 0 102.68 93.68 3.18 o -3 7 0 11.92 13.54 0.88 o -2 7 0 22.80 23.81 0.90 o -1 7 0 71.88 74.26 1.89 o 0 7 0 2.69 1.24 0.26 o 1 7 0 129.63 133.84 2.41 o 2 7 0 398.85 397.13 5.80 o 3 7 0 123.15 130.39 4.18 o 4 7 0 3.18 2.58 0.39 o 5 7 0 124.69 124.44 2.59 o 6 7 0 123.54 123.98 2.39 o 7 7 0 8.75 7.88 0.75 o 8 7 0 51.39 46.82 1.38 o -7 8 0 18.04 15.56 0.70 o -6 8 0 60.31 61.48 2.03 o -5 8 0 55.52 49.08 1.41 o -4 8 0 127.63 118.12 2.46 o -3 8 0 163.09 159.97 2.96 o -2 8 0 178.42 158.86 3.39 o -1 8 0 158.27 148.05 4.08 o 0 8 0 226.15 210.34 3.29 o 1 8 0 350.74 341.21 4.05 o 2 8 0 736.27 713.74 8.59 o 3 8 0 160.12 152.92 2.71 o 4 8 0 95.88 93.65 2.15 o 5 8 0 297.30 304.93 3.69 o 6 8 0 57.29 53.50 1.30 o 7 8 0 8.61 7.75 0.59 o -5 9 0 0.14 0.24 0.13 o -4 9 0 21.22 20.45 1.19 o -3 9 0 0.05 0.19 0.19 o -2 9 0 15.47 20.99 0.80 o -1 9 0 0.68 0.64 0.26 o 0 9 0 102.42 97.61 2.20 o 1 9 0 16.17 13.75 1.23 o 2 9 0 5.71 4.15 0.71 o 3 9 0 1.39 1.91 0.49 o 4 9 0 122.23 128.71 3.41 o 5 9 0 25.25 25.06 0.83 o 6 9 0 39.38 32.65 1.02 o -4 10 0 55.57 54.53 1.44 o -3 10 0 0.43 0.61 0.21 o -2 10 0 4.21 2.51 0.46 o -1 10 0 14.73 19.57 1.29 o 0 10 0 10.85 9.19 0.91 o 1 10 0 25.00 32.85 1.71 o 2 10 0 0.00 -0.14 0.30 o 3 10 0 0.27 0.80 0.32 o 4 10 0 15.57 18.01 1.02 o -1 11 0 10.59 12.84 0.50 o 0 11 0 113.91 125.59 2.64 o 1 11 0 68.03 79.32 2.13 o 2 11 0 9.43 9.51 0.70 o -3 -10 1 13.00 16.06 0.98 o -2 -10 1 4.17 3.98 0.57 o -1 -10 1 3.13 3.67 0.55 o 0 -10 1 18.29 15.64 0.68 o 1 -10 1 1.85 2.85 0.31 o 2 -10 1 35.07 32.63 1.95 o 3 -10 1 31.18 33.41 1.19 o -5 -9 1 49.85 49.26 1.52 o -4 -9 1 4.95 4.69 0.64 o -3 -9 1 1.59 2.54 0.54 o -2 -9 1 129.75 122.42 3.48 o -1 -9 1 0.00 0.21 0.21 o 0 -9 1 3.18 5.47 0.75 o 1 -9 1 4.60 4.17 0.68 o 2 -9 1 21.78 18.57 1.03 o 3 -9 1 73.63 75.33 4.01 o 4 -9 1 0.46 0.27 0.14 o 5 -9 1 72.21 69.95 1.60 o -6 -8 1 8.16 7.68 0.62 o -5 -8 1 298.21 299.61 5.08 o -4 -8 1 395.24 399.59 6.50 o -3 -8 1 138.54 148.58 4.07 o -2 -8 1 24.98 26.93 1.73 o -1 -8 1 26.77 23.51 1.60 o 0 -8 1 76.23 59.10 1.75 o 1 -8 1 93.81 87.42 1.72 o 2 -8 1 1.67 0.77 0.20 o 3 -8 1 60.31 52.51 1.66 o 4 -8 1 29.62 27.47 2.23 o 5 -8 1 10.96 9.05 0.87 o 6 -8 1 16.25 13.57 0.87 o -7 -7 1 28.11 26.83 1.23 o -6 -7 1 35.88 33.67 1.11 