# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2239110 _cell_angle_alpha 84.614 _cell_angle_beta 67.682 _cell_angle_gamma 63.134 _cell_length_a 7.9910 _cell_length_b 8.4273 _cell_length_c 9.6172 _exptl_crystal_F_000 328.00 _reflns_d_resolution_high 0.8156 _cod_data_source_file nk2214Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BALA11_0m in P-1 New: P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 118.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1121.78 1518.99 10.03 o 3 0 0 7126.95 7541.45 175.85 o 4 0 0 3652.03 4203.19 42.10 o 5 0 0 185.56 207.98 4.70 o 6 0 0 3458.42 3838.58 30.32 o 7 0 0 3348.81 3956.91 45.54 o 8 0 0 227.79 231.57 9.60 o -7 1 0 78.99 83.72 1.79 o -6 1 0 0.08 2.16 0.59 o -5 1 0 9.80 11.14 0.62 o -4 1 0 1.08 3.98 0.39 o -3 1 0 1.77 4.91 0.33 o -2 1 0 0.68 0.43 0.21 o -1 1 0 23.02 31.65 0.61 o 0 1 0 0.05 10.41 0.20 o 1 1 0 1.13 -0.17 0.17 o 2 1 0 21.11 29.27 0.46 o 3 1 0 73.16 63.17 0.73 o 4 1 0 130.45 135.75 1.70 o 5 1 0 35.25 43.55 1.07 o 6 1 0 58.58 65.65 1.34 o 7 1 0 36.89 38.58 1.03 o 8 1 0 0.53 0.86 0.29 o -7 2 0 1455.52 1540.14 40.70 o -6 2 0 2850.12 3340.62 79.89 o -5 2 0 167.10 186.88 3.30 o -4 2 0 2198.28 2440.04 27.04 o -3 2 0 13932.07 17294.15 365.77 o -2 2 0 3836.29 4572.36 31.26 o -1 2 0 998.68 955.50 9.03 o 2 2 0 1425.31 2060.88 12.79 o 5 2 0 1545.59 1838.87 16.79 o 6 2 0 1210.52 1335.02 12.40 o 7 2 0 2157.45 2472.33 24.29 o 8 2 0 255.43 279.81 5.21 o -6 3 0 79.71 76.81 1.57 o -5 3 0 64.15 72.85 1.14 o -4 3 0 0.73 2.35 0.51 o -3 3 0 55.67 55.71 1.24 o -2 3 0 65.72 68.71 1.65 o -1 3 0 50.73 75.31 1.80 o 0 3 0 32.80 63.50 0.92 o 1 3 0 151.49 129.16 2.04 o 2 3 0 18.77 16.46 0.55 o 3 3 0 78.46 121.39 1.19 o 4 3 0 80.47 62.07 0.87 o 5 3 0 55.96 75.93 1.55 o 6 3 0 143.80 159.66 1.96 o 7 3 0 240.86 263.48 3.02 o 8 3 0 72.30 78.90 1.73 o -5 4 0 373.59 433.74 3.66 o -4 4 0 947.64 1126.00 7.28 o -3 4 0 5677.17 6596.18 42.22 o -2 4 0 1598.12 1841.72 14.45 o -1 4 0 259.70 235.09 3.37 o 0 4 0 9101.63 11040.24 215.83 o 2 4 0 2707.60 3223.31 21.26 o 3 4 0 5226.12 5960.26 53.23 o 4 4 0 4803.85 5463.32 27.92 o 5 4 0 366.28 416.03 3.61 o 6 4 0 879.34 975.30 8.40 o 7 4 0 2901.14 3299.11 23.64 o 8 4 0 1324.45 1452.25 15.73 o 9 4 0 871.06 826.26 20.75 o -5 5 0 3.97 3.83 0.52 o -4 5 0 15.65 21.09 0.59 o -3 5 0 22.40 26.09 0.74 o -2 5 0 1.89 2.74 0.32 o -1 5 0 120.02 134.84 2.01 o 0 5 0 56.77 80.15 1.41 o 1 5 0 163.62 163.54 1.92 o 2 5 0 6.15 2.78 0.88 o 3 5 0 184.71 226.92 2.39 o 4 5 0 214.54 217.30 2.41 o 5 5 0 80.43 80.96 1.01 o 6 5 0 219.62 238.65 2.36 o 7 5 0 14.69 15.43 0.73 o 8 5 0 73.11 84.46 1.36 o 9 5 0 215.93 186.18 5.88 o -4 6 0 985.74 973.19 9.04 o -3 6 0 3862.39 4405.18 26.99 o -2 6 0 1410.75 1685.39 10.99 o -1 6 0 575.16 682.06 5.35 o 0 6 0 5027.85 5642.77 39.56 o 1 6 0 4077.98 4787.68 61.13 o 2 6 0 472.02 537.00 5.33 o 3 6 0 2366.05 2540.31 24.39 o 4 6 0 4366.78 4984.09 57.50 o 5 6 0 1669.04 1944.72 12.44 o 6 6 0 2297.28 2531.67 24.57 o 7 6 0 2354.71 2713.78 21.02 o 8 6 0 391.55 444.45 4.70 o -3 7 0 1.09 