#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:50:46 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181891 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/91/2239123.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2239123 _cell_angle_alpha 94.491 _cell_angle_beta 101.972 _cell_angle_gamma 106.229 _cell_length_a 11.1254 _cell_length_b 14.3871 _cell_length_c 15.9525 _exptl_crystal_F_000 944.00 _reflns_d_resolution_high 0.7828 _cod_data_source_file is5322Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dt18a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 236.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 482.53 463.14 7.09 o 2 0 0 4745.21 4824.23 67.07 o 3 0 0 264.16 299.61 8.92 o 4 0 0 3847.97 3784.52 47.27 o 5 0 0 34.10 44.03 3.09 o 6 0 0 5480.27 5204.85 68.36 o 7 0 0 34.61 26.20 2.57 o 8 0 0 713.29 701.28 11.54 o 9 0 0 306.56 303.95 8.19 o 10 0 0 1749.49 1719.04 29.13 o 11 0 0 656.47 682.99 15.10 o 12 0 0 1471.09 1467.34 26.00 o 13 0 0 461.64 517.78 18.27 o -13 1 0 902.13 895.71 25.80 o -12 1 0 56.77 60.70 7.94 o -11 1 0 5505.68 5549.28 67.62 o -10 1 0 223.05 213.80 7.45 o -9 1 0 1686.88 1675.71 22.16 o -8 1 0 10.72 12.86 2.39 o -7 1 0 4421.06 4414.42 49.15 o -6 1 0 873.02 945.32 13.69 o -5 1 0 19156.12 19627.76 234.62 o -4 1 0 493.28 554.94 9.41 o -3 1 0 4099.22 4037.86 57.29 o -2 1 0 53.11 71.12 3.13 o -1 1 0 2265.74 2423.39 28.06 o 0 1 0 9926.17 9104.15 197.86 o 1 1 0 2311.04 2420.98 44.43 o 2 1 0 2589.25 2548.28 47.55 o 3 1 0 608.52 622.11 11.06 o 4 1 0 726.05 677.86 13.04 o 5 1 0 4700.31 4742.88 92.85 o 6 1 0 681.73 670.33 11.13 o 7 1 0 3143.15 3106.34 39.02 o 8 1 0 1261.90 1264.18 18.03 o 9 1 0 1946.80 1876.81 37.49 o 10 1 0 759.01 767.45 15.72 o 11 1 0 288.26 286.16 11.29 o 12 1 0 425.76 419.11 14.03 o -13 2 0 2.69 5.06 5.31 o -12 2 0 605.30 614.54 17.29 o -11 2 0 356.91 330.77 10.10 o -10 2 0 4654.74 4679.20 50.44 o -9 2 0 13.40 15.44 2.44 o -8 2 0 1568.58 1584.75 19.10 o -7 2 0 10.52 8.19 1.86 o -6 2 0 5569.21 5476.79 59.57 o -5 2 0 6166.54 6477.73 77.91 o -4 2 0 2501.48 2399.06 29.66 o -3 2 0 526.15 464.41 7.46 o -2 2 0 2515.60 2604.18 36.34 o -1 2 0 653.46 575.89 10.74 o 0 2 0 709.74 740.33 10.19 o 1 2 0 2716.26 2809.98 40.20 o 2 2 0 1693.77 1703.41 24.04 o 3 2 0 3337.14 3288.00 41.62 o 4 2 0 1535.78 1545.67 23.56 o 5 2 0 1931.13 1853.47 31.11 o 6 2 0 1814.27 1726.13 28.53 o 7 2 0 7229.42 7259.45 80.26 o 8 2 0 204.29 202.82 7.59 o 9 2 0 2266.33 2260.25 33.55 o 