#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:53:09 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181307 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/85/2238545.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238545_Fobs loop_ _publ_author_name 'Bunev, Alexander S.' 'Sklyuev, Prokofij V.' 'Ostapenko, Gennady I.' 'Purygin, Petr P.' 'Khrustalev, Victor N.' _publ_section_title ; 2-(Adamantan-1-yl)-N-(6-methoxy-1,3-benzothiazol-2-yl)acetamide ; _journal_coeditor_code RK2412 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1472 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 61.554 _cell_angle_beta 80.252 _cell_angle_gamma 89.782 _cell_length_a 11.0114 _cell_length_b 13.6647 _cell_length_c 13.9230 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.8108 _cod_data_source_file rk2412Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_Bun3_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 202.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10.14 4.38 4.08 o 2 0 0 2979.85 2942.54 53.82 o 3 0 0 83.45 100.01 18.68 o 4 0 0 39.92 40.70 4.27 o 5 0 0 197.58 195.24 24.13 o 6 0 0 455.76 420.02 32.04 o 7 0 0 47.84 24.30 23.10 o 8 0 0 288.82 241.44 40.86 o 9 0 0 132.16 127.07 33.43 o 10 0 0 86.65 48.18 67.70 o 11 0 0 68.13 28.98 30.35 o 12 0 0 72.32 99.41 40.66 o 13 0 0 490.20 432.58 54.51 o -13 1 0 98.77 115.76 45.01 o -12 1 0 904.35 899.21 66.58 o -11 1 0 18.00 37.93 33.43 o -10 1 0 431.59 390.92 43.67 o -9 1 0 56.11 0.00 26.21 o -8 1 0 588.51 603.68 46.68 o -7 1 0 54.57 23.00 24.33 o -6 1 0 1851.06 1595.16 151.50 o -5 1 0 64.80 85.47 13.86 o -4 1 0 4.31 12.34 8.41 o -3 1 0 2.33 23.70 16.55 o -2 1 0 13539.99 13594.59 246.98 o -1 1 0 42.56 41.48 4.92 o 1 1 0 0.04 0.00 4.10 o 2 1 0 621.92 662.04 18.46 o 3 1 0 135.24 139.88 10.81 o 4 1 0 15.38 21.67 4.74 o 5 1 0 825.78 856.50 83.85 o 6 1 0 1323.39 1376.72 55.12 o 7 1 0 0.72 1.91 21.85 o 8 1 0 22.27 0.00 27.12 o 9 1 0 181.18 197.56 47.59 o 10 1 0 433.27 539.07 51.51 o 11 1 0 211.23 230.35 44.13 o 12 1 0 1.84 0.00 33.70 o 13 1 0 434.99 437.32 67.45 o -13 2 0 6.90 75.36 38.60 o -12 2 0 78.06 87.53 40.58 o -11 2 0 518.66 393.33 58.52 o -10 2 0 77.72 85.07 30.51 o -9 2 0 178.65 176.20 34.32 o -8 2 0 53.27 49.61 36.17 o -7 2 0 623.35 643.29 24.75 o -6 2 0 1787.05 1963.70 46.86 o -5 2 0 3559.05 3617.50 74.93 o -4 2 0 22.42 20.10 11.58 o -3 2 0 2103.05 2087.58 46.13 o -2 2 0 1515.21 1339.77 32.37 o -1 2 0 11388.14 11918.85 216.34 o 0 2 0 3369.83 3542.92 58.09 o 1 2 0 6291.09 6572.28 248.96 o 2 2 0 12.12 7.93 10.17 o 3 2 0 381.25 449.40 18.91 o 4 2 0 139.43 169.74 12.81 o 5 2 0 26.14 40.27 10.88 o 6 2 0 937.07 875.10 26.32 o 7 2 0 229.58 192.70 32.00 o 8 2 0 56.86 63.28 30.71 o 9 2 0 156.68 167.71 54.95 o 10 2 0 206.42 201.34 39.82 o 11 2 0 25.08 14.31 30.19 o 12 2 0 126.25 137.70 39.37 o 13 2 0 380.16 322.46 51.31 o -13 3 0 8.34 12.10 72.15 o -12 3 0 396.30 450.84 50.76 o -11 3 0 115.00 90.73 47.30 o -10 3 0 203.52 183.06 35.78 o -9 3 0 151.81 205.41 30.17 o -8 3 0 306.52 277.27 28.03 o -7 3 0 25.36 39.47 14.41 o -6 3 0 34.35 27.05 12.85 o -5 3 0 6.70 9.43 11.68 o -4 3 0 13.71 22.50 10.47 o -3 3 0 692.47 700.53 23.70 o -2 3 0 338.12 398.27 26.26 o -1 3 0 2166.55 2190.47 50.52 o 0 3 0 764.47 721.87 28.99 o 1 3 0 914.73 837.45 24.96 o 2 3 0 89.06 89.68 12.35 o 3 3 0 4838.47 4656.12 92.61 o 4 3 0 105.47 119.80 13.43 o 5 3 0 313.53 350.22 19.68 o 6 3 0 1300.28 1340.76 37.91 o 7 3 0 739.31 684.71 46.93 o 8 3 0 3440.37 3143.73 105.63 o 9 3 0 3.72 0.00 29.89 o 10 3 0 230.87 233.60 41.56 o 11 3 0 17.66 57.96 34.27 o 12 3 0 21.47 2.19 35.02 o -13 4 0 126.75 145.51 39.17 o -12 4 0 219.10 231.19 40.92 o -11 4 0 162.60 186.07 36.26 o -10 4 0 954.13 886.15 57.55 o -9 4 0 104.35 81.07 17.54 o -8 4 0 50.20 30.28 15.54 o -7 4 0 325.32 340.66 23.20 o -6 4 0 46.31 45.94 14.02 o -5 4 0 47.36 30.74 13.12 o -4 4 0 541.78 567.12 34.97 o -3 4 0 417.70 426.41 31.74 o -2 4 0 362.03 428.76 20.42 o -1 4 0 1166.18 1175.94 40.71 o 0 4 0 258.88 305.02 15.74 o 1 4 0 38.48 47.36 10.92 o 2 4 0 1631.88 1674.33 41.16 o 3 4 0 3511.65 3366.63 71.65 o 4 4 0 51.25 60.44 18.69 o 5 4 0 2003.85 2046.40 51.16 o 6 4 0 2.72 40.96 14.74 o 7 4 0 1254.52 1231.95 46.14 o 8 4 0 56.65 60.31 16.69 o 9 4 0 155.64 140.60 35.22 o 10 4 0 302.66 265.95 42.43 o 11 4 0 3.05 0.00 31.67 o 12 4 0 2.28 0.00 40.74 o -12 5 0 293.96 336.50 44.99 o -11 5 0 45.97 99.36 38.01 o -10 5 0 3.64 17.17 27.27 o -9 5 0 31.33 12.51 21.14 o -8 5 0 257.06 284.78 25.63 o -7 5 0 237.54 251.10 22.27 o -6 5 0 255.42 264.70 21.62 o -5 5 0 843.13 746.16 29.38 o -4 5 0 576.32 621.89 25.80 o -3 5 0 1307.46 1455.38 38.94 o -2 5 0 739.68 736.21 25.48 o -1 5 0 465.41 482.33 19.93 o 