data_2239486 _cell_angle_alpha 85.394 _cell_angle_beta 85.107 _cell_angle_gamma 82.659 _cell_length_a 7.8152 _cell_length_b 9.2949 _cell_length_c 17.5420 _exptl_crystal_F_000 632.00 _reflns_d_resolution_high 0.6500 _cod_data_source_file bh2490Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cher01' _shelx_refln_list_code 4 _shelx_f_calc_maximum 194.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3876.37 3546.34 81.65 o 4 0 0 181.91 149.39 24.21 o 5 0 0 324.92 353.50 42.34 o 6 0 0 1769.17 1649.47 102.28 o 7 0 0 671.41 737.63 75.76 o 8 0 0 210.88 186.63 41.11 o 9 0 0 128.78 131.26 36.84 o 10 0 0 111.54 107.20 25.84 o 11 0 0 45.57 57.80 20.41 o -11 1 0 192.15 228.62 42.79 o -10 1 0 162.62 140.93 24.39 o -9 1 0 719.53 722.66 61.30 o -8 1 0 337.35 321.15 42.46 o -7 1 0 0.04 4.25 16.70 o -6 1 0 1018.41 1037.04 83.16 o -5 1 0 1269.48 1299.74 85.52 o -4 1 0 2026.76 2057.37 94.36 o -3 1 0 12742.70 12736.48 327.77 o -2 1 0 21251.54 21312.67 266.87 o -1 1 0 12835.22 13036.06 795.83 o 1 1 0 10053.00 10310.40 200.16 o 2 1 0 2181.11 2361.39 60.43 o 3 1 0 703.02 575.37 39.15 o 4 1 0 7282.63 7069.83 165.22 o 5 1 0 2432.07 2584.11 112.72 o 6 1 0 16.28 4.22 6.86 o 7 1 0 303.94 302.41 47.51 o 8 1 0 661.15 723.13 78.76 o 9 1 0 149.54 165.58 40.35 o 10 1 0 119.56 114.01 34.85 o 11 1 0 8.20 15.19 165.82 o -11 2 0 12.89 27.76 19.34 o -10 2 0 7.23 5.81 8.20 o -9 2 0 36.14 35.69 13.62 o -8 2 0 399.41 390.00 43.49 o -7 2 0 1787.56 1844.92 86.49 o -6 2 0 57.25 61.43 12.40 o -5 2 0 328.21 331.84 29.97 o -4 2 0 900.46 825.58 50.75 o -3 2 0 1522.87 1676.90 63.09 o -2 2 0 4963.50 4781.61 78.50 o -1 2 0 170.41 200.25 16.26 o 1 2 0 3187.71 3004.42 133.69 o 2 2 0 15760.12 15935.44 353.64 o 3 2 0 41.15 66.55 11.83 o 4 2 0 205.23 255.84 29.47 o 5 2 0 3494.84 3705.75 128.39 o 6 2 0 1002.98 1047.55 76.37 o 7 2 0 32.51 70.61 21.89 o 8 2 0 164.40 172.29 37.08 o 9 2 0 187.89 206.47 39.72 o 10 2 0 13.79 0.20 15.14 o 11 2 0 72.59 73.51 41.92 o -11 3 0 199.02 217.47 56.69 o -10 3 0 103.90 111.56 30.27 o -9 3 0 32.59 34.70 16.51 o -8 3 0 44.25 47.80 14.70 o -7 3 0 501.91 560.58 47.04 o -6 3 0 1187.87 1163.60 62.17 o -5 3 0 1519.61 1492.53 63.96 o -4 3 0 1187.34 1235.44 64.58 o -3 3 0 7493.05 7573.30 125.49 o -2 3 0 15175.45 15103.63 144.32 o 0 3 0 20084.42 19460.20 668.93 o 2 3 0 48.14 42.52 19.56 o 3 3 0 5043.99 5050.20 249.83 o 5 3 0 64.75 77.67 16.19 o 6 3 0 2198.96 2202.80 98.53 o 7 3 0 936.31 917.56 70.50 o 8 3 0 235.96 237.76 37.67 o 9 3 