#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:53:24 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181894 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/94/2239402.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2239402 _cell_angle_alpha 90.000 _cell_angle_beta 108.262 _cell_angle_gamma 90.000 _cell_length_a 15.1015 _cell_length_b 5.7704 _cell_length_c 9.9549 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.7570 _cod_data_source_file hg5383Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' HR600_0ma in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 122.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10651.67 10318.32 239.35 o 3 0 0 18.68 17.47 0.38 o 4 0 0 9808.46 9408.75 183.26 o 5 0 0 4.82 6.02 0.35 o 6 0 0 3453.13 3150.44 54.40 o 7 0 0 48.52 51.07 1.23 o 8 0 0 638.64 832.95 14.04 o 9 0 0 8.92 8.23 0.53 o 10 0 0 7347.38 7173.42 129.88 o 11 0 0 18.55 18.18 0.73 o 12 0 0 2398.76 2376.17 43.16 o 13 0 0 3.92 2.55 0.65 o 14 0 0 70.29 76.08 2.95 o 15 0 0 0.05 0.43 0.85 o 16 0 0 169.81 177.66 6.23 o 17 0 0 0.07 -0.07 1.31 o 18 0 0 20.51 17.53 1.91 o 1 1 0 2.44 2.17 0.10 o 2 1 0 7503.57 7613.52 96.74 o 3 1 0 22.15 24.18 0.33 o 4 1 0 444.12 401.71 4.49 o 5 1 0 10.84 10.81 0.23 o 6 1 0 4.61 10.38 0.26 o 7 1 0 32.67 33.01 0.52 o 8 1 0 2283.00 2160.24 25.00 o 9 1 0 2.63 2.21 0.23 o 10 1 0 1931.08 1795.66 21.75 o 11 1 0 8.01 6.63 0.33 o 12 1 0 182.10 190.51 2.63 o 13 1 0 0.00 -0.56 0.37 o 14 1 0 611.32 587.24 10.89 o 15 1 0 0.06 -0.01 0.59 o 16 1 0 25.91 19.68 1.24 o 17 1 0 6.43 5.25 0.96 o 18 1 0 109.38 125.08 4.83 o 0 2 0 266.43 281.49 11.28 o 1 2 0 14.29 15.92 0.36 o 2 2 0 695.66 728.25 9.97 o 3 2 0 55.05 56.45 0.80 o 4 2 0 4254.37 4817.65 57.67 o 5 2 0 6.81 7.05 0.21 o 6 2 0 1177.67 1412.80 16.86 o 7 2 0 17.34 17.89 0.38 o 8 2 0 0.21 0.08 0.17 o 9 2 0 0.56 0.33 0.19 o 10 2 0 149.83 112.21 1.57 o 11 2 0 2.90 1.87 0.29 o 12 2 0 425.53 391.85 6.44 o 13 2 0 2.88 1.87 0.51 o 14 2 0 140.50 143.75 3.25 o 15 2 0 5.65 5.01 0.79 o 16 2 0 15.28 11.94 1.19 o 17 2 0 3.15 1.36 1.03 o 18 2 0 1.31 1.99 1.10 o 1 3 0 7.38 7.69 0.39 o 2 3 0 973.31 926.79 13.95 o 3 3 0 7.39 6.92 0.23 o 4 3 0 873.35 889.25 12.65 o 5 3 0 0.88 0.42 0.15 o 6 3 0 9.93 14.77 0.38 o 7 3 0 17.11 18.47 0.45 o 8 3 0 603.57 606.80 8.01 o 9 3 0 0.98 0.64 0.28 o 10 3 0 530.74 575.27 8.44 o 11 3 0 0.76 0.74 0.38 o 12 3 0 124.23 132.26 2.70 o 13 3 0 2.76 1.72 0.61 o 14 3 0 625.22 