# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2239006 _cell_angle_alpha 90.000 _cell_angle_beta 91.520 _cell_angle_gamma 90.000 _cell_length_a 11.4250 _cell_length_b 9.6790 _cell_length_c 15.2050 _exptl_crystal_F_000 788.00 _reflns_d_resolution_high 0.7835 _cod_data_source_file lh5680Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MEEDCu Final Cycles refine 2 of the NH atoms' _shelx_refln_list_code 4 _shelx_f_calc_maximum 317.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x, y, -z-1/2' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 76552.62 84235.52 3401.69 o 4 0 0 13207.74 12958.21 521.54 o 6 0 0 35895.45 37403.23 1501.34 o 8 0 0 11856.42 12125.24 491.97 o 10 0 0 8916.70 8920.54 366.40 o 12 0 0 3898.81 3778.10 164.04 o 14 0 0 381.66 364.65 20.97 o 1 1 0 865.29 1055.04 43.55 o 3 1 0 7027.72 7905.77 318.73 o 5 1 0 285.11 281.58 15.86 o 7 1 0 332.47 332.15 18.21 o 9 1 0 32.96 35.14 6.15 o 11 1 0 53.98 60.56 7.34 o 13 1 0 1.09 -2.38 12.22 o 0 2 0 101011.82 89474.36 3620.20 o 2 2 0 39012.21 40332.32 1650.77 o 4 2 0 18978.03 18854.47 757.94 o 6 2 0 13262.34 13351.71 539.39 o 8 2 0 7753.68 7851.56 321.44 o 10 2 0 5615.76 5666.97 236.58 o 12 2 0 1792.06 1778.94 85.09 o 14 2 0 373.55 377.55 22.79 o 1 3 0 3306.46 3346.67 136.96 o 3 3 0 3565.07 3582.36 146.98 o 5 3 0 7600.35 7737.97 314.48 o 7 3 0 1358.72 1406.60 63.72 o 9 3 0 346.05 323.92 18.39 o 11 3 0 363.60 364.77 20.71 o 13 3 0 1.11 10.70 20.10 o 0 4 0 22042.24 21647.66 869.95 o 2 4 0 17210.51 17373.88 699.14 o 4 4 0 10882.80 10850.29 439.05 o 6 4 0 11658.09 11914.70 483.08 o 8 4 0 5678.06 5743.47 238.41 o 10 4 0 1373.39 1391.25 67.74 o 12 4 0 886.11 882.55 48.84 o 1 5 0 3019.22 3126.85 130.20 o 3 5 0 1046.51 993.17 46.04 o 5 5 0 5445.91 5504.89 226.90 o 7 5 0 2298.94 2420.24 105.74 o 9 5 0 29.66 39.90 6.57 o 11 5 0 106.31 102.20 8.98 o 13 5 0 63.85 55.06 9.04 o 0 6 0 1930.32 2086.60 89.86 o 2 6 0 4507.32 4709.94 194.83 o 4 6 0 2225.07 2249.89 97.68 o 6 6 0 1172.71 1172.15 57.16 o 8 6 0 2125.69 2198.86 98.83 o 10 6 0 724.06 705.80 39.00 o 12 6 0 188.38 192.88 12.34 o 1 7 0 2439.93 2416.77 104.67 o 3 7 0 609.49 605.61 32.25 o 5 7 0 211.26 209.99 12.37 o 7 7 0 519.54 528.81 29.85 o 9 7 0 181.00 174.42 10.82 o 11 7 0 64.82 62.64 8.56 o 