data_2239505 _cell_angle_alpha 90.000 _cell_angle_beta 129.898 _cell_angle_gamma 90.000 _cell_length_a 11.6359 _cell_length_b 13.2501 _cell_length_c 17.7412 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.7233 _[local]_cod_data_source_file tk5309Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' rodolfo_c4s in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 427.05 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4566.87 5339.76 79.38 o 3 0 0 864.87 656.48 15.59 o 4 0 0 2099.05 2278.52 45.43 o 5 0 0 3202.34 3305.05 90.09 o 6 0 0 295.03 275.57 23.85 o 7 0 0 776.55 872.37 46.81 o 8 0 0 722.93 774.79 33.39 o 9 0 0 140.37 210.36 27.41 o 10 0 0 861.14 915.44 40.89 o 11 0 0 16.54 -14.05 14.05 o 2 1 0 670.48 519.15 7.67 o 3 1 0 150.46 250.25 6.66 o 4 1 0 16.95 41.85 4.58 o 5 1 0 456.65 437.52 15.69 o 6 1 0 597.62 595.63 20.28 o 7 1 0 2786.61 2777.65 52.95 o 8 1 0 249.12 257.32 19.75 o 9 1 0 73.87 72.03 9.37 o 10 1 0 194.18 188.35 15.83 o 11 1 0 667.87 729.56 55.23 o 1 2 0 125.75 143.39 6.93 o 2 2 0 30.12 16.97 2.20 o 3 2 0 754.35 764.92 11.30 o 4 2 0 3391.03 3653.22 40.68 o 5 2 0 646.23 703.16 20.16 o 6 2 0 7.87 7.31 4.95 o 7 2 0 113.39 127.04 10.46 o 8 2 0 525.19 466.81 34.54 o 9 2 0 194.69 168.53 13.60 o 10 2 0 281.92 295.84 27.66 o 12 2 0 5.00 17.38 15.75 o 1 3 0 556.37 499.97 11.33 o 2 3 0 1979.75 2265.42 22.78 o 3 3 0 740.79 787.33 15.44 o 4 3 0 184.94 251.41 8.20 o 5 3 0 821.57 795.89 26.54 o 6 3 0 144.69 144.84 10.17 o 7 3 0 1587.89 1545.59 37.50 o 8 3 0 938.22 869.48 28.79 o 9 3 0 151.45 154.24 13.44 o 10 3 0 174.11 216.12 32.52 o 11 3 0 4.08 -16.92 16.92 o 0 4 0 182370.44 176002.81 2159.07 o 1 4 0 123.93 163.24 12.07 o 2 4 0 320.55 251.57 9.46 o 3 4 0 0.23 8.63 4.22 o 4 4 0 268.47 239.32 8.65 o 5 4 0 1427.35 1498.26 26.49 o 6 4 0 114.43 129.87 23.41 o 7 4 0 223.92 231.37 21.20 o 8 4 0 420.31 426.32 23.95 o 9 4 0 22.67 50.77 18.66 o 10 4 0 71.01 64.90 20.53 o 11 4 0 63.05 44.39 18.10 o 1 5 0 182.16 171.71 6.43 o 2 5 0 279.13 263.86 14.49 o 3 5 0 311.16 262.19 7.96 o 4 5 0 189.90 218.56 8.43 o 5 5 0 150.65 148.13 7.70 o 6 5 0 479.04 430.43 20.35 o 7 5 0 2482.33 2391.88 105.44 o 8 5 0 278.62 254.17 18.53 o 9 5 0 58.07 86.78 22.94 o 10 5 0 189.06 154.11 30.41 o 11 5 0 494.59 545.43 53.50 o 0 6 0 908.81 871.50 23.60 o 1 6 0 637.19 681.79 16.30 o 2 6 0 271.02 195.91 8.17 o 3 6 0 347.79 336.57 10.51 o 4 6 0 4862.16 5379.93 86.92 o 5 6 0 2301.81 2277.60 34.69 o 6 6 0 24.20 30.82 7.85 o 7 6 0 140.61 163.04 14.13 o 8 6 