# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared), status flag # data_2239108 _cell_angle_alpha 90.000 _cell_angle_beta 104.051 _cell_angle_gamma 90.000 _cell_length_a 11.9339 _cell_length_b 12.4369 _cell_length_c 17.9627 _exptl_crystal_F_000 1488.00 _reflns_d_resolution_high 0.7601 _cod_data_source_file is5307Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ZnF4BDC in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 306.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6341.51 6484.22 219.15 o 4 0 0 1463.77 1688.95 247.32 o 6 0 0 1249.77 1785.54 160.06 o 8 0 0 671.38 914.61 295.13 o 10 0 0 10068.13 10873.46 564.17 o 12 0 0 0.17 -264.38 264.38 o 14 0 0 596.36 803.48 385.07 o 1 1 0 1294.53 1329.08 55.75 o 2 1 0 596.09 613.31 40.63 o 3 1 0 1452.78 1580.79 84.80 o 4 1 0 3525.93 3659.56 102.29 o 5 1 0 1.33 -35.01 62.72 o 6 1 0 4664.83 4530.33 127.58 o 7 1 0 6560.85 6958.08 160.17 o 8 1 0 4151.51 4221.11 182.06 o 9 1 0 3.19 52.64 156.45 o 10 1 0 90.21 15.72 146.48 o 11 1 0 37.28 -193.88 193.88 o 12 1 0 78.00 109.48 222.92 o 13 1 0 7.63 -37.59 185.74 o 14 1 0 838.90 534.08 254.37 o 0 2 0 108.28 48.84 108.80 o 1 2 0 17274.74 15809.26 351.09 o 2 2 0 9654.20 8337.58 149.81 o 3 2 0 3176.61 3186.58 130.31 o 4 2 0 5008.05 5073.39 116.41 o 5 2 0 10425.35 10373.27 176.10 o 6 2 0 4606.81 5000.05 124.74 o 7 2 0 3407.79 3466.49 124.89 o 8 2 0 10721.58 10087.84 278.12 o 9 2 0 1229.07 1601.07 193.43 o 10 2 0 234.74 -20.69 194.98 o 11 2 0 471.11 492.83 240.15 o 12 2 0 3230.05 3724.07 328.87 o 13 2 0 312.36 257.90 245.71 o 14 2 0 79.36 -88.90 323.82 o 1 3 0 3776.31 3953.30 165.53 o 2 3 0 8147.58 7921.75 175.25 o 3 3 0 10738.42 10743.90 161.49 o 4 3 0 1480.53 1556.34 92.64 o 5 3 0 302.18 397.02 84.86 o 6 3 0 5784.09 5392.21 148.67 o 7 3 0 2110.39 2536.42 139.13 o 8 3 0 655.34 924.28 140.81 o 9 3 0 1970.73 2130.56 277.66 o 10 3 0 326.59 438.00 222.33 o 11 3 0 418.51 222.63 229.78 o 12 3 0 194.10 80.14 327.96 o 13 3 0 34.78 -190.30 232.34 o 14 3 0 266.89 -375.77 375.77 o 0 4 0 752.55 909.44 227.42 o 1 4 0 20438.81 17689.84 1328.87 o 2 4 0 1742.58 1691.99 143.88 o 3 4 0 20187.92 19669.79 212.15 o 4 4 0 593.07 600.72 84.33 o 5 4 0 4507.94 4119.98 135.58 o 6 4 0 2629.95 2747.92 137.16 o 7 4 0 809.43 1002.94 150.71 o 8 4 0 2532.55 2742.14 235.22 o 9 4 0 1178.70 1066.88 260.00 o 10 4 0 3229.39 3334.93 485.47 o 11 4 0 1582.17 1897.37 368.66 o 12 4 0 1287.98 972.83 288.90 o 13 4 0 406.20 363.67 268.63 o 14 4 0 360.77 