0 8 0 206.20 189.31 10.65 o 2 8 0 383.84 405.78 23.12 o 4 8 0 448.50 425.75 23.69 o 6 8 0 211.34 201.70 11.30 o 8 8 0 192.35 224.23 13.06 o 10 8 0 159.22 140.27 10.85 o 1 9 0 153.16 191.36 11.36 o 3 9 0 47.98 62.05 7.55 o 5 9 0 219.25 235.07 14.34 o 7 9 0 22.80 41.32 7.82 o 9 9 0 1.62 34.81 8.29 o 0 10 0 58.39 46.35 7.08 o 2 10 0 59.13 62.88 7.37 o 4 10 0 0.49 9.07 9.42 o 6 10 0 4.23 -22.89 22.89 o 8 10 0 6.97 2.41 10.79 o 1 11 0 77.10 101.62 9.22 o 3 11 0 326.67 317.24 17.61 o 5 11 0 35.70 48.55 8.47 o 0 12 0 0.59 -15.07 20.57 o 2 12 0 32.36 10.61 22.74 o -13 1 1 37.27 30.89 7.52 o -11 1 1 544.87 543.85 30.92 o -9 1 1 10.39 8.95 7.88 o -7 1 1 378.73 394.82 22.08 o -5 1 1 470.33 418.99 22.07 o -3 1 1 5361.96 5579.70 225.76 o -1 1 1 8802.87 8850.03 355.40 o 1 1 1 3168.65 3083.71 124.71 o 3 1 1 0.12 36.03 3.30 o 5 1 1 7589.28 7945.72 321.98 o 7 1 1 340.68 407.21 22.83 o 9 1 1 10.42 9.25 5.74 o 11 1 1 405.15 414.83 23.27 o 13 1 1 85.05 76.06 8.59 o -14 2 1 55.26 55.33 8.71 o -12 2 1 17.91 25.77 7.16 o -10 2 1 671.67 717.67 39.15 o -8 2 1 2340.41 2375.50 102.87 o -6 2 1 232.27 216.68 12.17 o -4 2 1 267.05 232.21 12.95 o -2 2 1 69.14 124.59 7.14 o 0 2 1 2107.07 2372.18 97.09 o 2 2 1 36088.32 36621.54 1502.98 o 4 2 1 1067.43 988.80 43.92 o 6 2 1 19.92 39.78 4.58 o 8 2 1 790.83 834.35 42.57 o 10 2 1 99.18 98.78 8.03 o 12 2 1 277.14 284.86 15.94 o 14 2 1 111.07 106.33 10.02 o -13 3 1 105.89 79.48 9.19 o -11 3 1 656.50 634.84 36.56 o -9 3 1 767.15 773.38 41.82 o -7 3 1 1301.92 1343.50 61.24 o -5 3 1 1421.06 1406.07 61.74 o -3 3 1 138.91 146.48 8.72 o -1 3 1 8853.34 8917.06 359.74 o 1 3 1 16306.15 16441.46 660.86 o 3 3 1 497.84 513.68 25.15 o 5 3 1 1217.20 1198.94 53.48 o 7 3 1 2577.66 2566.06 109.95 o 9 3 1 856.88 874.92 46.20 o 11 3 1 655.02 667.70 37.66 o 13 3 1 335.03 308.82 18.09 o -12 4 1 79.40 58.39 8.83 o -10 4 1 880.53 858.03 46.97 o -8 4 1 3815.32 3903.02 164.98 o -6 4 1 1735.25 1703.74 75.22 o -4 4 1 6683.21 6656.63 271.33 o -2 4 1 7004.01 7036.12 285.61 o 0 4 1 740.66 660.82 31.12 o 2 4 1 17457.21 17599.55 708.23 o 4 4 1 12774.19 12923.48 522.03 o 6 4 1 1256.56 1335.14 60.99 o 8 4 1 1195.52 1211.35 58.65 o 10 4 1 547.00 519.96 29.11 o 12 4 1 327.74 303.26 17.76 o -13 5 1 267.79 261.96 15.17 o -11 5 1 