data_2239389 _cell_angle_alpha 81.875 _cell_angle_beta 88.386 _cell_angle_gamma 85.460 _cell_length_a 3.8338 _cell_length_b 12.6784 _cell_length_c 24.9180 _exptl_crystal_F_000 640.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file gg2134Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' rodolfo_2013br in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 295.55 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 4 5124.47 5516.77 103.89 o 0 0 -5 291.93 311.15 16.73 o 0 0 5 291.93 273.41 15.64 o 0 0 -5 291.93 278.46 28.96 o 0 0 -6 8824.95 8913.76 94.40 o 0 0 -6 8824.95 8965.59 166.44 o 0 0 6 8824.95 8933.58 95.18 o 0 0 -7 1050.87 1813.84 80.70 o 0 0 7 1050.87 1584.68 44.46 o 0 0 -7 1050.87 1610.31 45.16 o 0 0 8 6857.61 6940.41 95.85 o 0 0 -8 6857.61 6827.43 95.74 o 0 0 -8 6857.61 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