1.53 0.30 o -2 7 0 41.02 50.40 0.87 o -1 7 0 30.11 30.41 0.75 o 0 7 0 67.20 74.81 1.23 o 1 7 0 127.73 131.22 1.79 o 2 7 0 17.86 17.57 1.28 o 3 7 0 138.08 151.83 1.90 o 4 7 0 44.81 45.27 1.58 o 5 7 0 16.81 13.10 0.56 o 6 7 0 356.93 390.06 3.25 o 7 7 0 0.46 2.46 0.31 o 8 7 0 270.34 310.74 3.87 o -1 8 0 386.15 410.45 4.82 o 0 8 0 3481.43 3685.97 27.77 o 1 8 0 3389.06 3725.17 26.45 o 2 8 0 400.98 470.68 4.31 o 3 8 0 1832.29 2199.01 18.04 o 4 8 0 3382.91 3972.98 25.87 o 5 8 0 635.66 769.58 5.80 o 6 8 0 840.36 1018.48 7.31 o 7 8 0 1934.46 2245.05 13.94 o 8 8 0 581.67 670.48 6.82 o 0 9 0 171.52 166.15 2.46 o 1 9 0 58.66 76.66 1.14 o 2 9 0 41.57 46.25 0.95 o 3 9 0 195.61 214.40 2.54 o 4 9 0 0.57 1.38 0.32 o 5 9 0 46.36 53.37 0.98 o 6 9 0 67.19 76.34 1.22 o 7 9 0 19.54 26.32 0.82 o 3 10 0 858.42 898.41 9.92 o 4 10 0 2851.77 3095.87 31.58 o 5 10 0 1047.21 1100.02 9.89 o -7 -9 1 848.79 817.68 10.43 o -6 -9 1 1021.86 1019.85 7.43 o -5 -9 1 962.66 990.03 7.97 o -4 -9 1 1491.80 1526.34 11.66 o -3 -9 1 1833.00 1714.54 15.29 o -2 -9 1 1469.76 1350.77 15.01 o -1 -9 1 1754.84 1723.66 18.90 o 0 -9 1 1419.31 1353.27 26.98 o -7 -8 1 10.91 12.51 0.48 o -6 -8 1 370.88 365.97 3.35 o -5 -8 1 31.68 30.39 0.85 o -4 -8 1 89.43 83.72 1.36 o -3 -8 1 240.73 245.46 2.73 o -2 -8 1 43.00 46.77 1.24 o -1 -8 1 224.51 235.62 2.88 o 0 -8 1 253.39 223.67 2.46 o 1 -8 1 32.17 28.24 0.71 o 2 -8 1 106.50 94.96 1.89 o -8 -7 1 998.50 959.58 8.73 o -7 -7 1 2365.13 2397.56 28.59 o -6 -7 1 1376.33 1404.04 9.85 o -5 -7 1 625.38 611.07 4.61 o -4 -7 1 2286.69 2250.97 15.02 o -3 -7 1 2515.59 2488.57 17.55 o -2 -7 1 919.37 845.92 7.48 o -1 -7 1 2308.72 2273.99 19.36 o 0 -7 1 3326.45 3337.20 25.46 o 1 -7 1 1294.74 1203.42 9.27 o 2 -7 1 1795.44 1676.47 11.39 o 3 -7 1 2597.40 2456.92 17.30 o -8 -6 1 104.36 112.16 2.59 o -7 -6 1 83.89 85.70 1.29 o -6 -6 1 420.82 420.78 3.47 o -5 -6 1 10.93 10.99 0.50 o -4 -6 1 474.21 422.47 3.37 o -3 -6 1 142.94 137.47 2.27 o -2 -6 1 17.45 16.05 1.89 o -1 -6 1 120.26 103.98 2.08 o 0 -6 1 525.87 505.11 4.73 o 1 -6 1 65.59 70.53 1.17 o 2 -6 1 814.21 814.39 5.78 o 3 -6 1 1.90 2.23 0.31 o 4 -6 1 294.37 276.84 2.88 o -8 -5 1 129.48 145.42 2.35 o -7 -5 1 1358.70 1393.20 10.73 o -6 -5 1 1651.30 1635.67 12.78 o -5 -5 1 580.86 536.92 3.86 o -4 -5 1 4846.21 4823.64 27.05 o -3 -5 1 8820.06 9008.05 66.58 o -2 -5 1 1558.21 1544.84 13.67 o -1 -5 1 2130.60 1922.13 16.25 o 0 -5 1 6563.22 6496.09 51.75 o 1 -5 1 1504.94 1609.14 16.90 o 2 -5 1 732.44 727.20 6.22 o 3 -5 1 3375.30 3505.95 20.83 o 4 -5 1 1648.95 1728.44 14.87 o 5 -5 1 780.19 759.43 9.36 o -8 -4 1 64.70 71.20 1.36 o -7 -4 1 110.65 117.18 1.64 o -6 -4 1 347.17 338.41 3.37 o -5 -4 1 1.71 7.38 1.99 o -4 -4 1 507.19 477.14 3.05 o -3 -4 1 329.91 380.04 3.96 o -2 -4 1 423.02 460.08 3.42 o -1 -4 1 419.69 332.41 2.77 o 0 -4 1 3.34 -0.50 0.50 o 1 -4 1 19.22 15.79 0.91 o 2 -4 1 478.83 450.82 4.52 o 3 -4 1 14.40 17.89 1.28 o 4 -4 1 808.83 815.78 5.56 o 5 -4 1 12.89 14.09 0.60 o 6 -4 1 277.66 272.91 3.55 o -8 -3 1 36.06 46.11 1.69 o -7 -3 1 2419.22 