data_2239253 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.5013 _cell_length_b 14.0417 _cell_length_c 17.2134 _exptl_crystal_F_000 1584.00 _reflns_d_resolution_high 0.8001 _cod_data_source_file bt6967Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' el14_d611_drx7_cet_a in P 21 21 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 332.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8185.44 7865.61 238.54 o 4 0 0 568.81 558.09 25.50 o 6 0 0 13633.68 12907.32 395.75 o 8 0 0 3417.80 3223.08 108.13 o 10 0 0 1768.88 1835.70 97.09 o 12 0 0 1564.84 1585.00 107.41 o 14 0 0 2206.99 2172.52 208.46 o 16 0 0 174.14 96.89 114.51 o 2 1 0 2388.50 2369.25 49.36 o 3 1 0 37104.17 35452.46 791.53 o 4 1 0 23477.15 23503.75 498.78 o 5 1 0 7085.45 6757.47 164.97 o 6 1 0 8055.84 8164.93 198.79 o 7 1 0 18044.07 18187.87 410.12 o 8 1 0 1069.68 1055.40 38.85 o 9 1 0 3724.16 3833.63 108.05 o 10 1 0 18218.59 18604.19 525.05 o 11 1 0 81.98 81.43 25.58 o 12 1 0 4077.19 4133.07 144.29 o 13 1 0 246.21 255.22 32.95 o 14 1 0 822.69 683.89 86.47 o 15 1 0 205.39 220.34 76.47 o 16 1 0 360.17 293.61 86.51 o 0 2 0 4179.72 3837.09 146.91 o 1 2 0 33.28 45.18 3.55 o 2 2 0 531.99 516.39 14.06 o 3 2 0 7865.29 8306.32 197.61 o 4 2 0 21592.89 21625.45 511.09 o 5 2 0 14122.10 14721.95 331.98 o 6 2 0 17214.25 17514.06 452.70 o 7 2 0 58.39 75.57 13.97 o 8 2 0 6017.81 5902.38 172.78 o 9 2 0 2607.03 2599.52 77.90 o 10 2 0 907.49 942.47 39.46 o 11 2 0 335.66 292.63 29.59 o 12 2 0 957.20 1042.21 52.87 o 13 2 0 743.62 812.30 46.56 o 14 2 0 10.24 33.99 66.07 o 15 2 0 100.51 111.43 73.70 o 16 2 0 425.74 315.68 91.51 o 1 3 0 9552.07 9989.98 251.39 o 2 3 0 144.13 160.55 8.43 o 3 3 0 13526.33 13046.03 331.52 o 4 3 0 22480.97 21726.74 597.35 o 5 3 0 323.63 431.70 18.67 o 6 3 0 4934.49 5185.47 147.61 o 7 3 0 8443.01 8418.40 221.73 o 8 3 0 343.12 322.71 25.36 o 9 3 0 351.10 332.99 24.53 o 10 3 0 5001.41 4778.76 132.59 o 11 3 0 22.82 18.98 23.74 o 12 3 0 3.91 36.94 38.13 o 13 3 0 3339.33 3470.49 154.94 o 14 3 0 810.77 817.91 72.22 o 15 3 0 1323.61 1340.27 116.80 o 16 3 0 38.05 -35.04 78.36 o 0 4 0 2023.40 2267.76 113.83 o 1 4 0 11760.47 12043.54 303.16 o 2 4 0 3427.96 3477.98 90.23 o 3 4 0 83171.66 76954.02 2282.11 o 4 4 0 469.51 458.83 22.28 o 5 4 0 21635.06 20853.11 624.35 o 6 4 0 2060.11 2131.37 61.15 o 7 4 0 1021.41 1098.08 40.82 o 8 4 0 1434.04 1519.36 49.96 o 9 4 0 1257.61 1381.21 66.37 o 10 4 0 3240.53 3296.68 120.15 o 11 4 0 323.51 