0 434.17 468.87 112.33 o 10 3 0 53.29 77.22 48.94 o 11 3 0 5.55 -24.97 42.32 o -11 4 0 15.80 1.61 22.84 o -10 4 0 20.41 13.49 9.58 o -9 4 0 3.18 19.88 17.37 o -8 4 0 549.85 555.16 61.67 o -7 4 0 149.62 150.03 23.62 o -6 4 0 498.84 514.96 41.75 o -5 4 0 1948.23 2028.17 94.61 o -4 4 0 2575.90 2538.12 84.81 o -3 4 0 6484.27 6488.37 113.64 o -2 4 0 34096.54 33532.46 250.02 o -1 4 0 5813.74 5675.95 139.47 o 0 4 0 8602.21 8600.65 164.99 o 1 4 0 3617.00 3501.79 124.82 o 2 4 0 753.85 843.95 48.00 o 3 4 0 1094.72 1205.09 130.43 o 4 4 0 1590.21 1687.39 170.89 o 5 4 0 1827.96 1884.27 191.76 o 6 4 0 66.80 86.25 46.03 o 7 4 0 8.32 35.20 42.12 o 8 4 0 500.06 485.13 109.32 o 9 4 0 91.48 115.23 60.07 o 10 4 0 4.70 -19.86 40.01 o 11 4 0 245.98 206.39 80.93 o -10 5 0 3.12 25.98 15.64 o -9 5 0 2.55 22.14 20.06 o -8 5 0 259.52 245.55 39.68 o -7 5 0 2.19 6.91 5.81 o -6 5 0 627.82 658.73 47.47 o -5 5 0 2234.33 2238.94 105.08 o -4 5 0 716.81 726.18 48.02 o -3 5 0 2449.39 2460.79 109.74 o -2 5 0 4292.67 4158.52 85.64 o -1 5 0 825.92 877.53 56.00 o 0 5 0 1822.80 1966.36 87.46 o 1 5 0 1.55 8.84 9.43 o 2 5 0 11418.86 11262.91 212.60 o 3 5 0 2478.53 2483.68 202.16 o 4 5 0 1282.66 1364.87 159.22 o 5 5 0 1622.74 1793.88 190.74 o 6 5 0 120.53 116.13 55.76 o 7 5 0 15.67 23.57 4.31 o 8 5 0 563.52 581.92 126.78 o 9 5 0 6.24 30.49 22.46 o 10 5 0 77.69 35.70 30.39 o 11 5 0 7.32 -57.26 57.26 o -10 6 0 163.29 152.95 50.89 o -9 6 0 338.65 390.42 77.64 o -8 6 0 0.12 37.49 25.43 o -7 6 0 299.49 310.34 45.15 o -6 6 0 292.48 287.80 48.40 o -5 6 0 123.64 115.11 29.61 o -4 6 0 221.59 232.11 43.51 o -3 6 0 0.20 2.64 10.88 o -2 6 0 5133.86 5092.91 108.81 o -1 6 0 218.89 307.45 32.04 o 0 6 0 55.81 67.48 19.75 o 1 6 0 169.93 196.57 35.31 o 2 6 0 431.14 540.08 52.56 o 3 6 0 928.45 849.15 47.33 o 4 6 0 591.87 565.71 107.12 o 5 6 0 391.27 382.53 88.26 o 6 6 0 649.14 576.83 118.36 o 7 6 0 244.50 247.12 84.85 o 8 6 0 0.72 -47.23 58.87 o 9 6 0 0.25 -11.33 29.78 o 10 6 0 159.06 162.27 68.70 o 11 6 0 25.64 -22.66 26.58 o -9 7 0 52.19 58.77 41.22 o -8 7 0 4.00 34.70 57.46 o -7 7 0 73.11 117.43 73.31 o -6 7 0 126.11 36.60 18.95 o -5 7 0 1728.73 1809.71 151.74 o -4 7 0 2172.33 2232.18 165.83 o -3 7 0 1743.34 1715.23 109.28 o -2 7 0 4047.34 3974.08 106.65 o -1 7 0 2408.87 2307.66 96.92 o 0 7 0 7.67 0.51 8.53 o 1 7 0 1553.44 1534.92 89.33 o 2 7 0 254.11 284.56 41.67 o 3 7 0 15.76 14.22 8.79 o 4 7 0 1432.66 1523.23 186.30 o 5 7 0 392.78 377.51 97.29 o 6 7 0 409.94 333.88 