2436.36 19.27 o -6 -3 1 7774.31 7396.92 52.29 o -5 -3 1 1689.01 1768.83 18.50 o -4 -3 1 748.80 650.75 5.06 o -3 -3 1 5135.36 5145.15 25.40 o -2 -3 1 1414.28 1406.03 8.89 o -1 -3 1 1856.34 1598.14 9.43 o 1 -3 1 7128.61 7631.00 109.67 o 2 -3 1 1565.91 1603.13 11.74 o 3 -3 1 5623.07 5572.91 40.49 o 4 -3 1 3307.50 3343.79 19.89 o 5 -3 1 390.98 416.88 3.04 o 6 -3 1 1240.12 1255.61 12.62 o -8 -2 1 12.66 12.36 0.54 o -7 -2 1 141.99 149.65 2.01 o -6 -2 1 242.06 237.78 2.62 o -5 -2 1 43.07 44.11 1.20 o -4 -2 1 517.30 498.15 4.07 o -3 -2 1 8.88 13.46 1.07 o -2 -2 1 177.96 180.14 1.22 o -1 -2 1 572.04 518.93 4.03 o 0 -2 1 0.19 -0.25 0.25 o 1 -2 1 801.23 882.71 5.34 o 2 -2 1 2.92 -0.07 0.25 o 3 -2 1 23.79 10.89 0.69 o 4 -2 1 61.55 67.39 1.24 o 5 -2 1 46.79 41.79 1.66 o 6 -2 1 189.31 187.57 2.06 o 7 -2 1 5.88 4.66 0.32 o -8 -1 1 485.83 439.69 11.07 o -7 -1 1 1239.10 1247.95 19.34 o -6 -1 1 2953.59 2915.96 22.76 o -5 -1 1 358.11 352.89 7.02 o -4 -1 1 214.53 183.51 6.47 o 1 -1 1 2992.69 2615.69 54.02 o 2 -1 1 671.10 618.06 7.79 o 3 -1 1 6061.36 6125.24 39.01 o 4 -1 1 5247.77 5487.70 39.73 o 5 -1 1 1000.12 1009.12 7.34 o 6 -1 1 2499.40 2512.58 17.99 o 7 -1 1 2735.33 2738.27 32.23 o -7 0 1 165.38 178.01 2.25 o -6 0 1 103.15 101.45 1.51 o -5 0 1 84.61 83.27 1.33 o -4 0 1 388.86 363.35 3.94 o -3 0 1 0.04 -0.29 0.29 o -2 0 1 588.05 630.39 3.88 o -1 0 1 4.16 6.89 0.35 o 0 0 1 2.36 2.75 0.13 o 1 0 1 36.51 21.32 0.23 o 2 0 1 344.21 356.03 2.53 o 3 0 1 37.10 25.47 1.20 o 4 0 1 47.19 58.91 0.99 o 5 0 1 17.73 20.66 2.17 o 6 0 1 8.73 12.47 0.77 o 7 0 1 3.88 5.32 0.59 o 8 0 1 1.36 2.38 0.31 o -7 1 1 615.41 589.65 6.94 o -6 1 1 2620.47 2662.22 29.07 o -5 1 1 1988.67 1992.73 14.62 o -4 1 1 2954.32 3007.87 24.29 o -3 1 1 7055.12 6911.44 58.29 o -2 1 1 2636.44 2565.51 15.73 o -1 1 1 713.02 582.49 4.02 o 4 1 1 5688.95 5690.67 61.87 o 5 1 1 329.54 331.83 6.52 o 6 1 1 1803.11 1796.35 14.61 o 7 1 1 2777.71 2764.61 21.79 o 8 1 1 332.02 334.29 3.29 o -6 2 1 13.68 11.48 0.58 o -5 2 1 79.55 85.23 1.26 o -4 2 1 111.87 99.76 1.37 o -3 2 1 8.75 4.59 0.34 o -2 2 1 135.02 149.72 1.47 o -1 2 1 90.92 78.08 0.84 o 0 2 1 130.42 89.29 1.56 o 1 2 1 47.75 70.37 0.86 o 2 2 1 16.30 17.15 0.59 o 3 2 1 197.85 262.67 1.91 o 4 2 1 45.85 72.56 1.10 o 5 2 1 142.00 145.19 1.92 o 6 2 1 15.97 16.69 1.61 o 7 2 1 2.03 3.13 0.53 o 8 2 1 25.50 22.38 0.82 o -6 3 1 2514.03 2376.56 21.89 o -5 3 1 875.85 931.82 8.96 o -4 3 1 675.66 704.55 5.15 o -3 3 1 3899.24 3637.07 41.79 o -2 3 1 2537.29 2603.49 19.85 o -1 3 1 3161.40 3648.16 25.52 o 2 3 1 92.74 66.56 0.89 o 3 3 1 5836.42 5858.66 107.07 o 4 3 1 6802.97 6841.68 46.66 o 5 3 1 482.32 489.28 4.65 o 6 3 1 2465.54 2348.77 26.82 o 7 3 1 5156.31 5038.48 38.85 o 8 3 1 690.05 683.47 10.09 o 9 3 1 331.73 285.29 7.26 o -5 4 1 31.25 31.53 1.01 o -4 4 1 23.88 24.23 0.60 o -3 4 1 35.10 39.82 1.48 o -2 4 1 40.44 47.09 2.67 o -1 4 1 38.87 47.99 0.99 o 0 4 1 18.86 35.97 0.88 o 1 4 1 0.60 0.12 0.29 o 2 4 1 61.63 61.32 0.86 o 3 4 1 46.00 38.69 0.71 o 4 4 1 8.46 1.71 0.37 o 5 4 1 0.03 0.56 0.18 