348.89 43.56 o 12 4 0 165.94 203.00 43.85 o 13 4 0 1.95 21.17 42.40 o 14 4 0 317.45 293.51 59.08 o 15 4 0 309.14 204.76 57.42 o 16 4 0 128.26 148.80 85.30 o 1 5 0 700.25 742.67 38.52 o 2 5 0 7770.38 7844.98 199.40 o 3 5 0 203.51 175.98 14.93 o 4 5 0 6304.25 6518.20 199.25 o 5 5 0 912.06 943.58 38.64 o 6 5 0 6009.12 5850.28 181.75 o 7 5 0 35024.05 33925.34 923.16 o 8 5 0 12109.16 12289.98 374.79 o 9 5 0 113.92 108.79 25.35 o 10 5 0 1002.12 1091.18 64.40 o 11 5 0 998.80 1071.82 88.15 o 12 5 0 645.65 632.95 56.73 o 13 5 0 1857.12 1689.13 95.24 o 14 5 0 13.71 61.06 54.37 o 15 5 0 874.89 751.76 99.59 o 16 5 0 151.22 147.13 92.00 o 0 6 0 7659.71 7609.68 294.13 o 1 6 0 25442.50 24943.71 677.65 o 2 6 0 8281.83 8379.67 254.87 o 3 6 0 6997.30 7404.94 226.05 o 4 6 0 3689.10 3963.78 125.22 o 5 6 0 403.29 391.48 24.53 o 6 6 0 603.45 573.51 45.87 o 7 6 0 1478.85 1535.03 61.54 o 8 6 0 4445.00 4507.03 134.33 o 9 6 0 1663.28 1772.06 97.36 o 10 6 0 41.83 77.41 32.24 o 11 6 0 1905.26 2039.18 99.03 o 12 6 0 10.76 -15.11 44.22 o 13 6 0 893.46 951.24 71.76 o 14 6 0 172.73 135.41 57.69 o 15 6 0 106.26 155.37 79.26 o 1 7 0 3761.49 3984.78 114.46 o 2 7 0 602.84 694.91 32.57 o 3 7 0 1308.55 1236.73 48.30 o 4 7 0 5.18 -6.59 16.06 o 5 7 0 17.54 2.11 18.07 o 6 7 0 2028.24 2066.18 75.52 o 7 7 0 8297.21 8183.37 254.42 o 8 7 0 922.64 967.11 45.03 o 9 7 0 39.28 61.02 33.43 o 10 7 0 2687.79 2903.77 112.16 o 11 7 0 3741.50 3746.32 155.02 o 12 7 0 871.18 1008.89 70.67 o 13 7 0 705.35 648.75 71.85 o 14 7 0 140.26 141.09 61.81 o 15 7 0 318.81 373.83 103.74 o 0 8 0 34049.06 34558.32 1156.00 o 1 8 0 2153.52 2036.17 72.23 o 2 8 0 3657.18 3512.61 166.99 o 3 8 0 11113.46 11104.46 337.75 o 4 8 0 353.48 296.64 25.17 o 5 8 0 24.55 20.70 20.77 o 6 8 0 2765.77 2900.95 100.65 o 7 8 0 7776.33 7780.32 244.09 o 8 8 0 1259.83 1213.31 65.18 o 9 8 0 952.76 1136.40 138.56 o 10 8 0 0.27 -3.04 43.37 o 11 8 0 547.04 591.02 57.13 o 12 8 0 328.44 289.74 53.27 o 13 8 0 1289.42 1331.33 136.04 o 14 8 0 644.37 618.26 94.54 o 15 8 0 13.75 -61.66 107.66 o 1 9 0 26.92 37.52 26.85 o 2 9 0 6066.27 6418.45 226.92 o 3 9 0 2374.54 2459.23 87.46 o 4 9 0 5614.77 5566.17 177.16 o 5 9 0 4519.55 4561.84 148.42 o 6 9 0 619.14 612.55 39.24 o 7 9 0 226.30 309.25 38.43 o 8 9 0 75.13 54.35 35.32 o 9 9 0 1468.65 1506.11 71.96 o 10 9 0 5378.34 5437.09 237.10 o 11 9 0 1088.03 1097.15 83.10 o 12 9 0 275.60 216.63 70.73 o 13 9 0 58.22 33.28 97.87 o 14 9 0 343.02 285.78 117.44 o 0 10 0 