#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:49:50 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181890 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/90/2239020.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2239020 _cell_angle_alpha 90.000 _cell_angle_beta 107.934 _cell_angle_gamma 90.000 _cell_length_a 13.2712 _cell_length_b 14.3999 _cell_length_c 20.1984 _exptl_crystal_F_000 1696.00 _reflns_d_resolution_high 0.6815 _cod_data_source_file lh5682Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 13RN067_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 426.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1668.03 1905.34 75.77 o 3 0 0 172654.91 184446.17 14333.37 o 4 0 0 39587.36 41804.13 1341.21 o 5 0 0 1083.22 1259.10 69.37 o 6 0 0 792.01 469.33 49.93 o 7 0 0 10179.35 10293.22 375.30 o 8 0 0 2679.49 2266.22 118.57 o 9 0 0 8974.31 8582.92 331.45 o 10 0 0 311.01 271.03 50.95 o 11 0 0 10873.70 10513.17 538.43 o 12 0 0 8679.76 7871.26 622.84 o 13 0 0 459.48 490.99 111.79 o 14 0 0 1203.70 1191.56 182.52 o 15 0 0 4911.40 4644.29 248.19 o 16 0 0 4.01 27.87 48.32 o 17 0 0 2080.68 2047.11 185.00 o 18 0 0 3.30 73.25 67.30 o 2 1 0 1845.60 1904.67 52.69 o 3 1 0 51173.01 56835.76 1513.81 o 4 1 0 3092.57 3254.54 91.51 o 5 1 0 3439.59 3451.32 122.67 o 6 1 0 3776.31 4118.86 119.41 o 8 1 0 121.68 133.07 24.58 o 9 1 0 2701.98 2701.81 137.52 o 10 1 0 8684.54 8267.46 232.10 o 11 1 0 1427.09 1457.21 96.16 o 12 1 0 753.64 797.24 66.89 o 13 1 0 896.84 863.59 71.52 o 14 1 0 7.52 -0.76 27.49 o 15 1 0 142.60 90.36 48.01 o 16 1 0 316.61 441.95 82.33 o 17 1 0 382.38 442.70 66.02 o 18 1 0 565.50 585.18 87.73 o 0 2 0 37605.62 40546.41 1836.59 o 1 2 0 4484.74 4864.14 115.57 o 2 2 0 650.13 723.77 23.82 o 3 2 0 22926.60 25466.14 879.65 o 4 2 0 5156.90 5100.25 153.78 o 5 2 0 2049.58 2153.03 80.68 o 6 2 0 1885.56 1821.60 66.67 o 7 2 0 867.26 931.87 47.83 o 8 2 0 1344.17 1410.88 61.69 o 9 2 0 33.85 9.43 16.43 o 10 2 0 1.66 -11.06 15.91 o 11 2 0 7929.90 7333.32 216.93 o 12 2 0 868.28 875.67 69.78 o 13 2 0 161.55 154.14 34.71 o 14 2 0 4553.10 4640.79 168.93 o 15 2 0 3903.61 3758.04 153.24 o 16 2 0 194.07 121.75 41.60 o 17 2 0 652.54 788.01 84.22 o 18 2 0 500.32 534.57 86.49 o 1 3 0 23688.75 25640.12 749.29 o 2 3 0 348.96 458.36 33.92 o 3 3 0 8864.60 9681.19 239.40 o 4 3 0 24132.09 25047.67 766.29 o 5 3 0 25064.28 25695.24 538.51 o 6 3 0 6974.79 7005.38 