data_2239478 _cell_angle_alpha 90.000 _cell_angle_beta 120.392 _cell_angle_gamma 90.000 _cell_length_a 9.5760 _cell_length_b 12.2310 _cell_length_c 9.9811 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file lh5658Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' Compound X New: P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 93.95 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 835.97 766.83 18.47 o 4 0 0 460.75 503.01 25.23 o 5 0 0 263.07 256.29 5.13 o 6 0 0 541.16 527.14 10.28 o 7 0 0 157.84 168.15 3.68 o 8 0 0 943.36 1025.31 26.16 o 9 0 0 109.65 121.40 3.56 o 2 1 0 2556.29 2280.30 155.42 o 3 1 0 8827.16 8351.25 421.19 o 5 1 0 2711.59 2618.53 45.57 o 6 1 0 984.67 952.58 14.06 o 7 1 0 355.99 346.93 5.48 o 8 1 0 9.00 9.93 0.71 o 9 1 0 4.36 5.51 0.69 o 2 2 0 1910.82 1851.97 34.80 o 3 2 0 180.79 235.74 3.94 o 4 2 0 291.32 283.74 6.17 o 5 2 0 46.47 46.26 0.81 o 6 2 0 43.46 46.51 0.95 o 7 2 0 333.75 352.31 6.50 o 8 2 0 620.57 655.87 15.60 o 9 2 0 565.47 585.31 13.91 o 1 3 0 421.03 444.79 8.36 o 2 3 0 756.68 758.53 10.81 o 3 3 0 88.61 111.96 4.81 o 4 3 0 1843.18 1939.00 30.64 o 5 3 0 511.56 494.10 8.51 o 6 3 0 392.46 395.23 6.42 o 7 3 0 9.63 6.43 1.22 o 8 3 0 206.11 206.18 4.88 o 9 3 0 268.41 276.69 8.27 o 0 4 0 887.49 864.08 20.93 o 1 4 0 1838.34 1849.17 23.62 o 2 4 0 24.24 29.34 0.47 o 3 4 0 303.64 334.46 5.45 o 4 4 0 31.83 50.25 0.80 o 5 4 0 1053.33 1033.03 15.03 o 6 4 0 922.78 934.71 16.85 o 7 4 0 258.06 242.06 4.83 o 8 4 0 13.76 12.89 1.37 o 9 4 0 1.40 1.90 0.53 o 1 5 0 811.38 887.06 11.45 o 2 5 0 304.45 323.55 4.49 o 3 5 0 245.57 246.70 4.17 o 4 5 0 46.11 50.47 1.72 o 5 5 0 5.44 5.34 0.40 o 6 5 0 16.06 16.91 0.57 o 7 5 0 74.68 63.07 1.36 o 8 5 0 320.13 320.83 6.56 o 9 5 0 385.13 412.16 10.48 o 0 6 0 1932.54 2044.65 36.20 o 1 6 0 124.18 139.16 1.91 o 2 6 0 1771.72 1936.20 24.64 o 3 6 0 29.40 31.97 1.68 o 4 6 0 127.90 120.35 1.85 o 5 6 0 369.21 354.83 5.22 o 6 6 0 496.12 480.02 9.42 o 7 6 0 0.06 0.93 0.54 o 8 6 0 230.19 215.01 4.70 o 1 7 0 162.98 147.53 2.88 o 2 7 0 683.88 723.07 10.61 o 3 7 0 70.51 71.34 1.81 o 4 7 0 97.00 99.64 1.64 o 5 7 0 37.98 34.81 0.78 o 6 7 0 35.22 31.63 1.30 o 7 7 0 1.45 1.60 1.42 o 8 7 0 3.46 4.87 1.19 o 0 8 0 301.58 317.67 5.56 o 1 8 0 213.73 222.03 3.68 o 2 8 0 16.35 20.08 0.38 o 3 8 0 0.01 0.67 1.06 o 4 