4208.08 4263.98 231.21 o 1 10 0 6838.56 6849.45 199.54 o 2 10 0 2395.96 2428.75 88.52 o 3 10 0 1351.86 1419.61 86.43 o 4 10 0 3462.82 3741.17 126.73 o 5 10 0 2696.31 2784.19 113.39 o 6 10 0 494.54 608.08 47.34 o 7 10 0 1961.54 2050.01 94.31 o 8 10 0 1023.50 1017.27 93.23 o 9 10 0 999.38 1156.18 71.24 o 10 10 0 118.29 145.66 73.89 o 11 10 0 39.09 52.29 68.12 o 12 10 0 5.12 -90.04 90.04 o 13 10 0 94.18 177.15 107.66 o 1 11 0 3539.32 3602.12 144.49 o 2 11 0 11.90 -25.84 25.84 o 3 11 0 2525.52 2560.97 129.26 o 4 11 0 299.59 364.97 43.65 o 5 11 0 1137.66 988.66 73.49 o 6 11 0 3804.39 3952.65 183.66 o 7 11 0 238.31 173.58 60.29 o 8 11 0 319.24 436.47 59.90 o 9 11 0 340.09 313.90 58.81 o 10 11 0 1162.88 1184.32 113.04 o 11 11 0 608.09 493.17 115.49 o 12 11 0 7.14 47.96 100.81 o 13 11 0 46.40 -98.85 105.70 o 0 12 0 10909.60 11338.35 573.59 o 1 12 0 21.70 -4.35 37.68 o 2 12 0 13.58 -0.45 37.89 o 3 12 0 1530.66 1555.89 82.68 o 4 12 0 6362.67 6062.81 230.80 o 5 12 0 1396.99 1557.02 97.61 o 6 12 0 640.76 593.99 78.87 o 7 12 0 87.27 49.20 50.57 o 8 12 0 457.48 507.96 107.94 o 9 12 0 451.01 271.10 97.87 o 10 12 0 2004.34 2054.10 204.55 o 11 12 0 38.04 93.96 102.76 o 12 12 0 249.48 374.84 121.36 o 1 13 0 44.84 28.18 43.21 o 2 13 0 174.36 242.03 57.02 o 3 13 0 32.35 51.94 51.70 o 4 13 0 197.55 119.97 53.87 o 5 13 0 1676.79 1693.11 107.91 o 6 13 0 404.02 418.49 82.19 o 7 13 0 3409.42 3739.79 190.02 o 8 13 0 1586.93 1761.71 141.81 o 9 13 0 36.43 -25.45 93.96 o 10 13 0 701.99 687.93 131.15 o 11 13 0 107.96 134.08 114.51 o 0 14 0 1.59 21.53 104.72 o 1 14 0 860.87 979.47 109.32 o 2 14 0 4452.09 4588.76 263.93 o 3 14 0 1198.99 1147.06 117.19 o 4 14 0 1703.70 1774.01 142.70 o 5 14 0 8.31 -66.19 81.23 o 6 14 0 37.11 59.94 78.54 o 7 14 0 175.02 54.15 116.47 o 8 14 0 9.69 141.91 111.57 o 9 14 0 3.90 104.72 111.57 o 10 14 0 3.67 184.00 122.34 o 1 15 0 18.98 101.04 82.68 o 2 15 0 619.57 562.21 97.83 o 3 15 0 670.87 672.68 104.74 o 4 15 0 509.83 562.04 97.62 o 5 15 0 234.97 345.03 94.53 o 6 15 0 10.98 57.52 86.39 o 7 15 0 471.51 332.33 99.35 o 8 15 0 420.30 268.16 127.23 o 0 16 0 3.67 67.53 132.12 o 1 16 0 473.85 354.07 104.11 o 2 16 0 69.30 105.02 92.61 o 3 16 0 401.20 515.82 107.43 o 4 16 0 161.69 122.56 102.27 o 5 16 0 7.28 46.76 94.74 o 6 16 0 893.49 761.31 122.84 o 1 17 0 91.73 317.30 108.15 o 2 17 0 1410.27 1459.01 321.94 o 3 17 0 248.77 216.71 104.47 o 4 17 0 88.73 23.06 100.28 o 2 0 1 82.33 57.14 5.70 o 3 0 1 21075.72 20123.93 