o -5 -7 1 63.97 68.04 1.82 o -4 -7 1 412.09 403.32 5.62 o -3 -7 1 7.60 11.44 1.16 o -2 -7 1 45.84 49.00 2.25 o -1 -7 1 97.59 99.50 4.20 o 0 -7 1 11.64 7.86 0.44 o 1 -7 1 0.87 1.89 0.36 o 2 -7 1 34.55 24.85 1.18 o 3 -7 1 13.16 9.96 0.78 o 4 -7 1 163.52 151.06 3.22 o 5 -7 1 46.48 39.61 1.39 o 6 -7 1 136.24 128.59 3.45 o 7 -7 1 0.03 0.01 0.15 o -8 -6 1 61.96 62.13 1.70 o -7 -6 1 70.74 71.06 2.14 o -6 -6 1 153.28 145.71 2.69 o -5 -6 1 96.87 97.46 2.35 o -4 -6 1 27.27 23.93 1.13 o -3 -6 1 8.66 9.65 0.73 o -2 -6 1 3.55 3.30 0.40 o -1 -6 1 663.53 690.19 7.93 o 0 -6 1 7.13 6.20 0.76 o 1 -6 1 188.90 181.61 4.01 o 2 -6 1 231.01 226.66 3.26 o 3 -6 1 34.49 35.09 1.10 o 4 -6 1 183.67 193.72 4.51 o 5 -6 1 0.02 2.52 0.51 o 6 -6 1 97.73 99.89 2.87 o 7 -6 1 59.80 59.79 1.50 o 8 -6 1 5.68 4.68 0.30 o -8 -5 1 121.21 123.97 2.87 o -7 -5 1 289.88 291.04 4.99 o -6 -5 1 101.17 97.94 2.36 o -5 -5 1 47.09 42.30 1.56 o -4 -5 1 26.91 26.97 0.95 o -3 -5 1 2.27 3.02 0.58 o -2 -5 1 0.92 2.90 0.53 o -1 -5 1 84.54 81.24 2.49 o 0 -5 1 49.96 57.58 2.05 o 1 -5 1 334.07 365.85 5.14 o 2 -5 1 205.78 212.82 3.98 o 3 -5 1 704.88 705.11 7.52 o 4 -5 1 0.71 0.53 0.28 o 5 -5 1 91.65 92.48 3.02 o 6 -5 1 4.23 5.14 0.77 o 7 -5 1 339.40 340.64 5.68 o 8 -5 1 160.40 153.64 2.31 o -9 -4 1 3.31 3.37 0.29 o -8 -4 1 5.53 5.45 0.71 o -7 -4 1 241.14 260.66 5.00 o -6 -4 1 153.86 158.71 3.04 o -5 -4 1 202.57 207.60 2.98 o -4 -4 1 2.65 5.46 0.73 o -3 -4 1 11.88 12.65 1.02 o -2 -4 1 420.08 432.80 3.35 o -1 -4 1 107.66 99.32 1.50 o 0 -4 1 890.55 942.26 4.06 o 1 -4 1 606.77 622.91 5.96 o 2 -4 1 32.55 44.14 1.61 o 3 -4 1 53.12 68.12 2.12 o 4 -4 1 334.32 343.09 5.19 o 5 -4 1 55.60 55.35 1.35 o 6 -4 1 2.39 3.81 0.50 o 7 -4 1 31.73 31.12 1.90 o 8 -4 1 6.69 6.64 0.81 o 9 -4 1 154.88 142.27 10.18 o -9 -3 1 78.78 80.79 2.06 o -8 -3 1 51.02 49.52 2.13 o -7 -3 1 26.61 30.83 1.77 o -6 -3 1 145.00 152.21 2.90 o -5 -3 1 151.92 145.79 3.68 o -4 -3 1 85.46 86.39 2.59 o -3 -3 1 13.20 11.79 0.88 o -2 -3 1 479.47 499.36 5.23 o -1 -3 1 116.70 130.17 2.43 o 0 -3 1 3376.26 3221.39 11.56 o 1 -3 1 0.07 1.56 0.32 o 2 -3 1 1129.02 1170.70 4.00 o 3 -3 1 391.41 417.05 4.71 o 4 -3 1 86.33 83.78 2.37 o 5 -3 1 97.79 103.43 2.95 o 6 -3 1 1.31 1.09 0.28 o 7 -3 1 75.94 75.07 2.13 