10 2 0 273.45 256.80 11.11 o 11 2 0 1898.36 1847.35 33.13 o 12 2 0 523.64 493.13 15.43 o -13 3 0 357.14 378.41 14.22 o -12 3 0 114.76 113.89 10.30 o -11 3 0 431.57 465.44 9.99 o -10 3 0 111.18 113.53 4.87 o -9 3 0 704.23 672.97 11.25 o -8 3 0 576.47 591.70 9.03 o -7 3 0 3639.22 3557.01 37.85 o -6 3 0 2175.93 2162.36 26.23 o -5 3 0 657.37 552.89 8.82 o -4 3 0 192.77 277.92 5.06 o -3 3 0 1712.10 1874.92 26.96 o -2 3 0 10471.63 10663.85 163.35 o -1 3 0 3189.47 3098.62 48.51 o 0 3 0 13462.36 13434.03 204.55 o 1 3 0 11940.75 11552.88 178.77 o 2 3 0 15612.13 15865.96 400.28 o 3 3 0 2.11 8.66 1.94 o 4 3 0 8551.36 8537.04 105.42 o 5 3 0 565.77 620.78 12.47 o 6 3 0 6191.55 6418.90 84.30 o 7 3 0 834.93 814.95 15.02 o 8 3 0 438.34 434.74 10.82 o 9 3 0 111.71 110.52 6.61 o 10 3 0 3667.83 3553.12 63.36 o 11 3 0 90.59 83.69 7.56 o 12 3 0 1394.34 1397.86 31.09 o -13 4 0 175.71 198.13 11.25 o -12 4 0 632.42 646.72 12.28 o -11 4 0 1216.60 1219.94 17.75 o -10 4 0 752.26 763.27 13.22 o -9 4 0 2222.66 2235.42 28.69 o -8 4 0 152.58 122.50 4.32 o -7 4 0 3397.48 3456.90 38.67 o -6 4 0 1627.57 1745.02 21.54 o -5 4 0 526.51 410.97 7.36 o -4 4 0 156.97 245.92 4.58 o -3 4 0 12125.18 12231.27 187.69 o -2 4 0 219.61 190.38 4.72 o -1 4 0 6848.26 6682.85 119.93 o 0 4 0 2665.98 2708.67 39.08 o 1 4 0 6179.90 5970.63 125.18 o 2 4 0 300.76 376.30 8.10 o 3 4 0 12635.53 13233.40 202.77 o 4 4 0 0.67 2.07 1.72 o 5 4 0 961.00 937.06 14.93 o 6 4 0 15.29 20.88 3.29 o 7 4 0 1436.35 1405.51 24.91 o 8 4 0 155.15 175.70 8.13 o 9 4 0 1590.64 1593.70 26.34 o 10 4 0 296.01 320.96 13.57 o 11 4 0 832.07 883.86 22.54 o 12 4 0 339.81 321.35 16.37 o -13 5 0 563.62 535.11 11.02 o -12 5 0 1123.57 1107.38 16.55 o -11 5 0 445.21 431.99 9.58 o -10 5 0 346.63 371.17 12.59 o -9 5 0 501.51 471.07 9.64 o -8 5 0 2593.44 2481.47 32.55 o -7 5 0 1233.03 1234.36 17.32 o -6 5 0 9007.73 9167.38 108.30 o -5 5 0 1.27 0.51 2.02 o -4 5 0 5341.06 5299.72 83.45 o -3 5 0 1591.83 1667.45 24.55 o -2 5 0 7447.29 7386.05 103.04 o -1 5 0 751.68 773.29 14.41 o 0 5 0 10013.71 10165.86 130.44 o 1 5 0 1029.90 1106.25 21.25 o 2 5 0 1009.41 1225.83 32.50 o 3 5 0 1060.38 1331.11 31.21 o 4 5 0 6951.41 6759.88 117.57 o 5 5 0 481.43 459.49 12.32 o 6 5 0 3946.56 3891.98 57.45 o 7 5 0 803.16 829.37 23.85 o 8 5 0 1513.12 1423.27 26.37 o 9 5 0 1059.31 1088.59 22.80 o 10 5 0 262.57 273.08 17.26 o 11 5 0 199.66 177.81 15.94 o -13 6 0 1121.86 1094.61 16.46 o -12 6 0 56.11 56.43 3.74 o -11 6 0 2212.82 2157.68 