8 0 107.09 116.37 2.12 o 5 8 0 1.67 3.00 0.80 o 6 8 0 38.46 32.35 1.02 o 7 8 0 41.24 39.68 1.40 o 8 8 0 23.39 20.46 1.11 o 1 9 0 7.14 5.22 0.47 o 2 9 0 154.61 159.25 2.39 o 3 9 0 98.22 86.13 1.31 o 4 9 0 423.72 401.27 6.74 o 5 9 0 45.93 39.07 1.26 o 6 9 0 33.71 24.14 1.36 o 7 9 0 156.60 150.96 3.29 o 0 10 0 36.08 28.01 0.66 o 1 10 0 29.55 24.11 0.93 o 2 10 0 142.08 145.86 2.78 o 3 10 0 177.20 181.31 3.21 o 4 10 0 4.36 6.10 0.36 o 5 10 0 207.14 216.15 5.08 o 6 10 0 358.61 320.20 8.81 o 7 10 0 55.94 61.12 2.27 o 1 11 0 172.98 167.78 3.64 o 2 11 0 0.07 -0.68 0.34 o 3 11 0 43.22 40.60 2.78 o 4 11 0 0.02 -0.16 0.34 o 5 11 0 0.01 -0.52 0.38 o 6 11 0 16.78 12.02 0.69 o 0 12 0 329.26 360.41 8.11 o 1 12 0 308.72 295.37 9.96 o 2 12 0 0.33 0.92 0.38 o 3 12 0 86.18 94.06 2.13 o 4 12 0 131.12 125.70 3.62 o 5 12 0 21.47 18.70 1.06 o 1 13 0 11.67 8.42 0.64 o 2 13 0 67.83 73.17 1.53 o 3 13 0 231.46 237.20 5.52 o 4 13 0 72.65 67.49 3.54 o 0 14 0 1178.75 1251.63 50.86 o 1 14 0 465.20 499.97 11.75 o 2 14 0 80.91 85.11 2.65 o -10 1 1 457.82 472.66 13.93 o -9 1 1 8.76 8.57 0.73 o -8 1 1 223.20 230.48 5.10 o -7 1 1 325.47 315.71 6.15 o -6 1 1 264.86 263.34 5.28 o -5 1 1 940.96 940.37 20.67 o -4 1 1 808.96 776.00 25.60 o -3 1 1 872.03 829.48 21.54 o -2 1 1 52.69 61.42 1.34 o 1 1 1 645.43 625.15 7.74 o 2 1 1 6198.18 5852.05 146.13 o 3 1 1 779.82 756.99 11.03 o 4 1 1 17.69 13.23 0.41 o 5 1 1 1643.40 1726.82 23.92 o 6 1 1 92.14 90.34 1.44 o 7 1 1 0.72 0.39 0.39 o 8 1 1 61.06 63.20 1.71 o 9 1 1 4.00 3.88 0.80 o -10 2 1 980.59 1046.21 27.33 o -9 2 1 19.63 22.83 1.12 o -8 2 1 1088.54 1136.02 57.41 o -7 2 1 1004.17 1005.09 18.33 o -6 2 1 1008.53 932.50 15.66 o -5 2 1 0.33 -1.01 0.51 o -4 2 1 379.99 420.90 23.81 o -3 2 1 0.36 0.59 0.35 o -1 2 1 2728.69 2621.92 66.26 o 1 2 1 2021.69 1980.65 46.40 o 2 2 1 5355.93 5135.67 83.71 o 3 2 1 123.21 164.07 7.37 o 4 2 1 53.65 36.06 1.01 o 5 2 1 856.49 877.27 16.81 o 6 2 1 71.06 67.46 1.25 o 7 2 1 125.65 126.70 2.61 o 8 2 1 132.53 142.38 5.94 o 9 2 1 0.01 0.06 0.72 o -10 3 1 117.24 126.45 3.79 o -9 3 1 165.66 169.37 3.94 o -8 3 1 120.78 118.18 3.34 o -7 3 1 391.19 386.27 5.76 o -6 3 1 164.28 149.31 2.44 o -5 3 1 1946.12 1923.80 30.34 o -4 3 1 3681.07 3606.33 122.27 o -3 3 1 5200.61 4696.46 387.63 o -2 3 1 1141.57 1112.42 22.64 o -1 3 1 998.46 975.26 