data_2239435 _cell_angle_alpha 102.718 _cell_angle_beta 105.175 _cell_angle_gamma 101.092 _cell_length_a 5.0784 _cell_length_b 8.1255 _cell_length_c 8.9003 _exptl_crystal_F_000 179.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file is5335Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' CellFormulaUnitsZ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 86.86 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 426.13 432.06 7.59 o 2 0 0 526.47 599.52 16.91 o 3 0 0 135.67 110.89 5.72 o 4 0 0 0.60 0.83 0.16 o 5 0 0 126.91 130.72 2.97 o 6 0 0 5.85 5.00 1.17 o -6 1 0 223.89 253.41 11.15 o -5 1 0 0.48 0.32 0.17 o -4 1 0 333.97 322.89 7.69 o -3 1 0 253.80 243.10 6.12 o -2 1 0 130.80 111.42 2.06 o -1 1 0 816.91 792.05 23.46 o 1 1 0 2055.94 2222.34 66.31 o 2 1 0 1070.48 1125.28 22.74 o 3 1 0 63.63 69.35 3.31 o 4 1 0 382.35 331.25 6.19 o 5 1 0 22.64 20.57 1.75 o -6 2 0 7.90 6.58 1.13 o -5 2 0 188.03 190.78 3.63 o -4 2 0 128.72 128.28 2.16 o -3 2 0 10.30 9.75 0.41 o -2 2 0 1761.13 1853.40 58.18 o -1 2 0 515.93 514.38 14.72 o 0 2 0 3.21 3.32 0.25 o 1 2 0 3034.20 3353.28 119.23 o 2 2 0 134.07 131.39 5.51 o 3 2 0 314.76 289.67 13.29 o 4 2 0 5.62 5.15 0.84 o 5 2 0 10.62 9.65 1.43 o -6 3 0 214.20 224.09 4.61 o -5 3 0 83.87 78.49 1.63 o -4 3 0 187.38 186.08 4.77 o -3 3 0 860.54 872.31 24.73 o -2 3 0 332.52 356.77 10.57 o -1 3 0 129.83 102.90 7.19 o 0 3 0 1321.31 1447.95 42.16 o 1 3 0 254.55 293.02 9.90 o 2 3 0 617.25 639.04 11.19 o 3 3 0 51.47 36.98 6.16 o 4 3 0 14.16 12.73 1.27 o 5 3 0 498.29 534.87 22.36 o -6 4 0 24.29 27.51 1.19 o -5 4 0 48.17 49.94 1.30 o -4 4 0 1009.87 996.50 22.74 o -3 4 0 18.13 20.97 1.54 o -2 4 0 7.53 12.84 0.80 o -1 4 0 2051.44 2244.36 109.75 o 0 4 0 0.94 0.75 0.13 o 1 4 0 313.87 313.89 4.94 o 2 4 0 352.03 339.55 7.78 o 3 4 0 76.01 55.94 14.71 o 4 4 0 126.74 132.23 5.30 o -6 5 0 0.60 0.55 0.39 o -5 5 0 435.86 456.43 9.18 o -4 5 0 38.23 42.49 3.67 o -3 5 0 12.49 12.82 1.03 o -2 5 0 363.62 368.95 11.38 o -1 5 0 51.22 55.24 1.11 o 0 5 0 895.88 1021.59 21.64 o 1 5 0 173.70 168.54 2.67 o 2 5 0 8.53 7.57 0.92 o 3 5 0 503.05 517.74 19.34 o 4 5 0 12.95 15.14 1.71 o -5 6 0 28.21 32.03 1.56 o -4 6 0 11.62 13.82 1.10 o -3 6 0 335.18 347.85 11.72 o -2 6 0 16.65 16.39 1.13 o -1 6 0 422.01 423.94 8.72 o 0 