335.28 917.71 o 1 5 0 74.02 -30.64 131.96 o 2 5 0 23456.63 22059.65 444.12 o 3 5 0 181.63 191.46 128.93 o 4 5 0 13237.89 13219.83 296.47 o 5 5 0 2271.00 2404.79 128.25 o 6 5 0 3220.24 3184.82 189.54 o 7 5 0 1153.36 1250.19 195.02 o 8 5 0 3960.99 3967.75 251.22 o 9 5 0 183.80 115.57 228.59 o 10 5 0 45.79 56.33 225.26 o 11 5 0 325.88 230.48 244.74 o 12 5 0 149.03 -91.34 242.98 o 13 5 0 237.85 37.97 283.14 o 14 5 0 686.90 870.07 311.83 o 0 6 0 3076.82 3364.84 350.44 o 1 6 0 900.52 789.31 190.50 o 2 6 0 22.65 -74.20 140.17 o 3 6 0 4332.61 4348.89 229.71 o 4 6 0 6693.89 6264.42 297.97 o 5 6 0 953.36 968.77 154.75 o 6 6 0 12890.64 12208.15 290.58 o 7 6 0 3762.72 3835.75 221.29 o 8 6 0 206.38 146.70 178.85 o 9 6 0 103.10 97.84 228.97 o 10 6 0 3766.76 3548.04 366.22 o 11 6 0 707.09 641.94 270.64 o 12 6 0 329.16 -65.99 237.64 o 13 6 0 1257.86 927.46 304.41 o 14 6 0 467.53 837.33 450.45 o 1 7 0 5709.38 5785.76 292.34 o 2 7 0 26.53 -9.25 163.80 o 3 7 0 1222.21 1116.09 192.86 o 4 7 0 3754.83 3490.88 242.93 o 5 7 0 261.09 290.98 163.00 o 6 7 0 4841.48 4621.12 238.58 o 7 7 0 54.84 148.92 159.48 o 8 7 0 750.67 947.82 214.39 o 9 7 0 14.06 -240.00 249.42 o 10 7 0 144.80 9.67 251.43 o 11 7 0 1057.79 987.64 353.93 o 12 7 0 58.27 -115.78 258.93 o 13 7 0 2.82 -176.84 276.49 o 0 8 0 56.13 -90.45 304.18 o 1 8 0 941.57 1247.51 253.31 o 2 8 0 16296.76 15145.80 452.65 o 3 8 0 2703.13 2688.06 264.69 o 4 8 0 1897.36 2192.53 213.61 o 5 8 0 760.39 731.33 182.08 o 6 8 0 3152.19 3610.03 245.20 o 7 8 0 301.78 150.25 170.05 o 8 8 0 1575.32 1738.55 243.16 o 9 8 0 65.78 46.42 268.07 o 10 8 0 180.79 -153.94 259.61 o 11 8 0 129.92 -142.04 252.78 o 12 8 0 2234.10 1917.32 560.29 o 13 8 0 30.88 528.24 392.82 o 1 9 0 1017.47 936.29 252.03 o 2 9 0 79.30 204.26 261.51 o 3 9 0 981.36 813.02 229.31 o 4 9 0 1399.13 1515.63 212.12 o 5 9 0 189.05 272.66 187.76 o 6 9 0 2431.16 2590.70 278.80 o 7 9 0 377.74 302.61 179.79 o 8 9 0 2425.70 2577.15 282.40 o 9 9 0 523.06 246.26 294.20 o 10 9 0 5.69 88.90 424.87 o 11 9 0 108.52 -266.49 266.49 o 12 9 0 249.92 -88.79 296.48 o 0 10 0 9346.52 7983.88 595.44 o 1 10 0 739.09 880.39 292.57 o 2 10 0 419.42 360.07 251.39 o 3 10 0 914.63 1119.20 237.67 o 4 10 0 2691.47 3108.11 252.68 o 5 10 0 4885.12 5156.79 268.44 o 6 10 0 2632.56 2931.17 250.52 o 7 10 0 390.46 307.91 190.15 o 8 10 0 17.63 -208.35 208.35 o 9 10 0 147.61 -204.58 291.81 o 10 10 0 1702.62 2033.29 391.89 o 11 10 0 265.75 -294.02 294.02 o 1 11 0 1195.90 1191.95 399.67 