656.55 14.61 o 15 3 0 0.10 -0.60 0.81 o 16 3 0 35.90 32.12 2.05 o 17 3 0 0.00 0.64 1.46 o 0 4 0 3126.62 2962.02 127.82 o 1 4 0 10.29 13.36 2.67 o 2 4 0 44.89 53.92 1.34 o 3 4 0 2.41 2.18 0.21 o 4 4 0 3132.47 2907.65 47.55 o 5 4 0 48.75 50.76 0.95 o 6 4 0 3039.03 3014.11 44.14 o 7 4 0 0.15 0.69 0.26 o 8 4 0 337.26 388.19 5.81 o 9 4 0 15.46 13.05 0.57 o 10 4 0 546.17 546.80 8.81 o 11 4 0 0.24 0.74 0.48 o 12 4 0 417.66 414.21 9.24 o 13 4 0 3.79 3.06 0.81 o 14 4 0 123.60 114.94 4.12 o 15 4 0 0.22 -0.17 1.14 o 16 4 0 355.49 383.86 14.09 o 1 5 0 10.67 10.76 0.86 o 2 5 0 1353.40 1409.20 36.34 o 3 5 0 11.83 12.84 0.67 o 4 5 0 328.05 336.03 7.48 o 5 5 0 0.92 0.22 0.26 o 6 5 0 23.37 19.87 0.64 o 7 5 0 3.82 3.87 0.39 o 8 5 0 412.48 433.86 7.83 o 9 5 0 0.04 0.19 0.39 o 10 5 0 257.96 252.35 5.26 o 11 5 0 0.53 0.30 0.56 o 12 5 0 77.86 77.22 2.55 o 13 5 0 0.27 0.51 0.91 o 14 5 0 172.74 169.60 7.46 o 0 6 0 0.04 0.32 3.00 o 1 6 0 14.69 14.78 1.38 o 2 6 0 17.94 19.83 1.15 o 3 6 0 0.45 1.00 0.46 o 4 6 0 3.11 2.85 0.60 o 5 6 0 16.03 15.07 0.72 o 6 6 0 30.57 31.83 1.17 o 7 6 0 1.96 2.04 0.49 o 8 6 0 226.62 222.31 5.09 o 9 6 0 6.78 5.75 0.83 o 10 6 0 2.22 1.81 0.80 o 11 6 0 4.31 3.76 1.36 o 1 7 0 0.81 0.48 0.92 o 2 7 0 6.12 7.59 2.53 o 3 7 0 3.92 3.87 1.22 o 4 7 0 29.69 29.04 2.78 o 5 7 0 6.67 5.69 1.09 o 6 7 0 1.85 1.36 1.06 o 7 7 0 4.91 7.07 1.71 o -19 1 1 0.82 -0.85 1.09 o -18 1 1 51.72 55.93 2.39 o -17 1 1 24.44 25.51 1.51 o -16 1 1 14.67 11.44 0.96 o -15 1 1 1.46 1.27 0.53 o -14 1 1 300.52 303.28 5.45 o -13 1 1 3.36 1.71 0.40 o -12 1 1 282.42 299.55 3.59 o -11 1 1 155.74 169.52 2.24 o -10 1 1 347.91 370.41 4.17 o -9 1 1 735.52 757.84 8.34 o -8 1 1 4301.38 4344.89 50.45 o -7 1 1 236.40 248.01 2.72 o -6 1 1 199.25 237.95 2.69 o -5 1 1 2279.90 2226.19 25.80 o -4 1 1 9534.93 9393.26 102.41 o -3 1 1 381.21 375.46 3.87 o -2 1 1 5474.90 5440.68 57.15 o -1 1 1 2767.70 2810.51 32.91 o 0 1 1 581.93 598.25 7.29 o 1 1 1 1598.83 1554.61 19.09 o 2 1 1 11045.22 10987.98 136.27 o 3 1 1 488.60 477.76 5.54 o 4 1 1 2934.43 2757.88 32.06 o 5 1 1 2015.36 2020.05 22.26 o 6 1 1 2687.84 2870.06 33.65 o 7 1 1 145.99 169.58 2.01 o 8 1 1 2131.44 2234.00 27.09 o 9 1 1 631.81 665.28 8.11 o 10 1 1 0.11 -0.36 0.24 o 11 1 1 24.57 26.28 0.64 o 12 1 1 293.82 313.65 5.29 o 13 1 1 10.23 10.36 0.71 o 14 1 1 262.36 264.33 6.69 o 15 1 1 15.14 15.66 1.06 o 16 1 1 0.41 1.54 0.81 o 17 1 1 2.93 2.58 0.98 o 18 1 1 117.00 