data_2239323 _cell_angle_alpha 90.000 _cell_angle_beta 105.800 _cell_angle_gamma 90.000 _cell_length_a 10.4303 _cell_length_b 6.8873 _cell_length_c 13.4991 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.8301 _[local]_cod_data_source_file is5344Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' OhnoNakamuraLab_130218' _shelx_refln_list_code 4 _shelx_f_calc_maximum 135.71 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13290.48 8466.01 262.15 o 4 0 0 975.07 1057.73 19.17 o 6 0 0 250.66 233.83 3.10 o 8 0 0 948.50 878.09 16.98 o 10 0 0 1886.23 1800.53 47.72 o 12 0 0 35.01 33.14 3.09 o 1 1 0 547.29 637.46 4.52 o 2 1 0 11924.82 9026.17 139.81 o 3 1 0 621.85 651.77 4.67 o 4 1 0 49.65 63.89 0.66 o 5 1 0 540.09 584.35 4.45 o 6 1 0 16.40 21.03 0.53 o 7 1 0 197.40 171.55 2.47 o 8 1 0 323.71 299.63 4.98 o 9 1 0 21.21 19.33 1.31 o 10 1 0 88.35 84.58 2.90 o 11 1 0 3.24 2.42 0.80 o 12 1 0 319.30 342.27 7.30 o 0 2 0 3068.47 3001.76 39.55 o 1 2 0 4990.78 4782.05 41.87 o 2 2 0 990.64 962.98 6.96 o 3 2 0 5.39 6.91 0.35 o 4 2 0 68.21 71.22 1.13 o 5 2 0 60.07 58.88 1.03 o 6 2 0 27.97 40.58 1.02 o 7 2 0 949.83 889.99 12.46 o 8 2 0 91.81 92.08 2.27 o 9 2 0 1400.53 1297.45 20.92 o 10 2 0 181.86 178.81 3.56 o 11 2 0 99.95 101.55 2.91 o 1 3 0 224.69 232.83 1.87 o 2 3 0 1407.93 1525.00 11.79 o 3 3 0 1299.47 1381.60 10.63 o 4 3 0 4325.61 4404.94 43.94 o 5 3 0 1160.42 1192.24 11.46 o 6 3 0 1502.75 1462.81 19.78 o 7 3 0 408.30 389.23 5.40 o 8 3 0 139.14 134.52 2.57 o 9 3 0 21.19 22.37 1.23 o 10 3 0 0.22 0.52 0.65 o 11 3 0 92.99 100.79 2.83 o 0 4 0 542.32 595.11 6.87 o 1 4 0 783.20 825.78 6.80 o 2 4 0 13.34 20.64 0.49 o 3 4 0 519.91 526.86 4.39 o 4 4 0 0.68 2.57 0.52 o 5 4 0 19.50 20.79 1.27 o 6 4 0 272.25 258.69 4.38 o 7 4 0 197.86 186.57 3.44 o 8 4 0 85.72 99.14 2.17 o 9 4 0 161.43 166.20 3.40 o 10 4 0 0.76 0.98 0.80 o 1 5 0 152.75 140.95 2.25 o 2 5 0 336.98 302.02 6.22 o 3 5 0 864.92 833.77 11.05 o 4 5 0 46.64 46.13 1.39 o 5 5 0 1251.85 1158.56 16.71 o 6 5 0 56.68 62.10 1.78 o 7 5 0 334.17 334.07 5.72 o 8 5 0 15.80 17.04 0.98 o 9 5 0 41.08 48.28 1.36 o 0 6 0 84.34 76.45 2.75 o 1 6 0 1096.60 997.22 15.16 o 2 6 0 83.16 72.57 2.10 o 3 6 0 688.91 622.91 11.16 o 4 6 0 115.08 99.08 2.78 o 5 6 0 6.82 7.86 0.97 o 6 6 0 39.26 45.19 1.81 o 7 6 0 295.88 320.14 5.71 o 8 6 0 7.27 8.05 0.98 o 1 