0 2332.38 2119.04 94.40 o 9 6 0 62.35 35.20 15.88 o 10 6 0 463.99 555.51 52.30 o 11 6 0 16.06 4.05 15.82 o 1 7 0 119.48 90.76 12.49 o 2 7 0 1091.37 1094.65 22.57 o 3 7 0 228.38 217.23 8.10 o 4 7 0 253.35 324.73 12.78 o 5 7 0 328.63 360.71 11.73 o 6 7 0 205.88 208.17 12.05 o 7 7 0 224.34 240.19 31.28 o 8 7 0 171.69 188.31 29.43 o 9 7 0 48.37 81.29 22.56 o 10 7 0 8.31 16.87 17.36 o 0 8 0 441.84 430.02 27.10 o 1 8 0 3322.88 3232.65 49.41 o 2 8 0 1363.20 1384.44 27.66 o 3 8 0 333.88 381.40 11.35 o 4 8 0 109.26 103.22 10.24 o 5 8 0 30.56 48.17 6.25 o 6 8 0 1058.09 1066.99 41.91 o 7 8 0 2.95 -11.17 13.35 o 8 8 0 48.05 55.49 19.56 o 9 8 0 0.63 17.89 15.55 o 10 8 0 109.96 104.68 26.87 o 1 9 0 1024.47 986.52 30.57 o 2 9 0 331.36 307.15 12.41 o 3 9 0 0.82 4.04 2.88 o 4 9 0 41.65 42.66 7.11 o 5 9 0 94.52 111.44 9.00 o 6 9 0 155.77 146.16 38.39 o 7 9 0 1342.99 1382.20 77.32 o 8 9 0 777.93 752.49 58.94 o 9 9 0 66.25 84.42 21.06 o 0 10 0 1570.33 1591.72 60.51 o 1 10 0 502.04 477.70 24.60 o 2 10 0 45.02 33.54 7.92 o 3 10 0 9.00 3.43 3.74 o 4 10 0 25.63 30.99 5.53 o 5 10 0 155.87 132.02 15.26 o 6 10 0 207.12 243.55 22.49 o 7 10 0 152.17 168.77 24.08 o 8 10 0 893.17 896.17 66.18 o 9 10 0 280.95 408.41 47.18 o 1 11 0 574.59 555.97 24.72 o 2 11 0 33.24 37.32 14.10 o 3 11 0 0.54 -1.96 4.02 o 4 11 0 618.56 699.75 32.08 o 5 11 0 4.27 7.67 7.71 o 6 11 0 18.16 32.83 10.61 o 7 11 0 189.52 230.18 36.03 o 8 11 0 40.41 56.05 20.93 o 0 12 0 1558.70 1541.10 64.26 o 1 12 0 781.97 805.62 31.61 o 2 12 0 18.06 15.83 6.49 o 3 12 0 145.33 141.76 14.61 o 4 12 0 343.94 382.71 24.76 o 5 12 0 20.35 16.04 10.57 o 6 12 0 203.63 236.69 32.00 o 7 12 0 12.72 17.06 20.57 o 8 12 0 0.13 -11.85 18.38 o 1 13 0 45.37 46.35 9.89 o 2 13 0 86.11 80.81 10.47 o 3 13 0 0.35 8.06 14.95 o 4 13 0 2.34 6.92 8.93 o 5 13 0 0.76 8.90 10.33 o 6 13 0 86.85 71.79 13.88 o 7 13 0 229.14 308.35 42.43 o 0 14 0 1566.16 1624.00 71.10 o 1 14 0 15.84 35.67 19.40 o 2 14 0 12.14 -3.38 13.67 o 3 14 0 0.18 12.72 11.02 o 4 14 0 429.30 409.04 41.90 o 5 14 0 232.31 221.97 33.27 o 6 14 0 382.98 512.07 51.25 o 1 15 0 195.54 142.89 22.78 o 2 15 0 119.72 115.67 22.21 o 3 15 0 64.16 94.94 21.30 o 4 15 0 613.50 577.60 51.49 o 5 15 0 115.17 106.30 25.94 o 1 16 0 47.86 41.60 14.81 o 2 16 0 186.87 105.92 23.93 o 3 16 0 64.61 68.49 19.36 o 4 16 0 196.83 180.53 31.37 o 2 17 0 22.53 23.50 11.69 o 3 17 0 197.91 224.58 32.40 o -12 1 1 88.05 103.88 21.68 o -11 1 1 113.86 107.99 10.95 o -10 1 1 213.90 242.08 17.02 o -9 1 1 209.61 