124.74 4.42 o -18 2 1 260.38 256.52 7.65 o -17 2 1 8.46 5.96 1.08 o -16 2 1 301.23 323.36 7.81 o -15 2 1 326.13 340.82 7.38 o -14 2 1 133.08 120.00 2.79 o -13 2 1 7.84 8.19 0.61 o -12 2 1 1303.46 1336.33 18.79 o -11 2 1 164.21 167.32 2.29 o -10 2 1 876.17 882.13 10.59 o -9 2 1 396.55 394.01 4.71 o -8 2 1 509.37 500.02 6.06 o -7 2 1 34.38 35.35 0.58 o -6 2 1 4728.21 4738.64 55.81 o -5 2 1 947.84 973.58 11.08 o -4 2 1 34.42 16.63 0.28 o -3 2 1 13.24 24.86 0.41 o -2 2 1 4302.97 4301.27 57.31 o -1 2 1 223.41 247.71 3.54 o 0 2 1 4672.89 4574.47 71.42 o 1 2 1 768.97 875.62 11.98 o 2 2 1 1593.48 1714.10 23.84 o 3 2 1 390.25 374.94 4.70 o 4 2 1 2848.57 2771.57 35.81 o 5 2 1 305.05 339.17 4.09 o 6 2 1 2912.46 2809.82 34.07 o 7 2 1 311.12 300.25 3.68 o 8 2 1 234.38 236.14 2.91 o 9 2 1 473.78 461.99 5.56 o 10 2 1 1399.96 1445.18 18.82 o 11 2 1 52.15 52.87 1.13 o 12 2 1 674.12 633.59 11.75 o 13 2 1 207.89 219.03 4.53 o 14 2 1 6.76 8.76 0.82 o 15 2 1 168.13 173.43 4.46 o 16 2 1 435.48 463.25 12.76 o 17 2 1 35.63 42.84 2.36 o -17 3 1 109.55 114.08 4.36 o -16 3 1 136.91 153.57 5.24 o -15 3 1 3.44 2.24 0.85 o -14 3 1 227.65 235.22 5.52 o -13 3 1 171.53 184.80 3.94 o -12 3 1 10.38 12.95 0.69 o -11 3 1 392.13 383.14 6.07 o -10 3 1 480.92 484.51 6.81 o -9 3 1 218.88 204.91 2.87 o -8 3 1 958.21 859.82 11.28 o -7 3 1 484.77 457.35 5.78 o -6 3 1 0.13 1.00 0.17 o -5 3 1 450.94 397.57 5.41 o -4 3 1 1537.60 1478.56 20.87 o -3 3 1 779.54 841.69 12.68 o -2 3 1 353.16 332.77 5.08 o -1 3 1 1044.47 981.58 17.37 o 0 3 1 10.00 8.87 0.70 o 1 3 1 1061.86 1007.97 16.10 o 2 3 1 1388.03 1339.04 20.53 o 3 3 1 13.60 25.47 0.50 o 4 3 1 1256.08 1232.43 17.30 o 5 3 1 823.53 766.95 10.45 o 6 3 1 556.48 503.05 6.91 o 7 3 1 10.18 10.58 0.39 o 8 3 1 1178.68 1090.85 14.68 o 9 3 1 239.18 211.67 3.14 o 10 3 1 83.51 90.05 1.65 o 11 3 1 252.62 254.11 4.55 o 12 3 1 83.08 80.63 2.01 o 13 3 1 48.67 51.05 1.71 o 14 3 1 306.40 310.15 7.38 o 15 3 1 59.91 68.65 2.98 o 16 3 1 2.56 0.08 1.19 o -16 4 1 0.42 0.51 1.24 o -15 4 1 0.24 1.13 1.07 o -14 4 1 43.56 40.51 2.07 o -13 4 1 2.30 1.93 0.71 o -12 4 1 13.34 12.09 0.82 o -11 4 1 33.81 28.47 0.96 o -10 4 1 1.77 0.11 0.36 o -9 4 1 75.00 71.85 1.48 o -8 4 1 11.70 11.53 0.44 o -7 4 1 502.43 489.37 7.05 o -6 4 1 11.36 7.33 0.35 o -5 4 1 20.68 24.62 0.57 o -4 4 1 77.94 77.01 1.34 o -3 4 1 550.17 582.19 9.98 o -2 4 1 291.00 280.25 5.28 o -1 4 1 137.29 134.71 2.85 o 0 4 1 23.12 22.89 