o 8 -3 1 176.70 181.57 3.07 o 9 -3 1 270.82 270.86 4.32 o -9 -2 1 0.11 0.47 0.18 o -8 -2 1 6.06 7.10 0.85 o -7 -2 1 70.49 70.26 2.62 o -6 -2 1 87.16 90.95 1.75 o -5 -2 1 221.74 204.60 4.12 o -4 -2 1 79.84 74.08 2.21 o -3 -2 1 54.80 48.82 0.95 o -2 -2 1 4.75 5.53 0.38 o -1 -2 1 184.97 158.43 2.22 o 0 -2 1 197.87 203.88 8.08 o 1 -2 1 1021.74 921.98 11.51 o 2 -2 1 131.12 119.94 1.23 o 3 -2 1 79.92 72.75 1.76 o 4 -2 1 122.40 132.34 2.77 o 5 -2 1 147.04 164.49 3.65 o 6 -2 1 76.30 89.06 2.28 o 7 -2 1 51.71 53.69 2.52 o 8 -2 1 53.78 53.85 1.73 o 9 -2 1 14.28 13.87 1.24 o -9 -1 1 3.17 3.93 0.62 o -8 -1 1 0.01 0.23 0.24 o -7 -1 1 11.96 11.77 1.11 o -6 -1 1 116.00 121.26 3.36 o -5 -1 1 63.43 77.56 2.47 o -4 -1 1 146.01 149.41 3.03 o -3 -1 1 414.88 410.33 2.31 o -2 -1 1 147.30 181.04 1.38 o -1 -1 1 330.34 353.97 2.27 o 0 -1 1 8.06 8.15 0.79 o 1 -1 1 109.11 110.69 1.46 o 3 -1 1 388.46 382.24 3.79 o 4 -1 1 457.11 482.93 5.21 o 5 -1 1 78.72 83.10 1.91 o 6 -1 1 1.09 1.87 0.53 o 7 -1 1 249.47 241.55 3.54 o 8 -1 1 12.11 11.32 0.64 o 9 -1 1 8.88 9.18 0.62 o 10 -1 1 86.11 67.87 1.41 o -10 0 1 0.06 0.01 0.10 o -9 0 1 0.08 0.38 0.15 o -8 0 1 68.65 70.85 2.88 o -7 0 1 10.53 10.64 1.00 o -6 0 1 17.47 19.12 1.37 o -5 0 1 0.50 0.58 0.29 o -4 0 1 164.18 167.70 3.24 o -3 0 1 937.85 880.49 6.34 o 1 0 1 194.06 182.91 3.74 o 2 0 1 2883.98 2626.30 7.61 o 3 0 1 5.95 6.18 0.52 o 4 0 1 1059.96 1043.19 8.53 o 5 0 1 117.95 116.95 3.26 o 6 0 1 115.08 118.51 3.56 o 7 0 1 284.99 292.38 4.04 o 8 0 1 5.47 5.33 0.45 o 9 0 1 179.98 190.79 2.19 o 10 0 1 17.72 15.54 0.74 o -9 1 1 0.07 0.41 0.18 o -8 1 1 1.32 2.01 0.59 o -7 1 1 60.42 63.35 2.80 o -6 1 1 0.33 0.83 0.42 o -5 1 1 210.10 195.61 4.14 o -4 1 1 70.41 72.14 2.24 o -3 1 1 13.31 18.86 1.94 o -1 1 1 1309.19 1240.74 4.37 o 0 1 1 456.14 413.10 1.43 o 1 1 1 978.10 874.85 13.35 o 2 1 1 1737.22 1471.62 6.47 o 3 1 1 332.00 306.35 4.03 o 4 1 1 0.27 0.29 0.23 o 5 1 1 37.46 42.86 1.88 o 6 1 1 86.64 94.34 3.02 o 7 1 1 270.70 275.31 7.25 o 8 1 1 200.72 210.81 2.68 o 9 1 1 41.08 41.41 1.31 o 10 1 1 23.11 19.57 0.84 o -9 2 1 59.67 58.71 2.21 o -8 2 1 25.16 30.28 1.88 o -7 2 1 384.17 386.98 6.90 o -6 2 1 3.55 4.56 1.38 o -5 2 1 156.33 153.73 3.88 o -4 2 1 12.04 19.73 1.16 o -3 2 1 1068.19 