210.68 o 7 3 0 7627.83 7115.11 193.09 o 8 3 0 3727.74 3873.55 123.25 o 9 3 0 1422.36 1375.20 75.03 o 10 3 0 8920.84 8492.42 238.90 o 11 3 0 418.16 353.61 43.80 o 12 3 0 7807.04 7638.85 230.34 o 13 3 0 5604.42 5692.03 191.07 o 14 3 0 701.42 712.55 69.51 o 15 3 0 1318.70 1312.50 97.93 o 16 3 0 4467.84 4679.02 180.36 o 17 3 0 44.49 56.31 38.06 o 18 3 0 420.06 474.53 141.45 o 0 4 0 6032.77 6822.34 231.49 o 1 4 0 15408.75 16562.96 444.98 o 2 4 0 2537.83 2826.91 76.73 o 3 4 0 0.90 -6.93 6.93 o 4 4 0 263.37 262.48 22.84 o 5 4 0 6930.51 7489.50 193.27 o 6 4 0 3538.59 3523.09 107.82 o 7 4 0 714.59 626.82 50.08 o 8 4 0 111.75 101.46 21.99 o 9 4 0 232.34 190.38 29.78 o 10 4 0 1641.00 1624.76 125.36 o 11 4 0 104.86 116.43 28.60 o 12 4 0 139.58 228.67 47.75 o 13 4 0 7.37 61.09 29.22 o 14 4 0 0.46 -31.61 31.61 o 15 4 0 76.99 51.41 34.71 o 16 4 0 103.34 110.65 40.46 o 17 4 0 125.56 94.97 65.81 o 1 5 0 14416.48 15971.11 433.40 o 2 5 0 7408.33 7336.43 214.47 o 3 5 0 356.18 327.09 22.29 o 4 5 0 937.19 714.01 40.50 o 5 5 0 2535.36 2341.74 88.58 o 6 5 0 8025.33 8280.42 216.49 o 7 5 0 3213.60 3002.22 100.04 o 8 5 0 716.73 781.09 53.64 o 9 5 0 3050.01 2895.38 106.24 o 10 5 0 5571.02 5342.04 209.44 o 11 5 0 751.74 787.09 63.36 o 12 5 0 1972.82 1854.09 130.95 o 13 5 0 2730.41 2572.49 140.98 o 14 5 0 895.33 961.73 81.01 o 15 5 0 382.03 313.18 73.28 o 16 5 0 2609.54 2699.70 180.49 o 17 5 0 10.06 -36.77 37.25 o 0 6 0 36571.93 39436.36 1263.14 o 1 6 0 496.57 621.51 37.37 o 2 6 0 19834.79 21072.96 571.32 o 3 6 0 11257.81 11029.44 548.62 o 4 6 0 718.09 708.85 45.11 o 5 6 0 22069.23 22341.72 526.27 o 6 6 0 15408.25 14633.60 439.95 o 7 6 0 34.64 73.91 18.91 o 8 6 0 1273.68 1251.34 66.11 o 9 6 0 7891.50 7744.63 219.57 o 10 6 0 2662.28 2683.08 105.50 o 11 6 0 6401.79 6252.00 195.76 o 12 6 0 3279.55 3137.58 129.17 o 13 6 0 227.59 213.56 80.87 o 14 6 0 974.02 1065.99 133.49 o 15 6 0 2028.19 2226.07 158.40 o 16 6 0 1236.47 1105.11 141.10 o 17 6 0 2765.77 2541.09 220.17 o 1 7 0 655.01 618.58 41.78 o 2 7 0 4029.10 3834.79 129.32 o 3 7 0 6.21 -7.20 13.57 o 4 7 0 47.77 43.23 9.76 o 5 7 0 11793.13 12800.12 339.51 o 6 7 0 1993.13 2142.06 132.34 o 7 7 0 1108.34 1069.87 57.13 o 8 7 0 631.05 647.95 70.14 o 9 7 0 6646.98 6514.53 226.83 o 10 7 0 126.88 121.92 62.14 o 11 7 0 986.91 1025.77 105.07 o 12 7 0 10.00 4.73 29.40 o 13 7 0 413.24 491.62 72.37 o 14 7 0 890.81 965.86 100.09 o 15 7 0 10.48 8.48 39.83 