89.86 o 7 7 0 366.88 336.48 92.07 o 8 7 0 328.37 274.20 84.14 o 9 7 0 38.85 40.21 12.54 o 10 7 0 10.35 -14.24 32.09 o 11 7 0 1.07 -45.63 45.63 o -8 8 0 30.01 41.22 77.32 o -7 8 0 63.24 94.77 70.50 o -6 8 0 181.06 193.36 108.31 o -5 8 0 903.43 830.04 111.27 o -4 8 0 3009.65 3055.47 209.69 o -3 8 0 326.45 330.77 49.89 o -2 8 0 2895.43 2841.18 97.51 o -1 8 0 10.78 9.74 12.03 o 0 8 0 1357.68 1377.81 81.97 o 1 8 0 733.64 782.01 61.26 o 2 8 0 410.42 449.48 56.88 o 3 8 0 2651.50 2864.45 117.63 o 4 8 0 3.66 -15.95 42.82 o 5 8 0 1154.84 1201.95 182.07 o 6 8 0 268.38 178.02 66.89 o 7 8 0 175.36 168.08 62.38 o 8 8 0 121.53 98.98 52.75 o 9 8 0 271.83 252.03 86.85 o 10 8 0 25.42 7.42 35.40 o -8 9 0 34.63 93.87 88.05 o -7 9 0 178.89 231.06 140.80 o -6 9 0 362.60 391.34 161.27 o -5 9 0 374.89 355.94 79.51 o -4 9 0 178.76 165.96 50.36 o -3 9 0 146.33 144.32 33.04 o -2 9 0 718.78 736.13 78.30 o -1 9 0 62.94 76.87 18.12 o 0 9 0 5828.73 5820.25 181.06 o 1 9 0 809.47 864.66 67.73 o 2 9 0 1205.62 1361.77 89.44 o 3 9 0 1219.86 1123.42 172.14 o 4 9 0 265.37 249.12 86.05 o 5 9 0 0.60 37.91 43.32 o 6 9 0 560.50 527.16 132.49 o 7 9 0 5.57 -21.86 48.94 o 8 9 0 0.20 -14.54 33.80 o 9 9 0 3.31 -38.81 45.73 o 10 9 0 9.64 10.63 33.80 o -7 10 0 19.51 56.86 74.51 o -6 10 0 44.48 123.95 111.12 o -5 10 0 15.14 15.21 28.18 o -4 10 0 355.13 368.20 80.40 o -3 10 0 58.65 47.69 24.76 o -2 10 0 53.44 43.29 10.57 o -1 10 0 87.84 89.75 24.14 o 0 10 0 234.61 278.87 40.65 o 1 10 0 111.94 89.67 22.50 o 2 10 0 172.51 158.50 29.07 o 3 10 0 43.80 45.43 48.24 o 4 10 0 460.35 527.55 121.46 o 5 10 0 193.13 214.02 81.74 o 6 10 0 1.06 19.25 10.13 o 7 10 0 57.43 108.31 61.78 o 8 10 0 31.89 52.95 15.24 o 9 10 0 32.27 -60.27 70.50 o -6 11 0 29.84 219.32 169.38 o -5 11 0 221.05 261.66 77.43 o -4 11 0 599.92 646.43 108.85 o -3 11 0 95.71 116.90 30.96 o -2 11 0 0.90 -6.10 6.10 o -1 11 0 278.64 281.28 51.45 o 0 11 0 399.23 435.34 53.87 o 1 11 0 21.76 23.18 16.87 o 2 11 0 67.33 43.09 20.89 o 3 11 0 10.26 6.09 37.08 o 4 11 0 231.76 210.61 81.64 o 5 11 0 73.36 70.40 51.95 o 6 11 0 241.23 134.59 67.39 o 7 11 0 50.26 56.26 45.63 o 8 11 0 8.85 -15.14 40.72 o -5 12 0 34.94 117.42 59.79 o -4 12 0 122.48 177.14 67.83 o -3 12 0 122.25 141.82 44.36 o -2 12 0 350.88 380.51 61.97 o -1 12 0 489.69 510.87 68.63 o 0 12 0 286.83 322.90 56.13 o 1 12 0 979.75 1053.67 106.51 o 2 12 0 97.88 82.55 24.50 o 3 12 0 801.40 870.37 110.38 o 4 12 0 130.23 158.31 47.48 o 5 12 0 319.01 208.28 86.70 