430.16 o 4 0 1 1886.88 1877.96 43.87 o 5 0 1 16572.19 16159.41 347.89 o 6 0 1 10980.19 11386.25 261.04 o 7 0 1 253.50 199.35 16.55 o 8 0 1 5659.46 5540.80 141.40 o 9 0 1 2438.15 2513.18 71.73 o 10 0 1 3059.95 3065.39 85.64 o 11 0 1 146.64 134.73 28.03 o 12 0 1 76.93 67.14 25.09 o 13 0 1 1383.40 1272.96 57.10 o 14 0 1 1784.40 1718.36 205.04 o 15 0 1 269.40 275.12 78.53 o 16 0 1 27.92 -63.13 77.51 o -16 1 1 254.55 353.64 86.75 o -15 1 1 1150.57 1223.88 134.57 o -14 1 1 483.82 476.37 58.67 o -13 1 1 718.22 616.28 60.51 o -12 1 1 204.85 222.61 20.85 o -11 1 1 1245.97 1242.21 49.61 o -10 1 1 2143.86 2067.03 72.33 o -9 1 1 772.49 805.36 39.67 o -8 1 1 10315.31 10757.24 276.18 o -7 1 1 56.75 52.55 13.04 o -6 1 1 5826.71 5615.75 130.37 o -5 1 1 7263.45 7350.61 172.24 o -4 1 1 33757.23 32909.39 727.63 o -3 1 1 2747.29 2907.31 73.19 o -2 1 1 2750.48 2828.78 68.81 o 3 1 1 2900.15 3003.31 73.21 o 4 1 1 33286.61 32104.59 727.40 o 5 1 1 6524.11 6765.83 171.46 o 6 1 1 5073.88 4883.08 128.85 o 7 1 1 122.16 146.53 16.11 o 8 1 1 10069.73 10356.77 255.72 o 9 1 1 958.80 1052.09 52.17 o 10 1 1 2181.65 2167.71 83.75 o 11 1 1 1208.75 1218.21 56.37 o 12 1 1 245.00 257.39 31.35 o 13 1 1 697.80 689.13 40.45 o 14 1 1 584.08 516.96 101.25 o 15 1 1 1137.41 1173.00 111.64 o 16 1 1 300.56 232.57 85.05 o -16 2 1 28.58 135.94 191.83 o -15 2 1 59.66 32.69 71.62 o -14 2 1 2449.37 2394.42 184.59 o -13 2 1 2583.39 2544.14 119.71 o -12 2 1 599.28 537.54 51.47 o -11 2 1 4414.17 4332.06 171.85 o -10 2 1 6530.91 6656.01 234.21 o -9 2 1 936.13 955.21 42.09 o -8 2 1 6961.31 6871.40 177.86 o -7 2 1 4907.71 4974.10 128.11 o -6 2 1 641.83 619.64 37.44 o -5 2 1 1663.29 1744.94 54.34 o -4 2 1 8808.95 8769.29 238.26 o -3 2 1 4004.51 4036.20 107.72 o -2 2 1 5681.72 5589.37 138.33 o -1 2 1 1100.86 1075.38 30.50 o 0 2 1 2630.72 2710.69 57.90 o 1 2 1 1182.25 1150.48 33.62 o 2 2 1 5306.92 5231.33 164.42 o 3 2 1 3683.78 3656.15 107.07 o 4 2 1 8763.94 8574.03 221.26 o 5 2 1 1897.17 1960.32 53.01 o 6 2 1 788.16 771.53 25.63 o 7 2 1 5233.76 5208.38 126.99 o 8 2 1 6581.32 6423.09 176.86 o 9 2 1 917.43 896.53 39.38 o 10 2 1 6281.66 6266.68 189.04 o 11 2 1 4465.53 4493.40 151.47 o 12 2 1 620.30 628.29 41.01 o 13 2 1 2676.59 2707.54 93.21 o 14 2 1 2589.04 2686.47 128.95 o 15 2 1 31.91 27.46 198.68 o 16 2 1 43.90 90.17 81.58 o -16 3 1 403.83 436.94 92.73 o -15 3 1 170.13 141.82 76.41 o -14 3 1 1097.98 1129.77 84.38 o -13 3 1 171.76 172.61 47.63 o -12 3 1 974.58 