6 0 329.66 355.26 7.83 o 1 6 0 5.56 7.98 0.51 o 2 6 0 454.03 439.33 29.99 o 3 6 0 0.39 0.61 0.56 o 4 6 0 9.30 8.53 2.01 o -5 7 0 4.63 4.33 0.79 o -4 7 0 817.03 767.24 22.23 o -3 7 0 89.83 85.05 3.56 o -2 7 0 1.20 1.06 0.53 o -1 7 0 30.65 27.85 1.26 o 0 7 0 34.25 32.21 1.88 o 1 7 0 1022.82 993.74 27.90 o 2 7 0 5.29 4.13 0.91 o 3 7 0 33.16 43.05 2.86 o -5 8 0 188.35 185.60 10.97 o -4 8 0 3.46 4.48 0.82 o -3 8 0 207.55 209.16 7.99 o -2 8 0 242.26 235.47 8.24 o -1 8 0 7.17 6.43 0.77 o 0 8 0 250.62 270.24 6.06 o 1 8 0 13.08 13.71 0.75 o 2 8 0 32.88 33.46 2.25 o -4 9 0 39.69 43.40 2.24 o -3 9 0 178.92 185.57 7.66 o -2 9 0 28.08 27.40 2.00 o -1 9 0 363.86 341.91 30.52 o 0 9 0 0.32 0.54 0.31 o 1 9 0 2.33 1.06 0.42 o -3 10 0 7.38 9.31 1.62 o -2 10 0 212.93 226.29 10.60 o -1 10 0 0.58 2.17 1.15 o 0 -10 1 72.83 72.69 2.53 o 1 -10 1 1.92 2.38 0.60 o 2 -10 1 162.78 166.92 10.53 o 3 -10 1 20.31 16.36 1.60 o -1 -9 1 188.06 188.12 3.87 o 0 -9 1 1.71 1.23 0.35 o 1 -9 1 191.65 186.56 11.75 o 2 -9 1 213.84 235.33 10.50 o 3 -9 1 0.70 1.35 0.57 o 4 -9 1 157.48 157.09 15.96 o -2 -8 1 255.87 268.43 9.79 o -1 -8 1 14.65 17.00 0.98 o 0 -8 1 228.28 238.74 5.70 o 1 -8 1 178.99 183.35 3.57 o 2 -8 1 25.20 23.96 1.74 o 3 -8 1 245.08 271.87 7.63 o 4 -8 1 19.74 22.55 2.57 o 5 -8 1 30.81 33.33 2.02 o -3 -7 1 111.09 108.75 4.79 o -2 -7 1 0.94 0.81 0.19 o -1 -7 1 750.30 763.98 20.04 o 0 -7 1 563.69 608.17 14.58 o 1 -7 1 299.06 295.59 5.78 o 2 -7 1 136.81 149.69 5.23 o 3 -7 1 135.34 136.62 3.71 o 4 -7 1 45.89 47.69 1.98 o 5 -7 1 151.65 167.35 6.30 o -4 -6 1 80.55 73.70 4.01 o -3 -6 1 24.46 27.90 1.93 o -2 -6 1 29.40 29.74 1.51 o -1 -6 1 326.17 359.59 11.17 o 0 -6 1 82.06 95.67 4.58 o 1 -6 1 1670.06 1861.71 82.17 o 2 -6 1 86.15 92.55 3.27 o 3 -6 1 16.82 14.69 1.21 o 4 -6 1 169.24 159.91 8.61 o 5 -6 1 9.22 10.75 1.00 o -4 -5 1 1.35 1.76 0.82 o -3 -5 1 61.26 68.90 3.12 o -2 -5 1 199.67 195.17 3.73 o -1 -5 1 72.12 76.28 1.72 o 0 -5 1 1329.07 1593.19 46.55 o 1 -5 1 718.50 831.09 40.71 o 2 -5 1 21.20 23.24 1.21 o 3 -5 1 255.86 237.84 13.50 o 4 -5 1 3.81 3.74 0.21 o 5 -5 1 190.51 194.89 8.98 o 6 -5 1 55.56 58.40 2.46 o -5 -4 1 1.28 1.05 0.79 o -4 -4 1 119.37 118.18 4.87 o -3 -4 1 705.94 643.95 23.90 o -2 -4 1 53.01 42.51 0.71 o -1 -4 1 296.26 304.97 7.05 o 0 -4 