28.12 o -10 6 0 19.11 17.67 2.45 o -9 6 0 177.96 178.63 5.30 o -8 6 0 7.42 8.46 1.89 o -7 6 0 10616.02 10904.31 140.23 o -6 6 0 183.27 204.01 4.81 o -5 6 0 6597.34 6759.76 80.68 o -4 6 0 590.54 684.32 13.14 o -3 6 0 1558.18 1429.09 21.73 o -2 6 0 940.04 896.99 16.23 o -1 6 0 11196.94 11143.79 274.47 o 0 6 0 1339.06 1391.10 20.25 o 1 6 0 3916.80 3958.67 59.38 o 2 6 0 20.43 13.65 2.94 o 3 6 0 5218.38 5369.70 85.43 o 4 6 0 2904.32 3053.67 39.07 o 5 6 0 2398.72 2421.82 49.26 o 6 6 0 54.64 70.23 6.35 o 7 6 0 351.07 373.28 13.43 o 8 6 0 2316.47 2203.21 45.65 o 9 6 0 551.30 501.71 18.36 o 10 6 0 434.57 427.99 21.81 o 11 6 0 118.56 105.30 12.94 o -13 7 0 59.78 62.17 5.29 o -12 7 0 1905.03 1843.19 30.40 o -11 7 0 17.95 10.04 4.31 o -10 7 0 2755.42 2728.11 43.22 o -9 7 0 562.10 563.82 11.48 o -8 7 0 862.83 868.27 15.71 o -7 7 0 3.13 9.75 1.76 o -6 7 0 1855.45 1944.74 26.71 o -5 7 0 2890.58 3048.14 37.47 o -4 7 0 655.32 611.13 9.42 o -3 7 0 1261.38 1231.48 19.52 o -2 7 0 3758.19 3765.47 59.11 o -1 7 0 1275.60 1200.52 22.08 o 0 7 0 2319.68 2351.55 34.36 o 1 7 0 5827.56 5918.97 78.28 o 2 7 0 582.22 475.61 10.91 o 3 7 0 2105.48 2055.87 34.64 o 4 7 0 1249.27 1314.67 23.10 o 5 7 0 2065.49 2110.39 34.58 o 6 7 0 1729.65 1741.53 44.79 o 7 7 0 1206.70 1215.40 38.92 o 8 7 0 256.11 263.35 15.31 o 9 7 0 1050.74 1096.84 30.23 o 10 7 0 284.09 291.49 19.44 o -13 8 0 795.72 811.14 18.63 o -12 8 0 1011.47 1041.11 22.46 o -11 8 0 1132.25 1129.83 19.93 o -10 8 0 906.68 896.73 16.20 o -9 8 0 1912.98 1915.64 28.50 o -8 8 0 337.62 319.71 7.30 o -7 8 0 3029.86 3025.17 38.11 o -6 8 0 1795.08 1835.38 23.64 o -5 8 0 1945.27 1863.28 23.78 o -4 8 0 1386.08 1433.71 18.87 o -3 8 0 870.89 781.85 13.66 o -2 8 0 5241.76 5139.24 72.41 o -1 8 0 4793.92 5072.95 67.96 o 0 8 0 6912.48 6906.16 82.19 o 1 8 0 389.73 406.25 8.34 o 2 8 0 2122.06 2023.73 31.18 o 3 8 0 0.92 6.01 2.65 o 4 8 0 5103.68 4858.22 104.09 o 5 8 0 93.96 102.63 6.68 o 6 8 0 2949.62 3017.03 59.28 o 7 8 0 106.42 83.63 10.15 o 8 8 0 1350.53 1334.03 32.65 o 9 8 0 3.72 -3.45 8.03 o 10 8 0 2669.70 2750.07 69.07 o -13 9 0 295.11 268.60 9.28 o -12 9 0 202.40 203.82 7.66 o -11 9 0 404.43 412.62 10.03 o -10 9 0 13.35 7.34 2.48 o -9 9 0 579.05 549.66 10.41 o -8 9 0 58.92 62.98 4.76 o -7 9 0 3899.18 3972.43 59.31 o -6 9 0 2114.22 2110.49 32.92 o -5 9 0 6901.93 7096.51 85.13 o -4 9 0 33.33 68.19 3.81 o -3 9 0 4549.09 4521.29 63.93 o -2 9 0 2.65 10.87 2.13 o -1 9 0 3769.00 3841.45 48.06 o 0 9 0 260.88 295.10 