data_2239474 _cell_angle_alpha 90.000 _cell_angle_beta 111.753 _cell_angle_gamma 90.000 _cell_length_a 11.6695 _cell_length_b 8.5238 _cell_length_c 11.8165 _exptl_crystal_F_000 1160.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file wm5002Isup2.hkl _[local]_cod_data_source_block I _shelx_title Rb2Lu[Si4O10]F _shelx_refln_list_code 4 _shelx_f_calc_maximum 590.81 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14283.99 14951.28 274.20 o 3 0 0 62802.70 64946.91 852.94 o 4 0 0 69476.95 70243.95 936.64 o 5 0 0 61181.52 63241.59 864.50 o 6 0 0 3583.66 3695.59 100.94 o 7 0 0 35096.41 34420.77 534.66 o 8 0 0 1530.61 1684.83 72.89 o 9 0 0 12.49 51.22 29.42 o 10 0 0 26820.97 27087.50 461.30 o 11 0 0 11126.25 11441.02 247.82 o 12 0 0 10065.42 9377.91 343.08 o 13 0 0 18208.19 18604.31 536.84 o 1 1 0 154.65 336.52 15.10 o 2 1 0 9175.12 9441.94 118.17 o 3 1 0 957.31 987.92 30.53 o 4 1 0 11411.53 11510.09 143.30 o 5 1 0 1361.63 1396.42 32.02 o 6 1 0 1580.28 1658.18 39.03 o 7 1 0 10.82 34.46 13.16 o 8 1 0 2760.59 2715.87 71.13 o 9 1 0 3.62 38.40 14.20 o 10 1 0 2068.34 1976.53 63.50 o 11 1 0 78.58 93.15 36.27 o 12 1 0 171.04 253.37 57.37 o 13 1 0 1928.12 1990.48 117.82 o 0 2 0 61549.42 64822.49 841.14 o 1 2 0 2119.75 2174.83 25.47 o 2 2 0 182838.34 177113.89 1295.77 o 3 2 0 42570.91 42810.89 338.83 o 4 2 0 2864.40 2783.53 44.89 o 5 2 0 55689.96 56975.29 427.67 o 6 2 0 498.83 521.45 48.29 o 7 2 0 9979.93 9939.04 127.82 o 8 2 0 68.00 305.42 29.61 o 9 2 0 19123.89 19255.03 254.10 o 10 2 0 27894.41 28046.45 310.23 o 11 2 0 4927.23 5147.65 138.74 o 12 2 0 12756.29 13410.86 250.44 o 13 2 0 80.97 38.01 56.56 o 1 3 0 173.75 202.98 12.24 o 2 3 0 1808.78 2182.11 28.98 o 3 3 0 973.50 799.91 22.56 o 4 3 0 426.94 501.27 19.26 o 5 3 0 2223.39 2323.73 41.85 o 6 3 0 767.65 719.26 24.13 o 7 3 0 2.07 53.65 11.86 o 8 3 0 6883.24 7057.59 112.48 o 9 3 0 843.64 816.83 61.12 o 10 3 0 3982.27 3976.91 101.77 o 11 3 0 288.65 358.64 39.74 o 12 3 0 7695.04 7717.11 185.07 o 13 3 0 124.69 182.14 71.95 o 0 4 0 349056.66 319083.88 2815.86 o 1 4 0 4897.47 4885.36 52.35 o 2 4 0 4465.62 4581.65 51.07 o 3 4 0 27143.84 27543.41 213.89 o 4 4 0 25600.95 25652.86 217.93 o 5 4 0 68556.59 69001.73 479.21 o 6 4 0 134.85 247.61 21.81 o 7 4 0 37775.48 37434.24 379.89 o 8 4 0 12746.96 13079.86 142.04 o 9 4 0 1788.29 1751.58 64.58 o 10 4 0 18685.31 18261.77 266.28 o 11 4 0 13496.23 