378.19 356.88 19.63 o -9 5 1 1632.16 1662.20 77.69 o -7 5 1 1368.50 1415.18 65.87 o -5 5 1 2360.52 2427.36 104.21 o -3 5 1 14723.39 15289.87 617.17 o -1 5 1 8834.53 8991.00 364.71 o 1 5 1 3269.61 3393.13 140.90 o 3 5 1 4599.33 4700.87 193.62 o 5 5 1 4404.28 4346.63 180.63 o 7 5 1 4180.26 4121.10 173.59 o 9 5 1 1875.40 1866.95 85.85 o 11 5 1 675.90 689.10 39.86 o 13 5 1 338.33 342.13 20.64 o -12 6 1 270.74 279.46 15.73 o -10 6 1 501.59 533.87 30.00 o -8 6 1 1586.19 1565.02 73.90 o -6 6 1 5149.66 5153.20 214.76 o -4 6 1 6841.81 6893.15 282.87 o -2 6 1 3944.72 3783.77 157.93 o 0 6 1 6629.09 6475.75 265.22 o 2 6 1 9854.00 9897.85 402.32 o 4 6 1 6612.48 6662.23 273.72 o 6 6 1 2633.53 2634.82 114.40 o 8 6 1 1892.81 1842.36 84.90 o 10 6 1 721.01 738.39 40.99 o 12 6 1 195.50 199.93 12.55 o -11 7 1 500.75 498.48 28.74 o -9 7 1 510.46 555.25 31.81 o -7 7 1 1407.02 1360.62 66.41 o -5 7 1 5115.19 5195.73 217.00 o -3 7 1 7130.45 7244.26 297.98 o -1 7 1 5040.82 5029.98 208.89 o 1 7 1 4493.53 4513.99 188.32 o 3 7 1 2556.87 2662.66 114.84 o 5 7 1 3352.17 3204.03 137.65 o 7 7 1 5059.84 4998.15 210.58 o 9 7 1 1597.68 1612.65 77.75 o 11 7 1 308.60 315.70 18.00 o -10 8 1 260.55 276.42 15.14 o -8 8 1 732.82 704.58 39.92 o -6 8 1 503.05 506.66 29.43 o -4 8 1 908.15 902.34 47.57 o -2 8 1 1922.49 1930.59 87.03 o 0 8 1 967.45 1024.11 51.46 o 2 8 1 1298.66 1325.12 63.13 o 4 8 1 1980.61 1973.70 89.38 o 6 8 1 98.61 97.50 7.85 o 8 8 1 272.78 287.14 16.27 o 10 8 1 726.71 714.70 41.35 o -9 9 1 1640.29 1678.46 83.87 o -7 9 1 1981.88 1931.06 91.85 o -5 9 1 2398.63 2437.99 110.29 o -3 9 1 6038.15 6079.92 254.29 o -1 9 1 8133.68 7786.28 321.97 o 1 9 1 5594.28 5388.71 226.03 o 3 9 1 6048.68 6001.84 251.28 o 5 9 1 3892.30 3743.11 162.20 o 7 9 1 1897.35 1869.82 89.33 o 9 9 1 2040.01 1986.54 96.58 o -8 10 1 90.82 43.59 8.86 o -6 10 1 389.24 435.92 25.41 o -4 10 1 751.79 724.25 40.82 o -2 10 1 339.73 368.64 20.41 o 0 10 1 354.16 375.73 22.10 o 2 10 1 575.10 569.38 32.35 o 4 10 1 267.34 279.32 15.47 o 6 10 1 216.63 219.00 12.82 o 8 10 1 228.18 232.15 13.83 o -5 11 1 1096.82 1130.95 62.37 o -3 11 1 1507.94 1533.82 77.15 o -1 11 1 2388.55 2331.23 107.62 o 1 11 1 2949.13 2865.49 129.32 o 3 11 1 2266.81 2220.18 104.24 o 5 11 1 1216.41 1253.81 67.66 