0 5 0 2717.79 2799.79 60.28 o 1 5 0 3844.89 3862.36 79.58 o 2 5 0 80.19 92.22 13.38 o 3 5 0 1072.89 988.09 50.22 o 4 5 0 2137.50 2368.59 57.40 o 5 5 0 32.46 25.19 15.42 o 6 5 0 0.14 20.88 16.15 o 7 5 0 158.23 129.05 19.82 o 8 5 0 1820.55 1735.42 60.51 o 9 5 0 525.20 435.37 150.58 o 10 5 0 507.06 553.62 58.36 o 11 5 0 5.67 8.60 30.70 o 12 5 0 0.30 0.00 38.91 o -12 6 0 235.79 272.15 41.22 o -11 6 0 60.73 102.75 33.87 o -10 6 0 222.31 260.55 38.55 o -9 6 0 242.67 291.87 40.08 o -8 6 0 617.26 673.27 68.46 o -7 6 0 599.49 572.25 31.33 o -6 6 0 286.37 326.14 25.27 o -5 6 0 232.02 224.10 28.06 o -4 6 0 0.17 17.61 13.81 o -3 6 0 413.85 574.18 25.62 o -2 6 0 8903.86 9055.22 173.35 o -1 6 0 39.77 43.42 12.54 o 0 6 0 1220.13 1219.53 35.04 o 1 6 0 1567.98 1584.60 41.41 o 2 6 0 24.98 31.97 12.56 o 3 6 0 208.41 220.56 27.43 o 4 6 0 0.88 11.09 23.60 o 5 6 0 8.36 0.00 16.46 o 6 6 0 266.15 268.02 24.80 o 7 6 0 1263.13 1264.46 44.55 o 8 6 0 45.00 52.96 17.71 o 9 6 0 29.51 13.31 29.30 o 10 6 0 388.38 366.18 140.92 o 11 6 0 263.84 294.59 47.31 o -12 7 0 73.77 58.70 32.61 o -11 7 0 47.53 80.32 33.45 o -10 7 0 813.39 809.55 39.83 o -9 7 0 101.98 107.16 21.66 o -8 7 0 568.08 565.36 33.31 o -7 7 0 3136.88 3133.37 77.36 o -6 7 0 29.31 42.67 17.86 o -5 7 0 1121.51 990.02 43.71 o -4 7 0 26.99 40.12 15.44 o -3 7 0 1296.35 1331.00 39.67 o -2 7 0 4352.22 4498.80 94.13 o -1 7 0 380.12 353.50 21.90 o 0 7 0 330.71 325.66 20.54 o 1 7 0 572.89 548.77 34.50 o 2 7 0 88.02 69.67 14.45 o 3 7 0 39.23 37.27 16.00 o 4 7 0 37.15 39.84 17.52 o 5 7 0 15.71 0.77 18.19 o 6 7 0 1776.95 1732.87 53.87 o 7 7 0 233.12 269.70 27.56 o 8 7 0 650.88 680.44 36.12 o 9 7 0 0.49 0.00 31.56 o 10 7 0 79.91 68.81 63.16 o 11 7 0 249.66 224.00 44.97 o -11 8 0 5.87 0.00 29.58 o -10 8 0 261.89 197.75 32.22 o -9 8 0 411.21 439.28 33.29 o -8 8 0 522.58 517.17 33.66 o -7 8 0 172.98 162.00 23.22 o -6 8 0 2244.51 2220.47 65.38 o -5 8 0 553.79 531.57 31.26 o -4 8 0 274.47 309.03 23.80 o -3 8 0 558.79 684.75 31.61 o -2 8 0 643.39 590.47 39.47 o -1 8 0 103.39 108.96 16.19 o 0 8 0 18.56 45.50 15.34 o 1 8 0 1248.87 1175.41 38.82 o 2 8 0 3.71 0.00 22.68 o 3 8 0 37.28 29.13 16.58 o 4 8 0 1348.52 1346.54 46.28 o 5 8 0 18.38 16.89 19.14 o 6 8 0 2.83 14.25 19.61 o 7 8 0 52.61 44.18 20.67 o 8 8 0 123.02 155.95 26.55 o 9 8 0 5.18 29.50 43.34 o 10 8 0 41.86 21.79 35.37 