o 6 4 1 44.32 42.82 0.99 o 7 4 1 26.04 24.55 1.00 o 8 4 1 16.04 16.47 0.70 o 9 4 1 0.72 1.28 0.32 o -4 5 1 234.40 257.18 3.75 o -3 5 1 3406.73 3499.97 20.65 o -2 5 1 2933.54 2892.91 17.31 o -1 5 1 493.99 503.72 3.91 o 0 5 1 4819.92 5013.86 40.27 o 1 5 1 5462.30 5351.03 40.24 o 2 5 1 385.38 360.33 3.89 o 3 5 1 5050.11 5409.12 40.91 o 4 5 1 10687.72 11144.65 82.02 o 5 5 1 731.32 722.74 6.76 o 6 5 1 465.15 455.16 3.95 o 7 5 1 3875.59 3797.92 25.74 o 8 5 1 1002.16 974.38 11.01 o 9 5 1 182.42 174.49 4.44 o -3 6 1 5.10 8.13 0.62 o -2 6 1 24.73 21.47 0.62 o -1 6 1 46.73 50.41 1.14 o 0 6 1 12.08 9.14 0.48 o 1 6 1 206.85 200.12 3.25 o 2 6 1 9.10 9.34 0.93 o 3 6 1 304.88 330.05 4.15 o 4 6 1 65.08 74.40 1.48 o 5 6 1 34.13 28.91 0.74 o 6 6 1 0.68 1.95 0.31 o 7 6 1 15.97 16.13 0.64 o 8 6 1 66.58 67.85 1.50 o 9 6 1 40.89 36.93 1.03 o -2 7 1 3186.71 3045.64 18.83 o -1 7 1 600.37 520.23 3.94 o 0 7 1 2084.07 2110.17 13.82 o 1 7 1 4486.36 4544.34 30.06 o 2 7 1 518.89 503.37 4.29 o 3 7 1 1133.42 1118.28 7.88 o 4 7 1 5637.77 5629.17 36.16 o 5 7 1 1343.99 1309.55 8.75 o 6 7 1 419.91 409.24 3.36 o 7 7 1 3195.30 3222.30 18.96 o 8 7 1 1604.60 1669.01 17.16 o -1 8 1 0.95 1.03 0.22 o 0 8 1 6.95 9.99 0.56 o 1 8 1 32.60 30.72 1.25 o 2 8 1 4.49 5.04 0.40 o 3 8 1 353.24 341.00 3.21 o 4 8 1 16.93 17.42 0.64 o 5 8 1 531.25 547.38 4.47 o 6 8 1 28.04 26.14 0.69 o 7 8 1 214.34 203.20 2.01 o 8 8 1 22.41 27.69 1.22 o 0 9 1 810.36 705.42 6.92 o 1 9 1 2678.42 2613.17 19.75 o 2 9 1 1078.88 982.76 7.52 o 3 9 1 1218.82 1125.73 8.74 o 4 9 1 3547.54 3575.29 24.51 o 5 9 1 1130.85 1191.82 8.80 o 6 9 1 147.64 159.81 2.06 o 7 9 1 1335.88 1364.77 9.71 o 3 10 1 50.46 38.02 0.77 o 4 10 1 17.54 17.03 1.08 o 5 10 1 176.33 173.19 1.93 o 6 10 1 52.60 47.50 0.89 o -6 -9 2 653.40 633.29 5.13 o -5 -9 2 45.81 48.44 0.95 o -4 -9 2 689.59 723.84 8.01 o -3 -9 2 337.95 330.22 6.05 o -7 -8 2 586.27 592.23 4.23 o -6 -8 2 1149.10 1177.96 8.16 o -5 -8 2 1228.05 1246.67 9.25 o -4 -8 2 895.41 914.24 7.08 o -3 -8 2 1311.24 1299.80 11.18 o -2 -8 2 1782.36 1731.95 24.77 o 0 -8 2 2519.17 2350.26 31.07 o 1 -8 2 1355.40 1255.59 12.21 o -7 -7 2 104.70 118.38 1.26 o -6 -7 2 327.37 327.79 2.96 o -5 -7 2 47.32 50.47 1.03 o -4 -7 2 950.16 952.84 7.48 o -3 -7 2 608.70 595.71 6.20 o -2 -7 2 1065.82 1017.73 12.59 o 0 -7 2 124.76 120.69 2.48 o 1 -7 2 411.37 386.43 3.87 o 2 -7 2 99.73 112.65 1.45 o 3 -7 2 110.37 122.96 1.43 o -8 -6 2 689.96 658.99 15.27 o -7 -6 2 620.81 628.72 7.51 o -6 -6 2 1752.13 1781.72 11.57 o -5 -6 2 2720.57 2817.16 17.78 o -4 -6 2 2007.78 1950.66 13.26 o -3 -6 2 2381.52 2198.23 16.81 o -2 -6 2 2946.47 2636.22 16.64 o 0 -6 2 1713.89 1583.62 29.05 o 1 -6 2 1045.28 1009.43 7.91 o 2 -6 2 1759.15 1778.25 12.27 o 3 -6 2 3651.50 3701.28 24.31 o 4 -6 2 1860.63 1809.75 12.04 o -8 -5 2 29.79 31.12 0.84 o -7 -5 2 311.27 324.80 3.51 o -6 -5 2 372.07 368.45 3.49 o -5 -5 2 119.26 126.08 1.62 o -4 -5 2 532.68 487.18 11.93 o -3 -5 2 297.55 328.30 2.43 o -2 -5 2 502.86 504.88 3.46 o -1 -5 2 1698.03 1629.36 30.38 o 0 -5 2 347.49 312.50 