7 0 2.27 2.26 0.69 o 2 7 0 111.39 107.22 2.80 o 3 7 0 108.74 106.13 2.69 o 4 7 0 52.38 52.22 2.07 o 5 7 0 393.36 428.96 8.43 o 6 7 0 114.43 129.92 3.25 o 0 8 0 118.13 132.30 3.95 o 1 8 0 61.29 67.15 2.80 o 2 8 0 103.51 111.90 2.59 o 3 8 0 85.90 93.59 2.58 o -11 0 1 8.14 9.60 1.77 o -9 0 1 78.40 77.38 4.23 o -7 0 1 302.31 301.11 4.81 o -5 0 1 32.48 47.72 0.75 o -3 0 1 1230.60 1288.97 14.06 o -1 0 1 1096.08 1198.07 15.64 o 1 0 1 5451.56 4606.23 100.80 o 3 0 1 2186.29 2133.44 27.57 o 5 0 1 463.26 474.71 8.79 o 7 0 1 10.10 12.18 1.17 o 9 0 1 296.93 286.60 6.17 o 11 0 1 671.52 714.74 38.62 o -12 1 1 0.06 0.76 0.94 o -11 1 1 80.19 85.46 2.84 o -10 1 1 0.60 1.07 0.91 o -9 1 1 58.25 57.28 2.05 o -8 1 1 2.61 3.99 0.88 o -7 1 1 116.28 111.15 1.95 o -6 1 1 12.85 10.69 1.07 o -5 1 1 428.29 409.39 3.08 o -4 1 1 397.50 496.95 4.47 o -3 1 1 64.38 45.98 0.58 o -2 1 1 2509.79 2514.39 20.76 o -1 1 1 274.17 328.57 2.17 o 0 1 1 297.69 245.60 2.05 o 1 1 1 33.21 23.19 0.40 o 2 1 1 228.95 220.82 1.55 o 3 1 1 2017.86 2043.99 15.84 o 4 1 1 587.73 584.16 4.64 o 5 1 1 3.17 8.17 0.52 o 6 1 1 9.99 11.02 0.46 o 7 1 1 4.26 3.81 0.64 o 8 1 1 9.04 8.40 1.13 o 9 1 1 254.12 237.08 4.29 o 10 1 1 141.01 137.42 2.88 o 11 1 1 8.44 9.58 1.14 o -11 2 1 0.46 1.09 0.77 o -10 2 1 164.38 157.18 3.64 o -9 2 1 68.87 61.74 1.93 o -8 2 1 879.68 837.45 12.68 o -7 2 1 152.29 144.00 2.46 o -6 2 1 127.40 121.56 1.53 o -5 2 1 12.44 16.21 0.96 o -4 2 1 5.99 6.52 0.63 o -3 2 1 200.43 235.52 1.76 o -2 2 1 2350.43 2445.00 20.13 o -1 2 1 2.05 2.01 0.23 o 0 2 1 60.06 91.73 0.91 o 1 2 1 1218.51 1175.03 8.22 o 2 2 1 2727.20 2796.05 22.20 o 3 2 1 119.84 147.17 1.20 o 4 2 1 310.72 335.50 2.56 o 5 2 1 21.54 30.27 0.73 o 6 2 1 123.75 118.56 1.95 o 7 2 1 107.45 102.21 2.02 o 8 2 1 72.99 64.84 1.77 o 9 2 1 48.80 52.36 1.80 o 10 2 1 34.95 35.73 1.41 o 11 2 1 162.52 172.62 3.41 o -11 3 1 55.17 68.63 2.37 o -10 3 1 172.87 172.80 4.94 o -9 3 1 19.79 22.71 1.36 o -8 3 1 16.14 14.64 0.98 o -7 3 1 39.10 33.38 1.08 o -6 3 1 1008.34 917.45 9.97 o -5 3 1 142.70 164.06 1.58 o -4 3 1 94.03 153.45 1.63 o -3 3 1 922.15 949.32 7.09 o -2 3 1 221.06 263.31 1.94 o -1 3 1 105.12 84.58 0.81 o 0 3 1 875.64 829.84 6.43 o 1 3 1 1404.18 1569.60 11.79 o 2 3 1 1551.58 1783.34 13.74 o 3 3 1 1591.00 1723.02 14.37 o 4 3 1 1864.33 1867.76 16.22 o 5 3 1 1188.19 1181.02 