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Information card for entry 2239294
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| Coordinates | 2239294.cif |
|---|---|
| Structure factors | 2239294.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis[2,6-bis(1<i>H</i>-pyrazol-1-yl)pyridine]decakis(μ~2~-3-nitrobenzoato)bis(3-nitrobenzoato)tetradysprosium(III) |
|---|---|
| Formula | C106 H66 Dy4 N22 O48 |
| Calculated formula | C106 H66 Dy4 N22 O48 |
| Title of publication | Bis[2,6-bis(1<i>H</i>-pyrazol-1-yl)pyridine]decakis(μ~2~-3-nitrobenzoato)bis(3-nitrobenzoato)tetradysprosium(III): a linear tetranuclear dysprosium compound based on mixed N- and O-donor ligands |
| Authors of publication | Hua, Rong; Wu, Xiao-Liu; Li, Jin-Ying |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2014 |
| Journal volume | 70 |
| Journal issue | 5 |
| Pages of publication | m162 - m163 |
| a | 14.2514 ± 0.0003 Å |
| b | 14.9274 ± 0.0005 Å |
| c | 14.9616 ± 0.0003 Å |
| α | 100.443 ± 0.002° |
| β | 111.754 ± 0.001° |
| γ | 99.695 ± 0.002° |
| Cell volume | 2808.88 ± 0.13 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0269 |
| Residual factor for significantly intense reflections | 0.0215 |
| Weighted residual factors for significantly intense reflections | 0.0544 |
| Weighted residual factors for all reflections included in the refinement | 0.0584 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.131 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181892 (current) | 2016-04-06 | hkl/2/23/ (antanas@echidna) Adding IUCr specific svn headers to multiple entries in subrange 2/23/92. |
2239294.cif 2239294.hkl |
| 181311 | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/92. |
2239294.cif 2239294.hkl |
| 176798 | 2016-02-21 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23. |
2239294.cif 2239294.hkl |
| 109235 | 2014-04-10 | cif/ hkl/ Adding structures of 2239294 via cif-deposit CGI script. |
2239294.cif 2239294.hkl |
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