13626.01 232.74 o 12 4 0 11058.06 11358.36 238.13 o 1 5 0 483.09 482.43 18.22 o 2 5 0 13310.16 13314.82 146.78 o 3 5 0 373.67 429.41 17.09 o 4 5 0 11624.59 11524.55 103.00 o 5 5 0 3871.37 3856.90 55.71 o 6 5 0 3956.55 3888.10 64.02 o 7 5 0 194.49 156.01 19.48 o 8 5 0 889.39 857.18 33.57 o 9 5 0 6.36 39.25 21.74 o 10 5 0 1273.64 1280.99 70.13 o 11 5 0 163.44 179.92 39.28 o 0 6 0 4327.05 4362.55 86.89 o 1 6 0 3954.02 4083.25 57.29 o 2 6 0 67674.57 67047.90 467.80 o 3 6 0 12985.92 12969.44 129.47 o 4 6 0 91.30 153.51 23.47 o 5 6 0 55194.24 54357.49 481.54 o 6 6 0 989.15 1150.08 37.62 o 7 6 0 15354.07 15205.78 174.77 o 8 6 0 9632.91 9705.34 134.10 o 9 6 0 24839.34 24909.12 308.39 o 10 6 0 15002.82 15130.33 249.68 o 11 6 0 888.29 963.53 69.50 o 1 7 0 194.49 198.48 16.05 o 2 7 0 159.69 143.29 18.26 o 3 7 0 674.95 697.24 33.30 o 4 7 0 284.92 286.24 30.83 o 5 7 0 354.27 391.59 28.31 o 6 7 0 754.08 810.11 37.68 o 7 7 0 389.05 420.68 34.21 o 8 7 0 2487.00 2544.17 70.57 o 9 7 0 204.43 257.18 43.27 o 10 7 0 946.97 922.29 66.87 o 0 8 0 49846.81 49323.98 727.73 o 1 8 0 3222.66 3174.65 77.27 o 2 8 0 1164.33 1178.02 48.56 o 3 8 0 8232.27 8288.40 177.79 o 4 8 0 7865.30 7738.71 151.56 o 5 8 0 41376.53 41309.94 512.05 o 6 8 0 381.55 506.05 42.65 o 7 8 0 28580.86 28904.38 339.26 o 8 8 0 18815.43 18483.45 307.49 o 1 9 0 1680.30 1675.19 72.97 o 2 9 0 992.69 902.29 70.53 o 3 9 0 202.60 169.33 40.36 o 4 9 0 2294.83 2238.86 86.25 o 5 9 0 79.34 74.66 36.81 o 6 9 0 959.27 1053.69 60.62 o 7 9 0 995.30 975.34 78.61 o 0 10 0 1516.51 1454.59 113.44 o 1 10 0 1230.92 1318.61 147.19 o 2 10 0 30258.98 29930.96 472.25 o 3 10 0 7026.23 7272.79 169.22 o 4 10 0 668.90 798.14 75.82 o -13 0 1 17219.60 16923.98 848.07 o -12 0 1 109.32 489.24 96.48 o -11 0 1 33106.46 33691.43 754.64 o -10 0 1 85.90 87.03 37.96 o -9 0 1 15051.72 14946.00 417.76 o -8 0 1 33350.02 33706.97 672.08 o -7 0 1 104141.67 102379.37 1378.89 o -6 0 1 44627.95 43544.37 537.29 o -5 0 1 9458.17 9799.18 190.02 o -4 0 1 102038.75 100904.91 1141.30 o -3 0 1 3647.63 3672.86 71.30 o -2 0 1 14854.59 15236.71 223.40 o 1 0 1 39531.46 39834.88 640.63 o 2 0 1 2915.50 2959.81 56.06 o 3 0 1 102081.85 100718.02 1011.57 o 4 0 1 11107.33 11187.91 142.09 o 5 0 1 502.30 521.90 24.84 o 6 0 1 70537.28 67424.95 1436.76 o 7 0 1 109.41 240.20 32.98 o 8 0 1 11622.93 11656.91 231.13 o 9 0 1 17532.75 17549.30 320.85 o 10 0 1 