12.88 o 6 3 1 95.10 85.02 1.84 o 7 3 1 708.67 677.88 9.77 o 8 3 1 246.05 235.17 4.09 o 9 3 1 171.74 161.92 3.62 o 10 3 1 109.16 104.90 2.48 o 11 3 1 0.46 0.42 0.79 o -10 4 1 21.51 26.82 1.59 o -9 4 1 1.59 2.45 0.91 o -8 4 1 131.05 127.17 3.02 o -7 4 1 30.16 32.77 1.33 o -6 4 1 47.54 52.24 2.43 o -5 4 1 922.39 896.65 11.69 o -4 4 1 416.89 419.12 6.06 o -3 4 1 53.05 58.56 0.81 o -2 4 1 24.33 30.74 0.56 o -1 4 1 329.07 306.82 2.51 o 0 4 1 198.52 200.69 1.86 o 1 4 1 0.93 2.31 0.36 o 2 4 1 200.51 159.97 1.51 o 3 4 1 107.13 95.09 1.15 o 4 4 1 68.00 55.38 1.44 o 5 4 1 55.65 55.88 1.54 o 6 4 1 2.44 5.77 0.96 o 7 4 1 93.48 90.81 2.21 o 8 4 1 0.79 2.16 0.69 o 9 4 1 34.47 39.35 1.45 o 10 4 1 27.62 29.17 2.34 o -9 5 1 1.95 1.46 0.69 o -8 5 1 80.57 88.72 2.20 o -7 5 1 204.34 195.34 4.91 o -6 5 1 380.63 364.05 9.37 o -5 5 1 175.15 160.25 3.91 o -4 5 1 1540.95 1423.10 26.71 o -3 5 1 143.34 141.46 2.65 o -2 5 1 33.50 34.66 1.12 o -1 5 1 0.10 2.83 0.63 o 0 5 1 8.37 12.99 1.88 o 1 5 1 32.75 33.60 1.17 o 2 5 1 264.79 225.48 3.25 o 3 5 1 47.69 48.13 1.19 o 4 5 1 355.97 343.09 5.69 o 5 5 1 0.36 0.95 0.70 o 6 5 1 557.06 530.56 9.59 o 7 5 1 7.45 8.27 1.01 o 8 5 1 2.84 1.62 0.67 o 9 5 1 3.29 2.58 0.70 o -8 6 1 59.21 57.34 2.01 o -7 6 1 6.85 4.54 0.75 o -6 6 1 314.44 312.50 7.44 o -5 6 1 0.10 0.36 0.63 o -4 6 1 45.79 44.16 1.73 o -3 6 1 0.38 0.80 0.76 o -2 6 1 749.74 684.92 11.38 o -1 6 1 366.10 349.65 5.52 o 0 6 1 93.08 88.55 2.63 o 1 6 1 260.51 240.37 3.93 o 2 6 1 437.99 405.61 6.02 o 3 6 1 0.09 0.66 0.74 o 4 6 1 703.13 653.99 10.93 o 5 6 1 4.16 2.93 0.90 o 6 6 1 42.17 55.12 1.73 o 7 6 1 29.85 34.92 1.27 o 8 6 1 410.11 459.98 10.92 o -6 7 1 1.53 0.86 0.67 o -5 7 1 17.72 16.82 1.32 o -4 7 1 95.86 97.07 2.46 o -3 7 1 4.02 5.64 1.22 o -2 7 1 31.11 34.83 1.79 o -1 7 1 124.13 123.89 2.82 o 0 7 1 17.53 16.38 1.08 o 1 7 1 45.05 45.77 1.57 o 2 7 1 54.01 55.64 1.98 o 3 7 1 59.44 62.69 2.01 o 4 7 1 19.45 20.82 1.52 o 5 7 1 59.49 57.44 1.98 o 6 7 1 231.53 257.32 5.41 o -3 8 1 0.42 0.48 0.76 o -2 8 1 54.77 57.04 1.81 o -1 8 1 49.16 49.96 1.71 o 0 8 1 145.66 151.17 2.87 o 1 8 1 104.17 115.28 2.61 o 2 8 1 99.28 105.80 2.55 o -12 0 2 215.44 220.95 9.18 o -10 0 2 62.35 56.00 3.38 o -8 0 2 23.34 23.62 1.60 o -6 0 2 133.66 130.97 1.84 o -4 0 2 1567.61 1451.21 16.10 o -2 0 2 6510.63 5550.90 74.47 o 0 0 2 