19.04 o 0 3 1 1095.34 1085.22 20.68 o 2 3 1 95.03 132.34 1.77 o 3 3 1 1679.75 1695.70 39.78 o 4 3 1 72.11 58.82 1.00 o 5 3 1 106.57 101.61 1.50 o 6 3 1 6.52 5.02 0.86 o 7 3 1 77.09 69.53 2.00 o 8 3 1 2.53 6.17 3.10 o 9 3 1 86.19 89.33 2.84 o -9 4 1 547.51 561.99 13.17 o -8 4 1 842.87 877.00 20.57 o -7 4 1 298.41 304.80 5.69 o -6 4 1 1084.25 1112.62 15.73 o -5 4 1 445.28 464.66 7.79 o -4 4 1 112.64 123.91 2.06 o -3 4 1 98.08 91.95 10.43 o -2 4 1 3471.80 3479.84 99.18 o -1 4 1 1213.85 1173.29 18.64 o 0 4 1 1881.13 1784.44 27.44 o 1 4 1 3897.88 3817.98 70.49 o 2 4 1 1080.91 1070.82 20.03 o 3 4 1 102.96 139.94 1.98 o 4 4 1 131.79 138.66 1.93 o 5 4 1 21.18 17.10 0.51 o 6 4 1 0.62 0.60 0.48 o 7 4 1 4.11 3.45 1.86 o 8 4 1 76.53 69.16 2.05 o -9 5 1 17.75 18.00 0.80 o -8 5 1 59.39 54.21 1.46 o -7 5 1 89.89 77.31 1.53 o -6 5 1 1250.89 1241.33 21.79 o -5 5 1 383.66 357.55 6.44 o -4 5 1 989.53 983.21 29.42 o -3 5 1 12.01 1.53 1.96 o -1 5 1 310.32 280.76 4.46 o 0 5 1 253.10 239.30 3.24 o 1 5 1 607.87 592.49 12.34 o 2 5 1 90.53 88.36 3.21 o 3 5 1 134.99 112.95 1.97 o 4 5 1 571.31 564.13 9.95 o 5 5 1 368.57 365.39 5.43 o 6 5 1 590.78 599.97 9.82 o 7 5 1 147.19 158.55 4.96 o 8 5 1 369.34 376.25 7.56 o -9 6 1 73.98 73.63 2.07 o -8 6 1 103.08 105.70 2.63 o -7 6 1 58.37 54.56 1.31 o -6 6 1 21.53 14.40 1.81 o -5 6 1 67.72 61.62 2.19 o -4 6 1 21.38 16.04 1.12 o -3 6 1 24.20 14.87 0.51 o -2 6 1 207.44 208.72 6.15 o -1 6 1 65.02 56.60 1.08 o 0 6 1 211.85 231.42 3.71 o 1 6 1 435.58 426.33 5.33 o 2 6 1 477.18 454.95 6.37 o 3 6 1 2283.92 2356.56 33.96 o 4 6 1 1335.12 1318.61 23.87 o 5 6 1 1184.48 1144.42 16.38 o 6 6 1 226.43 226.16 4.18 o 7 6 1 207.23 196.32 3.74 o 8 6 1 39.75 38.03 1.07 o -9 7 1 0.04 1.27 0.69 o -8 7 1 0.05 0.35 0.76 o -7 7 1 0.02 -0.39 0.55 o -6 7 1 58.63 47.86 2.94 o -5 7 1 10.41 10.00 0.44 o -4 7 1 36.89 32.75 0.72 o -3 7 1 939.35 1001.35 14.50 o -2 7 1 96.15 80.70 1.34 o -1 7 1 778.05 763.83 10.44 o 0 7 1 1568.02 1560.27 24.67 o 1 7 1 1441.93 1467.63 18.33 o 2 7 1 951.21 894.78 13.03 o 3 7 1 372.02 352.86 4.56 o 4 7 1 201.39 199.71 3.05 o 5 7 1 31.25 27.90 3.28 o 6 7 1 42.81 48.89 1.06 o 7 7 1 877.88 878.38 17.85 o 8 7 1 403.32 423.04 13.78 o -8 8 1 21.90 17.94 0.81 o -7 8 1 21.25 20.42 0.87 o -6 8 1 6.64 3.06 1.38 o -5 8 1 381.69 354.88 6.15 o -4 8 1 448.98 