6.22 o 1 9 0 5821.39 5981.86 74.45 o 2 9 0 186.78 174.54 6.32 o 3 9 0 2634.36 2591.88 44.39 o 4 9 0 813.12 735.30 16.40 o 5 9 0 2027.44 1988.82 34.13 o 6 9 0 85.88 95.11 14.94 o 7 9 0 1798.14 1736.48 95.57 o 8 9 0 118.44 109.49 12.58 o 9 9 0 1211.00 1269.58 39.78 o -13 10 0 301.43 324.77 9.32 o -12 10 0 1112.89 1109.63 19.25 o -11 10 0 29.92 35.04 5.67 o -10 10 0 2393.29 2362.07 44.35 o -9 10 0 95.71 86.85 7.63 o -8 10 0 3126.83 3126.09 54.40 o -7 10 0 940.30 924.33 22.59 o -6 10 0 730.82 712.19 13.48 o -5 10 0 200.71 211.72 4.85 o -4 10 0 2817.19 2776.67 34.55 o -3 10 0 492.33 524.20 10.34 o -2 10 0 4843.96 4864.68 69.76 o -1 10 0 48.54 46.35 3.15 o 0 10 0 4032.25 3865.58 46.14 o 1 10 0 607.24 644.79 15.85 o 2 10 0 4543.35 4422.24 57.40 o 3 10 0 120.44 125.18 7.87 o 4 10 0 458.73 507.95 13.71 o 5 10 0 392.81 397.01 12.81 o 6 10 0 719.80 746.12 26.70 o 7 10 0 294.06 296.11 24.81 o 8 10 0 398.71 373.51 21.12 o -13 11 0 1213.30 1202.86 29.52 o -12 11 0 54.39 54.55 6.65 o -11 11 0 894.13 863.64 21.14 o -10 11 0 5.28 1.41 4.67 o -9 11 0 3366.22 3237.17 56.89 o -8 11 0 392.15 372.34 10.71 o -7 11 0 1597.50 1605.37 30.45 o -6 11 0 5.77 5.91 2.80 o -5 11 0 1365.74 1391.93 20.01 o -4 11 0 33.39 29.25 2.65 o -3 11 0 2435.83 2469.57 37.29 o -2 11 0 876.37 882.00 16.40 o -1 11 0 814.92 814.45 13.87 o 0 11 0 459.33 486.90 11.18 o 1 11 0 1968.59 1940.54 27.87 o 2 11 0 2183.39 2189.46 34.56 o 3 11 0 1652.33 1612.84 31.53 o 4 11 0 1656.66 1762.46 31.54 o 5 11 0 1411.52 1326.59 34.20 o 6 11 0 929.53 898.86 30.82 o 7 11 0 531.00 513.13 23.77 o 8 11 0 1673.30 1725.63 71.30 o -12 12 0 1167.43 1144.12 26.44 o -11 12 0 85.23 81.76 6.72 o -10 12 0 653.99 702.85 17.72 o -9 12 0 468.98 478.92 13.18 o -8 12 0 1476.59 1418.48 28.05 o -7 12 0 5.83 3.29 3.07 o -6 12 0 1437.84 1428.00 26.02 o -5 12 0 300.50 305.30 7.06 o -4 12 0 870.91 867.39 15.41 o -3 12 0 2204.86 2109.96 33.05 o -2 12 0 276.96 290.68 7.92 o -1 12 0 532.44 576.07 12.67 o 0 12 0 104.91 103.03 5.71 o 1 12 0 2034.38 1990.56 28.86 o 2 12 0 1066.83 1043.24 19.88 o 3 12 0 1340.16 1321.92 27.91 o 4 12 0 127.33 134.07 8.53 o 5 12 0 1627.22 1637.74 31.50 o 6 12 0 6.52 3.55 7.52 o 7 12 0 1580.33 1596.20 46.71 o -12 13 0 74.84 85.85 7.18 o -11 13 0 42.50 58.48 6.16 o -10 13 0 959.04 980.71 21.99 o -9 13 0 338.48 348.42 20.10 o -8 13 0 1132.03 1092.88 25.55 o -7 13 0 421.68 436.05 11.02 o -6 13 0 2424.69 2468.03 42.54 o -5 13 0 69.19 69.58 3.90 o -4 13 0 2167.07 2175.00 33.82 o -3 13 