o -11 9 0 12.74 0.06 28.06 o -10 9 0 0.52 0.00 20.83 o -9 9 0 26.17 0.00 20.35 o -8 9 0 77.87 65.70 22.15 o -7 9 0 1024.24 991.15 56.08 o -6 9 0 143.95 159.07 22.45 o -5 9 0 46.30 62.25 19.15 o -4 9 0 265.95 280.23 40.17 o -3 9 0 66.18 77.69 17.72 o -2 9 0 1.31 3.02 14.98 o -1 9 0 401.35 409.80 29.97 o 0 9 0 52.57 58.48 19.71 o 1 9 0 747.50 789.53 43.83 o 2 9 0 189.21 209.41 21.77 o 3 9 0 0.26 0.00 16.98 o 4 9 0 483.06 488.17 31.53 o 5 9 0 3.41 3.72 18.89 o 6 9 0 9.76 22.77 26.42 o 7 9 0 279.38 289.67 29.54 o 8 9 0 1.62 0.00 28.59 o 9 9 0 82.21 32.72 35.69 o -10 10 0 18.18 14.69 23.06 o -9 10 0 1.65 0.00 20.77 o -8 10 0 286.21 295.68 29.86 o -7 10 0 113.89 101.08 23.37 o -6 10 0 0.84 0.00 17.78 o -5 10 0 55.25 53.80 20.46 o -4 10 0 15.06 9.28 17.15 o -3 10 0 78.86 57.89 18.12 o -2 10 0 226.83 250.68 33.50 o -1 10 0 480.79 392.70 38.34 o 0 10 0 395.26 351.02 38.02 o 1 10 0 1644.28 1787.94 52.40 o 2 10 0 24.56 37.31 18.32 o 3 10 0 1109.37 1146.38 42.82 o 4 10 0 170.35 192.45 27.72 o 5 10 0 145.92 184.86 24.86 o 6 10 0 36.21 44.03 21.51 o 7 10 0 0.02 0.00 22.65 o 8 10 0 59.08 77.62 35.50 o 9 10 0 191.61 220.62 44.45 o -9 11 0 133.11 98.34 33.41 o -8 11 0 99.33 53.85 31.39 o -7 11 0 354.35 414.63 67.40 o -6 11 0 70.40 31.29 29.22 o -5 11 0 385.02 368.62 41.36 o -4 11 0 2.28 0.00 26.63 o -3 11 0 5.48 0.00 25.17 o -2 11 0 123.08 162.91 32.49 o -1 11 0 807.77 755.44 52.92 o 0 11 0 0.36 23.93 27.71 o 1 11 0 1663.22 1590.89 67.14 o 2 11 0 145.73 138.34 29.46 o 3 11 0 84.66 64.81 28.63 o 4 11 0 5.85 0.00 27.07 o 5 11 0 7.38 11.09 27.49 o 6 11 0 1.70 0.00 28.00 o 7 11 0 151.75 165.08 36.46 o 8 11 0 46.93 9.59 56.49 o -8 12 0 56.24 19.26 30.69 o -7 12 0 104.39 101.21 34.33 o -6 12 0 292.42 264.15 42.14 o -5 12 0 20.23 0.00 42.87 o -4 12 0 184.84 200.05 36.26 o -3 12 0 295.74 216.43 37.89 o -2 12 0 634.33 534.71 81.08 o -1 12 0 134.05 168.21 35.81 o 0 12 0 1.72 0.00 28.73 o 1 12 0 6.95 16.83 27.12 o 2 12 0 0.02 0.00 27.35 o 3 12 0 72.38 56.85 31.19 o 4 12 0 73.70 49.00 30.17 o 5 12 0 1.59 0.00 68.07 o 6 12 0 0.18 37.22 32.80 o -7 13 0 226.01 285.08 43.28 o -6 13 0 25.36 66.56 34.48 o -5 13 0 21.49 0.00 29.21 o -4 13 0 173.65 208.22 40.89 o -3 13 0 54.89 53.08 31.42 o -2 13 0 655.03 539.93 49.79 o -1 13 0 199.09 176.82 39.12 o 0 13 0 301.79 281.51 42.16 o 1 13 0 98.51 70.98 33.08 o 2 13 0 8.67 0.00 