1.63 28.52 0.66 o 2 0 2 1622.84 1785.64 20.52 o 4 0 2 159.22 201.68 2.49 o 6 0 2 68.57 79.76 1.43 o 8 0 2 10.35 9.72 1.27 o 10 0 2 560.84 538.13 13.81 o -12 1 2 153.20 174.25 4.03 o -11 1 2 61.31 57.69 2.39 o -10 1 2 440.21 408.95 7.11 o -9 1 2 844.58 766.59 13.00 o -8 1 2 661.24 609.11 10.13 o -7 1 2 456.21 427.30 5.65 o -6 1 2 885.71 911.77 7.59 o -5 1 2 21.24 25.99 0.47 o -4 1 2 144.06 122.10 1.12 o -3 1 2 432.62 519.79 4.02 o -2 1 2 8183.32 7046.20 68.58 o -1 1 2 32.73 51.77 0.59 o 0 1 2 12059.90 9154.73 107.95 o 1 1 2 1765.71 1906.39 14.21 o 2 1 2 2641.82 2645.40 20.82 o 3 1 2 31.71 34.78 0.62 o 4 1 2 111.60 107.25 0.99 o 5 1 2 110.51 111.65 1.22 o 6 1 2 84.87 83.48 1.24 o 7 1 2 63.86 68.15 1.72 o 8 1 2 569.28 508.31 8.15 o 9 1 2 105.21 100.30 2.47 o 10 1 2 450.38 449.62 7.82 o 11 1 2 6.50 5.73 1.30 o -12 2 2 50.42 56.60 2.02 o -11 2 2 33.27 32.83 1.51 o -10 2 2 5.39 5.30 1.08 o -9 2 2 10.26 9.95 1.32 o -8 2 2 1.22 4.09 1.75 o -7 2 2 408.87 392.45 6.05 o -6 2 2 1056.81 1095.07 9.61 o -5 2 2 128.40 114.67 1.58 o -4 2 2 4752.06 4952.36 47.76 o -3 2 2 670.28 737.64 5.24 o -2 2 2 26.85 35.52 0.48 o -1 2 2 3.51 7.09 0.25 o 0 2 2 171.92 171.32 1.34 o 1 2 2 32.47 28.71 0.77 o 2 2 2 2.34 2.93 0.28 o 3 2 2 2377.52 2456.55 19.55 o 4 2 2 996.45 1050.54 8.61 o 5 2 2 567.80 625.42 5.97 o 6 2 2 369.08 358.53 4.94 o 7 2 2 1.23 7.00 1.75 o 8 2 2 3.09 3.99 0.82 o 9 2 2 4.35 5.90 0.96 o 10 2 2 85.25 83.35 1.96 o 11 2 2 11.15 11.19 0.88 o -11 3 2 116.97 114.65 2.43 o -10 3 2 63.02 72.02 2.22 o -9 3 2 783.61 730.50 17.69 o -8 3 2 226.98 234.55 6.24 o -7 3 2 1534.43 1453.39 24.21 o -6 3 2 920.18 931.61 18.10 o -5 3 2 17.01 25.69 0.51 o -4 3 2 17.58 20.27 0.45 o -3 3 2 364.43 329.90 2.39 o -2 3 2 236.78 230.64 1.59 o -1 3 2 14.01 21.10 0.87 o 0 3 2 439.55 526.05 3.95 o 1 3 2 2940.52 3121.85 28.69 o 2 3 2 55.35 65.74 0.66 o 3 3 2 2107.00 2214.07 18.80 o 4 3 2 1.11 4.33 0.49 o 5 3 2 801.51 803.78 9.53 o 6 3 2 293.26 287.93 4.45 o 7 3 2 652.64 621.98 9.64 o 8 3 2 185.71 184.84 3.43 o 9 3 2 70.23 67.26 1.77 o 10 3 2 6.70 8.21 0.91 o -10 4 2 4.26 4.08 1.40 o -9 4 2 7.64 8.41 1.98 o -8 4 2 30.77 37.55 1.85 o -7 4 2 341.42 332.30 6.22 o -6 4 2 414.87 402.74 8.84 o -5 4 2 1523.93 1477.04 31.25 o -4 4 2 715.74 674.54 9.24 o -3 4 2 292.86 303.05 3.11 o -2 4 2 75.11 67.46 0.82 o -1 4 2 145.13 147.36 