0.82 o 1 4 1 174.56 184.48 4.20 o 2 4 1 86.27 81.11 1.63 o 3 4 1 524.32 542.70 8.72 o 4 4 1 11.47 10.23 0.41 o 5 4 1 111.39 109.69 1.77 o 6 4 1 8.05 12.10 0.43 o 7 4 1 324.32 298.82 4.55 o 8 4 1 53.31 48.87 1.18 o 9 4 1 1.83 1.62 0.40 o 10 4 1 2.33 1.36 0.44 o 11 4 1 0.02 -0.08 0.48 o 12 4 1 31.63 31.15 1.42 o 13 4 1 0.57 -0.72 0.76 o 14 4 1 31.40 29.33 1.86 o 15 4 1 0.00 -0.01 1.31 o -14 5 1 54.98 59.15 3.06 o -13 5 1 10.77 8.72 1.23 o -12 5 1 113.16 117.28 3.34 o -11 5 1 12.68 15.20 0.89 o -10 5 1 26.69 28.43 1.01 o -9 5 1 0.22 0.22 0.42 o -8 5 1 240.94 251.01 4.48 o -7 5 1 130.18 140.04 2.55 o -6 5 1 3.54 1.88 0.29 o -5 5 1 300.26 286.44 4.91 o -4 5 1 241.56 247.20 4.74 o -3 5 1 12.75 13.05 0.62 o -2 5 1 560.61 547.41 13.47 o -1 5 1 134.19 131.04 5.75 o 0 5 1 1.10 2.01 0.48 o 1 5 1 16.03 16.50 0.65 o 2 5 1 634.85 638.41 13.47 o 3 5 1 288.19 281.68 6.08 o 4 5 1 151.38 147.80 3.09 o 5 5 1 172.67 177.14 3.22 o 6 5 1 98.84 91.28 1.87 o 7 5 1 1.66 2.60 0.40 o 8 5 1 248.14 256.72 4.69 o 9 5 1 81.09 88.22 1.98 o 10 5 1 1.15 0.65 0.50 o 11 5 1 1.53 0.32 0.58 o 12 5 1 118.21 109.62 3.58 o 13 5 1 69.38 67.72 3.59 o -12 6 1 93.86 91.22 5.02 o -11 6 1 0.69 0.33 1.17 o -10 6 1 76.85 81.46 2.80 o -9 6 1 71.70 71.52 2.39 o -8 6 1 168.06 176.14 4.06 o -7 6 1 47.95 45.36 1.40 o -6 6 1 550.19 551.38 12.11 o -5 6 1 53.21 55.49 1.63 o -4 6 1 56.08 53.35 1.60 o -3 6 1 230.90 215.49 6.25 o -2 6 1 92.12 98.70 3.50 o -1 6 1 3.89 2.96 1.00 o 0 6 1 202.94 208.56 9.01 o 1 6 1 146.05 141.75 4.62 o 2 6 1 0.17 0.53 0.46 o 3 6 1 162.82 148.64 4.18 o 4 6 1 339.63 341.17 9.01 o 5 6 1 2.25 3.77 0.52 o 6 6 1 321.63 329.34 7.43 o 7 6 1 137.01 135.76 3.12 o 8 6 1 10.64 10.68 0.94 o 9 6 1 22.03 19.23 1.22 o 10 6 1 55.12 55.25 2.74 o 11 6 1 37.99 45.32 3.80 o -7 7 1 165.86 162.94 8.24 o -6 7 1 24.71 26.03 2.19 o -5 7 1 129.63 135.56 5.95 o -4 7 1 171.19 171.89 7.94 o -3 7 1 0.34 0.54 1.23 o -2 7 1 53.38 53.56 4.49 o -1 7 1 30.13 32.11 2.41 o 0 7 1 2.71 1.50 0.93 o 1 7 1 15.49 18.57 3.03 o 2 7 1 138.95 139.68 6.64 o 3 7 1 8.04 7.70 1.53 o 4 7 1 96.38 96.54 4.99 o 5 7 1 186.47 187.40 7.55 o 6 7 1 23.87 24.58 2.54 o -19 0 2 58.30 64.95 3.97 o -18 0 2 152.17 155.20 6.66 o -17 0 2 5.67 4.81 1.09 o -16 0 2 110.38 122.14 4.56 o -15 0 2 261.17 259.02 7.10 o -14 0 2 51.46 50.96 1.74 o -13 0 2 553.75 571.12 11.87 o -12 0 2 250.48 254.12 4.54 o -11 0 2 535.08 488.67 8.59 o -10 0 2 0.67 0.49 0.30 o -9 0 2 2422.80 