205.91 18.65 o -8 1 1 524.24 487.15 20.95 o -7 1 1 57.82 52.20 7.55 o -6 1 1 462.65 475.71 17.31 o -5 1 1 366.10 342.32 12.56 o -4 1 1 92.84 92.32 5.25 o -3 1 1 178.14 215.29 5.53 o -2 1 1 2723.29 2725.14 23.96 o 1 1 1 4830.60 4938.78 39.92 o 2 1 1 1793.88 1723.15 16.61 o 3 1 1 485.75 462.88 9.84 o 4 1 1 28.73 10.19 4.77 o 5 1 1 274.86 242.17 15.19 o 6 1 1 261.74 252.56 17.07 o 7 1 1 992.30 929.02 28.71 o 8 1 1 717.73 617.94 34.76 o 9 1 1 108.20 73.53 10.07 o 10 1 1 43.51 72.62 28.13 o 11 1 1 139.05 134.18 24.36 o -11 2 1 204.65 263.33 23.83 o -10 2 1 412.17 474.31 22.99 o -9 2 1 964.66 833.90 29.08 o -8 2 1 457.33 483.85 26.36 o -7 2 1 1357.20 1259.41 40.88 o -6 2 1 3.85 1.56 6.15 o -5 2 1 7836.44 8288.54 88.21 o -4 2 1 786.06 798.76 15.44 o -3 2 1 160.33 173.10 5.65 o -2 2 1 7394.23 6915.05 56.17 o -1 2 1 5.94 10.52 3.61 o 0 2 1 66.22 53.47 3.73 o 1 2 1 26048.89 25896.88 267.06 o 2 2 1 5470.54 5385.42 51.31 o 3 2 1 23883.90 24392.27 183.77 o 4 2 1 536.85 667.22 16.57 o 5 2 1 1020.86 963.78 25.13 o 6 2 1 514.74 495.35 19.08 o 7 2 1 2105.12 1944.62 43.69 o 8 2 1 504.58 451.81 21.15 o 9 2 1 153.39 165.84 14.65 o 10 2 1 391.17 356.76 35.45 o 11 2 1 58.22 81.78 21.49 o -12 3 1 1.36 -4.69 13.59 o -11 3 1 143.08 172.28 20.24 o -10 3 1 921.71 980.48 43.22 o -9 3 1 0.53 -1.72 5.93 o -8 3 1 796.22 733.76 25.44 o -7 3 1 49.74 44.35 8.29 o -6 3 1 203.19 203.02 11.34 o -5 3 1 2817.10 2806.26 39.50 o -4 3 1 259.84 276.92 7.83 o -3 3 1 303.12 261.48 5.56 o -2 3 1 3066.30 3233.54 37.97 o -1 3 1 458.55 455.41 8.26 o 0 3 1 0.76 5.59 2.48 o 1 3 1 7860.43 8047.55 80.89 o 2 3 1 1396.49 1241.65 25.95 o 3 3 1 1416.19 1550.81 22.06 o 4 3 1 1253.19 1247.48 23.40 o 5 3 1 2214.01 2161.23 36.10 o 6 3 1 58.34 65.67 12.43 o 7 3 1 2708.22 2592.60 51.97 o 8 3 1 66.00 86.32 10.14 o 9 3 1 90.86 106.30 11.37 o 10 3 1 65.49 49.93 20.06 o -12 4 1 0.39 12.92 18.37 o -11 4 1 420.73 457.95 46.61 o -10 4 1 155.81 176.50 29.55 o -9 4 1 50.24 44.46 7.88 o -8 4 1 68.57 66.32 8.38 o -7 4 1 1884.95 1837.47 39.87 o -6 4 1 547.72 531.20 14.83 o -5 4 1 10.90 28.77 5.54 o -4 4 1 1524.49 1608.23 23.39 o -3 4 1 2996.31 3059.88 41.66 o -2 4 1 3243.72 3656.80 41.46 o -1 4 1 73167.13 74413.57 650.24 o 0 4 1 53451.35 53937.78 472.16 o 1 4 1 614.39 608.32 12.19 o 2 4 1 851.94 860.12 22.59 o 3 4 1 340.69 281.27 11.41 o 4 4 1 1590.33 1738.55 28.85 o 5 4 1 347.44 270.17 13.67 o 6 4 1 0.68 -4.65 10.20 o 7 4 1 41.91 59.09 10.18 o 8 4 1 237.68 277.48 20.27 o 9 4 1 49.63 40.92 17.84 o 10 