1135.72 7.17 o -1 2 1 1428.58 1254.16 4.84 o 1 2 1 422.83 410.93 1.60 o 2 2 1 124.07 139.89 1.39 o 3 2 1 18.54 13.44 0.53 o 4 2 1 702.27 699.23 12.86 o 5 2 1 222.57 206.07 3.94 o 6 2 1 21.64 21.10 1.42 o 7 2 1 106.74 106.47 2.43 o 8 2 1 37.11 43.25 2.23 o 9 2 1 118.15 115.01 2.19 o 10 2 1 1.56 1.37 0.23 o -9 3 1 86.67 86.80 1.69 o -8 3 1 104.08 108.80 3.46 o -7 3 1 7.59 8.59 1.10 o -6 3 1 23.84 28.38 1.03 o -5 3 1 3.04 3.33 0.44 o -4 3 1 704.21 775.07 7.26 o -3 3 1 32.91 33.68 1.28 o -2 3 1 42.63 38.71 1.17 o -1 3 1 90.97 104.05 1.69 o 1 3 1 31.35 37.40 0.56 o 2 3 1 183.38 182.57 1.79 o 3 3 1 584.78 560.11 3.55 o 4 3 1 3.65 7.47 0.49 o 5 3 1 139.19 156.67 2.69 o 6 3 1 169.54 157.00 5.49 o 7 3 1 113.50 111.02 2.54 o 8 3 1 24.15 23.48 1.67 o 9 3 1 55.55 54.41 1.48 o 10 3 1 0.05 -0.05 0.10 o -9 4 1 8.48 6.79 0.61 o -8 4 1 11.70 11.00 0.75 o -7 4 1 55.51 54.60 2.62 o -6 4 1 110.63 112.73 2.55 o -5 4 1 84.17 117.32 3.39 o -4 4 1 826.28 864.40 7.97 o -3 4 1 3.47 4.40 0.52 o -2 4 1 306.74 299.75 3.67 o -1 4 1 6.10 7.88 0.57 o 0 4 1 54.70 45.87 1.31 o 1 4 1 116.35 118.77 1.20 o 2 4 1 1822.47 1807.95 7.59 o 3 4 1 175.95 169.13 2.15 o 4 4 1 96.70 92.43 1.76 o 5 4 1 387.41 425.05 5.31 o 6 4 1 18.81 18.37 0.98 o 7 4 1 5.09 6.30 0.92 o 8 4 1 17.42 16.76 1.37 o 9 4 1 5.39 6.34 0.71 o -9 5 1 0.88 0.92 0.20 o -8 5 1 17.30 19.00 1.20 o -7 5 1 2.85 3.61 0.71 o -6 5 1 31.29 31.02 1.38 o -5 5 1 30.88 26.17 0.99 o -4 5 1 204.37 225.25 4.34 o -3 5 1 0.58 0.62 0.25 o -2 5 1 50.89 49.75 1.71 o -1 5 1 3.38 4.29 0.51 o 0 5 1 2.19 1.72 0.33 o 1 5 1 21.12 19.21 1.01 o 2 5 1 784.75 745.73 4.70 o 3 5 1 46.12 51.48 1.32 o 4 5 1 335.72 353.85 3.69 o 5 5 1 309.52 343.30 7.29 o 6 5 1 11.88 12.51 1.24 o 7 5 1 67.53 68.50 2.85 o 8 5 1 9.69 9.72 1.02 o 9 5 1 17.57 18.97 1.10 o -8 6 1 5.48 6.36 0.56 o -7 6 1 2.59 3.59 0.56 o -6 6 1 169.39 170.34 4.08 o -5 6 1 43.84 45.58 2.36 o -4 6 1 7.97 6.34 0.48 o -3 6 1 543.14 577.55 6.83 o -2 6 1 83.27 75.38 2.33 o -1 6 1 46.07 51.45 1.87 o 0 6 1 42.45 30.04 1.41 o 1 6 1 24.56 16.18 1.05 o 2 6 1 42.83 33.59 1.12 o 3 6 1 99.20 96.92 1.98 o 4 6 1 71.30 75.07 1.86 o 5 6 1 132.61 134.32 3.78 o 6 6 1 181.09 192.24 4.76 o 7 6 1 61.30 62.99 2.62 o 8 6 1 9.55 10.45 0.95 o 9 6 1 61.91 61.94 