2419.60 40.11 o -8 0 2 1167.24 1187.17 21.74 o -7 0 2 913.20 919.96 15.35 o -6 0 2 1929.55 2002.24 34.95 o -5 0 2 84.90 72.84 1.34 o -4 0 2 28.33 36.47 0.68 o -3 0 2 14732.47 14930.31 284.00 o -2 0 2 639.94 603.87 10.58 o -1 0 2 60.21 64.23 1.12 o 0 0 2 938.86 937.57 16.40 o 1 0 2 15074.13 15682.09 280.31 o 2 0 2 5.18 6.57 0.23 o 3 0 2 94.49 74.19 1.32 o 4 0 2 1083.07 1141.53 18.20 o 5 0 2 839.86 833.29 13.50 o 6 0 2 1268.35 1344.41 21.84 o 7 0 2 2250.52 2113.75 33.19 o 8 0 2 17.65 15.44 0.68 o 9 0 2 891.18 852.23 14.78 o 10 0 2 739.69 741.19 12.41 o 11 0 2 389.31 386.12 8.96 o 12 0 2 210.45 216.38 6.11 o 13 0 2 360.10 355.28 11.20 o 14 0 2 113.04 135.17 5.53 o 15 0 2 0.33 -0.77 0.98 o 16 0 2 144.35 137.66 6.30 o 17 0 2 77.24 88.66 4.79 o -19 1 2 38.54 40.03 2.14 o -18 1 2 0.49 0.63 0.90 o -17 1 2 52.46 57.69 2.08 o -16 1 2 42.84 43.38 1.63 o -15 1 2 30.94 26.04 1.06 o -14 1 2 73.04 72.95 1.67 o -13 1 2 1486.62 1437.80 20.46 o -12 1 2 6.23 5.78 0.34 o -11 1 2 1375.62 1306.65 15.72 o -10 1 2 218.04 219.25 2.55 o -9 1 2 4.65 0.66 0.19 o -8 1 2 731.74 725.15 8.19 o -7 1 2 106.09 154.15 1.74 o -6 1 2 124.66 111.68 1.25 o -5 1 2 878.66 1023.33 11.25 o -4 1 2 2403.46 2248.24 25.74 o -3 1 2 1784.06 1867.26 20.64 o -2 1 2 973.07 922.33 10.31 o -1 1 2 13907.88 14166.82 171.25 o 0 1 2 1366.09 1293.51 13.72 o 1 1 2 2126.28 2133.88 25.11 o 2 1 2 2622.31 2568.19 29.51 o 3 1 2 648.90 769.63 8.95 o 4 1 2 3.44 1.70 0.14 o 5 1 2 193.68 267.31 3.05 o 6 1 2 733.71 763.40 8.66 o 7 1 2 2.46 0.50 0.17 o 8 1 2 263.96 252.08 3.08 o 9 1 2 1280.12 1223.22 14.63 o 10 1 2 4.61 4.24 0.33 o 11 1 2 1594.71 1548.95 23.06 o 12 1 2 125.31 126.35 2.81 o 13 1 2 51.14 44.62 1.65 o 14 1 2 9.42 7.60 0.92 o 15 1 2 35.62 37.54 1.85 o 16 1 2 3.49 2.47 0.91 o 17 1 2 35.50 35.14 2.07 o -19 2 2 15.11 14.92 1.51 o -18 2 2 4.84 3.49 1.11 o -17 2 2 0.59 -1.15 0.83 o -16 2 2 3.01 1.43 0.71 o -15 2 2 17.31 14.02 0.94 o -14 2 2 1.51 0.30 0.49 o -13 2 2 2.21 -0.41 0.40 o -12 2 2 65.86 61.54 1.16 o -11 2 2 209.89 197.36 2.58 o -10 2 2 39.56 39.14 0.72 o -9 2 2 176.88 159.95 2.06 o -8 2 2 17.24 14.52 0.34 o -7 2 2 39.74 43.76 0.65 o -6 2 2 5.03 3.94 0.20 o -5 2 2 8.71 2.91 0.15 o -4 2 2 34.20 36.12 0.49 o -3 2 2 153.63 164.99 1.86 o -2 2 2 240.03 230.09 2.68 o -1 2 2 34.90 33.73 0.47 o 0 2 2 49.86 47.43 0.66 o 1 2 2 131.91 140.53 1.77 o 2 2 2 101.90 104.70 1.24 o 3 2 2 34.38 29.00 0.45 o 4 2 2 31.82 35.16 0.54 o 5 2 2 