o 16 7 0 296.66 289.66 71.56 o 17 7 0 354.76 234.92 84.41 o 0 8 0 30584.36 30882.90 1209.18 o 1 8 0 5658.92 5423.42 172.14 o 2 8 0 5533.89 6087.30 191.81 o 3 8 0 13179.35 12892.90 582.99 o 4 8 0 7920.47 7687.55 268.09 o 5 8 0 8351.20 8018.48 253.61 o 6 8 0 10603.80 10196.54 315.08 o 7 8 0 1875.70 1767.80 164.09 o 8 8 0 5850.72 5643.31 303.04 o 9 8 0 19120.63 17589.54 525.05 o 10 8 0 1140.15 1020.69 90.54 o 11 8 0 2999.44 3031.90 153.20 o 12 8 0 5932.36 5720.81 290.65 o 13 8 0 716.04 717.86 87.46 o 14 8 0 400.14 449.97 74.91 o 15 8 0 256.01 225.73 74.78 o 16 8 0 950.73 1198.01 122.16 o 1 9 0 4727.70 4443.47 265.45 o 2 9 0 254.88 222.34 35.74 o 3 9 0 151.49 74.50 24.92 o 4 9 0 547.09 493.24 48.25 o 5 9 0 6031.82 5782.74 203.08 o 6 9 0 7688.99 7183.29 346.06 o 7 9 0 1400.45 1178.36 85.36 o 8 9 0 1915.78 1927.43 119.23 o 9 9 0 618.37 576.14 67.50 o 10 9 0 5560.05 5755.84 221.20 o 11 9 0 410.58 362.42 60.23 o 12 9 0 545.69 552.37 75.95 o 13 9 0 305.11 331.36 64.46 o 14 9 0 0.71 10.95 41.06 o 15 9 0 576.54 559.63 87.58 o 16 9 0 1162.28 1284.66 159.32 o 0 10 0 8572.78 9335.80 513.33 o 1 10 0 20.52 25.73 15.86 o 2 10 0 569.15 614.89 50.93 o 3 10 0 3217.21 3032.48 119.64 o 4 10 0 702.99 688.74 59.04 o 5 10 0 1017.97 1051.01 78.02 o 6 10 0 8622.17 8105.73 266.24 o 7 10 0 3951.46 3690.03 152.88 o 8 10 0 587.33 569.96 64.72 o 9 10 0 1149.79 1042.46 90.84 o 10 10 0 372.20 407.33 62.70 o 11 10 0 154.50 187.49 47.82 o 12 10 0 420.03 377.02 67.46 o 13 10 0 677.82 777.49 93.83 o 14 10 0 466.66 443.92 76.61 o 15 10 0 736.39 793.46 101.58 o 1 11 0 1401.79 1375.46 134.61 o 2 11 0 5.43 12.99 17.05 o 3 11 0 14814.84 14898.28 435.79 o 4 11 0 22472.65 21617.95 635.93 o 5 11 0 2012.18 2177.51 113.49 o 6 11 0 1895.04 1662.11 104.97 o 7 11 0 4976.27 4495.47 267.57 o 8 11 0 2129.35 2350.56 179.22 o 9 11 0 4.74 26.21 30.92 o 10 11 0 1763.94 1591.76 179.44 o 11 11 0 121.34 124.59 47.11 o 12 11 0 3389.15 3531.35 184.60 o 13 11 0 3233.86 3227.84 196.38 o 14 11 0 32.10 -12.48 50.98 o 15 11 0 2553.70 2586.28 186.38 o 0 12 0 2634.36 2491.37 209.90 o 1 12 0 4014.66 3470.98 183.06 o 2 12 0 21.99 106.45 39.95 o 3 12 0 1889.01 1922.23 148.31 o 4 12 0 140.77 89.30 29.15 o 5 12 0 551.94 501.43 58.33 o 6 12 0 8559.77 8153.67 287.77 o 7 12 0 635.94 574.18 66.85 o 8 12 0 7.80 -15.32 25.15 o 9 12 0 2066.12 2069.01 135.63 o 10 12 0 678.08 713.44 107.17 o 11 12 0 599.33 600.07 80.23 o 12 12 0 90.27 86.59 