1 438.42 510.40 20.86 o 1 -4 1 57.49 56.07 1.70 o 2 -4 1 433.10 396.25 22.01 o 3 -4 1 2.42 1.89 0.15 o 4 -4 1 567.61 573.21 21.21 o 5 -4 1 193.17 203.16 4.11 o 6 -4 1 38.19 44.25 2.17 o -5 -3 1 112.80 119.79 5.38 o -4 -3 1 118.80 124.48 5.57 o -3 -3 1 346.34 347.58 11.30 o -2 -3 1 779.33 850.66 30.17 o -1 -3 1 1145.83 1378.53 87.24 o 0 -3 1 48.07 45.26 1.42 o 1 -3 1 1998.48 2020.11 81.46 o 2 -3 1 117.27 109.18 2.90 o 3 -3 1 54.52 55.26 1.12 o 4 -3 1 2.34 3.70 0.48 o 5 -3 1 4.49 4.12 0.40 o 6 -3 1 444.75 486.43 15.75 o -5 -2 1 205.31 201.17 7.85 o -4 -2 1 29.83 30.93 1.78 o -3 -2 1 364.25 313.40 9.54 o -2 -2 1 372.54 361.29 10.36 o -1 -2 1 2.56 2.57 0.23 o 0 -2 1 3165.18 3928.34 121.13 o 1 -2 1 172.12 188.97 4.65 o 2 -2 1 731.97 727.87 23.84 o 3 -2 1 312.16 280.51 7.83 o 4 -2 1 99.34 95.85 2.14 o 5 -2 1 225.20 235.04 7.79 o 6 -2 1 32.59 34.55 1.07 o -6 -1 1 181.59 184.06 8.09 o -5 -1 1 1.12 1.18 0.84 o -4 -1 1 337.91 297.67 4.31 o -3 -1 1 268.33 253.27 10.81 o -2 -1 1 82.64 80.61 1.47 o -1 -1 1 563.86 586.13 13.91 o 0 -1 1 4.39 3.79 0.14 o 1 -1 1 2986.21 3486.99 128.05 o 2 -1 1 1753.92 2076.14 65.41 o 3 -1 1 51.27 50.97 1.41 o 4 -1 1 309.11 270.59 5.66 o 5 -1 1 14.03 14.16 0.65 o 6 -1 1 2.78 2.46 0.93 o -6 0 1 9.99 9.75 1.39 o -5 0 1 266.64 266.72 6.48 o -4 0 1 466.56 443.24 11.32 o -3 0 1 223.61 233.12 3.61 o -2 0 1 73.36 57.07 1.75 o -1 0 1 283.66 309.36 3.67 o 1 0 1 1719.79 1821.30 52.84 o 2 0 1 133.92 158.30 2.59 o 3 0 1 897.42 954.62 24.03 o 4 0 1 19.90 22.73 0.73 o 5 0 1 32.69 32.41 0.94 o -6 1 1 69.46 76.34 4.30 o -5 1 1 349.00 340.75 10.74 o -4 1 1 39.14 34.63 0.73 o -3 1 1 1157.97 1197.43 31.62 o -2 1 1 0.40 0.47 0.09 o -1 1 1 11.26 12.08 0.35 o 0 1 1 283.28 306.12 8.22 o 1 1 1 39.47 41.96 2.77 o 2 1 1 1717.77 1846.68 55.49 o 3 1 1 363.11 351.29 6.97 o 4 1 1 2.18 1.15 0.24 o 5 1 1 165.86 162.09 6.42 o -6 2 1 54.90 54.44 2.45 o -5 2 1 7.17 7.03 0.41 o -4 2 1 806.60 780.67 15.76 o -3 2 1 282.23 271.15 5.23 o -2 2 1 75.64 65.38 2.55 o -1 2 1 688.16 709.03 32.57 o 0 2 1 136.64 147.34 2.43 o 1 2 1 1624.61 1766.80 59.34 o 2 2 1 429.25 408.73 7.96 o 3 2 1 0.51 1.01 0.48 o 4 2 1 285.76 271.68 5.62 o 5 2 1 2.77 2.73 1.20 o -6 3 1 1.68 1.25 0.29 o -5 3 1 41.11 42.72 1.02 o -4 3 1 1.36 3.12 0.28 o -3 3 1 470.81 475.35 9.86 