29.12 35.83 0.58 o 6 2 2 20.47 28.32 0.51 o 7 2 2 229.75 205.46 2.67 o 8 2 2 1.14 -0.11 0.22 o 9 2 2 256.09 244.71 3.06 o 10 2 2 16.69 20.25 0.60 o 11 2 2 2.94 0.72 0.42 o 12 2 2 7.60 7.09 0.68 o 13 2 2 9.16 5.06 0.68 o 14 2 2 0.44 -0.69 0.70 o 15 2 2 0.09 -0.28 0.81 o 16 2 2 4.42 2.61 1.06 o 17 2 2 8.25 6.21 1.25 o -18 3 2 11.73 8.84 1.54 o -17 3 2 193.94 209.67 6.29 o -16 3 2 0.01 0.65 0.89 o -15 3 2 8.91 8.95 0.99 o -14 3 2 61.56 62.54 2.08 o -13 3 2 91.81 107.41 2.49 o -12 3 2 48.38 48.06 1.27 o -11 3 2 54.43 39.79 0.99 o -10 3 2 75.29 86.18 1.47 o -9 3 2 855.04 875.62 12.37 o -8 3 2 691.88 677.77 9.09 o -7 3 2 454.65 483.27 6.16 o -6 3 2 57.69 44.98 0.73 o -5 3 2 179.01 172.24 2.26 o -4 3 2 1786.55 1843.86 23.42 o -3 3 2 324.01 360.21 4.81 o -2 3 2 792.54 842.78 11.80 o -1 3 2 756.90 910.93 12.63 o 0 3 2 781.36 821.21 11.84 o 1 3 2 388.97 443.84 6.87 o 2 3 2 1564.66 1636.89 22.92 o 3 3 2 288.11 290.58 4.10 o 4 3 2 4.24 10.12 0.32 o 5 3 2 500.41 490.11 6.49 o 6 3 2 635.28 653.54 8.45 o 7 3 2 707.56 744.17 10.22 o 8 3 2 173.11 188.16 2.69 o 9 3 2 48.31 40.47 0.97 o 10 3 2 64.05 57.81 1.42 o 11 3 2 59.58 67.47 1.92 o 12 3 2 69.72 70.10 2.22 o 13 3 2 17.55 18.07 1.22 o 14 3 2 1.10 0.60 0.98 o 15 3 2 198.89 208.69 6.57 o 16 3 2 1.64 0.32 1.20 o -16 4 2 1.28 -0.79 1.11 o -15 4 2 308.21 313.45 9.35 o -14 4 2 70.46 75.67 3.10 o -13 4 2 277.61 273.44 6.60 o -12 4 2 109.03 112.40 2.66 o -11 4 2 192.72 220.55 4.12 o -10 4 2 10.03 9.19 0.56 o -9 4 2 778.11 777.89 12.59 o -8 4 2 19.18 22.24 0.63 o -7 4 2 162.27 145.13 2.22 o -6 4 2 87.26 81.61 1.32 o -5 4 2 526.39 540.81 7.86 o -4 4 2 0.05 1.08 0.22 o -3 4 2 2306.74 2152.35 33.72 o -2 4 2 252.13 250.28 3.95 o -1 4 2 10.92 8.96 0.30 o 0 4 2 267.00 290.84 4.71 o 1 4 2 2439.89 2396.41 41.13 o 2 4 2 51.72 56.14 1.37 o 3 4 2 819.37 825.99 13.32 o 4 4 2 96.97 98.12 1.62 o 5 4 2 143.31 126.81 2.09 o 6 4 2 197.42 198.81 3.15 o 7 4 2 869.18 869.66 13.36 o 8 4 2 3.85 3.65 0.44 o 9 4 2 217.18 233.73 4.31 o 10 4 2 200.19 204.89 4.27 o 11 4 2 308.50 299.94 6.69 o 12 4 2 65.14 65.26 2.50 o 13 4 2 366.37 403.32 10.94 o 14 4 2 7.29 5.64 1.32 o -14 5 2 14.25 15.60 1.68 o -13 5 2 153.17 155.01 4.51 o -12 5 2 40.72 41.72 1.59 o -11 5 2 303.62 306.12 6.42 o -10 5 2 107.09 111.67 2.33 o -9 5 2 102.74 115.98 2.38 o -8 5 2 0.10 0.83 0.38 o -7 5 2 1045.69 1001.62 17.82 o -6 5 2 87.55 90.79 1.74 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