4 1 556.26 556.77 51.84 o 11 4 1 234.27 271.36 40.39 o -12 5 1 170.37 175.54 32.62 o -11 5 1 4.52 19.46 16.12 o -10 5 1 74.24 67.91 20.61 o -9 5 1 1595.06 1617.36 81.06 o -8 5 1 92.45 97.86 11.54 o -7 5 1 0.30 12.81 6.46 o -6 5 1 1446.56 1451.53 28.69 o -5 5 1 851.79 888.18 17.61 o -4 5 1 0.80 1.19 2.46 o -3 5 1 309.69 277.49 8.62 o -2 5 1 3464.82 3577.20 45.33 o -1 5 1 206.43 237.79 7.47 o 0 5 1 1789.73 1762.21 31.02 o 1 5 1 265.62 179.04 6.88 o 2 5 1 6.38 8.90 4.28 o 3 5 1 836.89 835.18 17.09 o 4 5 1 1632.19 1650.84 28.15 o 5 5 1 994.28 1049.09 27.71 o 6 5 1 95.32 78.81 20.01 o 7 5 1 4.39 2.89 13.00 o 8 5 1 140.90 142.49 14.99 o 9 5 1 254.66 232.39 32.81 o 10 5 1 120.09 98.06 24.65 o 11 5 1 0.07 -1.03 17.05 o -11 6 1 2.09 35.81 19.34 o -10 6 1 2.51 19.97 16.45 o -9 6 1 0.31 22.19 17.88 o -8 6 1 55.78 71.99 20.02 o -7 6 1 101.52 115.19 16.20 o -6 6 1 702.46 713.95 18.15 o -5 6 1 920.80 958.22 23.10 o -4 6 1 508.28 520.76 13.95 o -3 6 1 508.47 467.25 10.24 o -2 6 1 455.41 484.13 12.39 o -1 6 1 19.34 28.39 3.55 o 0 6 1 728.16 773.58 16.36 o 1 6 1 3670.75 3796.30 52.49 o 2 6 1 3380.60 3251.38 46.91 o 3 6 1 0.25 6.31 3.36 o 4 6 1 2826.93 2733.65 56.87 o 5 6 1 927.55 928.13 26.36 o 6 6 1 47.37 73.07 8.85 o 7 6 1 90.27 80.75 10.83 o 8 6 1 22.73 0.57 12.41 o 9 6 1 943.04 969.10 67.06 o 10 6 1 84.64 89.18 26.33 o -11 7 1 6.34 52.17 22.49 o -10 7 1 242.58 190.39 31.90 o -9 7 1 260.82 297.69 37.50 o -8 7 1 123.59 123.80 25.22 o -7 7 1 37.66 33.67 16.64 o -6 7 1 375.29 366.02 13.97 o -5 7 1 629.42 633.85 13.85 o -4 7 1 51.11 64.71 5.67 o -3 7 1 301.71 272.33 8.31 o -2 7 1 3080.14 3213.55 46.90 o -1 7 1 427.11 401.90 13.10 o 0 7 1 597.98 668.06 18.12 o 1 7 1 0.87 4.93 3.58 o 2 7 1 60.11 60.79 7.68 o 3 7 1 1714.24 1753.46 28.28 o 4 7 1 23.41 37.10 5.87 o 5 7 1 143.33 155.12 13.16 o 6 7 1 143.04 154.95 14.49 o 7 7 1 2121.99 1975.27 91.15 o 8 7 1 114.17 113.37 23.52 o 9 7 1 407.25 380.86 43.21 o 10 7 1 26.38 36.47 22.37 o -10 8 1 8.90 2.28 15.15 o -9 8 1 26.26 36.21 18.55 o -8 8 1 1.07 -6.22 11.43 o -7 8 1 544.22 533.63 44.48 o -6 8 1 126.94 131.27 15.35 o -5 8 1 307.03 310.93 12.63 o -4 8 1 0.91 4.38 2.53 o -3 8 1 1029.47 980.68 18.43 o -2 8 1 64.16 78.44 5.90 o -1 8 1 11412.01 12330.46 201.02 o 0 8 1 4134.33 4247.46 75.32 o 1 8 1 83.57 84.84 6.92 o 2 8 1 2095.99 2150.08 37.87 o 3 8 1 121.63 133.92 7.32 o 4 8 1 957.29 925.14 19.98 o 5 8 1 417.10 422.99 17.33 o 6 8 1 0.21 9.61 9.05 o 7 8 1 3.10 19.63 11.15 o 8 8 1 258.97 305.78 38.94 o 9 8 1 