o -2 3 1 1117.88 1118.51 23.15 o -1 3 1 281.46 318.12 6.81 o 0 3 1 2401.39 2842.77 99.17 o 1 3 1 1333.50 1527.26 43.48 o 2 3 1 110.45 97.16 1.67 o 3 3 1 97.19 95.07 1.58 o 4 3 1 5.64 5.91 0.23 o 5 3 1 96.58 100.21 5.09 o -6 4 1 169.48 179.82 3.77 o -5 4 1 222.40 231.03 9.04 o -4 4 1 123.30 122.71 2.39 o -3 4 1 387.39 384.31 11.93 o -2 4 1 92.74 94.40 1.99 o -1 4 1 257.39 247.28 6.67 o 0 4 1 98.05 82.26 1.61 o 1 4 1 16.48 17.27 0.62 o 2 4 1 1620.98 1628.93 48.87 o 3 4 1 48.87 43.86 1.09 o 4 4 1 0.39 0.43 0.55 o -6 5 1 39.77 45.97 4.02 o -5 5 1 53.95 53.20 1.83 o -4 5 1 437.48 441.66 15.34 o -3 5 1 3.54 2.68 0.60 o -2 5 1 494.24 396.63 95.12 o -1 5 1 182.53 184.01 6.25 o 0 5 1 177.30 186.90 5.78 o 1 5 1 530.34 537.21 12.57 o 2 5 1 173.82 159.97 2.77 o 3 5 1 165.02 151.37 2.41 o 4 5 1 90.33 92.64 4.52 o -6 6 1 3.63 4.51 0.87 o -5 6 1 212.25 211.51 5.73 o -4 6 1 0.50 0.53 0.52 o -3 6 1 363.82 368.59 12.60 o -2 6 1 776.55 753.59 27.68 o -1 6 1 0.74 1.23 0.24 o 0 6 1 160.53 173.51 3.08 o 1 6 1 8.76 7.21 0.42 o 2 6 1 67.82 62.89 1.43 o 3 6 1 231.91 235.80 9.21 o -5 7 1 0.36 12.65 7.86 o -4 7 1 483.00 453.25 17.25 o -3 7 1 330.54 306.19 10.82 o -2 7 1 188.38 188.36 7.16 o -1 7 1 313.67 294.20 23.33 o 0 7 1 171.21 158.00 3.38 o 1 7 1 20.55 17.67 0.75 o 2 7 1 124.67 126.94 6.21 o 3 7 1 6.99 7.14 1.30 o -5 8 1 21.77 26.83 2.05 o -4 8 1 150.65 158.77 6.64 o -3 8 1 2.73 2.59 0.85 o -2 8 1 366.92 375.26 13.79 o -1 8 1 36.69 31.42 2.68 o 0 8 1 26.85 25.88 2.63 o 1 8 1 200.39 188.80 4.56 o 2 8 1 13.96 13.68 1.93 o -4 9 1 4.69 3.90 1.19 o -3 9 1 335.69 355.32 14.23 o -2 9 1 102.99 105.96 4.69 o -1 9 1 5.76 4.73 1.25 o 0 9 1 111.56 107.75 3.18 o 1 9 1 5.90 5.91 2.08 o -2 10 1 17.66 17.44 2.03 o 0 -10 2 27.38 24.41 1.19 o 1 -10 2 165.51 172.36 5.05 o 2 -10 2 4.83 5.74 0.86 o 3 -10 2 54.18 56.27 2.56 o -2 -9 2 3.77 4.18 1.26 o -1 -9 2 41.26 43.86 1.39 o 0 -9 2 282.84 306.24 5.87 o 1 -9 2 51.03 50.37 1.95 o 2 -9 2 297.47 315.36 8.92 o 3 -9 2 6.00 4.94 0.84 o 4 -9 2 0.23 0.58 0.55 o -3 -8 2 10.50 10.76 1.48 o -2 -8 2 35.96 40.50 2.24 o -1 -8 2 220.78 251.45 7.98 o 0 -8 2 11.05 11.46 0.46 o 1 -8 2 666.51 673.16 17.57 o 2 -8 2 61.57 63.15 2.11 o 3 -8 2 0.25 0.11 0.32 o 4 -8 2 124.86 145.49 5.40 o -3 -7 2 0.67 0.63 0.58 o -2 -7 2 291.29 270.52 