453.13 7.30 o -3 8 1 50.57 44.62 1.50 o -2 8 1 383.18 395.06 5.97 o -1 8 1 31.22 27.05 0.59 o 0 8 1 0.49 3.03 0.54 o 1 8 1 129.93 135.56 2.21 o 2 8 1 129.13 125.02 1.90 o 3 8 1 686.21 678.09 9.37 o 4 8 1 1082.53 1049.49 15.30 o 5 8 1 1312.52 1267.13 23.76 o 6 8 1 978.57 999.88 20.78 o 7 8 1 214.07 235.56 5.24 o -8 9 1 34.62 32.83 1.30 o -7 9 1 11.14 13.55 0.69 o -6 9 1 168.71 143.61 3.24 o -5 9 1 199.47 187.37 7.58 o -4 9 1 3.61 3.92 0.76 o -3 9 1 4.16 1.43 0.80 o -2 9 1 275.20 256.22 4.54 o -1 9 1 1029.78 1050.62 18.07 o 0 9 1 81.11 81.34 1.18 o 1 9 1 1472.64 1534.38 20.03 o 2 9 1 208.24 213.79 3.23 o 3 9 1 220.47 240.18 5.16 o 4 9 1 49.89 48.03 0.98 o 5 9 1 190.85 183.83 3.56 o 6 9 1 133.15 139.06 2.88 o 7 9 1 431.25 443.76 13.80 o -7 10 1 34.56 38.21 1.19 o -6 10 1 55.73 51.47 1.32 o -5 10 1 1.64 2.03 0.41 o -4 10 1 14.81 14.55 0.50 o -3 10 1 0.05 0.17 0.90 o -2 10 1 61.49 55.71 1.95 o -1 10 1 55.37 50.55 0.80 o 0 10 1 2.58 3.91 0.27 o 1 10 1 714.63 720.88 9.84 o 2 10 1 277.23 268.10 4.35 o 3 10 1 617.58 624.04 10.59 o 4 10 1 344.13 343.58 5.75 o 5 10 1 378.81 378.18 7.97 o 6 10 1 56.70 51.80 1.28 o -6 11 1 146.29 141.69 4.18 o -5 11 1 28.59 33.29 1.02 o -4 11 1 1079.36 1112.01 25.21 o -3 11 1 388.03 402.66 10.59 o -2 11 1 37.58 37.12 1.98 o -1 11 1 329.74 337.05 12.75 o 0 11 1 160.97 161.71 5.14 o 1 11 1 37.16 37.23 2.50 o 2 11 1 39.71 37.56 0.76 o 3 11 1 21.21 17.41 0.48 o 4 11 1 69.42 68.79 1.38 o 5 11 1 10.75 6.44 0.60 o -5 12 1 53.61 56.94 1.86 o -4 12 1 17.43 11.89 1.03 o -3 12 1 26.40 28.07 0.91 o -2 12 1 62.66 61.16 5.43 o -1 12 1 1560.12 1630.14 30.44 o 0 12 1 369.83 373.45 18.59 o 1 12 1 38.61 39.98 2.83 o 2 12 1 6.96 9.16 0.46 o 3 12 1 45.48 44.34 1.20 o 4 12 1 16.34 19.03 1.29 o 5 12 1 110.35 94.16 5.27 o -4 13 1 253.35 260.18 9.53 o -3 13 1 133.75 139.35 2.65 o -2 13 1 237.29 243.36 5.69 o -1 13 1 57.31 58.70 1.67 o 0 13 1 44.92 42.00 1.10 o 1 13 1 12.78 10.42 0.54 o 2 13 1 530.47 538.95 11.69 o 3 13 1 145.14 142.58 3.29 o -3 14 1 79.79 77.08 2.34 o -2 14 1 273.76 269.24 9.62 o -1 14 1 3.27 2.90 0.62 o 0 14 1 297.89 288.04 8.40 o 1 14 1 0.65 1.10 0.68 o 2 14 1 146.97 138.76 4.74 o -10 0 2 857.61 912.41 46.02 o -8 0 2 3017.18 3182.09 115.16 o -7 0 2 1351.82 1361.08 48.09 o -6 0 2 872.97 820.87 31.77 o -5 0 2 960.76 976.29 25.40 o -4 0 2 