1.62 o -7 7 1 24.28 21.05 0.97 o -5 7 1 1.40 1.64 0.41 o -4 7 1 3.28 4.51 0.74 o -3 7 1 0.62 0.87 0.65 o -2 7 1 109.55 113.08 2.30 o -1 7 1 310.93 317.62 5.10 o 0 7 1 98.71 103.04 2.90 o 1 7 1 174.57 173.10 3.76 o 2 7 1 4.11 3.44 0.40 o 3 7 1 87.66 84.40 1.58 o 4 7 1 203.74 206.43 3.17 o 5 7 1 0.00 0.50 0.31 o 6 7 1 3.04 2.86 0.62 o 7 7 1 140.04 136.23 3.04 o 8 7 1 65.63 67.11 1.98 o -7 8 1 136.94 127.74 2.26 o -6 8 1 17.05 16.25 1.12 o -5 8 1 5.45 5.11 0.49 o -4 8 1 1.10 0.88 0.34 o -3 8 1 11.65 11.88 0.83 o -2 8 1 941.57 902.38 14.56 o -1 8 1 121.35 124.92 3.71 o 0 8 1 1496.87 1464.51 12.42 o 1 8 1 0.43 0.37 0.21 o 2 8 1 47.11 48.52 1.49 o 3 8 1 1649.79 1622.84 13.74 o 4 8 1 22.67 24.34 1.12 o 5 8 1 150.20 146.97 2.73 o 6 8 1 38.36 36.01 1.77 o 7 8 1 12.35 12.84 0.75 o -6 9 1 7.56 7.17 0.49 o -5 9 1 8.65 8.81 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153.17 3.32 o 1 3 11 77.60 74.91 1.30 o 2 3 11 17.82 19.30 0.66 o 3 3 11 3.78 2.54 0.32 o 4 3 11 51.84 47.01 1.93 o 5 3 11 11.16 10.52 0.85 o 6 3 11 61.19 60.25 1.64 o -3 4 11 3.14 2.61 0.34 o -2 4 11 2.19 2.12 0.39 o -1 4 11 2.29 1.53 0.27 o 0 4 11 53.17 50.91 1.45 o 1 4 11 12.17 10.62 0.53 o 2 4 11 173.65 160.18 2.56 o 3 4 11 3.46 2.19 0.33 o 4 4 11 15.96 13.80 0.74 o 5 4 11 49.87 58.32 1.37 o 6 4 11 4.72 4.04 0.31 o -3 5 11 11.84 11.08 0.76 o -2 5 11 18.02 17.96 1.14 o -1 5 11 0.26 0.53 0.26 o 0 5 11 14.54 12.98 1.16 o 1 5 11 1.59 2.22 0.34 o 2 5 11 0.28 0.43 0.20 o 3 5 11 3.97 4.07 0.36 o 4 5 11 9.21 9.75 0.65 o 5 5 11 10.89 11.49 0.65 o 6 5 11 11.66 14.27 0.89 o 7 5 11 44.24 45.56 1.23 o -3 6 11 0.23 0.01 0.15 o -2 6 11 100.90 104.35 2.74 o -1 6 11 167.86 180.49 3.99 o 0 6 11 143.42 153.24 3.87 o 1 6 11 6.08 6.73 0.56 o 2 6 11 0.47 4.05 3.10 o 3 6 11 183.35 190.02 2.37 o 4 6 11 21.12 20.42 0.76 o 5 6 11 137.77 139.08 3.20 o 6 6 11 42.31 51.99 1.74 o 7 6 11 248.08 266.02 3.19 o -3 7 11 44.52 41.48 1.46 o -2 7 11 1000.57 965.65 7.80 o -1 7 11 41.88 41.63 1.84 o 0 7 11 7.48 8.27 0.88 o 1 7 11 22.13 22.30 1.46 o 2 7 11 168.57 165.78 5.22 o 3 7 11 0.15 0.23 0.21 o 4 7 11 122.65 132.79 2.35 o 5 7 11 0.83 1.46 0.57 o 6 7 11 16.15 17.63 1.67 o 7 7 11 22.66 33.47 1.10 o -2 8 11 130.36 117.81 2.33 o -1 8 11 204.13 200.04 3.59 o 0 8 11 