o 6 12 0 173.57 202.18 89.16 o 7 12 0 92.21 99.78 66.79 o -3 13 0 101.83 150.74 46.35 o -2 13 0 957.79 1041.32 109.43 o -1 13 0 212.02 200.52 46.32 o 0 13 0 283.79 257.01 58.02 o 1 13 0 246.35 277.87 73.89 o 2 13 0 10.75 14.22 16.06 o 3 13 0 1.43 16.83 20.25 o 4 13 0 125.61 92.93 34.50 o 5 13 0 23.59 17.48 15.77 o 6 13 0 22.17 145.22 55.71 o 0 14 0 32.88 17.13 51.90 o 1 14 0 0.91 -7.65 24.95 o 2 14 0 55.21 31.29 36.25 o 3 14 0 17.13 41.72 27.38 o -3 -14 1 38.18 51.28 26.84 o -2 -14 1 5.84 44.75 27.14 o -1 -14 1 14.04 8.08 42.72 o 0 -14 1 28.19 2.27 21.76 o -6 -13 1 40.44 173.93 130.72 o -5 -13 1 121.33 129.57 36.37 o -4 -13 1 245.07 172.66 62.63 o -3 -13 1 84.62 82.21 37.27 o -2 -13 1 119.23 130.56 38.69 o -1 -13 1 44.95 16.25 10.88 o 0 -13 1 53.07 37.56 39.26 o 1 -13 1 42.96 39.07 31.08 o 2 -13 1 57.44 58.85 29.97 o 3 -13 1 46.88 96.46 50.38 o -7 -12 1 69.71 81.13 55.06 o -6 -12 1 1.43 51.85 53.75 o -5 -12 1 37.21 91.26 62.98 o -4 -12 1 183.83 198.54 54.58 o -3 -12 1 160.54 187.10 53.00 o -2 -12 1 122.71 123.87 25.32 o -1 -12 1 147.13 176.60 42.98 o 0 -12 1 434.60 481.96 57.83 o 1 -12 1 275.72 236.59 39.92 o 2 -12 1 31.24 2.34 13.75 o 3 -12 1 163.94 181.37 48.15 o 4 -12 1 42.52 94.99 51.08 o 5 -12 1 43.96 83.55 51.00 o -8 -11 1 169.11 146.32 83.44 o -7 -11 1 13.86 -20.06 20.56 o -6 -11 1 4.65 0.10 44.53 o -5 -11 1 156.45 163.77 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713.15 131.60 o -6 -4 1 17.89 26.27 19.15 o -5 -4 1 1027.40 1175.53 150.48 o -4 -4 1 4826.20 5177.53 302.60 o -3 -4 1 294.61 219.05 58.17 o -2 -4 1 488.76 540.36 84.06 o -1 -4 1 97.53 122.76 23.75 o 0 -4 1 3630.27 3572.85 109.05 o 1 -4 1 129.93 164.17 21.68 o 2 -4 1 1890.13 2145.90 58.27 o 3 -4 1 1795.74 1750.56 44.75 o 4 -4 1 218.15 181.80 21.65 o 5 -4 1 488.22 487.90 44.90 o 6 -4 1 4142.86 4243.52 118.59 o 7 -4 1 152.29 145.88 23.95 o 8 -4 1 452.32 438.95 52.65 o 9 -4 1 823.29 845.64 77.32 o 10 -4 1 18.56 38.30 26.11 o 11 -4 1 7.87 -7.60 24.85 o -11 -3 1 4.98 -12.33 36.90 o -10 -3 1 10.29 11.13 27.38 o -9 -3 1 61.29 35.00 20.96 o -8 -3 1 71.07 77.67 22.92 o -7 -3 1 866.51 952.41 73.93 o -6 -3 1 15.85 40.92 14.67 o -5 -3 1 34.91 28.76 9.56 o -4 -3 1 824.12 956.33 121.79 o -3 -3 1 9648.82 9088.10 349.62 o -2 -3 1 6140.69 5902.63 256.65 o -1 -3 1 4330.39 4194.93 198.74 o 0 -3 1 35447.33 34683.52 1507.45 o 1 -3 1 6692.65 7077.47 372.87 o 2 -3 1 774.65 780.16 25.01 o 3 -3 1 6263.45 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