340.58 523.34 89.84 o 11 0 1 15262.85 14648.71 435.10 o 12 0 1 330.48 509.92 102.39 o 13 0 1 8223.95 8662.98 348.12 o -13 1 1 400.56 395.53 65.65 o -12 1 1 2.16 18.90 35.18 o -11 1 1 1576.25 1552.88 55.94 o -10 1 1 633.69 661.97 29.32 o -9 1 1 282.18 315.86 30.89 o -8 1 1 3749.75 3920.29 63.46 o -7 1 1 5772.44 5828.78 83.29 o -6 1 1 2862.78 2815.37 64.70 o -5 1 1 22603.25 22841.41 214.95 o -4 1 1 5949.78 6143.17 82.30 o -3 1 1 61124.81 62621.78 542.77 o -2 1 1 276.95 314.36 15.28 o -1 1 1 20.79 42.08 13.04 o 1 1 1 41.94 75.31 10.22 o 2 1 1 1124.28 1223.61 23.44 o 3 1 1 10266.71 10358.76 115.49 o 4 1 1 78.65 119.93 17.90 o 5 1 1 2153.48 1987.70 51.36 o 6 1 1 18140.07 18123.78 211.80 o 7 1 1 2447.96 2459.42 42.34 o 8 1 1 6602.08 6719.76 100.72 o 9 1 1 388.36 460.25 42.17 o 10 1 1 5189.52 5348.18 131.21 o 11 1 1 400.80 352.59 59.68 o 12 1 1 695.73 876.99 92.27 o 13 1 1 16.26 24.54 58.62 o -13 2 1 4740.86 5048.83 178.37 o -12 2 1 953.36 1073.20 69.07 o -11 2 1 28636.34 28494.76 356.01 o -10 2 1 2267.93 2283.22 89.20 o -9 2 1 48050.73 46719.10 459.52 o -8 2 1 8177.20 8272.02 109.62 o -7 2 1 1798.46 1723.03 46.89 o -6 2 1 57865.02 56825.04 492.50 o -5 2 1 3216.75 3038.38 47.25 o -4 2 1 40285.37 39809.33 308.04 o -3 2 1 20212.94 20318.91 187.72 o -2 2 1 10950.67 10833.11 107.22 o -1 2 1 28132.29 28379.18 250.56 o 0 2 1 1753.44 1902.89 26.33 o 1 2 1 51067.24 51037.95 309.86 o 2 2 1 922.15 979.37 18.21 o 3 2 1 2910.87 2551.01 34.83 o 4 2 1 66586.09 65861.36 491.57 o 5 2 1 46948.00 45781.68 400.02 o 6 2 1 19463.13 19252.15 219.95 o 7 2 1 20214.52 20039.56 256.51 o 8 2 1 26921.55 26390.35 267.70 o 9 2 1 3547.10 3693.29 90.15 o 10 2 1 3960.30 4214.31 97.52 o 11 2 1 21068.50 20716.62 327.09 o 12 2 1 76.47 210.90 60.93 o -13 3 1 966.56 1016.88 87.66 o -12 3 1 77.52 -16.48 42.66 o -11 3 1 7272.73 7347.02 171.98 o -10 3 1 1699.98 1662.26 65.96 o -9 3 1 1800.72 1733.55 40.96 o -8 3 1 10875.06 10712.38 126.46 o -7 3 1 745.92 769.71 24.81 o -6 3 1 2953.42 2943.00 51.48 o -5 3 1 20395.32 20762.26 185.77 o -4 3 1 1764.46 1764.33 34.42 o -3 3 1 151.78 156.77 13.45 o -2 3 1 7825.68 7496.26 67.82 o -1 3 1 10521.42 10225.59 85.89 o 0 3 1 10800.46 10962.00 102.47 o 1 3 1 22616.88 22258.38 169.27 o 2 3 1 2762.68 2598.32 32.08 o 3 3 1 11561.50 11783.11 96.23 o 4 3 1 3910.20 3892.56 49.71 o 5 3 1 27002.94 26706.97 204.29 o 6 3 1 3227.71 3173.30 58.46 o 7 3 1 