98.84 104.24 3.76 o -3 0 2 1851.07 1768.91 49.35 o 0 0 2 3207.56 3106.46 86.62 o 1 0 2 1202.54 1275.73 28.17 o 2 0 2 966.63 1039.33 17.56 o 3 0 2 268.84 314.64 5.01 o 4 0 2 222.66 234.47 4.20 o 5 0 2 29.08 28.46 0.74 o 6 0 2 213.87 205.35 4.80 o 7 0 2 9.63 7.80 0.81 o 8 0 2 226.44 224.05 6.23 o -10 1 2 1245.50 1311.57 40.89 o -9 1 2 20.72 21.31 0.88 o -8 1 2 18.68 20.10 1.15 o -7 1 2 346.12 335.32 9.72 o -6 1 2 232.10 203.42 4.18 o -5 1 2 2664.34 2575.13 46.67 o -4 1 2 639.49 581.43 11.83 o -3 1 2 1247.40 1228.76 23.51 o -1 1 2 2234.09 2105.00 55.66 o 0 1 2 2014.87 1988.40 30.18 o 1 1 2 2847.34 2777.23 43.02 o 2 1 2 105.74 100.20 1.27 o 3 1 2 0.81 1.03 0.31 o 4 1 2 501.58 509.61 6.35 o 5 1 2 0.08 2.79 1.06 o 6 1 2 356.50 329.86 5.19 o 7 1 2 0.51 0.62 1.32 o 8 1 2 1.83 2.33 0.82 o -10 2 2 179.51 186.00 4.45 o -9 2 2 1137.99 1177.91 26.72 o -8 2 2 255.15 242.33 4.78 o -7 2 2 580.14 551.78 11.29 o -6 2 2 2241.17 2225.09 40.20 o -5 2 2 851.24 818.77 14.22 o -4 2 2 1268.15 1274.81 26.25 o -3 2 2 349.87 348.98 7.08 o -2 2 2 794.99 786.23 17.46 o -1 2 2 701.66 650.04 23.83 o 0 2 2 2562.07 2486.06 46.49 o 1 2 2 990.49 1023.69 13.46 o 2 2 2 648.24 660.52 9.64 o 3 2 2 62.18 78.78 2.07 o 4 2 2 919.33 984.68 14.52 o 5 2 2 37.48 35.04 1.19 o 6 2 2 9.75 8.82 0.87 o 7 2 2 71.75 78.82 2.20 o 8 2 2 265.88 279.31 8.16 o -10 3 2 9.09 10.81 2.77 o -9 3 2 400.10 413.25 8.97 o -8 3 2 254.23 251.63 4.81 o -7 3 2 13.36 10.11 0.70 o -6 3 2 37.22 44.67 1.02 o -5 3 2 506.50 564.80 10.06 o -4 3 2 8.22 32.14 2.17 o -3 3 2 37.32 42.50 1.77 o -2 3 2 4725.16 4715.63 116.85 o -1 3 2 2118.29 2056.61 64.84 o 0 3 2 2375.66 2294.31 34.45 o 1 3 2 2137.97 2099.68 27.74 o 2 3 2 1475.04 1451.70 21.19 o 3 3 2 2.08 3.49 1.17 o 4 3 2 221.87 212.77 3.05 o 5 3 2 417.70 429.79 6.77 o 6 3 2 157.61 175.66 3.02 o 7 3 2 75.37 82.23 2.94 o 8 3 2 263.50 256.43 6.13 o -10 4 2 55.40 57.47 2.00 o -9 4 2 137.25 136.84 3.63 o -8 4 2 206.39 207.14 4.28 o -7 4 2 27.73 24.77 1.33 o -6 4 2 337.40 340.72 4.97 o -5 4 2 1428.94 1352.90 25.30 o -4 4 2 313.13 274.52 7.03 o -3 4 2 230.83 191.76 6.50 o -2 4 2 150.47 134.89 2.73 o -1 4 2 454.34 465.41 11.62 o 0 4 2 0.65 0.60 0.46 o 1 4 2 17.41 19.17 2.13 o 2 4 2 89.33 100.85 2.43 o 3 4 2 5029.49 4850.77 78.06 o 4 4 2 1031.32 994.53 14.21 o 5 4 2 1060.77 1052.90 18.32 o 6 4 2 