30.09 o 3 13 0 2.79 0.00 31.40 o 4 13 0 487.14 502.77 50.28 o 5 13 0 0.04 0.00 30.58 o -5 14 0 39.91 34.99 36.14 o -4 14 0 158.20 159.70 39.17 o -3 14 0 94.79 87.59 36.20 o -2 14 0 50.35 29.51 32.89 o -1 14 0 29.89 25.03 44.38 o 0 14 0 89.47 145.71 35.54 o 1 14 0 44.40 59.61 35.27 o 2 14 0 317.27 326.65 43.88 o 3 14 0 96.22 148.74 38.24 o -1 -14 1 78.67 120.92 37.19 o 0 -14 1 5.11 0.00 30.11 o 1 -14 1 172.08 123.77 39.97 o 2 -14 1 242.30 208.25 42.39 o 3 -14 1 28.89 9.14 32.96 o 4 -14 1 41.14 1.42 67.54 o -4 -13 1 148.83 172.28 40.14 o -3 -13 1 5.73 0.00 31.07 o -2 -13 1 240.19 194.37 39.31 o -1 -13 1 60.87 83.26 34.03 o 0 -13 1 157.68 115.29 60.52 o 1 -13 1 20.60 33.18 28.99 o 2 -13 1 667.81 537.80 50.60 o 3 -13 1 1.33 0.00 28.24 o 4 -13 1 5.71 24.49 33.67 o 5 -13 1 90.90 220.14 59.45 o 6 -13 1 14.60 0.00 32.53 o -6 -12 1 37.31 0.00 40.52 o -5 -12 1 66.22 0.89 31.34 o -4 -12 1 6.25 0.00 30.51 o -3 -12 1 69.87 74.60 32.23 o -2 -12 1 516.90 492.90 47.58 o -1 -12 1 93.92 22.20 29.72 o 0 -12 1 88.27 96.10 34.25 o 1 -12 1 135.24 112.78 34.07 o 2 -12 1 64.09 45.37 30.71 o 3 -12 1 77.00 75.82 32.58 o 4 -12 1 3.07 0.00 27.17 o 5 -12 1 115.50 124.96 36.52 o 6 -12 1 31.27 5.68 33.51 o 7 -12 1 16.25 10.95 35.42 o 8 -12 1 248.62 307.89 55.72 o -7 -11 1 65.76 64.47 34.76 o -6 -11 1 47.29 0.00 30.31 o -5 -11 1 206.42 245.03 37.96 o -4 -11 1 38.35 21.32 28.36 o -3 -11 1 63.31 37.41 30.25 o -2 -11 1 246.44 244.34 46.30 o -1 -11 1 1.46 0.00 27.12 o 0 -11 1 95.56 146.79 33.84 o 1 -11 1 2.65 6.58 24.98 o 2 -11 1 7.72 46.13 30.62 o 3 -11 1 66.03 66.59 29.87 o 4 -11 1 31.43 0.00 63.03 o 5 -11 1 324.00 349.79 42.46 o 6 -11 1 0.21 0.00 29.72 o 7 -11 1 76.79 25.41 30.60 o 8 -11 1 18.31 0.00 31.07 o 9 -11 1 76.88 51.07 43.26 o -8 -10 1 269.98 113.19 65.40 o -7 -10 1 196.53 190.29 36.21 o -6 -10 1 70.90 41.98 37.21 o -5 -10 1 36.29 55.06 29.93 o -4 -10 1 834.41 799.02 53.07 o -3 -10 1 15.81 16.48 28.05 o -2 -10 1 196.45 172.14 39.06 o -1 -10 1 302.83 277.80 36.66 o 0 -10 1 8.29 84.85 29.00 o 1 -10 1 310.90 263.54 36.01 o 2 -10 1 180.16 168.78 32.37 o 3 -10 1 47.31 30.07 26.70 o 4 -10 1 120.17 66.03 27.03 o 5 -10 1 828.63 712.29 94.20 o 6 -10 1 0.18 0.00 30.21 o 7 -10 1 55.96 64.96 30.98 o 8 -10 1 237.49 235.51 38.10 o 9 -10 1 19.05 0.00 27.18 o 10 -10 1 10.43 0.00 68.72 o -9 -9 1 24.50 36.65 37.18 o -8 -9 1 197.81 