5.72 o 1 -5 2 908.23 937.91 10.10 o 2 -5 2 34.62 33.73 1.13 o 3 -5 2 33.18 31.57 0.81 o 4 -5 2 87.70 84.31 1.16 o 5 -5 2 18.28 21.50 0.62 o -8 -4 2 2361.41 2074.45 45.83 o -7 -4 2 1765.47 1806.77 20.98 o -6 -4 2 784.93 785.08 6.59 o -5 -4 2 1083.10 1011.57 6.87 o -4 -4 2 1950.32 1963.83 16.31 o -3 -4 2 2730.98 2760.65 18.24 o -2 -4 2 3552.77 3589.30 19.09 o -1 -4 2 5346.33 5368.50 34.66 o 0 -4 2 6267.50 6223.86 37.47 o 1 -4 2 3496.52 3377.40 24.64 o 2 -4 2 2930.10 2938.07 26.16 o 3 -4 2 3968.62 3911.36 24.43 o 4 -4 2 1164.63 1191.79 8.15 o 5 -4 2 189.50 205.27 2.07 o 6 -4 2 1797.24 1787.23 13.45 o -8 -3 2 5.51 5.33 0.67 o -7 -3 2 237.75 259.10 3.16 o -6 -3 2 294.00 271.65 3.26 o -5 -3 2 88.95 84.09 1.39 o -4 -3 2 1503.25 1473.97 11.46 o -3 -3 2 2.43 6.54 0.40 o -2 -3 2 1240.67 1345.39 7.45 o -1 -3 2 455.94 401.61 2.63 o 0 -3 2 5.33 2.84 0.32 o 1 -3 2 1624.52 1708.04 10.67 o 2 -3 2 97.70 97.62 1.32 o 3 -3 2 563.56 536.14 4.72 o 4 -3 2 49.11 51.89 0.90 o 5 -3 2 33.11 36.04 0.79 o 6 -3 2 38.27 40.39 0.74 o -8 -2 2 628.69 556.21 7.76 o -7 -2 2 838.83 852.44 7.26 o -6 -2 2 676.63 680.31 5.77 o -5 -2 2 1319.07 1234.23 12.99 o -4 -2 2 6894.27 7283.41 57.47 o -3 -2 2 9333.90 9587.03 101.29 o -2 -2 2 2014.82 1931.15 14.12 o -1 -2 2 2565.14 2407.11 14.21 o 1 -2 2 3098.74 2984.24 19.05 o 2 -2 2 1498.98 1484.29 10.28 o 3 -2 2 6760.60 7099.18 57.07 o 4 -2 2 4895.00 5089.06 40.01 o 5 -2 2 1015.57 1047.38 6.86 o 6 -2 2 2401.63 2478.03 16.53 o 7 -2 2 2417.03 2332.99 17.68 o -7 -1 2 344.80 356.04 5.34 o -6 -1 2 37.21 33.16 1.75 o -5 -1 2 256.32 251.28 2.68 o -4 -1 2 602.30 564.30 9.01 o -3 -1 2 73.41 113.51 1.18 o -2 -1 2 2594.80 2801.56 21.91 o -1 -1 2 1524.01 1570.43 14.70 o 0 -1 2 1882.13 1805.52 11.12 o 1 -1 2 1261.21 1325.75 7.79 o 2 -1 2 131.90 129.25 1.26 o 3 -1 2 410.08 380.86 3.07 o 4 -1 2 861.23 972.27 9.71 o 5 -1 2 91.04 91.03 1.63 o 6 -1 2 283.12 276.88 3.11 o 7 -1 2 52.42 53.75 1.29 o 8 -1 2 10.21 8.44 0.45 o -7 0 2 1486.43 1485.17 19.12 o -6 0 2 2929.53 2953.05 23.33 o -5 0 2 1069.66 1008.03 8.49 o -4 0 2 1208.39 1202.56 12.95 o -3 0 2 5207.03 5287.45 45.31 o -2 0 2 2114.72 1943.98 12.36 o -1 0 2 1560.60 1361.62 13.63 o 2 0 2 1583.32 1437.49 9.47 o 3 0 2 7612.18 7249.36 153.05 o 4 0 2 6851.94 7115.16 47.45 o 5 0 2 368.82 383.30 4.28 o 6 0 2 1168.62 1145.78 8.88 o 7 0 2 3617.39 3573.01 36.72 o 8 0 2 795.59 776.28 7.21 o -6 1 2 16.52 15.23 0.99 o -5 1 2 335.49 336.21 3.51 o -4 1 2 372.21 345.16 4.83 o -3 1 2 225.85 209.37 3.82 o -2 1 2 793.70 850.94 5.93 o -1 1 2 109.46 97.28 1.09 o 0 1 2 875.94 737.90 5.69 o 1 1 2 2404.37 2610.87 37.89 o 2 1 2 264.11 305.26 1.89 o 3 1 2 1389.66 1314.46 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535.65 508.81 4.44 o -5 -9 3 1121.21 1072.50 10.01 o -4 -9 3 1098.43 1101.95 11.57 o -6 -8 3 7.40 6.40 0.39 o -5 -8 3 75.74 71.46 1.15 o -4 -8 3 11.68 11.02 0.55 o -3 -8 3 145.18 144.87 2.28 o -7 -7 3 1000.60 980.94 9.77 o -6 -7 3 641.57 668.03 5.34 o -5 -7 3 1804.21 1773.59 12.24 o -4 -7 3 2356.80 2351.12 16.89 o -3 -7 3 