0 362.73 387.43 9.20 o -2 13 0 3656.47 3614.02 50.24 o -1 13 0 0.94 -4.80 3.20 o 0 13 0 1001.69 1009.97 21.40 o 1 13 0 899.35 906.11 18.48 o 2 13 0 989.75 924.16 19.28 o 3 13 0 0.08 -0.37 4.61 o 4 13 0 1343.98 1411.97 30.17 o 5 13 0 14.81 12.23 5.62 o 6 13 0 418.10 354.77 23.75 o -11 14 0 766.46 710.82 23.61 o -10 14 0 155.36 146.46 8.03 o -9 14 0 1654.71 1683.68 36.87 o -8 14 0 405.79 416.66 13.36 o -7 14 0 1741.78 1779.09 32.40 o -6 14 0 156.32 166.26 7.97 o -5 14 0 601.15 610.54 12.22 o -4 14 0 285.81 260.29 7.38 o -3 14 0 1174.13 1114.37 18.98 o -2 14 0 36.75 34.30 4.88 o -1 14 0 1915.40 1967.76 34.82 o 0 14 0 120.15 138.81 8.59 o 1 14 0 2757.43 2792.23 62.84 o 2 14 0 67.89 67.24 5.48 o 3 14 0 2706.20 2739.83 50.16 o 4 14 0 294.63 285.55 12.97 o 5 14 0 947.46 1071.31 25.05 o -11 15 0 14.36 10.31 9.02 o -10 15 0 510.76 517.32 22.11 o -9 15 0 44.80 40.46 4.01 o -8 15 0 720.53 692.84 15.81 o -7 15 0 196.18 208.17 8.89 o -6 15 0 1476.42 1544.25 28.85 o -5 15 0 603.27 589.19 11.47 o -4 15 0 2352.93 2333.77 37.15 o -3 15 0 476.89 490.94 15.31 o -2 15 0 2179.93 2076.92 40.24 o -1 15 0 599.61 638.95 18.10 o 0 15 0 774.26 829.04 26.61 o 1 15 0 181.55 183.00 16.81 o 2 15 0 385.59 438.58 25.89 o 3 15 0 55.79 48.03 7.22 o 4 15 0 630.44 648.98 18.76 o -10 16 0 12.25 5.30 5.50 o -9 16 0 1775.94 1808.22 33.16 o -8 16 0 101.39 95.71 6.32 o -7 16 0 245.12 266.96 10.48 o -6 16 0 208.65 218.16 11.22 o -5 16 0 997.03 1004.39 18.63 o -4 16 0 102.54 109.79 7.09 o -3 16 0 65.04 61.44 6.17 o -2 16 0 780.81 763.83 23.16 o -1 16 0 691.67 683.37 19.58 o 0 16 0 785.25 715.66 25.43 o 1 16 0 512.40 531.95 22.69 o 2 16 0 429.85 415.95 18.51 o -8 17 0 10.62 9.80 4.26 o -7 17 0 305.74 298.07 12.26 o -6 17 0 674.12 711.15 19.91 o -5 17 0 454.25 500.60 12.08 o -4 17 0 787.26 787.04 20.21 o -3 17 0 350.08 395.14 13.65 o -2 17 0 331.00 323.59 13.08 o -1 17 0 369.07 367.51 22.23 o 0 17 0 254.26 271.90 21.05 o 1 17 0 1409.11 1460.40 41.88 o -6 18 0 659.78 629.09 19.31 o -5 18 0 157.86 169.90 8.39 o -4 18 0 563.31 536.21 15.58 o -3 18 0 86.14 74.30 7.27 o -2 18 0 445.28 472.76 16.62 o 2 -18 1 638.85 676.81 19.60 o 3 -18 1 1.50 3.57 4.31 o 4 -18 1 946.47 932.50 21.40 o 5 -18 1 13.16 18.23 4.74 o 6 -18 1 764.97 792.27 21.73 o -1 -17 1 2112.40 2201.03 67.68 o 0 -17 1 107.69 64.60 11.99 o 1 -17 1 959.86 994.94 25.04 o 2 -17 1 30.69 34.63 5.71 o 3 -17 1 612.73 572.08 16.25 o 4 -17 1 59.13 49.00 5.18 o 5 -17 1 889.11 892.94 16.89 o 6 -17 1 6.46 5.50 4.26 