o 2 11 0 299.05 226.94 189.75 o 3 11 0 21.99 -104.87 171.31 o 4 11 0 444.56 497.23 211.47 o 5 11 0 12.58 -9.44 188.36 o 6 11 0 417.10 280.58 198.47 o 7 11 0 110.21 -117.42 213.03 o 8 11 0 371.62 133.64 232.35 o 9 11 0 124.34 -296.00 296.00 o 10 11 0 7.48 -219.85 296.37 o 0 12 0 1989.46 2816.70 511.19 o 1 12 0 602.64 741.11 294.08 o 2 12 0 243.19 376.95 322.21 o 3 12 0 2586.83 2939.32 331.64 o 4 12 0 3.13 -191.13 191.13 o 5 12 0 1178.73 1255.30 257.14 o 6 12 0 388.44 337.34 208.98 o 7 12 0 1587.90 1896.97 307.02 o 8 12 0 497.17 434.92 287.16 o 9 12 0 172.29 -244.64 329.51 o 1 13 0 1763.51 2435.85 374.63 o 2 13 0 217.22 399.62 291.29 o 3 13 0 587.17 673.33 236.12 o 4 13 0 570.80 442.06 230.08 o 5 13 0 42.34 -88.05 215.34 o 6 13 0 178.00 325.73 228.72 o 7 13 0 8.48 -284.38 284.38 o 8 13 0 10.77 68.96 606.57 o 0 14 0 9.28 -24.29 444.77 o 1 14 0 305.15 139.62 360.78 o 2 14 0 2155.56 2112.98 372.56 o 3 14 0 149.87 -277.86 277.86 o 4 14 0 39.97 -68.81 210.59 o 5 14 0 1846.81 2308.72 289.81 o 6 14 0 471.95 1173.95 303.02 o 7 14 0 24.97 237.12 305.06 o 1 15 0 494.52 576.75 342.78 o 2 15 0 174.81 176.82 317.88 o 3 15 0 769.19 1037.62 361.58 o 4 15 0 400.78 72.49 323.27 o 5 15 0 32.66 203.10 273.08 o 6 15 0 330.78 1030.42 322.32 o 1 16 0 0.75 64.87 495.16 o 2 16 0 226.33 58.92 474.75 o -15 0 1 4433.25 4343.80 541.17 o -13 0 1 23.22 -259.21 259.21 o -11 0 1 2915.20 2986.22 283.28 o -9 0 1 11303.58 11518.25 527.47 o -7 0 1 8868.54 9476.82 381.06 o -5 0 1 11793.51 11261.63 484.96 o -3 0 1 1916.40 2315.59 189.43 o -1 0 1 94050.51 98991.49 744.30 o 1 0 1 20221.12 21627.51 274.20 o 3 0 1 5711.67 5904.18 147.09 o 5 0 1 13435.58 11602.84 217.97 o 7 0 1 7768.69 7377.27 235.70 o 9 0 1 13220.99 12862.64 582.52 o 11 0 1 1601.17 1762.47 721.81 o 13 0 1 220.16 -266.19 266.19 o -15 1 1 5.30 -291.26 291.26 o -14 1 1 166.23 -125.10 226.29 o -13 1 1 1108.82 1233.16 285.06 o -12 1 1 200.88 157.91 215.41 o -11 1 1 102.71 106.47 227.55 o -10 1 1 27.26 208.67 162.53 o -9 1 1 6573.98 6901.48 265.90 o -8 1 1 0.95 -20.45 100.03 o -7 1 1 16.27 -11.02 82.05 o -6 1 1 288.82 336.75 79.22 o -5 1 1 14.34 -31.72 63.47 o -4 1 1 857.12 944.66 86.64 o -3 1 1 1323.27 1860.71 94.74 o -2 1 1 233.12 336.61 43.86 o -1 1 1 39146.55 37994.16 815.05 o 0 1 1 5038.14 4635.29 135.22 o 1 1 1 15062.66 14641.96 213.78 o 2 1 1 40.67 24.39 42.44 o 3 1 1 21702.11 20487.05 461.64 o 4 1 1 3039.43 3087.55 81.28 o 5 1 1 122.85 156.03 59.41 o 6 1 1 3409.35 3479.58 102.16 o 