951.43 61.69 o -11 3 1 369.52 377.89 43.97 o -10 3 1 1709.46 1707.68 76.17 o -9 3 1 2409.14 2543.35 90.25 o -8 3 1 2525.36 2612.69 79.01 o -7 3 1 8372.77 8224.18 236.46 o -6 3 1 649.01 598.86 28.32 o -5 3 1 8213.88 8436.71 222.58 o -4 3 1 11792.23 11962.40 399.94 o -3 3 1 15098.44 15129.49 421.48 o -2 3 1 9064.27 9078.87 225.70 o -1 3 1 15826.54 15780.80 368.09 o 0 3 1 32028.94 30776.95 768.19 o 1 3 1 13701.85 13382.42 402.60 o 2 3 1 8719.68 8700.29 266.72 o 3 3 1 15364.62 15715.03 392.61 o 4 3 1 13823.91 14276.43 339.62 o 5 3 1 7658.92 7707.34 192.08 o 6 3 1 553.80 547.29 22.22 o 7 3 1 8357.25 8397.88 237.70 o 8 3 1 2190.71 2186.16 75.92 o 9 3 1 2846.17 2892.30 81.99 o 10 3 1 1986.90 2004.56 63.09 o 11 3 1 261.31 303.44 35.62 o 12 3 1 675.26 652.54 46.79 o 13 3 1 159.09 220.65 36.65 o 14 3 1 1099.36 1141.79 79.20 o 15 3 1 185.84 132.70 72.51 o 16 3 1 471.26 430.63 90.26 o -16 4 1 39.77 -75.76 75.76 o -15 4 1 824.21 887.74 102.73 o -14 4 1 864.08 829.70 88.39 o -13 4 1 1151.72 1018.30 73.55 o -12 4 1 2064.86 2046.29 98.95 o -11 4 1 4067.64 4180.54 170.80 o -10 4 1 1560.97 1542.69 68.62 o -9 4 1 5158.40 5215.85 149.63 o -8 4 1 2736.48 2713.62 86.40 o -7 4 1 12616.13 12982.48 399.01 o -6 4 1 2679.62 2736.51 81.91 o -5 4 1 6239.66 6395.34 197.82 o -4 4 1 7267.66 7374.15 214.36 o -3 4 1 12323.59 12111.50 354.95 o -2 4 1 31293.44 30607.71 839.03 o -1 4 1 3146.21 3257.68 89.89 o 0 4 1 13866.20 13935.65 349.75 o 1 4 1 3059.44 3052.59 98.16 o 2 4 1 32191.79 31343.30 838.22 o 3 4 1 11642.70 11584.00 300.55 o 4 4 1 6704.80 6834.42 180.56 o 5 4 1 6190.61 6433.09 180.75 o 6 4 1 2492.79 2595.93 74.09 o 7 4 1 12907.79 13267.74 366.62 o 8 4 1 2705.80 2553.77 77.52 o 9 4 1 4654.29 4731.27 147.73 o 10 4 1 1516.76 1530.96 54.42 o 11 4 1 4335.84 4506.89 149.93 o 12 4 1 1972.80 1958.33 80.64 o 13 4 1 1133.91 1131.99 61.70 o 14 4 1 776.59 743.41 68.64 o 15 4 1 833.27 788.66 102.76 o 16 4 1 35.86 -59.53 77.83 o -16 5 1 18.79 -10.98 82.01 o -15 5 1 125.40 142.96 78.45 o -14 5 1 116.62 134.13 70.58 o -13 5 1 358.16 401.38 98.27 o -12 5 1 1294.45 1270.91 77.71 o -11 5 1 216.36 225.76 42.83 o -10 5 1 2246.43 2305.39 129.24 o -9 5 1 2724.04 2817.71 96.81 o -8 5 1 6482.36 6617.85 214.52 o -7 5 1 9313.55 9274.46 266.77 o -6 5 1 1716.35 1865.54 61.16 o -5 5 1 5500.15 5559.08 176.15 o -4 5 1 7160.69 7477.47 239.49 o -3 5 1 26563.91 26288.49 752.09 o -2 5 1 12630.01 12995.46 326.59 o -1 5 1 25135.07 25086.47 665.68 o 0 5 1 2431.49 