o -2 12 1 6.38 16.05 7.79 o 0 12 1 87.11 65.02 8.65 o 2 12 1 0.32 -1.90 21.26 o -14 0 2 185.13 175.99 11.72 o -12 0 2 2795.25 2761.60 123.64 o -10 0 2 3685.15 3788.62 161.50 o -8 0 2 6103.22 6117.41 251.87 o -6 0 2 34341.11 34771.33 1396.22 o -4 0 2 33358.20 34282.55 1374.99 o -2 0 2 26109.84 25369.52 1043.82 o 0 0 2 57714.80 61650.22 2491.12 o 2 0 2 37494.86 40191.05 1638.64 o 4 0 2 70994.35 70561.29 2878.90 o 6 0 2 36236.14 36935.29 1482.89 o 8 0 2 8450.74 8338.43 340.68 o 10 0 2 4594.64 4711.30 198.24 o 12 0 2 2085.23 2093.49 96.90 o 14 0 2 1142.96 1132.89 63.60 o -13 1 2 0.62 3.54 12.25 o -11 1 2 87.68 96.57 7.91 o -9 1 2 67.56 61.31 6.72 o -7 1 2 0.56 3.81 5.68 o -5 1 2 46.92 40.97 3.87 o -3 1 2 3215.78 3602.07 146.95 o -1 1 2 420.90 318.03 15.50 o 1 1 2 2410.80 2654.56 107.96 o 3 1 2 143.31 162.04 9.28 o 5 1 2 882.48 956.18 43.24 o 7 1 2 94.83 103.10 6.33 o 9 1 2 93.27 92.92 7.26 o 11 1 2 36.27 34.78 9.13 o 13 1 2 2.07 -4.61 20.66 o -14 2 2 363.37 373.32 20.97 o -12 2 2 1510.05 1545.30 75.53 o -10 2 2 1527.16 1596.69 74.82 o -8 2 2 3564.41 3662.74 154.24 o -6 2 2 12060.75 12116.66 490.08 o -4 2 2 16325.21 16323.05 656.81 o -2 2 2 32413.74 34236.75 1409.64 o 0 2 2 15453.72 14994.55 602.27 o 2 2 2 1167.48 1068.78 45.95 o 4 2 2 34739.50 34762.56 1394.73 o 6 2 2 25658.41 25692.20 1033.46 o 8 2 2 3707.90 3724.04 156.84 o 10 2 2 2453.56 2528.80 111.86 o 12 2 2 1543.91 1590.05 77.62 o 14 2 2 598.24 615.17 34.82 o -13 3 2 94.02 90.89 9.04 o -11 3 2 258.19 260.11 15.05 o -9 3 2 50.27 53.90 6.72 o -7 3 2 1311.99 1338.98 61.20 o -5 3 2 266.56 242.81 13.93 o -3 3 2 1047.31 1026.87 45.26 o -1 3 2 31499.12 31675.62 1270.60 o 1 3 2 2807.96 2767.62 114.00 o 3 3 2 771.05 846.30 38.19 o 5 3 2 4333.86 4326.67 178.34 o 7 3 2 153.48 135.38 7.79 o 9 3 2 504.87 501.01 28.28 o 11 3 2 681.65 675.17 38.05 o 13 3 2 18.11 21.85 7.82 o -12 4 2 836.03 810.65 45.29 o -10 4 2 1132.57 1042.71 54.77 o -8 4 2 572.77 682.37 35.69 o -6 4 2 4458.09 4358.23 181.15 o -4 4 2 17898.37 18304.08 737.45 o -2 4 2 12117.28 12146.87 490.24 o 0 4 2 12579.87 12122.40 489.04 o 2 4 2 8065.79 7840.05 317.96 o 4 4 2 4721.52 4501.90 185.30 o 6 4 2 10994.09 10856.17 441.01 o 8 4 2 4753.88 4799.38 200.95 o 10 4 2 868.16 867.34 47.41 o 12 4 2 927.74 914.06 