327.11 373.19 44.50 o -10 9 1 158.86 145.65 30.82 o -9 9 1 352.59 366.00 43.31 o -8 9 1 93.38 102.00 22.30 o -7 9 1 31.27 37.31 17.19 o -6 9 1 167.87 184.25 17.65 o -5 9 1 749.03 763.15 21.11 o -4 9 1 19.50 11.42 4.78 o -3 9 1 907.98 913.47 18.63 o -2 9 1 238.61 237.71 12.76 o -1 9 1 171.44 171.94 12.55 o 0 9 1 236.45 218.20 14.21 o 1 9 1 16.20 17.38 6.80 o 2 9 1 38.65 42.03 5.17 o 3 9 1 0.38 1.06 2.95 o 4 9 1 192.99 206.98 12.43 o 5 9 1 303.87 281.06 25.69 o 6 9 1 5.18 2.18 11.27 o 7 9 1 330.38 335.44 26.47 o 8 9 1 1.89 -9.22 15.59 o 9 9 1 72.58 89.23 25.40 o -9 10 1 116.68 115.86 25.72 o -8 10 1 94.61 62.48 20.24 o -7 10 1 283.27 249.63 34.54 o -6 10 1 1109.95 1158.20 44.54 o -5 10 1 367.60 392.84 30.14 o -4 10 1 55.34 76.23 7.02 o -3 10 1 870.05 844.34 23.09 o -2 10 1 2.57 12.81 6.87 o -1 10 1 148.28 176.95 13.38 o 0 10 1 549.12 571.61 39.19 o 1 10 1 79.84 76.92 8.66 o 2 10 1 487.87 475.36 27.49 o 3 10 1 1314.99 1304.60 32.05 o 4 10 1 3249.69 3355.76 72.91 o 5 10 1 18.34 34.38 10.29 o 6 10 1 53.61 39.85 13.12 o 7 10 1 596.24 640.81 37.14 o 8 10 1 315.20 308.27 40.56 o -9 11 1 172.88 238.30 37.57 o -8 11 1 258.30 287.67 38.71 o -7 11 1 1.31 -15.14 16.63 o -6 11 1 7.63 5.52 19.73 o -5 11 1 73.56 71.09 19.54 o -4 11 1 103.44 125.59 13.82 o -3 11 1 39.30 46.50 6.41 o -2 11 1 430.78 428.11 24.69 o -1 11 1 751.12 739.45 28.68 o 0 11 1 199.71 195.54 15.13 o 1 11 1 179.66 192.53 14.78 o 2 11 1 141.90 121.15 12.13 o 3 11 1 475.09 471.77 18.87 o 4 11 1 16.19 9.25 8.12 o 5 11 1 271.94 272.65 22.33 o 6 11 1 643.78 632.53 35.73 o 7 11 1 749.36 764.39 41.58 o 8 11 1 0.47 24.39 20.62 o -8 12 1 29.57 51.05 22.91 o -7 12 1 7.40 -10.84 16.03 o -6 12 1 768.66 842.16 39.58 o -5 12 1 337.96 346.96 42.11 o -4 12 1 117.23 95.97 12.27 o -3 12 1 331.58 321.90 20.19 o -2 12 1 25.29 23.31 6.39 o -1 12 1 138.43 118.38 12.60 o 0 12 1 488.58 467.81 23.99 o 1 12 1 15.09 12.29 6.37 o 2 12 1 2840.35 3000.15 150.12 o 3 12 1 32.01 33.33 8.79 o 4 12 1 581.25 630.46 40.32 o 5 12 1 45.21 46.68 35.88 o 6 12 1 0.04 7.53 12.80 o 7 12 1 150.19 154.01 19.81 o -7 13 1 110.08 175.49 32.63 o -6 13 1 91.61 86.06 13.22 o -5 13 1 55.47 56.57 11.73 o -4 13 1 161.38 155.36 23.94 o -3 13 1 30.18 23.63 7.17 o -2 13 1 94.93 87.82 16.63 o -1 13 1 0.33 -0.74 6.79 o 0 13 1 107.30 105.14 14.21 o 1 13 1 176.64 200.12 17.01 o 2 13 1 248.08 250.09 18.51 o 3 13 1 0.98 -5.11 7.69 o 4 13 1 36.85 50.71 11.76 o 5 13 1 183.35 180.59 19.49 o 6 13 1 41.19 79.82 15.03 o 7 13 1 312.08 304.59 37.24 