2287.43 61.92 o 1 5 1 23888.42 23991.46 665.24 o 2 5 1 10454.62 10749.35 351.23 o 3 5 1 24016.63 24322.08 682.98 o 4 5 1 7700.84 8122.64 219.77 o 5 5 1 5760.84 5763.24 160.88 o 6 5 1 1406.37 1464.87 52.19 o 7 5 1 9412.77 9690.76 247.79 o 8 5 1 6748.14 6963.33 195.86 o 9 5 1 2924.66 3010.25 87.35 o 10 5 1 2005.17 1961.60 72.41 o 11 5 1 173.39 157.93 38.62 o 12 5 1 1361.42 1312.96 78.10 o 13 5 1 360.57 315.15 42.04 o 14 5 1 116.71 66.58 49.72 o 15 5 1 105.63 155.52 78.86 o 16 5 1 14.54 -63.96 78.55 o -15 6 1 176.85 277.95 87.59 o -14 6 1 324.07 306.65 65.75 o -13 6 1 582.13 564.32 69.98 o -12 6 1 27.68 -16.17 43.45 o -11 6 1 1911.64 2046.03 114.48 o -10 6 1 2214.32 2237.77 103.18 o -9 6 1 765.39 822.60 83.91 o -8 6 1 4740.30 4757.80 142.91 o -7 6 1 11328.36 11074.00 339.96 o -6 6 1 1733.89 1795.89 68.67 o -5 6 1 4011.59 4133.45 140.95 o -4 6 1 47.11 34.84 16.05 o -3 6 1 15469.81 15886.66 483.42 o -2 6 1 487.57 496.46 23.72 o -1 6 1 2392.48 2355.60 71.65 o 0 6 1 482.97 450.88 20.62 o 1 6 1 2450.73 2464.27 71.02 o 2 6 1 507.21 549.49 27.02 o 3 6 1 15521.91 16228.59 438.77 o 4 6 1 66.06 72.20 14.15 o 5 6 1 4546.26 4743.25 139.99 o 6 6 1 1799.02 1907.80 66.72 o 7 6 1 10999.53 11109.48 338.58 o 8 6 1 4842.31 4816.66 141.12 o 9 6 1 672.96 716.07 77.82 o 10 6 1 2287.19 2371.66 120.33 o 11 6 1 2077.47 2208.47 99.91 o 12 6 1 13.50 -0.07 41.02 o 13 6 1 526.75 606.43 51.00 o 14 6 1 327.32 334.96 108.15 o 15 6 1 175.62 192.41 102.27 o -15 7 1 1212.14 1296.23 121.42 o -14 7 1 296.83 320.34 79.96 o -13 7 1 670.85 716.33 91.51 o -12 7 1 287.75 320.43 52.95 o -11 7 1 159.25 187.98 45.73 o -10 7 1 242.84 195.86 38.78 o -9 7 1 165.34 128.30 36.96 o -8 7 1 607.56 609.21 38.34 o -7 7 1 2786.81 2784.49 98.49 o -6 7 1 467.76 508.14 32.41 o -5 7 1 985.78 1023.89 44.65 o -4 7 1 2355.22 2377.48 84.84 o -3 7 1 12268.00 12018.42 369.99 o -2 7 1 4336.45 4712.39 135.37 o -1 7 1 8240.30 8239.96 247.04 o 0 7 1 8589.58 8210.83 228.58 o 1 7 1 9304.99 9570.38 246.92 o 2 7 1 4506.11 4748.52 162.48 o 3 7 1 12931.73 12371.39 368.84 o 4 7 1 2593.57 2573.82 83.43 o 5 7 1 952.39 902.71 40.74 o 6 7 1 442.54 395.47 31.90 o 7 7 1 2869.41 2825.84 96.86 o 8 7 1 715.18 709.59 41.29 o 9 7 1 208.62 189.10 35.00 o 10 7 1 220.07 247.38 55.66 o 11 7 1 149.80 136.20 41.01 o 12 7 1 286.62 275.88 48.77 o 13 7 1 662.16 646.15 61.72 o 14 7 1 292.18 196.75 73.64 o 15 7 1 1156.84 1117.58 162.46 o -15 8 1 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