o 7 -17 1 544.71 553.98 15.59 o 8 -17 1 189.63 178.67 11.13 o -2 -16 1 1086.19 1106.09 30.55 o -1 -16 1 1037.65 1003.75 37.85 o 0 -16 1 383.70 422.99 22.99 o 1 -16 1 21.94 18.68 5.06 o 2 -16 1 1043.29 1022.06 23.82 o 3 -16 1 156.47 164.20 12.23 o 4 -16 1 1296.05 1327.85 23.45 o 5 -16 1 421.06 384.22 12.61 o 6 -16 1 1565.77 1567.06 33.47 o 7 -16 1 50.68 62.08 5.43 o 8 -16 1 240.56 275.07 16.13 o 9 -16 1 764.53 766.55 20.28 o 10 -16 1 187.76 193.16 9.60 o -4 -15 1 102.93 107.80 9.03 o -3 -15 1 329.68 329.11 11.81 o -2 -15 1 553.95 552.57 20.00 o -1 -15 1 1147.69 1149.88 33.56 o 0 -15 1 546.19 523.32 16.86 o 1 -15 1 655.00 683.02 18.71 o 2 -15 1 217.52 248.96 10.50 o 3 -15 1 266.89 264.89 10.85 o 4 -15 1 2691.98 2611.73 40.41 o 5 -15 1 11.68 20.13 2.69 o 6 -15 1 1101.71 1106.62 25.06 o 7 -15 1 331.89 312.36 10.67 o 8 -15 1 1021.98 1048.15 24.87 o 9 -15 1 247.51 233.83 9.75 o 10 -15 1 1018.15 996.22 28.40 o -5 -14 1 344.41 351.20 16.14 o -4 -14 1 368.02 325.24 13.77 o -3 -14 1 259.05 235.87 10.98 o -2 -14 1 970.53 941.69 20.38 o -1 -14 1 1830.08 1769.19 38.51 o 0 -14 1 138.45 137.70 9.09 o 1 -14 1 5087.61 4962.44 84.66 o 2 -14 1 88.13 93.51 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274.48 227.77 7.11 o 1 5 3 855.38 861.71 14.55 o 2 5 3 1158.63 1106.83 22.29 o 3 5 3 1629.27 1623.45 38.60 o 4 5 3 1584.12 1502.20 27.82 o 5 5 3 736.84 770.32 17.75 o 6 5 3 341.40 339.54 14.27 o 7 5 3 75.97 73.40 10.89 o 8 5 3 1589.85 1627.87 29.92 o 9 5 3 125.75 125.73 7.91 o 10 5 3 785.17 864.25 21.04 o -14 6 3 274.90 287.46 12.38 o -13 6 3 145.55 148.40 7.23 o -12 6 3 1967.03 1860.22 35.89 o -11 6 3 37.98 47.64 5.48 o -10 6 3 1026.94 966.51 16.27 o -9 6 3 17.54 22.23 2.93 o -8 6 3 6083.09 6061.55 74.26 o -7 6 3 138.57 106.48 3.89 o -6 6 3 4967.83 5060.96 61.71 o -5 6 3 2148.35 2165.35 27.94 o -4 6 3 1502.04 1435.26 20.67 o -3 6 3 3182.65 3218.37 39.83 o -2 6 3 4.40 8.53 1.75 o -1 6 3 6572.96 6796.60 88.87 o 0 6 3 997.45 1013.77 17.84 o 1 6 3 10252.43 10609.71 151.54 o 2 6 3 14.35 9.79 2.89 o 3 6 3 4035.65 3925.36 61.53 o 4 6 3 2050.98 2013.60 36.25 o 5 6 3 2276.71 2238.36 59.57 o 6 6 3 1092.47 1104.22 24.10 o 7 6 3 330.15 366.60 20.48 o 8 6 3 0.07 0.54 5.63 o 9 6 3 1245.26 1244.09 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612.98 613.69 34.05 o 7 9 3 1455.41 1396.22 44.19 o 8 9 3 131.12 94.02 20.11 o -13 10 3 200.78 215.02 10.13 o -12 10 3 2.33 7.47 3.48 o -11 10 3 545.68 586.94 13.02 o -10 10 3 696.42 668.04 13.66 