1677.28 1583.23 36.66 o 8 3 1 9233.64 9246.56 159.79 o 9 3 1 120.86 161.85 31.44 o 10 3 1 528.99 630.15 68.91 o 11 3 1 2054.41 2061.27 91.76 o 12 3 1 1988.03 2036.30 143.57 o -12 4 1 2501.74 2603.60 107.93 o -11 4 1 17228.52 17537.53 278.53 o -10 4 1 522.79 516.19 45.46 o -9 4 1 9198.76 9088.40 111.13 o -8 4 1 19393.73 19359.62 178.27 o -7 4 1 36717.08 35841.18 278.95 o -6 4 1 27551.12 27472.66 260.98 o -5 4 1 6196.42 6386.57 76.02 o -4 4 1 56298.11 55504.74 404.45 o -3 4 1 4052.04 3959.52 51.52 o -2 4 1 25483.76 24996.96 185.58 o -1 4 1 37983.14 36525.77 256.20 o 0 4 1 3410.86 3499.68 41.79 o 1 4 1 42170.64 41282.30 301.57 o 2 4 1 7762.46 7563.41 61.48 o 3 4 1 66026.32 65052.81 423.48 o 4 4 1 5468.19 5503.00 65.21 o 5 4 1 184.61 312.99 18.36 o 6 4 1 54318.50 53497.46 543.28 o 7 4 1 2641.54 2825.08 60.70 o 8 4 1 10996.27 11117.16 133.04 o 9 4 1 18840.46 18448.80 311.31 o 10 4 1 5351.70 5333.48 115.99 o 11 4 1 12940.33 12781.52 249.82 o 12 4 1 37.21 210.53 50.44 o -12 5 1 3.86 -10.55 43.29 o -11 5 1 215.74 191.40 40.85 o -10 5 1 108.60 81.51 33.16 o -9 5 1 1410.79 1384.59 51.43 o -8 5 1 1927.93 2067.13 46.40 o -7 5 1 9543.09 9493.51 158.95 o -6 5 1 1705.52 1725.11 43.97 o -5 5 1 9494.01 9322.70 113.74 o -4 5 1 4888.96 4920.03 59.95 o -3 5 1 62511.89 63270.13 478.49 o -2 5 1 82.44 79.80 12.01 o -1 5 1 1030.70 1109.28 24.15 o 0 5 1 55.58 80.71 12.17 o 1 5 1 1551.03 1624.07 35.14 o 2 5 1 520.17 515.73 19.56 o 3 5 1 3820.47 3918.03 45.88 o 4 5 1 621.63 647.08 21.61 o 5 5 1 132.84 164.72 16.25 o 6 5 1 13155.65 12976.09 147.16 o 7 5 1 1236.54 1294.48 45.51 o 8 5 1 3517.05 3659.57 78.93 o 9 5 1 613.73 657.53 44.12 o 10 5 1 8530.19 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2038.20 98.25 o -4 9 1 1551.18 1551.02 87.43 o -3 9 1 5526.68 5418.82 137.69 o -2 9 1 4560.45 4322.17 119.87 o -1 9 1 482.72 449.89 47.87 o 0 9 1 142.73 178.39 36.66 o 1 9 1 1644.79 1603.68 72.85 o 2 9 1 4577.38 4461.76 120.33 o 3 9 1 1358.96 1338.77 66.73 o 4 9 1 1056.11 1119.78 62.99 o 5 9 1 7672.84 7418.36 310.86 o 6 9 1 189.29 249.82 58.12 o -4 10 1 8483.89 8227.65 212.18 o -3 10 1 4743.17 4811.45 136.76 o -2 10 1 9225.13 8869.50 193.10 o -1 10 1 14024.58 13761.00 274.76 o 0 10 1 979.56 1007.98 69.80 o 1 10 1 20587.14 19990.62 784.32 o 2 10 1 855.69 911.52 90.87 o 3 10 1 2464.92 2503.45 136.44 o 4 10 1 14537.08 14903.71 364.06 o -14 0 2 208.31 148.75 75.72 