51.11 o 13 12 0 362.34 369.36 71.73 o 14 12 0 927.31 715.09 97.87 o 1 13 0 1391.91 1485.95 157.42 o 2 13 0 1473.55 1372.39 127.42 o 3 13 0 310.45 305.76 63.71 o 4 13 0 973.70 841.00 99.87 o 5 13 0 110.14 101.85 45.08 o 6 13 0 356.88 296.07 63.99 o 7 13 0 2266.26 1922.22 124.34 o 8 13 0 536.84 447.21 77.29 o 9 13 0 711.36 502.90 73.44 o 10 13 0 1226.29 1215.92 173.18 o 11 13 0 1010.55 995.58 123.09 o 12 13 0 1.46 10.02 41.70 o 13 13 0 385.57 379.68 79.14 o 14 13 0 5.71 -25.13 57.12 o 0 14 0 13424.41 14197.63 782.55 o 1 14 0 3182.68 3140.38 288.61 o 2 14 0 607.85 529.92 110.65 o 3 14 0 5586.73 5591.15 271.83 o 4 14 0 1223.25 1206.90 144.87 o 5 14 0 2832.57 2839.61 260.09 o 6 14 0 2454.16 2448.06 189.43 o 7 14 0 186.76 127.38 58.18 o 8 14 0 4234.36 4346.21 346.78 o 9 14 0 4233.87 4615.80 320.55 o 10 14 0 1173.55 899.13 149.44 o 11 14 0 3503.41 3510.55 192.32 o 12 14 0 978.54 1061.77 112.25 o 13 14 0 114.30 156.64 74.38 o 1 15 0 886.56 935.69 113.66 o 2 15 0 309.21 404.64 161.98 o 3 15 0 207.56 141.97 60.46 o 4 15 0 54.36 27.87 93.54 o 5 15 0 1019.23 1133.01 248.68 o 6 15 0 301.00 325.64 76.43 o 7 15 0 154.56 84.41 86.70 o 8 15 0 55.23 155.78 63.34 o 9 15 0 20.51 -48.32 48.32 o 10 15 0 219.54 227.80 78.26 o 11 15 0 7.33 80.29 70.93 o 12 15 0 357.01 511.91 109.38 o 0 16 0 1472.00 1576.50 219.02 o 1 16 0 2009.83 1854.34 168.58 o 2 16 0 672.32 788.85 111.00 o 3 16 0 5332.26 5259.96 666.19 o 4 16 0 1744.78 1554.48 155.62 o 5 16 0 537.21 739.18 110.43 o 6 16 0 2876.44 2655.98 704.98 o 7 16 0 1794.71 1619.38 165.07 o 8 16 0 849.07 808.17 121.79 o 9 16 0 1693.39 1798.89 252.10 o 10 16 0 20.11 1.56 60.29 o 11 16 0 253.00 143.73 107.23 o 1 17 0 4756.58 5209.90 281.51 o 2 17 0 2199.16 1985.10 183.38 o 3 17 0 80.04 9.99 46.77 o 4 17 0 1089.69 1087.30 140.32 o 5 17 0 158.16 95.06 57.47 o 6 17 0 844.73 858.23 126.57 o 7 17 0 234.84 391.09 171.11 o 8 17 0 741.81 784.39 126.02 o 9 17 0 821.30 866.46 131.41 o 0 18 0 96.01 123.20 88.98 o 1 18 0 152.19 82.13 77.57 o 2 18 0 945.13 1062.81 138.29 o 3 18 0 393.50 362.95 89.52 o 4 18 0 118.90 122.76 66.94 o 5 18 0 18.50 21.84 50.64 o 6 18 0 913.92 856.73 339.94 o 7 18 0 473.10 389.07 97.51 o 8 18 0 47.32 -28.66 60.46 o 1 19 0 79.12 107.31 63.99 o 2 19 0 987.95 1107.07 154.00 o 3 19 0 685.28 739.01 123.34 o 4 19 0 356.50 360.67 95.98 o 5 19 0 462.58 361.33 120.92 o 6 19 0 214.96 130.04 114.07 o 0 20 0 881.80 1170.40 223.58 o 1 20 0 