1.45 o 0 4 2 85.41 98.49 1.17 o 1 4 2 161.80 168.25 1.66 o 2 4 2 43.78 46.58 0.78 o 3 4 2 1376.08 1382.05 14.81 o 4 4 2 330.61 315.24 4.69 o 5 4 2 830.31 770.98 12.73 o 6 4 2 655.43 632.34 10.69 o 7 4 2 74.43 74.02 1.95 o 8 4 2 67.25 63.32 1.71 o 9 4 2 84.41 83.96 1.92 o 10 4 2 14.79 18.00 1.72 o -9 5 2 174.76 190.09 4.37 o -8 5 2 16.10 21.33 1.19 o -7 5 2 92.53 101.45 2.63 o -6 5 2 0.02 0.62 0.67 o -5 5 2 75.93 71.38 2.02 o -4 5 2 6.73 8.05 0.87 o -3 5 2 532.47 494.95 7.48 o -2 5 2 0.92 12.38 4.66 o -1 5 2 685.85 647.02 9.34 o 0 5 2 57.27 65.56 1.52 o 1 5 2 981.41 928.28 12.22 o 2 5 2 153.45 151.97 2.66 o 3 5 2 248.97 233.61 3.38 o 4 5 2 3.14 3.65 0.82 o 5 5 2 169.87 153.37 3.32 o 6 5 2 0.03 0.59 0.76 o 7 5 2 235.06 231.67 4.28 o 8 5 2 2.66 2.32 0.74 o 9 5 2 37.37 34.57 3.80 o -8 6 2 0.05 0.31 0.49 o -7 6 2 182.24 186.34 3.48 o -6 6 2 3.56 4.19 0.85 o -5 6 2 618.21 582.40 8.88 o -4 6 2 53.81 52.46 1.91 o -3 6 2 616.87 571.43 9.64 o -2 6 2 30.86 30.37 1.60 o -1 6 2 302.75 278.60 4.63 o 0 6 2 1.32 6.34 2.53 o 1 6 2 1.36 2.86 0.74 o 2 6 2 36.86 31.74 1.27 o 3 6 2 347.54 326.40 5.35 o 4 6 2 88.63 86.96 2.48 o 5 6 2 280.02 275.52 5.39 o 6 6 2 56.48 66.17 1.85 o 7 6 2 0.10 0.44 0.53 o -6 7 2 113.99 123.17 3.29 o -5 7 2 1.80 2.16 0.82 o -4 7 2 0.82 2.18 0.94 o -3 7 2 85.43 79.35 2.33 o -2 7 2 28.71 31.14 2.51 o -1 7 2 213.15 206.62 3.88 o 0 7 2 11.11 11.67 0.97 o 1 7 2 211.07 212.62 3.78 o 2 7 2 0.95 1.05 0.56 o 3 7 2 28.12 30.07 1.69 o 4 7 2 0.72 1.69 0.86 o 5 7 2 86.63 89.31 2.75 o -3 8 2 76.03 79.60 2.45 o -2 8 2 0.69 1.17 0.69 o -1 8 2 8.77 10.94 1.00 o 0 8 2 8.00 7.43 0.69 o 1 8 2 55.24 62.01 2.03 o 2 8 2 2.00 1.69 0.87 o -11 0 3 19.76 23.68 2.18 o -9 0 3 6.85 3.77 1.87 o -7 0 3 276.14 315.37 5.97 o -5 0 3 3354.79 3463.03 51.85 o -3 0 3 8002.13 6954.81 98.14 o -1 0 3 5.84 10.34 0.87 o 1 0 3 347.07 393.21 3.97 o 3 0 3 1402.61 1538.79 22.57 o 5 0 3 142.10 135.80 1.89 o 7 0 3 426.76 400.52 7.45 o 9 0 3 3.15 5.62 1.28 o 11 0 3 9.84 10.37 1.86 o -12 1 3 78.10 84.60 2.55 o -11 1 3 62.64 68.00 2.65 o -10 1 3 386.56 356.01 6.27 o -9 1 3 287.45 281.82 8.86 o -8 1 3 199.51 189.08 3.78 o -7 1 3 261.98 268.42 10.55 o -6 1 3 8.42 7.11 1.26 o -5 1 3 3.46 2.69 0.27 o -4 1 3 0.18 0.95 0.21 o -3 1 3 2643.01 2672.45 24.40 o -2 1 3 582.23 587.68 3.99 o -1 1 3 6167.48 5700.46 53.76 o 0 1 