o -9 10 3 1588.97 1551.96 24.69 o -8 10 3 819.49 834.72 15.04 o -7 10 3 4085.55 4100.57 55.44 o -6 10 3 1245.35 1227.54 21.18 o -5 10 3 1194.54 1158.13 20.37 o -4 10 3 1559.30 1554.58 23.32 o -3 10 3 419.70 401.98 9.02 o -2 10 3 1217.66 1189.86 18.67 o -1 10 3 295.18 300.54 7.27 o 0 10 3 261.80 262.26 7.36 o 1 10 3 92.16 102.28 5.77 o 2 10 3 5566.81 5332.21 106.71 o 3 10 3 3048.34 2884.46 55.58 o 4 10 3 1445.57 1379.18 35.09 o 5 10 3 198.61 217.57 15.31 o 6 10 3 1623.08 1568.20 43.88 o 7 10 3 17.87 40.44 9.47 o 8 10 3 779.73 733.51 29.57 o -13 11 3 24.33 29.60 4.18 o -12 11 3 1015.77 972.49 18.40 o -11 11 3 55.86 67.79 5.58 o -10 11 3 3.21 3.98 2.71 o -9 11 3 671.58 668.01 13.20 o -8 11 3 2116.83 2094.30 30.52 o -7 11 3 739.51 720.65 14.46 o -6 11 3 182.59 176.28 6.58 o -5 11 3 2015.22 2007.37 29.11 o -4 11 3 54.89 58.44 4.27 o -3 11 3 1318.13 1329.25 21.36 o -2 11 3 1879.63 1822.01 32.66 o -1 11 3 1601.54 1615.18 23.50 o 0 11 3 1149.10 1118.72 18.31 o 1 11 3 2823.18 2776.54 41.96 o 2 11 3 118.53 98.01 7.50 o 3 11 3 489.39 550.03 20.76 o 4 11 3 637.71 670.25 23.11 o 5 11 3 1282.86 1285.36 38.18 o 6 11 3 7.78 -2.20 7.22 o 7 11 3 601.31 600.49 32.49 o -12 12 3 36.05 39.95 5.59 o -11 12 3 229.19 234.35 7.60 o -10 12 3 104.14 113.84 6.85 o -9 12 3 27.88 27.73 3.36 o -8 12 3 1634.21 1618.41 27.25 o -7 12 3 785.42 768.82 15.33 o -6 12 3 414.60 442.52 12.29 o -5 12 3 511.17 500.84 13.21 o -4 12 3 3050.36 2972.38 61.52 o -3 12 3 81.48 92.61 5.86 o -2 12 3 3373.08 3375.62 53.38 o -1 12 3 0.20 0.01 2.92 o 0 12 3 1983.71 2035.06 34.90 o 1 12 3 217.62 207.90 10.15 o 2 12 3 512.15 544.36 17.84 o 3 12 3 388.56 418.19 22.35 o 4 12 3 2148.77 2200.42 42.67 o 5 12 3 8.55 8.04 8.10 o 6 12 3 2379.36 2339.28 60.81 o -12 13 3 190.18 201.70 14.26 o -11 13 3 991.47 1010.78 27.48 o -10 13 3 175.75 181.89 10.10 o -9 13 3 1640.63 1583.46 26.65 o -8 13 3 12.35 14.14 3.07 o -7 13 3 659.63 655.88 12.65 o -6 13 3 211.32 205.48 7.58 o -5 13 3 3508.53 3328.97 50.72 o -4 13 3 163.01 177.91 7.49 o -3 13 3 19.10 19.99 3.87 o -2 13 3 4.95 5.87 3.54 o -1 13 3 1196.47 1203.73 24.45 o 0 13 3 495.27 503.77 12.14 o 1 13 3 1937.84 1908.96 31.63 o 2 13 3 95.28 94.89 9.27 o 3 13 3 707.91 655.79 19.49 o 4 13 3 215.13 192.16 12.08 o 5 13 3 978.64 999.25 34.28 o -11 14 3 54.88 56.40 8.27 o -10 14 3 1458.11 1483.13 35.78 o -9 14 3 69.41 70.12 5.37 o -8 14 3 731.05 721.60 13.50 o -7 14 3 42.09 41.76 4.67 o -6 14 3 2057.69 2051.22 33.24 o -5 14 3 425.00 415.76 