o -13 0 2 5178.30 5543.33 262.03 o -12 0 2 18076.48 18464.55 367.56 o -11 0 2 15364.93 15335.74 316.77 o -10 0 2 95734.32 94587.52 1331.77 o -9 0 2 9852.53 9285.53 162.67 o -8 0 2 14063.71 14116.42 306.30 o -7 0 2 11772.68 11965.33 183.38 o -6 0 2 48980.36 48628.48 597.35 o -5 0 2 89820.62 90628.19 1052.62 o -4 0 2 15240.39 16665.18 323.94 o -3 0 2 46786.80 47714.79 689.82 o -2 0 2 16975.77 16795.32 263.18 o -1 0 2 18324.40 18754.38 599.73 o 0 0 2 19878.94 22477.54 1268.25 o 1 0 2 1045.43 1060.88 42.12 o 2 0 2 63070.78 61077.62 577.14 o 3 0 2 78472.19 77972.69 732.24 o 4 0 2 1920.65 1829.48 49.06 o 5 0 2 11187.85 11232.90 161.34 o 6 0 2 11200.29 10571.52 173.20 o 7 0 2 34697.55 35295.88 1105.52 o 8 0 2 1804.68 1968.35 206.00 o 9 0 2 70947.42 68011.71 1270.30 o 10 0 2 6386.89 6320.71 261.57 o 11 0 2 2363.63 2406.02 306.97 o 12 0 2 9799.84 10321.27 372.51 o -14 1 2 643.88 756.38 81.86 o -13 1 2 129.55 144.14 57.74 o -12 1 2 1789.06 1792.60 65.80 o -11 1 2 349.19 384.81 39.80 o -10 1 2 7774.01 7688.18 123.83 o -9 1 2 880.09 911.11 55.31 o -8 1 2 607.00 704.51 30.08 o -7 1 2 2504.19 2513.53 55.59 o -6 1 2 65.73 55.17 15.06 o -5 1 2 6934.50 7147.92 82.37 o -4 1 2 6631.26 6858.50 77.24 o -3 1 2 7336.36 7638.15 82.09 o -2 1 2 403.59 477.60 18.25 o -1 1 2 2201.00 2250.55 44.77 o 0 1 2 153.32 187.21 13.61 o 1 1 2 1129.33 1209.62 32.30 o 2 1 2 191.13 228.41 15.08 o 3 1 2 814.13 972.52 26.43 o 4 1 2 1127.02 1303.29 27.11 o 5 1 2 1321.87 1300.23 37.28 o 6 1 2 30.24 32.38 14.47 o 7 1 2 7812.16 7990.48 109.03 o 8 1 2 2318.23 2325.38 62.41 o 9 1 2 11.60 36.88 22.91 o 10 1 2 1696.02 1771.91 100.77 o 11 1 2 165.13 119.87 51.88 o 12 1 2 568.36 640.52 74.90 o -13 2 2 28492.63 28409.37 570.91 o -12 2 2 16818.42 16737.17 286.83 o -11 2 2 87.89 144.45 24.65 o -10 2 2 39370.77 38904.36 405.83 o -9 2 2 287.46 330.16 35.81 o -8 2 2 64759.64 64007.73 656.14 o -7 2 2 31068.58 30149.82 276.65 o -6 2 2 20831.66 21098.97 203.94 o -5 2 2 19889.68 21119.08 186.88 o -4 2 2 496.58 826.01 32.84 o -3 2 2 82610.62 81310.74 588.58 o -2 2 2 22927.90 24157.71 188.91 o -1 2 2 8982.44 8862.22 94.64 o 0 2 2 181398.77 177073.36 2052.17 o 1 2 2 1308.91 1438.21 25.50 o 2 2 2 308.54 561.83 18.15 o 3 2 2 1311.70 1794.72 37.04 o 4 2 2 37436.93 36039.53 298.05 o 5 2 2 40417.28 39399.06 426.35 o 6 2 2 194.24 226.18 15.47 o 7 2 2 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