7 1 1 785.83 897.40 87.56 o 8 1 1 25.32 -23.28 146.51 o 9 1 1 3891.00 3967.35 243.25 o 10 1 1 156.04 219.52 164.65 o 11 1 1 1529.64 1688.17 272.40 o 12 1 1 609.44 715.76 242.97 o 13 1 1 618.61 552.14 229.78 o 14 1 1 505.63 213.91 254.51 o -15 2 1 652.59 730.34 339.33 o -14 2 1 340.60 598.28 370.60 o -13 2 1 638.43 647.99 428.36 o -12 2 1 121.49 273.96 224.22 o -11 2 1 1049.35 1155.08 240.63 o -10 2 1 928.37 642.15 221.47 o -9 2 1 256.95 159.87 148.19 o -8 2 1 6106.32 6416.94 162.45 o -7 2 1 18020.06 17619.01 266.79 o -6 2 1 3490.16 3687.90 117.28 o -5 2 1 879.64 830.56 75.64 o -4 2 1 487.41 684.07 73.92 o -3 2 1 9917.63 9406.05 226.88 o -2 2 1 6125.03 6006.56 151.53 o -1 2 1 1389.67 1374.40 86.75 o 0 2 1 8858.21 8852.14 639.28 o 1 2 1 2800.50 2663.77 75.69 o 2 2 1 30484.54 29711.99 453.22 o 3 2 1 17481.11 16811.03 353.18 o 4 2 1 699.72 780.34 76.95 o 5 2 1 640.51 869.73 85.35 o 6 2 1 1148.03 1403.92 99.93 o 7 2 1 6565.50 6820.09 165.15 o 8 2 1 9687.64 9298.33 297.71 o 9 2 1 799.60 888.51 186.39 o 10 2 1 45.11 0.27 204.68 o 11 2 1 326.58 243.94 235.40 o 12 2 1 433.86 245.27 232.11 o 13 2 1 1751.22 1862.44 318.54 o 14 2 1 121.26 -268.77 283.76 o -14 3 1 197.62 -270.07 363.62 o -13 3 1 559.45 793.88 291.14 o -12 3 1 76.36 -201.17 201.17 o -11 3 1 3387.06 3393.83 324.51 o -10 3 1 27.01 -46.07 200.55 o -9 3 1 1005.88 1196.56 251.43 o -8 3 1 1200.69 1192.59 155.23 o -7 3 1 939.46 1132.21 117.32 o -6 3 1 343.90 362.60 89.34 o -5 3 1 124.04 153.98 81.04 o -4 3 1 654.19 930.22 84.50 o -3 3 1 8586.02 8440.21 203.71 o -2 3 1 277.22 427.93 116.07 o -1 3 1 1619.81 1569.96 129.59 o 0 3 1 84302.23 81124.31 555.46 o 1 3 1 867.09 1288.27 87.84 o 2 3 1 4684.07 5102.80 147.80 o 3 3 1 1328.79 1518.48 92.11 o 4 3 1 930.97 1332.58 91.58 o 5 3 1 297.10 336.80 86.15 o 6 3 1 254.26 197.85 92.74 o 7 3 1 7472.66 7914.49 193.66 o 8 3 1 960.65 1013.62 172.20 o 9 3 1 942.59 1132.95 245.84 o 10 3 1 67.29 305.85 222.35 o 11 3 1 2447.44 2583.79 333.92 o 12 3 1 38.10 -335.06 335.06 o 13 3 1 249.52 483.71 456.01 o 14 3 1 118.14 -162.67 264.47 o -14 4 1 921.12 1075.99 305.84 o -13 4 1 80.88 -231.09 231.09 o -12 4 1 2174.41 1880.62 311.39 o -11 4 1 1.02 -196.03 196.03 o -10 4 1 560.15 563.32 229.00 o -9 4 1 3694.92 3754.64 334.36 o -8 4 1 711.33 548.08 154.78 o -7 4 1 1121.06 1126.39 155.73 o -6 4 1 2894.11 2622.40 125.47 o -5 4 1 7776.28 7250.44 155.02 o -4 4 1 17190.43 16397.23 282.48 o -3 4 1 16024.91 15864.16 273.81 o -2 4 1 2746.60 2852.38 