12.76 o -4 14 3 2180.43 2161.86 40.85 o -3 14 3 65.06 55.98 5.50 o -2 14 3 2386.71 2414.04 41.42 o -1 14 3 804.61 778.08 21.53 o 0 14 3 581.44 594.28 19.14 o 1 14 3 457.32 463.31 13.48 o 2 14 3 940.71 1001.39 27.03 o 3 14 3 101.93 88.99 9.01 o 4 14 3 284.54 311.06 15.32 o -11 15 3 308.06 294.17 14.07 o -10 15 3 98.80 114.06 10.77 o -9 15 3 1031.45 977.06 22.13 o -8 15 3 1.50 3.04 2.58 o -7 15 3 235.99 252.65 9.95 o -6 15 3 385.11 395.00 17.64 o -5 15 3 804.71 801.28 19.48 o -4 15 3 1224.93 1196.16 26.33 o -3 15 3 969.62 1020.52 24.38 o -2 15 3 1151.77 1124.54 21.94 o -1 15 3 1234.07 1257.02 40.02 o 0 15 3 442.10 449.82 20.41 o 1 15 3 337.92 327.51 13.89 o 2 15 3 1447.25 1476.95 32.33 o 3 15 3 217.16 212.54 12.49 o -10 16 3 162.28 161.75 12.05 o -9 16 3 453.91 445.50 14.28 o -8 16 3 649.82 638.79 13.48 o -7 16 3 695.87 676.86 19.59 o -6 16 3 5.12 -2.09 3.50 o -5 16 3 666.64 660.84 17.75 o -4 16 3 178.78 155.85 9.41 o -3 16 3 847.77 832.03 19.71 o -2 16 3 107.54 117.06 12.09 o -1 16 3 1120.94 1123.94 28.91 o 0 16 3 0.98 3.23 7.25 o 1 16 3 1400.93 1443.19 41.46 o -8 17 3 1658.19 1605.11 30.05 o -7 17 3 151.03 142.51 9.33 o -6 17 3 489.08 518.49 15.10 o -5 17 3 7.32 -3.38 5.37 o -4 17 3 277.15 296.29 12.79 o -3 17 3 0.20 -1.36 4.01 o -2 17 3 602.20 553.70 22.62 o -1 17 3 8.67 15.42 8.20 o 2 -18 4 260.63 256.03 11.41 o 3 -18 4 514.86 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816.42 18.47 o 5 -13 4 1052.72 1012.47 20.67 o 6 -13 4 1525.38 1474.28 47.59 o 7 -13 4 307.54 352.70 21.88 o 8 -13 4 688.04 709.67 30.74 o 9 -13 4 220.45 216.67 22.97 o 10 -13 4 379.19 366.03 10.59 o 11 -13 4 8.73 24.19 3.96 o -7 -12 4 150.51 134.92 12.28 o -6 -12 4 1042.23 1065.45 26.34 o -5 -12 4 1106.00 1142.47 26.43 o -4 -12 4 755.42 867.85 21.43 o -3 -12 4 1148.31 1156.37 19.98 o -2 -12 4 610.25 641.40 12.82 o -1 -12 4 1316.85 1284.98 22.75 o 0 -12 4 1257.32 1205.35 25.21 o 1 -12 4 1878.90 1845.64 29.97 o 2 -12 4 405.30 427.76 9.80 o 3 -12 4 1895.14 1903.23 28.79 o 4 -12 4 72.82 83.13 4.62 o 5 -12 4 1504.40 1519.20 21.06 o 6 -12 4 71.41 69.96 11.01 o 7 -12 4 654.89 646.99 41.29 o 8 -12 4 176.32 207.57 25.15 o 9 -12 4 625.50 655.53 29.95 o 10 -12 4 15.26 24.30 3.95 o 11 -12 4 920.81 906.32 20.93 o -8 -11 4 622.93 581.80 40.10 o -7 -11 4 819.59 844.69 45.58 o -6 -11 4 662.62 695.33 26.11 o -5 -11 4 839.54 781.28 20.30 o -4 -11 4 247.93 303.77 13.59 o -3 -11 4 222.02 204.67 8.83 o -2 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