49.43 o -13 5 2 84.75 71.03 9.54 o -11 5 2 349.31 363.49 21.09 o -9 5 2 2.49 4.37 7.82 o -7 5 2 157.85 187.06 10.17 o -5 5 2 2030.10 2021.20 88.10 o -3 5 2 2145.43 2214.94 94.59 o -1 5 2 4595.79 4711.49 193.70 o 1 5 2 2625.51 2572.05 108.27 o 3 5 2 197.05 165.57 8.69 o 5 5 2 2015.02 2014.67 88.03 o 7 5 2 1650.72 1692.42 76.99 o 9 5 2 167.36 171.26 10.08 o 11 5 2 124.31 140.68 10.20 o 13 5 2 29.92 35.76 11.62 o -12 6 2 107.16 114.03 10.20 o -10 6 2 376.25 361.25 19.78 o -8 6 2 528.12 554.18 32.14 o -6 6 2 240.54 257.36 14.19 o -4 6 2 1031.96 1057.83 51.16 o -2 6 2 2487.70 2499.04 107.06 o 0 6 2 3369.35 3337.51 139.98 o 2 6 2 2349.40 2371.01 101.74 o 4 6 2 615.86 577.59 32.67 o 6 6 2 925.52 884.35 46.12 o 8 6 2 819.86 846.66 45.95 o 10 6 2 573.36 566.00 32.02 o 12 6 2 539.49 510.20 29.64 o -11 7 2 30.66 30.83 8.06 o -9 7 2 78.05 79.36 8.03 o -7 7 2 183.27 168.74 10.20 o -5 7 2 329.70 339.40 19.43 o -3 7 2 223.60 258.22 14.28 o -1 7 2 582.92 660.36 35.85 o 1 7 2 1411.00 1315.28 61.48 o 3 7 2 272.58 256.88 15.26 o 5 7 2 659.56 650.17 34.99 o 7 7 2 339.80 344.09 19.93 o 9 7 2 9.91 17.27 7.19 o 11 7 2 75.12 80.01 9.16 o -10 8 2 52.04 49.14 8.41 o -8 8 2 43.88 57.02 7.79 o -6 8 2 0.42 -5.80 17.09 o -4 8 2 30.95 22.98 8.38 o -2 8 2 334.33 280.83 18.06 o 0 8 2 172.66 176.69 10.02 o 2 8 2 153.33 167.93 9.75 o 4 8 2 129.75 122.51 8.33 o 6 8 2 45.93 36.48 6.45 o 8 8 2 158.89 168.96 10.71 o 10 8 2 128.39 122.36 10.23 o -9 9 2 8.48 -5.05 24.35 o -7 9 2 17.52 38.68 10.61 o -5 9 2 110.75 109.36 8.62 o -3 9 2 299.20 294.61 16.66 o -1 9 2 150.53 179.67 10.59 o 1 9 2 39.69 47.78 6.96 o 3 9 2 67.35 89.85 8.18 o 5 9 2 1.60 8.92 7.02 o 7 9 2 35.25 44.30 7.82 o 9 9 2 204.11 205.20 13.17 o -8 10 2 57.45 46.32 12.72 o -6 10 2 43.93 39.96 7.97 o -4 10 2 19.54 21.82 7.11 o -2 10 2 48.58 50.75 7.22 o 0 10 2 378.23 399.22 22.07 o 2 10 2 154.96 166.08 10.38 o 4 10 2 4.02 -2.14 7.13 o 6 10 2 8.70 17.39 7.25 o 8 10 2 31.85 25.66 11.39 o -5 11 2 76.93 90.21 9.48 o -3 11 2 157.48 157.42 10.94 o -1 11 2 304.15 322.88 18.03 o 1 11 2 643.88 635.48 35.39 o 3 11 2 386.88 370.82 20.53 o 5 11 2 53.06 52.65 8.62 o -2 12 2 4.22 -6.72 22.12 o 0 12 2 34.17 36.06 8.21 o 2 12 2 4.35 -10.97 10.97 o -13 1 3 168.77 170.27 11.18 o -11 1 3 11.00 9.33 