403.90 372.86 190.50 o 2 20 0 1610.01 1282.19 250.96 o -18 1 1 1809.27 1843.22 128.93 o -17 1 1 0.28 13.87 38.83 o -16 1 1 1721.40 1631.23 111.47 o -15 1 1 9.67 53.28 33.18 o -14 1 1 4522.93 4448.52 164.22 o -13 1 1 5554.24 5072.73 173.74 o -12 1 1 2796.80 2696.28 143.91 o -11 1 1 3863.45 3667.04 135.01 o -10 1 1 14092.35 13330.46 346.12 o -9 1 1 1728.76 1904.77 78.81 o -8 1 1 610.68 640.91 46.51 o -7 1 1 113.94 27.62 14.50 o -6 1 1 1199.20 1176.25 51.14 o -5 1 1 24471.02 24496.48 568.81 o -4 1 1 5048.25 4745.46 183.09 o -3 1 1 7579.70 8207.70 196.98 o -2 1 1 6780.51 7279.42 171.60 o -1 1 1 39778.73 44107.79 1959.79 o 1 1 1 35585.89 35824.63 2418.59 o 2 1 1 6167.34 6745.52 161.10 o 3 1 1 4346.46 4433.07 127.82 o 4 1 1 14896.38 15343.80 361.28 o 5 1 1 34063.98 33997.23 1397.62 o 6 1 1 158.44 271.38 33.56 o 7 1 1 6910.09 6726.21 203.84 o 8 1 1 780.63 883.99 68.82 o 9 1 1 1706.75 1440.22 78.41 o 10 1 1 9329.99 8814.47 245.72 o 11 1 1 913.71 818.74 75.74 o 12 1 1 7415.52 7157.66 219.21 o 13 1 1 3585.40 3503.75 136.73 o 14 1 1 3440.38 3408.18 139.11 o 15 1 1 1139.73 1104.46 88.59 o 16 1 1 2658.21 2900.42 179.47 o 17 1 1 359.88 453.16 88.01 o 18 1 1 105.98 181.49 73.39 o -18 2 1 201.63 166.55 58.95 o -17 2 1 1709.11 1505.86 113.28 o -16 2 1 142.85 92.73 39.21 o -15 2 1 945.35 1013.76 94.84 o -14 2 1 603.84 673.42 66.69 o -13 2 1 143.30 59.36 30.63 o -12 2 1 1475.05 1552.89 95.17 o -11 2 1 4668.09 4836.47 159.01 o -10 2 1 176.18 169.61 29.18 o -9 2 1 7305.68 7363.87 350.38 o -8 2 1 2171.92 2128.09 109.17 o -7 2 1 2221.86 2244.40 92.53 o -6 2 1 12038.70 12382.23 304.67 o -5 2 1 4137.00 4520.06 139.16 o -4 2 1 34179.94 34345.11 809.50 o -3 2 1 217.71 322.50 22.39 o -2 2 1 7255.44 8075.21 224.58 o -1 2 1 8534.67 9100.92 209.99 o 0 2 1 37565.12 34303.18 4438.61 o 1 2 1 192.29 196.44 12.83 o 2 2 1 9765.47 10214.14 239.20 o 3 2 1 2952.15 2720.79 76.62 o 4 2 1 2778.93 3033.92 87.44 o 5 2 1 5042.85 4915.08 161.69 o 6 2 1 3268.17 2896.20 92.60 o 7 2 1 1777.42 1660.77 66.92 o 8 2 1 5694.91 5380.02 241.71 o 9 2 1 5663.06 5364.32 223.93 o 10 2 1 1330.37 1245.20 84.37 o 11 2 1 6242.40 6205.49 191.32 o 12 2 1 2036.81 2023.41 109.97 o 13 2 1 334.31 356.61 47.92 o 14 2 1 207.76 286.61 48.82 o 15 2 1 2594.56 2198.48 127.45 o 16 2 1 235.99 260.69 53.41 o 17 2 1 2055.95 2072.04 207.79 o 18 2 1 93.94 63.70 48.30 o -18 3 1 65.45 94.84 50.95 o -17 3 1 336.00 484.18 65.90 o -16 3 1 2.18 