9.97 9.52 0.87 o 1 8 11 50.62 52.03 2.05 o 2 8 11 0.00 0.19 0.18 o 3 8 11 1.62 1.70 0.23 o 4 8 11 18.48 18.65 0.67 o 5 8 11 30.80 32.15 1.91 o 6 8 11 8.80 6.79 0.39 o -2 9 11 14.03 11.84 0.69 o -1 9 11 5.72 4.81 0.35 o 0 9 11 0.01 0.28 0.18 o 1 9 11 9.65 9.29 0.53 o 2 9 11 6.00 6.95 0.51 o 3 9 11 0.20 0.22 0.15 o 4 9 11 125.71 132.93 2.06 o 5 9 11 7.23 6.65 0.40 o 6 9 11 15.47 16.77 0.52 o -1 10 11 21.57 20.15 0.89 o 0 10 11 0.21 0.54 0.13 o 1 10 11 0.56 1.22 0.17 o 2 10 11 53.86 53.33 2.48 o 3 10 11 153.21 154.58 1.79 o 4 10 11 15.42 15.23 0.80 o 5 10 11 1.07 2.14 0.30 o 1 11 11 68.16 72.01 1.55 o 2 11 11 82.12 92.23 1.82 o 3 11 11 3.38 5.78 0.47 o 0 2 12 0.20 0.38 0.15 o 1 2 12 1.89 0.87 0.18 o 2 2 12 20.44 16.34 0.68 o 3 2 12 0.84 1.05 0.23 o 4 2 12 168.50 171.34 2.38 o 0 3 12 90.12 82.60 1.83 o 1 3 12 0.00 -0.01 0.15 o 2 3 12 85.17 75.10 1.81 o 3 3 12 77.60 79.63 1.98 o 4 3 12 10.49 14.54 0.83 o 5 3 12 19.01 20.55 0.85 o -1 4 12 12.26 9.58 0.52 o 0 4 12 198.04 168.08 2.56 o 1 4 12 1.28 0.71 0.22 o 2 4 12 33.11 29.34 0.85 o 3 4 12 0.09 0.40 0.13 o 4 4 12 14.25 14.60 1.10 o 5 4 12 30.16 29.66 1.14 o -1 5 12 2.21 1.61 0.29 o 0 5 12 2.61 2.93 0.42 o 1 5 12 3.93 3.35 0.47 o 2 5 12 3.91 3.76 0.50 o 3 5 12 4.67 6.19 0.44 o 4 5 12 0.73 0.37 0.22 o 5 5 12 26.32 26.49 1.00 o -2 6 12 67.53 63.86 1.38 o -1 6 12 22.21 19.22 0.98 o 0 6 12 10.06 8.06 0.72 o 1 6 12 29.61 30.20 1.42 o 2 6 12 41.50 40.51 1.65 o 3 6 12 109.58 108.74 2.63 o 4 6 12 0.01 0.27 0.20 o 5 6 12 130.26 142.10 2.56 o 6 6 12 0.31 1.38 0.21 o -1 7 12 25.87 28.42 1.14 o 0 7 12 93.87 84.27 4.23 o 1 7 12 33.33 33.47 0.96 o 2 7 12 6.38 7.27 0.48 o 3 7 12 3.00 2.57 0.30 o 4 7 12 4.73 5.37 0.58 o 5 7 12 21.78 28.91 1.16 o 6 7 12 14.41 20.92 0.80 o -1 8 12 2.73 2.78 0.32 o 0 8 12 263.37 253.44 7.81 o 1 8 12 83.37 82.68 3.29 o 2 8 12 60.24 58.63 1.40 o 3 8 12 14.85 14.36 0.65 o 4 8 12 33.68 32.99 1.30 o 5 8 12 195.58 220.64 2.95 o 0 9 12 22.76 23.15 0.79 o 1 9 12 8.16 7.84 0.41 o 2 9 12 119.04 119.01 1.65 o 3 9 12 22.63 23.71 0.74 o 4 9 12 13.29 14.42 0.72 o 1 10 12 63.55 61.10 1.38 o 2 10 12 11.54 10.02 0.61 o 3 10 12 0.88 1.22 0.22 o 2 6 13 10.57 10.31 0.55 o 1 7 13 41.58 37.35 1.02 o 2 7 13 50.52 48.35 1.25 o 3 7 13 45.85 52.97 1.28 o