187.67 o -1 4 1 1810.67 2052.56 152.20 o 0 4 1 38161.40 32429.04 1836.19 o 1 4 1 33230.20 27466.36 1581.82 o 2 4 1 9624.27 9528.73 155.77 o 3 4 1 694.64 806.17 87.20 o 4 4 1 13289.23 12408.35 282.63 o 5 4 1 5798.20 5667.25 157.46 o 6 4 1 14501.29 14255.65 226.08 o 7 4 1 8118.64 8042.54 195.42 o 8 4 1 2387.12 2456.98 292.20 o 9 4 1 42.00 206.58 231.57 o 10 4 1 2305.20 2394.30 426.55 o 11 4 1 13.76 -225.95 225.95 o 12 4 1 630.45 229.68 252.96 o 13 4 1 294.30 322.61 271.96 o 14 4 1 315.16 478.44 309.22 o -14 5 1 110.54 103.50 395.02 o -13 5 1 1915.69 1839.64 344.18 o -12 5 1 1449.01 1246.20 312.65 o -11 5 1 2456.02 2013.51 324.73 o -10 5 1 1792.13 1775.64 286.31 o -9 5 1 3122.61 3322.62 252.81 o -8 5 1 132.04 65.52 149.47 o -7 5 1 123.12 -101.16 144.83 o -6 5 1 1914.05 2026.98 166.21 o -5 5 1 559.26 725.89 157.57 o -4 5 1 752.40 621.16 146.07 o -3 5 1 1494.64 1353.24 157.30 o -2 5 1 1.43 -81.24 118.33 o -1 5 1 2715.90 2534.62 211.76 o 0 5 1 627.34 557.28 156.91 o 1 5 1 696.30 628.29 140.71 o 2 5 1 5099.66 5249.63 190.39 o 3 5 1 9792.17 8858.13 172.83 o 4 5 1 3050.66 2876.49 134.25 o 5 5 1 95.88 34.94 96.40 o 6 5 1 325.59 368.21 124.25 o 7 5 1 142.66 300.29 146.93 o 8 5 1 20.23 147.84 164.35 o 9 5 1 6253.10 6065.21 413.50 o 10 5 1 80.84 14.61 210.98 o 11 5 1 32.75 -100.43 312.58 o 12 5 1 350.08 609.04 283.61 o 13 5 1 1306.71 1357.71 426.55 o 14 5 1 11.62 -320.20 388.95 o -14 6 1 95.33 -350.70 350.70 o -13 6 1 435.42 363.48 263.82 o -12 6 1 221.86 233.52 473.58 o -11 6 1 596.62 429.25 265.42 o -10 6 1 10.22 -235.54 235.54 o -9 6 1 2303.74 2658.30 248.37 o -8 6 1 911.11 829.58 178.44 o -7 6 1 5.65 -76.43 142.09 o -6 6 1 7680.76 7649.43 254.70 o -5 6 1 15331.77 14834.18 349.98 o -4 6 1 9107.63 8386.90 279.48 o -3 6 1 464.36 759.27 166.10 o -2 6 1 1852.52 1556.68 281.94 o -1 6 1 7502.65 5849.51 283.22 o 0 6 1 1627.74 1966.62 219.91 o 1 6 1 8285.38 7463.20 297.93 o 2 6 1 13930.67 13634.79 619.19 o 3 6 1 1488.34 1696.30 148.27 o 4 6 1 177.95 194.34 101.99 o 5 6 1 43422.85 41994.54 603.55 o 6 6 1 5979.23 5796.54 284.61 o 7 6 1 758.05 970.93 170.80 o 8 6 1 97.60 -89.26 157.62 o 9 6 1 449.72 485.10 255.94 o 10 6 1 758.36 329.41 258.23 o 11 6 1 1061.06 850.97 287.13 o 12 6 1 789.10 550.83 289.74 o 13 6 1 152.90 -102.98 405.49 o -13 7 1 563.65 19.77 272.60 o -12 7 1 975.75 1065.81 567.78 o -11 7 1 619.10 423.16 282.26 o -10 7 1 138.07 -139.89 266.32 o -9 7 1 1693.67 1908.77 346.23 o -8 7 1 1206.74 1271.26 225.61 o -7 7 1 1046.10 