10.97 o -9 1 3 758.97 766.75 41.25 o -7 1 3 0.56 -13.41 13.41 o -5 1 3 41.28 45.67 4.04 o -3 1 3 349.50 354.24 18.92 o -1 1 3 149.00 167.34 9.41 o 1 1 3 21471.99 23102.83 933.34 o 3 1 3 5032.77 5333.38 216.46 o 5 1 3 1903.81 2025.40 85.76 o 7 1 3 26.40 22.06 4.52 o 9 1 3 3.88 21.55 5.86 o 11 1 3 34.90 45.78 6.84 o 13 1 3 15.86 5.32 12.78 o -14 2 3 22.19 24.08 11.24 o -12 2 3 2.10 19.35 9.75 o -10 2 3 797.08 834.98 44.37 o -8 2 3 973.32 985.84 48.14 o -6 2 3 1191.84 1177.47 53.43 o -4 2 3 8407.99 8403.15 340.21 o -2 2 3 444.85 356.25 18.96 o 0 2 3 1754.14 1662.64 69.68 o 2 2 3 8995.84 9046.24 364.93 o 4 2 3 1120.88 1096.53 48.57 o 6 2 3 1345.28 1311.66 58.77 o 8 2 3 1435.55 1475.82 67.65 o 10 2 3 232.84 215.10 12.34 o 12 2 3 146.46 148.53 10.41 o 14 2 3 27.93 32.11 8.47 o -13 3 3 50.79 45.78 8.35 o -11 3 3 176.36 182.98 10.74 o -9 3 3 18.05 22.53 9.51 o -7 3 3 110.51 118.89 7.49 o -5 3 3 1571.74 1525.16 66.75 o -3 3 3 13.57 17.60 3.15 o -1 3 3 131.42 168.82 9.49 o 1 3 3 1620.70 1753.11 73.81 o 3 3 3 889.53 854.30 39.04 o 5 3 3 919.89 856.70 40.56 o 7 3 3 78.04 67.73 6.01 o 9 3 3 15.58 27.56 6.12 o 11 3 3 480.25 489.11 27.53 o 13 3 3 244.07 230.70 13.35 o -12 4 3 179.57 181.49 11.72 o -10 4 3 1096.57 1047.61 54.92 o -8 4 3 2237.74 2217.72 98.32 o -6 4 3 2081.98 2048.57 89.16 o -4 4 3 10570.48 10863.04 439.96 o -2 4 3 18179.33 18530.05 745.88 o 0 4 3 10326.46 9997.78 404.33 o 2 4 3 4824.15 4656.22 190.80 o 4 4 3 4128.17 3970.14 164.32 o 6 4 3 5999.43 6088.76 250.55 o 8 4 3 4182.65 4251.52 179.23 o 10 4 3 736.39 719.01 39.33 o 12 4 3 171.41 169.65 11.30 o -13 5 3 205.40 221.55 13.53 o -11 5 3 314.69 318.76 17.76 o -9 5 3 434.27 464.64 26.16 o -7 5 3 892.16 933.15 47.49 o -5 5 3 1527.62 1457.96 66.02 o -3 5 3 1317.70 1195.83 54.52 o -1 5 3 4450.57 4433.19 182.83 o 1 5 3 4780.23 4761.97 195.94 o 3 5 3 1069.22 997.94 46.48 o 5 5 3 3736.34 3708.90 155.51 o 7 5 3 1337.44 1370.73 65.02 o 9 5 3 75.72 79.48 7.55 o 11 5 3 830.01 851.63 45.91 o 13 5 3 401.90 391.55 21.33 o -12 6 3 369.93 361.19 20.50 o -10 6 3 1386.23 1302.25 66.53 o -8 6 3 1794.54 1751.23 81.63 o -6 6 3 1793.85 1839.13 83.28 o -4 6 3 9479.92 9461.20 385.94 o -2 6 3 12366.99 11923.29 483.75 o 0 6 3 6673.73 6486.35 265.98 o 2 6 3 11514.95 11406.45 463.04 