9.96 o -1 -7 2 58.79 57.70 2.10 o 0 -7 2 176.29 189.36 4.58 o 1 -7 2 6.24 5.15 0.59 o 2 -7 2 228.26 230.09 10.37 o 3 -7 2 899.41 891.06 25.70 o 4 -7 2 43.02 48.57 4.91 o 5 -7 2 33.78 37.87 3.60 o -4 -6 2 48.77 50.57 3.12 o -3 -6 2 129.46 144.98 5.59 o -2 -6 2 122.80 110.14 4.30 o -1 -6 2 288.56 333.80 5.75 o 0 -6 2 328.54 362.79 6.19 o 1 -6 2 176.47 179.07 3.81 o 2 -6 2 833.58 822.01 21.73 o 3 -6 2 2.69 1.66 0.50 o 4 -6 2 62.47 61.56 4.93 o 5 -6 2 34.85 34.90 1.76 o -4 -5 2 473.48 527.13 20.86 o -3 -5 2 3.54 2.24 0.70 o -2 -5 2 107.38 98.12 2.84 o -1 -5 2 18.43 25.64 0.55 o 0 -5 2 144.09 173.69 3.92 o 1 -5 2 1311.44 1387.30 31.29 o 2 -5 2 33.25 28.64 2.35 o 3 -5 2 142.98 124.67 16.21 o 4 -5 2 323.08 336.00 13.05 o 5 -5 2 1.43 1.08 0.40 o -5 -4 2 76.72 79.59 4.23 o -4 -4 2 55.61 54.30 2.85 o -3 -4 2 804.09 827.21 31.83 o -2 -4 2 10.52 7.86 0.18 o -1 -4 2 115.83 142.77 2.14 o 0 -4 2 2012.66 2484.16 67.19 o 1 -4 2 9.08 9.14 0.26 o 2 -4 2 42.49 37.54 1.47 o 3 -4 2 636.22 632.83 22.19 o 4 -4 2 43.74 41.58 1.21 o 5 -4 2 141.06 151.42 4.50 o -5 -3 2 0.43 0.28 0.53 o -4 -3 2 4.52 4.60 0.87 o -3 -3 2 61.42 61.38 2.36 o -2 -3 2 133.14 128.04 3.59 o -1 -3 2 1202.50 1353.23 66.35 o 0 -3 2 29.52 43.22 0.68 o 1 -3 2 2267.30 2631.74 128.05 o 2 -3 2 1880.52 1884.21 83.69 o 3 -3 2 315.78 323.09 10.03 o 4 -3 2 40.09 38.23 2.02 o 5 -3 2 50.07 55.39 2.36 o -6 -2 2 0.29 0.79 0.77 o -5 -2 2 193.73 194.85 7.51 o -4 -2 2 151.78 154.29 5.37 o -3 -2 2 18.05 17.84 1.06 o -2 -2 2 1591.39 1654.23 101.46 o -1 -2 2 289.03 334.44 7.54 o 0 -2 2 153.06 188.90 5.46 o 1 -2 2 2809.11 3340.47 188.49 o 2 -2 2 499.92 528.79 11.69 o 3 -2 2 619.56 610.80 20.50 o 4 -2 2 0.67 0.51 0.34 o 5 -2 2 0.12 0.34 0.29 o -6 -1 2 42.71 47.20 3.09 o -5 -1 2 285.49 270.15 9.77 o -4 -1 2 68.25 64.61 1.25 o -3 -1 2 1200.29 1226.46 25.59 o -2 -1 2 0.56 0.50 0.06 o -1 -1 2 52.16 57.15 1.66 o 0 -1 2 104.35 115.18 2.03 o 1 -1 2 65.28 68.51 3.49 o 2 -1 2 2023.09 2257.56 74.21 o 3 -1 2 470.44 475.30 10.84 o 4 -1 2 13.43 10.25 1.02 o 5 -1 2 165.36 151.20 9.06 o -6 0 2 0.79 1.42 0.77 o -5 0 2 0.71 1.05 0.26 o -4 0 2 971.18 931.28 19.01 o -3 0 2 36.03 41.20 1.03 o -2 0 2 31.84 23.82 0.35 o -1 0 2 7545.47 8029.68 327.79 o 0 0 2 22.70 22.73 0.73 o 1 0 2 48.00 64.51 2.65 o 2 0 2 54.49 