176.79 38.91 o -7 -9 1 330.45 344.68 31.51 o -6 -9 1 132.38 138.86 24.40 o -5 -9 1 19.85 19.52 22.06 o -4 -9 1 9.17 1.18 16.50 o -3 -9 1 342.21 318.97 25.08 o -2 -9 1 581.60 599.86 30.50 o -1 -9 1 164.51 184.28 35.76 o 0 -9 1 173.55 188.14 31.38 o 1 -9 1 57.37 49.82 29.19 o 2 -9 1 246.97 228.44 33.37 o 3 -9 1 118.19 101.88 15.97 o 4 -9 1 7.54 2.92 16.00 o 5 -9 1 621.93 591.76 32.81 o 6 -9 1 57.37 53.58 19.26 o 7 -9 1 558.24 585.56 35.78 o 8 -9 1 347.64 384.20 31.36 o 9 -9 1 326.25 343.94 31.57 o 10 -9 1 41.05 0.00 30.28 o 11 -9 1 277.33 267.95 41.81 o -10 -8 1 590.08 600.61 59.81 o -9 -8 1 154.55 179.99 62.85 o -8 -8 1 58.97 79.28 32.85 o -7 -8 1 74.86 68.88 22.62 o -6 -8 1 1045.00 1095.84 51.57 o -5 -8 1 1357.01 1344.71 47.18 o -4 -8 1 294.22 323.23 27.05 o -3 -8 1 933.56 905.33 36.54 o -2 -8 1 108.68 108.82 21.01 o -1 -8 1 715.71 697.60 62.84 o 0 -8 1 205.00 235.39 43.48 o 1 -8 1 0.15 9.25 21.79 o 2 -8 1 363.21 363.83 19.47 o 3 -8 1 505.41 542.37 34.07 o 4 -8 1 33.82 47.75 16.58 o 5 -8 1 281.61 257.07 29.11 o 6 -8 1 258.52 276.24 26.06 o 7 -8 1 640.78 610.39 34.94 o 8 -8 1 351.62 417.33 32.10 o 9 -8 1 387.55 336.51 34.83 o 10 -8 1 92.30 50.59 30.87 o 11 -8 1 85.82 110.66 47.76 o -10 -7 1 57.54 13.27 51.17 o -9 -7 1 1.86 0.00 29.28 o -8 -7 1 3.30 0.41 25.09 o -7 -7 1 45.73 71.23 22.98 o -6 -7 1 0.03 13.97 23.37 o -5 -7 1 70.37 96.62 21.08 o -4 -7 1 301.30 292.70 24.79 o -3 -7 1 578.04 502.25 32.35 o -2 -7 1 171.39 163.81 24.96 o -1 -7 1 1041.77 1081.39 38.18 o 0 -7 1 213.64 241.04 15.10 o 1 -7 1 257.97 254.60 56.94 o 2 -7 1 920.86 901.35 29.03 o 3 -7 1 1708.68 1682.42 45.39 o 4 -7 1 467.19 465.56 32.19 o 5 -7 1 106.37 115.86 20.19 o 6 -7 1 24.07 25.73 18.89 o 7 -7 1 739.79 691.35 64.37 o 8 -7 1 2985.42 3018.16 76.80 o 9 -7 1 216.65 198.39 24.51 o 10 -7 1 40.15 58.50 22.63 o 11 -7 1 6.72 16.35 28.47 o 12 -7 1 3.90 22.77 32.38 o -11 -6 1 19.00 1.72 33.25 o -10 -6 1 812.66 924.08 85.43 o -9 -6 1 106.18 84.56 33.54 o -8 -6 1 0.03 0.00 18.01 o -7 -6 1 59.31 46.71 19.71 o -6 -6 1 158.15 167.33 22.55 o -5 -6 1 753.21 745.66 35.10 o -4 -6 1 258.11 262.52 22.69 o -3 -6 1 462.83 444.63 24.96 o -2 -6 1 195.49 192.23 17.20 o -1 -6 1 64.82 64.12 12.10 o 0 -6 1 535.74 577.57 21.65 o 1 -6 1 31.71 59.40 19.30 o 2 -6 1 302.06 286.83 17.84 o 3 -6 1 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