3 1052.41 1184.63 8.62 o 1 1 3 165.62 195.79 1.51 o 2 1 3 220.92 273.41 2.41 o 3 1 3 153.60 151.93 1.41 o 4 1 3 31.82 31.73 0.60 o 5 1 3 175.11 176.37 1.75 o 6 1 3 62.42 68.15 1.27 o 7 1 3 231.47 204.27 3.18 o 8 1 3 6.42 6.44 0.88 o 9 1 3 439.17 408.41 8.15 o 10 1 3 7.38 7.74 0.90 o 11 1 3 54.11 57.01 2.14 o -12 2 3 89.70 96.34 2.75 o -11 2 3 62.19 67.61 2.06 o -10 2 3 19.70 22.69 1.48 o -9 2 3 17.00 17.74 1.50 o -8 2 3 210.60 193.57 3.75 o -7 2 3 461.12 453.57 6.38 o -6 2 3 4.52 7.68 0.70 o -5 2 3 1767.40 1847.65 15.34 o -4 2 3 644.10 747.16 5.90 o -3 2 3 3019.49 3166.20 26.80 o -2 2 3 347.89 279.59 2.00 o -1 2 3 20.37 17.12 0.33 o 0 2 3 3.65 5.24 0.34 o 1 2 3 2822.29 2936.35 23.80 o 2 2 3 2151.85 2306.83 18.59 o 3 2 3 549.90 620.25 4.53 o 4 2 3 729.01 770.04 6.51 o 5 2 3 490.03 457.35 5.08 o 6 2 3 35.05 37.48 1.33 o 7 2 3 671.42 634.98 8.86 o 8 2 3 117.27 112.12 2.46 o 9 2 3 4.79 5.01 0.93 o 10 2 3 116.72 120.74 2.41 o -11 3 3 61.12 68.04 2.15 o -10 3 3 356.02 341.30 6.31 o -9 3 3 45.44 65.42 7.61 o -8 3 3 322.12 303.51 8.28 o -7 3 3 263.88 260.64 5.27 o -6 3 3 74.53 83.13 1.10 o -5 3 3 845.90 845.18 6.64 o -4 3 3 157.04 142.65 1.29 o -3 3 3 0.10 1.28 0.21 o -2 3 3 222.01 262.82 1.93 o 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10.23 10.78 0.94 o -4 5 3 13.23 19.48 2.33 o -3 5 3 130.70 135.32 2.78 o -2 5 3 599.01 535.72 7.98 o -1 5 3 378.56 361.87 5.08 o 0 5 3 252.83 239.52 3.65 o 1 5 3 313.43 285.85 4.05 o 2 5 3 242.87 225.18 3.61 o 3 5 3 91.21 78.49 1.92 o 4 5 3 229.74 207.57 3.77 o 5 5 3 36.57 36.98 1.70 o 6 5 3 61.13 76.33 2.24 o 7 5 3 38.32 38.78 1.67 o 8 5 3 152.10 171.72 3.11 o -8 6 3 14.51 13.23 1.16 o -7 6 3 11.19 10.06 0.97 o -6 6 3 178.62 171.46 5.38 o -5 6 3 63.95 63.24 1.96 o -4 6 3 768.52 720.96 11.75 o -3 6 3 39.52 39.77 1.71 o -2 6 3 533.02 498.89 9.04 o -1 6 3 292.50 266.66 4.75 o 0 6 3 195.23 182.98 3.37 o 1 6 3 222.88 210.50 3.48 o 2 6 3 115.02 96.14 1.97 o 3 6 3 6.60 11.93 1.37 o 4 6 3 166.17 180.49 3.77 o 5 6 3 106.71 112.01 2.93 o 6 6 3 288.74 307.74 5.26 o 7 6 3 16.65 17.06 1.02 o -6 7 3 28.04 32.66 1.55 o -5 7 3 49.23 52.08 1.86 o -4 7 3 71.50 71.11 1.87 o -3 7 3 54.13 54.29 1.75 o -2 7 3 320.34 311.44 5.42 o -1 7 3 151.10 146.06 3.73 o 0 7 3 667.95 670.66 10.16 o 1 7 3 43.91 43.05 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