o 4 6 3 5052.11 4982.15 206.93 o 6 6 3 1848.06 1863.06 84.15 o 8 6 3 4764.22 4754.50 201.09 o 10 6 3 1275.98 1170.10 61.93 o 12 6 3 78.61 88.01 9.34 o -11 7 3 476.17 465.43 26.12 o -9 7 3 513.71 580.54 32.73 o -7 7 3 357.89 371.68 20.17 o -5 7 3 2434.87 2440.89 107.43 o -3 7 3 4042.53 3935.25 166.02 o -1 7 3 1679.47 1543.19 70.54 o 1 7 3 3372.09 3423.97 145.04 o 3 7 3 3568.13 3619.80 153.21 o 5 7 3 1591.25 1549.80 72.24 o 7 7 3 1590.65 1631.27 76.87 o 9 7 3 956.86 944.37 52.33 o 11 7 3 349.87 353.06 20.20 o -10 8 3 322.86 316.40 18.83 o -8 8 3 1504.88 1525.95 75.58 o -6 8 3 714.75 746.28 41.03 o -4 8 3 289.43 279.00 15.50 o -2 8 3 2610.23 2627.16 115.07 o 0 8 3 3147.51 3126.17 134.65 o 2 8 3 2794.52 2784.36 121.26 o 4 8 3 1812.58 1770.31 81.94 o 6 8 3 295.27 298.47 17.13 o 8 8 3 624.62 620.81 34.79 o 10 8 3 477.97 443.26 24.49 o -9 9 3 925.74 942.64 52.53 o -7 9 3 2677.34 2680.84 121.91 o -5 9 3 2180.68 2193.87 100.63 o -3 9 3 3067.65 3036.05 133.18 o -1 9 3 4299.97 4188.87 178.54 o 1 9 3 3858.36 3818.36 163.71 o 3 9 3 5524.05 5418.31 228.64 o 5 9 3 3331.25 3244.18 142.60 o 7 9 3 1376.49 1415.15 71.83 o 9 9 3 1062.95 1085.61 59.33 o -8 10 3 295.11 296.86 16.51 o -6 10 3 191.38 209.68 12.64 o -4 10 3 775.17 775.54 42.99 o -2 10 3 815.67 800.71 43.18 o 0 10 3 960.67 944.43 52.12 o 2 10 3 1510.66 1513.67 74.33 o 4 10 3 447.70 465.28 26.54 o 6 10 3 199.02 205.64 12.31 o 8 10 3 471.70 464.07 26.36 o -5 11 3 1073.56 1147.35 62.85 o -3 11 3 1615.42 1608.56 80.03 o -1 11 3 850.41 854.06 46.63 o 1 11 3 1371.36 1321.08 68.76 o 3 11 3 2483.56 2451.26 114.17 o 5 11 3 947.07 961.73 52.53 o -2 12 3 76.47 85.66 9.48 o 0 12 3 99.67 97.52 9.90 o 2 12 3 1.87 11.59 10.49 o -14 0 4 552.05 555.61 31.33 o -12 0 4 1106.93 1136.21 59.73 o -10 0 4 1920.86 1968.35 89.40 o -8 0 4 9371.92 9468.59 386.44 o -6 0 4 20031.06 19914.82 802.31 o -4 0 4 19908.99 18291.84 735.77 o -2 0 4 25545.96 23182.80 930.35 o 0 0 4 22989.89 23475.74 941.71 o 2 0 4 50342.09 55315.31 2257.07 o 4 0 4 35970.38 35512.98 1424.82 o 6 0 4 5628.46 5438.53 223.21 o 8 0 4 4955.32 5025.17 208.70 o 10 0 4 5413.60 5534.87 231.87 o 12 0 4 2068.94 2056.80 96.20 o 14 0 4 514.39 466.10 25.86 o -13 1 4 3.59 6.09 12.57 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