1386.70 1409.62 11.27 o -2 -7 3 1088.46 1025.41 13.23 o 1 -7 3 2974.07 2818.67 30.47 o 2 -7 3 2291.71 2236.63 17.31 o 3 -7 3 1263.65 1209.41 9.48 o -7 -6 3 169.53 177.08 2.02 o -6 -6 3 216.33 216.55 2.07 o -5 -6 3 264.67 259.34 2.86 o -4 -6 3 452.09 443.32 3.86 o -3 -6 3 3.89 3.09 0.37 o -2 -6 3 121.96 126.83 1.98 o 1 -6 3 1665.43 1601.92 15.86 o 2 -6 3 125.20 130.18 1.71 o 3 -6 3 440.46 464.60 4.04 o 4 -6 3 390.91 375.21 3.16 o -7 -5 3 763.24 760.32 8.49 o -6 -5 3 745.55 770.19 5.43 o -5 -5 3 1233.22 1206.80 7.77 o -4 -5 3 2019.64 1944.09 13.36 o -3 -5 3 2624.49 2583.53 21.13 o -2 -5 3 3030.90 2996.51 16.82 o -1 -5 3 3510.77 3089.03 23.52 o 1 -5 3 3056.53 3058.02 34.25 o 2 -5 3 1062.77 1007.21 7.40 o 3 -5 3 1042.73 1070.29 7.87 o 4 -5 3 1950.16 2056.28 14.96 o 5 -5 3 1782.98 1775.53 11.93 o -7 -4 3 368.34 389.97 3.82 o -6 -4 3 1.03 1.00 0.34 o -5 -4 3 224.08 225.30 2.18 o -4 -4 3 727.76 673.00 5.87 o -3 -4 3 0.21 0.76 0.23 o -2 -4 3 2104.55 2242.47 16.95 o -1 -4 3 226.61 192.24 1.44 o 0 -4 3 442.19 421.15 7.21 o 1 -4 3 1406.49 1473.49 12.03 o 2 -4 3 155.28 141.38 1.96 o 3 -4 3 2119.75 2126.33 13.73 o 4 -4 3 447.87 454.04 3.47 o 5 -4 3 712.14 727.29 4.92 o 6 -4 3 266.78 283.90 2.48 o -7 -3 3 814.17 811.31 7.59 o -6 -3 3 1877.19 1934.15 21.09 o -5 -3 3 2402.76 2375.26 18.10 o -4 -3 3 2015.14 1951.00 16.21 o -3 -3 3 3306.98 3307.29 27.06 o -2 -3 3 3684.27 3854.01 26.69 o -1 -3 3 2038.73 1897.12 12.41 o 0 -3 3 3210.28 2948.20 14.57 o 1 -3 3 4795.39 4811.97 32.30 o 2 -3 3 3589.42 3658.08 26.34 o 3 -3 3 4325.05 4457.14 34.97 o 4 -3 3 3987.31 4032.44 34.36 o 5 -3 3 1193.12 1211.12 7.82 o 6 -3 3 791.42 786.96 5.20 o 7 -3 3 1277.19 1160.87 17.38 o -7 -2 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139.64 1.44 o 5 2 3 949.95 1014.47 8.62 o 6 2 3 3.05 2.47 0.48 o 7 2 3 92.47 90.09 1.63 o 8 2 3 10.53 13.28 0.64 o 9 2 3 41.59 36.34 0.80 o -5 3 3 757.16 789.80 7.89 o -4 3 3 1067.78 1131.10 10.18 o -3 3 3 2907.79 2836.63 19.22 o -2 3 3 3377.65 3376.93 39.48 o -1 3 3 2080.36 2167.29 15.93 o 0 3 3 4878.16 4900.49 32.11 o 1 3 3 6297.57 6208.31 50.30 o 2 3 3 1166.28 1127.55 7.69 o 3 3 3 2625.95 2616.67 17.35 o 4 3 3 9272.09 9338.68 178.73 o 5 3 3 3573.39 3650.76 31.89 o 6 3 3 846.73 835.19 10.54 o 7 3 3 2792.56 2646.41 20.79 o 8 3 3 2003.13 1990.06 15.89 o 9 3 3 392.27 384.47 4.58 o -4 4 3 1.52 4.10 0.70 o -3 4 3 1113.92 1120.90 10.23 o -2 4 3 228.92 236.13 2.28 o -1 4 3 701.30 730.51 6.37 o 0 4 3 568.71 567.76 5.04 o 1 4 3 19.56 34.03 1.43 o 2 4 3 752.17 804.41 5.79 o 3 4 3 1400.93 1485.79 10.92 o 4 4 3 319.54 303.85 3.86 o 5 4 3 1541.26 1688.48 14.17 o 6 4 3 5.17 6.99 1.08 o 7 4 3 431.36 411.20 3.94 o 8 4 3 22.23 24.26 1.20 o 9 4 3 15.85 14.66 0.73 o -4 5 3 852.71 777.93 12.19 o -3 5 3 1600.97 1628.53 13.87 o -2 5 3 1702.91 1690.81 11.74 o -1 5 3 326.21 319.96 3.46 o 0 5 3 2060.35 1974.48 13.68 o 1 5 3 7743.52 7910.70 85.58 o 2 5 3 3064.74 3173.24 24.34 o 3 5 3 1923.22 1984.82 14.54 o 4 5 3 6218.62 6309.41 47.69 o 5 5 3 2220.94 2212.79 17.40 o 6 5 3 306.66 294.89 2.80 