604.50 586.10 9.77 o 7 4 2 585.59 583.47 15.15 o 8 4 2 17.75 17.92 0.85 o -10 5 2 1.82 4.26 1.12 o -9 5 2 182.14 182.65 5.13 o -8 5 2 0.07 -0.49 0.55 o -7 5 2 575.00 585.83 9.56 o -6 5 2 231.66 229.68 3.32 o -5 5 2 777.21 780.47 15.91 o -4 5 2 227.22 250.61 4.26 o -3 5 2 196.32 221.08 5.63 o -2 5 2 2.71 2.90 0.46 o -1 5 2 2518.29 2541.93 47.08 o 0 5 2 2858.96 2809.10 66.53 o 1 5 2 3017.36 2970.00 49.03 o 2 5 2 25.32 50.05 0.76 o 3 5 2 2827.25 2820.08 38.83 o 4 5 2 327.47 303.61 4.47 o 5 5 2 7.34 4.36 0.95 o 6 5 2 392.28 394.58 7.34 o 7 5 2 554.77 583.19 12.58 o 8 5 2 217.55 233.41 6.14 o -9 6 2 13.46 16.44 0.79 o -8 6 2 175.73 181.47 3.93 o -7 6 2 0.30 3.11 0.80 o -6 6 2 56.69 55.49 1.06 o -5 6 2 391.75 388.43 6.46 o -4 6 2 674.63 648.96 10.97 o -3 6 2 1508.82 1498.87 21.70 o -2 6 2 3099.85 3241.10 56.01 o -1 6 2 257.21 230.62 6.40 o 0 6 2 1569.94 1575.24 25.08 o 1 6 2 708.63 696.98 10.64 o 2 6 2 1457.45 1457.11 17.89 o 3 6 2 458.25 445.90 5.54 o 4 6 2 856.34 833.69 11.14 o 5 6 2 186.68 184.10 3.15 o 6 6 2 116.04 116.96 2.11 o 7 6 2 32.64 31.90 1.06 o -9 7 2 24.69 20.95 1.30 o -8 7 2 1.49 2.80 0.66 o -7 7 2 2.40 2.30 0.60 o -6 7 2 15.85 17.15 0.51 o -5 7 2 115.24 112.07 3.33 o -4 7 2 935.54 969.81 15.31 o -3 7 2 13.77 24.39 0.85 o -2 7 2 0.00 0.64 0.66 o -1 7 2 987.28 1034.24 13.60 o 0 7 2 17.47 18.68 0.48 o 1 7 2 471.23 466.84 6.12 o 2 7 2 4.49 7.73 0.31 o 3 7 2 116.80 117.22 1.79 o 4 7 2 6.87 8.43 0.94 o 5 7 2 44.14 43.41 1.25 o 6 7 2 0.20 0.88 0.43 o 7 7 2 82.24 66.97 1.58 o -9 8 2 20.61 20.53 0.95 o -8 8 2 13.92 13.89 0.71 o -7 8 2 27.18 23.70 0.91 o -6 8 2 3.90 4.92 1.12 o -5 8 2 0.99 3.72 0.31 o -4 8 2 29.37 27.02 1.96 o -3 8 2 1095.15 1148.96 17.13 o -2 8 2 970.68 1004.56 15.21 o -1 8 2 49.07 58.25 0.86 o 0 8 2 74.25 77.24 1.16 o 1 8 2 80.97 80.74 1.15 o 2 8 2 195.96 205.02 5.60 o 3 8 2 11.16 14.31 1.43 o 4 8 2 0.22 0.91 1.31 o 5 8 2 14.32 14.24 2.10 o 6 8 2 20.39 22.88 1.71 o 7 8 2 46.54 45.10 1.55 o -8 9 2 114.05 112.66 2.79 o -7 9 2 111.06 112.51 4.67 o -6 9 2 378.74 357.84 14.19 o -5 9 2 100.63 97.38 3.94 o -4 9 2 255.26 249.61 7.71 o -3 9 2 212.75 225.02 3.53 o -2 9 2 1.08 4.02 0.58 o -1 9 2 119.65 121.33 1.78 o 0 9 2 1541.53 1576.41 22.09 o 1 9 2 989.98 971.47 14.64 o 2 9 2 436.08 421.12 8.04 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