o -7 14 1 31.42 39.30 20.46 o -6 14 1 44.85 61.71 19.92 o -5 14 1 205.74 223.93 32.95 o -4 14 1 24.77 -7.54 14.50 o -3 14 1 66.40 57.84 17.93 o -2 14 1 241.81 230.45 28.77 o -1 14 1 180.23 174.46 16.54 o 0 14 1 4.47 5.57 6.63 o 1 14 1 0.28 -8.18 8.18 o 2 14 1 1.44 0.74 11.52 o 3 14 1 265.23 240.47 20.51 o 4 14 1 98.90 123.17 16.55 o 5 14 1 6.43 3.56 8.96 o 6 14 1 29.98 31.89 12.76 o -6 15 1 0.02 -6.38 14.05 o -5 15 1 272.10 308.26 39.72 o -4 15 1 5.39 1.92 13.09 o -3 15 1 35.62 16.45 12.64 o -2 15 1 0.20 -10.60 10.60 o -1 15 1 193.65 195.85 27.57 o 0 15 1 222.02 211.55 18.72 o 1 15 1 66.73 48.95 15.49 o 2 15 1 8.33 9.24 11.66 o 3 15 1 2.36 -11.17 12.92 o 4 15 1 10.42 -2.45 14.29 o 5 15 1 63.24 94.22 26.39 o -5 16 1 243.86 213.41 34.85 o -4 16 1 0.19 -12.21 12.21 o -3 16 1 95.13 70.09 19.84 o -2 16 1 3.96 18.70 13.83 o -1 16 1 397.99 421.26 39.36 o 1 16 1 92.93 73.68 18.61 o 2 16 1 364.33 390.36 40.19 o 3 16 1 16.36 31.12 19.40 o 4 16 1 128.97 164.58 30.04 o -4 17 1 58.14 29.39 16.93 o -3 17 1 2.70 30.80 15.40 o -2 17 1 122.87 171.61 29.71 o 2 17 1 74.33 55.77 18.98 o 3 17 1 21.93 23.08 19.39 o -12 0 2 684.55 756.83 58.83 o -11 0 2 253.06 340.67 25.11 o -10 0 2 612.34 632.61 32.60 o -9 0 2 435.41 488.68 36.31 o -8 0 2 5409.67 5074.27 135.23 o -7 0 2 4090.54 4236.64 113.18 o -6 0 2 881.66 969.59 41.17 o -5 0 2 2129.67 2276.78 44.94 o -4 0 2 3453.02 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432.07 428.32 43.97 o -11 3 22 55.95 74.45 20.87 o -10 3 22 3.95 -9.51 9.51 o -9 3 22 230.68 285.22 33.84 o -8 3 22 35.57 24.29 9.99 o -7 3 22 87.61 101.64 46.61 o -6 3 22 14.39 45.48 21.50 o -14 4 22 51.23 53.83 18.83 o -13 4 22 318.08 291.33 39.26 o -12 4 22 54.58 83.77 21.17 o -11 4 22 56.37 105.54 25.65 o -10 4 22 36.45 38.98 12.52 o -9 4 22 7.81 3.58 11.82 o -8 4 22 45.25 33.25 12.40 o -7 4 22 13.54 12.82 18.16 o -6 4 22 1.59 9.60 19.02 o -12 5 22 103.07 152.34 30.35 o -11 5 22 166.14 142.99 27.73 o -10 5 22 8.12 3.78 14.50 o -9 5 22 30.00 53.31 19.32 o -8 5 22 442.71 487.38 49.18 o -7 5 22 324.87 413.43 48.84 o -6 5 22 4.56 23.36 20.09 o -8 6 22 370.25 421.69 46.39 o -7 6 22 550.87 683.30 60.82 o -7 7 22 40.88 51.82 20.20 o -12 1 23 0.95 5.96 11.42 o -11 1 23 162.19 173.67 23.53 o -10 1 23 10.12 7.26 11.06 o -9 1 23 19.32 9.09 20.65 o -8 1 23 162.66 196.03 35.91 o -13 2 23 0.15 1.57 13.89 o -12 2 23 342.41 329.58 40.01 o -11 2 23 60.89 49.10 14.48 o -10 2 23 46.57 50.92 20.33 o 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