46.45 1.04 o 3 0 2 237.33 243.33 4.89 o 4 0 2 408.77 439.06 15.01 o 5 0 2 40.16 36.01 1.42 o -6 1 2 17.35 21.87 1.71 o -5 1 2 236.89 237.51 4.50 o -4 1 2 129.71 128.88 3.10 o -3 1 2 400.31 355.70 6.01 o -2 1 2 1299.82 1310.94 24.68 o -1 1 2 468.89 484.99 22.64 o 0 1 2 1172.46 1307.94 34.96 o 1 1 2 442.34 444.81 15.12 o 2 1 2 2.39 2.16 0.54 o 3 1 2 842.32 807.87 25.09 o 4 1 2 7.49 7.55 1.24 o 5 1 2 9.51 12.45 1.58 o -6 2 2 145.51 140.42 3.32 o -5 2 2 0.36 1.51 0.31 o -4 2 2 61.10 60.21 2.64 o -3 2 2 1784.51 1837.24 39.87 o -2 2 2 9.47 7.76 0.31 o -1 2 2 9.04 7.31 0.87 o 0 2 2 390.66 457.63 13.42 o 1 2 2 274.45 262.45 4.97 o 2 2 2 1048.33 1056.30 47.76 o 3 2 2 7.63 7.52 0.46 o 4 2 2 57.50 51.06 1.13 o -6 3 2 4.63 5.71 0.48 o -5 3 2 64.02 64.37 1.88 o -4 3 2 482.33 480.77 17.53 o -3 3 2 226.94 223.03 3.64 o -2 3 2 687.99 714.71 13.46 o -1 3 2 61.93 54.20 1.23 o 0 3 2 2.08 2.95 0.37 o 1 3 2 1124.84 1196.47 72.58 o 2 3 2 41.38 38.23 1.55 o 3 3 2 29.81 28.02 0.85 o 4 3 2 445.22 416.41 16.00 o -6 4 2 12.09 14.71 0.75 o -5 4 2 682.40 451.18 179.43 o -4 4 2 0.15 0.36 0.35 o -3 4 2 196.76 158.53 4.87 o -2 4 2 885.87 911.86 23.77 o -1 4 2 13.81 17.39 0.67 o 0 4 2 48.99 37.42 0.98 o 1 4 2 0.26 0.20 0.17 o 2 4 2 458.18 439.10 10.13 o 3 4 2 474.42 460.28 10.50 o 4 4 2 41.02 39.27 2.55 o -6 5 2 136.18 141.04 5.19 o -5 5 2 2.17 2.49 0.70 o -4 5 2 88.23 82.07 3.84 o -3 5 2 400.69 346.60 27.41 o -2 5 2 158.69 170.75 3.79 o -1 5 2 1083.74 1192.76 36.12 o 0 5 2 38.54 39.17 1.11 o 1 5 2 8.61 7.26 0.55 o 2 5 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0 1 10 44.03 47.79 2.51 o -4 2 10 0.05 -0.02 0.25 o -3 2 10 74.15 80.13 4.26 o -2 2 10 2.42 1.68 0.73 o -1 2 10 36.51 41.60 2.31 o -3 3 10 20.30 21.85 1.34 o -2 3 10 0.09 0.28 0.56 o -2 -5 11 5.46 2.80 0.84 o -1 -5 11 29.15 30.78 1.55 o -2 -4 11 21.08 22.63 1.26 o -1 -4 11 15.65 14.91 1.29 o 0 -4 11 60.96 65.96 3.29 o -3 -3 11 81.14 86.13 2.61 o -2 -3 11 30.34 33.54 1.71 o -1 -3 11 6.79 6.06 0.89 o 0 -3 11 35.84 40.51 2.38 o -3 -2 11 0.40 0.49 0.41 o -2 -2 11 1.59 1.76 0.65 o -1 -2 11 114.26 127.08 4.64 o 0 -2 11 6.20 5.49 1.22 o -3 -1 11 0.67 0.69 0.43 o -2 -1 11 85.14 88.94 2.83 o -1 -1 11 0.35 0.56 0.55 o -3 0 11 53.41 61.11 2.34 o -2 0 11 34.30 37.51 2.23 o -1 0 11 6.27 6.71 1.10 o