o 7 5 3 2532.85 2454.99 19.39 o 8 5 3 2297.80 2269.02 16.83 o 9 5 3 367.95 353.58 4.47 o -3 6 3 428.39 408.13 5.22 o -2 6 3 78.50 76.92 1.34 o -1 6 3 734.52 713.52 4.96 o 0 6 3 498.64 454.19 3.37 o 1 6 3 390.27 357.05 2.95 o 2 6 3 702.10 700.28 5.18 o 3 6 3 23.52 22.42 1.52 o 4 6 3 167.79 164.35 3.35 o 5 6 3 177.72 181.56 1.73 o 6 6 3 0.83 2.39 0.30 o 7 6 3 333.46 324.57 3.04 o 8 6 3 9.13 12.25 1.65 o 9 6 3 121.41 106.34 2.49 o -2 7 3 2095.26 1994.91 25.74 o -1 7 3 1302.96 1234.78 7.71 o 0 7 3 1794.33 1755.94 14.10 o 1 7 3 4342.91 4339.65 26.22 o 2 7 3 926.24 809.70 6.04 o 3 7 3 101.71 104.53 1.98 o 4 7 3 3416.37 3334.59 20.39 o 5 7 3 3476.96 3482.72 21.35 o 6 7 3 713.95 730.72 4.94 o 7 7 3 2479.58 2466.90 15.80 o 8 7 3 2434.63 2373.38 34.67 o 9 7 3 150.05 146.36 2.94 o 0 8 3 23.95 22.34 0.74 o 1 8 3 77.59 74.02 1.09 o 2 8 3 207.32 219.50 2.14 o 3 8 3 35.41 31.16 0.87 o 4 8 3 230.46 244.13 2.27 o 5 8 3 5.90 7.51 0.43 o 6 8 3 94.62 94.07 1.44 o 7 8 3 8.80 8.76 0.40 o 8 8 3 0.22 2.13 0.32 o 1 9 3 1999.25 1894.29 14.34 o 2 9 3 1496.84 1465.72 10.16 o 3 9 3 625.24 619.71 4.79 o 4 9 3 3259.23 3296.76 20.93 o 5 9 3 2869.84 2926.65 18.80 o 6 9 3 137.57 141.02 1.42 o 7 9 3 625.10 647.90 4.79 o 8 9 3 1703.13 1656.49 28.40 o 4 10 3 0.76 2.43 0.35 o 5 10 3 21.81 20.55 0.82 o 6 10 3 2.40 2.08 0.27 o -5 -8 4 2013.94 2005.19 15.18 o -4 -8 4 854.57 846.60 6.97 o -3 -8 4 115.24 121.65 4.64 o -6 -7 4 12.85 10.48 0.40 o -5 -7 4 140.32 140.85 1.76 o -4 -7 4 354.72 358.74 3.20 o -3 -7 4 240.42 239.99 2.77 o -2 -7 4 472.97 457.29 5.60 o 2 -7 4 6.33 6.49 0.52 o 3 -7 4 456.89 481.46 5.82 o -6 -6 4 235.24 235.98 2.18 o -5 -6 4 2124.96 2150.06 14.60 o -4 -6 4 2294.66 2285.12 15.55 o -3 -6 4 921.73 897.04 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74.30 75.24 2.73 o 1 2 9 1.18 2.40 0.57 o 2 2 9 87.85 91.06 1.33 o 3 2 9 12.00 12.13 0.72 o 4 2 9 403.26 410.04 4.36 o 5 2 9 122.05 124.75 1.88 o 6 2 9 31.54 28.75 1.17 o 7 2 9 12.19 13.72 0.59 o 8 2 9 25.44 26.54 0.73 o -1 3 9 471.74 442.35 6.69 o 0 3 9 1537.71 1575.51 19.21 o 1 3 9 1433.02 1465.69 15.86 o 2 3 9 479.77 476.07 4.70 o 3 3 9 1791.28 1749.19 14.33 o 4 3 9 2374.39 2399.63 17.78 o 5 3 9 596.89 627.84 5.93 o 6 3 9 1531.14 1515.62 12.62 o 7 3 9 2669.63 2730.76 21.06 o 8 3 9 360.51 384.17 4.28 o 0 4 9 50.91 58.47 2.20 o 1 4 9 134.37 128.95 2.31 o 2 4 9 99.92 94.70 1.51 o 3 4 9 9.55 13.19 0.88 o 4 4 9 0.74 0.68 0.38 o 5 4 9 22.09 20.86 0.99 o 6 4 9 91.46 94.65 1.66 o 7 4 9 11.40 11.19 0.63 o 8 4 9 79.08 80.32 1.42 o 1 5 9 1427.55 1485.53 17.94 o 2 5 9 436.27 449.52 5.48 o 3 5 9 1480.57 1502.69 14.35 o 4 5 9 2710.99 2841.32 48.40 o 5 5 9 317.29 352.45 3.63 o 6 5 9 530.84 557.71 7.93 o 7 5 9 2974.48 3067.92 23.40 o 8 5 9 867.49 911.32 9.49 o 2 6 9 37.55 37.49 1.17 o 3 6 9 13.57 14.10 0.64 o 4 6 9 11.45 15.38 0.58 o 5 6 9 18.00 16.56 0.75 o 6 6 9 37.73 39.27 0.82 o 7 6 9 3.19 2.74 0.34 o 8 6 9 8.10 10.38 0.95 o 4 7 9 1662.37 1646.68 21.76 o 5 7 9 620.64 652.79 16.80 o 6 7 9 473.16 484.30 5.11 o 7 7 9 2413.88 2438.59 33.30 o 0 -4 10 729.75 709.10 5.19 o 1 -4 10 661.09 652.47 6.78 o 2 -4 10 836.15 839.42 5.94 o 3 -4 10 1419.38 1430.65 12.36 o -1 -3 10 95.79 103.67 1.31 o 0 -3 10 1.29 3.70 0.29 o 1 -3 10 493.60 506.22 3.80 o 2 -3 10 0.34 0.77 0.25 o 3 -3 10 185.83 188.88 1.84 o 4 -3 10 127.44 120.05 1.87 o -1 -2 10 721.65 733.12 9.70 o 0 -2 10 1530.14 1538.94 10.56 o 1 -2 10 1106.67 1129.24 8.79 o 2 -2 10 815.63 840.89 6.51 o 3 -2 10 1673.66 1684.09 11.10 o 4 -2 10 1326.93 1332.16 12.44 o 5 -2 10 412.55 424.52 3.20 o -1 -1 10 0.20 1.11 0.28 o 0 -1 10 104.91 112.64 2.55 o 1 -1 10 117.30 117.80 2.17 o 2 -1 10 46.76 46.97 0.87 o 3 -1 10 354.68 367.17 2.90 o 4 -1 10 202.46 194.83 2.39 o 5 -1 10 139.05 130.33 1.36 o 6 -1 10 131.41 128.23 1.88 o -1 0 10 584.97 602.19 10.23 o 0 0 10 1856.33 1888.76 20.07 o 1 0 10 1265.01 1259.59 9.69 o 2 0 10 276.86 302.93 3.59 o 3 0 10 1305.59 1329.07 12.69 o 4 0 10 2246.00 2278.03 20.57 o 5 0 10 631.56 642.05 9.24 o 6 0 10 1021.87 1069.45 9.96 o 7 0 10 2171.88 2073.29 27.88 o -1 1 10 70.82 76.67 3.29 o 0 1 10 314.47 333.06 4.33 o 1 1 10 252.62 254.81 2.94 o 2 1 10 221.12 221.47 3.62 o 3 1 10 140.01 145.68 2.03 o 4 1 10 43.07 45.01 1.22 o 5 1 10 115.27 120.98 1.81 o 6 1 10 293.93 310.88 5.51 o 7 1 10 26.20 31.36 0.77 o 0 2 10 925.47 987.49 11.51 o 1 2 10 1657.81 1628.25 18.50 o 2 2 10 486.95 501.37 8.42 o 3 2 10 1071.53 1106.09 16.53 o 4 2 10 2643.69 2750.33 27.10 o 5 2 10 759.49 801.72 8.61 o 6 2 10 617.56 659.83 7.18 o 7 2 10 2079.09 2112.23 25.01 o 1 3 10 101.12 96.75 2.85 o 2 3 10 31.10 32.29 1.22 o 3 3 10 302.74 312.21 3.25 o 4 3 10 8.48 8.55 0.52 o 5 3 10 209.12 218.93 3.86 o 6 3 10 6.25 7.12 0.48 o 7 3 10 9.30 10.00 0.58 o 1 4 10 1855.82 1795.48 38.57 o 2 4 10 580.20 599.28 6.50 o 3 4 10 422.68 474.45 6.47 o 4 4 10 1807.78 1934.65 17.26 o 5 4 10 1085.75 1100.68 16.86 o 6 4 10 610.28 650.63 12.10 o 7 4 10 1792.37 1913.34 30.38 o 3 5 10 59.03 65.68 1.38 o 4 5 10 7.93 7.31 0.51 o 5 5 10 97.25 86.63 1.71 o 6 5 10 34.78 42.59 1.05 o 7 5 10 40.61 39.56 1.82 o 4 6 10 1882.80 1944.17 25.49 o 5 6 10 1158.97 1201.42 13.90 o 6 6 10 378.79 384.25 10.73 o 1 -2 11 83.29 79.99 1.45 o 2 -2 11 43.64 38.32 0.69 o 3 -2 11 244.83 275.36 2.43 o 4 -2 11 60.07 63.03 2.25 o 1 -1 11 867.28 863.34 9.77 o 2 -1 11 786.86 798.36 10.85 o 3 -1 11 693.04 734.28 6.88 o 4 -1 11 1278.33 1336.63 17.94 o 5 -1 11 1203.82 1173.22 11.79 o 1 0 11 87.76 83.89 1.57 o 2 0 11 76.24 77.55 1.56 o 3 0 11 206.57 220.04 4.37 o 4 0 11 0.14 0.46 0.30 o 5 0 11 188.76 185.66 2.75 o 1 1 11 849.38 876.64 12.48 o 2 1 11 762.69 755.50 6.83 o 3 1 11 832.26 855.35 8.11 o 4 1 11 1598.63 1740.34 18.12 o 5 1 11 1125.60 1194.18 15.03 o 6 1 11 446.41 441.81 4.80 o 2 2 11 90.15 93.29 1.77 o 3 2 11 109.80 121.49 3.19 o 4 2 11 2.28 2.53 0.36 o 5 2 11 279.02 287.90 2.82 o 6 2 11 39.14 45.15 1.01 o 2 3 11 535.51 531.10 10.90 o 3 3 11 849.76 854.92 8.70 o 4 3 11 1621.59 1736.08 13.77 o 5 3 11 858.13 927.89 9.74 o 6 3 11 300.02 309.40 3.67 o 4 4 11 68.38 85.28 1.42 o 5 4 11 216.32 240.48 2.98 o 6 4 11 2.58 3.65 0.61 o