1096.52 189.91 o -6 7 1 28.59 -101.68 162.29 o -5 7 1 2408.58 2361.46 238.30 o -4 7 1 49.24 143.98 182.41 o -3 7 1 1496.44 1600.27 202.60 o -2 7 1 1885.73 2045.54 205.99 o -1 7 1 222.93 236.56 196.30 o 0 7 1 1091.72 1049.05 215.17 o 1 7 1 12898.23 11073.29 619.99 o 2 7 1 2564.81 2535.35 181.56 o 3 7 1 2014.50 2268.91 183.34 o 4 7 1 167.50 103.03 141.10 o 5 7 1 76.00 115.32 159.55 o 6 7 1 5334.97 5304.26 248.96 o 7 7 1 83.20 137.38 190.51 o 8 7 1 47.89 -113.45 177.15 o 9 7 1 1115.39 1554.52 300.92 o 10 7 1 551.21 601.05 277.58 o 11 7 1 442.36 412.48 584.07 o 12 7 1 128.70 -42.53 276.47 o 13 7 1 6.38 -69.86 295.42 o -13 8 1 1602.08 1728.94 465.19 o -12 8 1 253.80 404.71 297.91 o -11 8 1 960.47 600.90 296.54 o -10 8 1 1023.57 1050.74 306.36 o -9 8 1 12.80 -47.33 177.34 o -8 8 1 40.11 10.69 179.24 o -7 8 1 2246.69 2895.87 231.98 o -6 8 1 14.15 126.70 168.76 o -5 8 1 22.31 -166.08 201.27 o -4 8 1 141.49 91.70 209.45 o -3 8 1 6507.01 5398.49 364.08 o -2 8 1 2831.13 2954.39 304.81 o -1 8 1 5821.44 5594.29 339.25 o 0 8 1 270.95 396.16 216.20 o 1 8 1 351.90 173.32 219.72 o 2 8 1 1460.04 1645.63 188.03 o 3 8 1 17825.93 16305.80 770.89 o 4 8 1 5.29 123.27 170.42 o 5 8 1 152.40 80.02 169.64 o 6 8 1 1.10 61.22 172.45 o 7 8 1 7162.64 7073.42 321.27 o 8 8 1 1466.58 1387.81 286.54 o 9 8 1 38.74 47.94 306.63 o 10 8 1 308.93 -38.75 263.43 o 11 8 1 1546.21 1119.60 325.67 o 12 8 1 496.27 215.03 306.36 o -12 9 1 9.44 -284.19 284.19 o -11 9 1 488.57 378.84 357.16 o -10 9 1 76.67 -35.12 585.49 o -9 9 1 112.95 -255.26 299.31 o -8 9 1 13.75 -102.02 213.86 o -7 9 1 1410.94 1471.82 257.62 o -6 9 1 4.89 -85.06 168.45 o -5 9 1 714.52 789.58 236.93 o -4 9 1 3490.86 3444.71 292.94 o -3 9 1 6855.46 6784.46 393.89 o -2 9 1 1547.11 1411.67 297.26 o -1 9 1 1317.28 1513.39 296.86 o 0 9 1 3150.11 3624.80 328.72 o 1 9 1 3853.99 4089.38 269.54 o 2 9 1 275.27 425.43 193.34 o 3 9 1 104.10 -101.67 176.52 o 4 9 1 2790.81 2672.93 225.65 o 5 9 1 690.37 641.87 193.19 o 6 9 1 507.85 546.46 183.66 o 7 9 1 142.68 -26.19 206.93 o 8 9 1 1160.18 1049.34 240.14 o 9 9 1 194.18 -191.73 257.53 o 10 9 1 275.00 -68.91 293.19 o 11 9 1 836.52 436.11 315.19 o 12 9 1 104.35 -226.23 320.98 o -11 10 1 64.73 -292.97 292.97 o -10 10 1 904.14 759.62 346.42 o -9 10 1 1657.19 1588.33 269.47 o -8 10 1 1.79 -48.08 249.02 o -7 10 1 103.46 -125.65 180.36 o -6 10 1 1421.88 1600.45 218.70 o -5 10 1 8260.77 7832.14 307.34 o -4 10 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