39.31 34.63 o -15 3 1 508.79 420.84 57.42 o -14 3 1 993.50 1073.58 86.27 o -13 3 1 52.72 6.62 25.90 o -12 3 1 1502.08 1632.72 96.81 o -11 3 1 239.68 278.32 39.16 o -10 3 1 39.54 46.13 22.02 o -9 3 1 0.92 -7.49 13.98 o -8 3 1 1269.12 1290.32 65.67 o -7 3 1 6976.64 7624.83 204.45 o -6 3 1 185.47 272.58 27.83 o -5 3 1 3303.31 3411.72 99.77 o -4 3 1 11063.22 12232.06 373.10 o -3 3 1 157.89 178.91 16.85 o -2 3 1 301.69 373.40 19.44 o -1 3 1 1197.76 1308.52 45.14 o 0 3 1 2180.88 2364.93 78.04 o 1 3 1 232.81 304.68 18.13 o 2 3 1 16826.78 17338.02 398.50 o 3 3 1 75.25 76.25 12.89 o 4 3 1 1178.77 1105.28 43.33 o 5 3 1 2883.48 2810.32 87.43 o 6 3 1 2787.51 2923.59 125.79 o 7 3 1 2105.97 1954.33 119.87 o 8 3 1 43.66 48.89 19.00 o 9 3 1 144.57 146.05 23.36 o 10 3 1 0.53 -15.85 16.68 o 11 3 1 296.09 285.59 40.12 o 12 3 1 375.44 398.03 48.06 o 13 3 1 815.14 845.34 101.77 o 14 3 1 541.43 592.86 85.95 o 15 3 1 151.03 206.93 46.61 o 16 3 1 397.30 445.75 62.21 o 17 3 1 272.65 251.11 53.16 o -17 4 1 3066.80 3504.46 212.78 o -16 4 1 71.57 58.52 35.80 o -15 4 1 6169.66 6354.34 217.46 o -14 4 1 1130.95 1211.81 121.51 o -13 4 1 186.18 223.39 39.95 o -12 4 1 2323.89 2080.04 137.32 o -11 4 1 8281.94 8140.95 236.37 o -10 4 1 80.23 55.20 30.30 o -9 4 1 17774.24 18329.30 455.14 o -8 4 1 5985.26 5487.80 161.28 o -7 4 1 1243.90 1261.81 62.31 o -6 4 1 42161.50 43786.93 1002.94 o -5 4 1 12109.76 12052.55 294.80 o -4 4 1 449.89 417.32 27.69 o -3 4 1 8582.39 9125.64 220.90 o -2 4 1 2468.78 2732.79 84.63 o -1 4 1 155.49 139.40 17.10 o 0 4 1 11442.69 12001.74 313.50 o 1 4 1 38656.39 42273.84 949.90 o 2 4 1 9781.83 10116.34 217.92 o 3 4 1 25360.11 26235.35 544.16 o 4 4 1 4031.84 4113.27 146.87 o 5 4 1 10003.80 9340.70 213.08 o 6 4 1 27629.23 28291.80 597.72 o 7 4 1 103.46 69.85 16.30 o 8 4 1 1874.93 1712.85 73.97 o 9 4 1 3583.64 3380.99 118.13 o 10 4 1 1376.12 1446.34 82.59 o 11 4 1 13295.00 11955.12 323.66 o 12 4 1 1099.10 1009.01 76.10 o 13 4 1 795.09 852.51 74.27 o 14 4 1 8924.15 8527.14 262.86 o 15 4 1 4122.70 3879.93 159.71 o 16 4 1 399.87 338.99 56.45 o 17 4 1 2876.12 3178.09 199.89 o -17 5 1 2.81 55.72 48.58 o -16 5 1 4612.52 5115.43 281.86 o -15 5 1 559.35 461.21 74.06 o -14 5 1 225.36 199.50 44.46 o -13 5 1 155.78 174.22 39.94 o -12 5 1 142.51 163.49 36.31 o -11 5 1 940.44 1009.84 71.67 o -10 5 1 585.68 642.75 55.32 o -9 5 1 4783.33 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