#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:54:21 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181895 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/95/2239555.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2239555 _cell_angle_alpha 90.000 _cell_angle_beta 93.043 _cell_angle_gamma 90.000 _cell_length_a 9.2547 _cell_length_b 19.3814 _cell_length_c 19.4249 _exptl_crystal_F_000 1520.00 _reflns_d_resolution_high 0.6877 _cod_data_source_file lh5703Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pc002 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 472.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2588.52 3170.97 91.73 o 4 0 0 3468.81 4286.64 133.88 o 6 0 0 18.04 7.44 19.83 o 8 0 0 17.27 32.23 29.75 o 10 0 0 25.53 57.02 37.19 o 12 0 0 2060.64 2330.50 146.28 o 1 1 0 28597.25 24534.76 577.67 o 2 1 0 9070.14 10127.84 318.58 o 3 1 0 1036.26 1145.58 34.93 o 4 1 0 2338.96 2209.07 57.85 o 5 1 0 7421.56 7370.43 151.23 o 6 1 0 36302.04 36206.60 629.36 o 7 1 0 129.50 148.76 32.23 o 8 1 0 9928.19 9455.90 204.19 o 9 1 0 308.02 302.79 38.57 o 10 1 0 2682.16 2323.59 90.17 o 11 1 0 91.36 121.03 68.18 o 12 1 0 2199.07 2248.68 100.70 o 1 2 0 2297.74 2593.83 376.85 o 2 2 0 32994.99 37379.69 718.99 o 3 2 0 8855.90 8982.36 233.05 o 4 2 0 24462.43 25841.33 632.21 o 5 2 0 91.87 126.44 24.79 o 6 2 0 2283.39 2179.30 78.10 o 7 2 0 1795.85 1832.04 171.07 o 8 2 0 30.06 23.71 20.10 o 9 2 0 8.76 -4.17 21.86 o 10 2 0 2134.14 2040.43 121.48 o 11 2 0 4.64 8.99 27.89 o 12 2 0 2214.05 2563.56 156.19 o 13 2 0 103.09 104.13 61.98 o 1 3 0 3458.04 3943.60 62.46 o 2 3 0 72814.55 79716.50 1078.23 o 3 3 0 787.72 792.10 60.74 o 4 3 0 20544.42 20093.37 354.97 o 5 3 0 4515.82 4562.03 105.96 o 6 3 0 3233.21 3048.04 97.93 o 7 3 0 565.43 572.79 81.82 o 8 3 0 5768.86 5361.03 293.79 o 9 3 0 1771.52 1733.99 74.37 o 10 3 0 1821.04 1826.88 81.39 o 11 3 0 565.30 344.62 69.42 o 12 3 0 250.72 322.30 76.86 o 13 3 0 56.17 114.05 59.50 o 0 4 0 2377.19 2453.30 56.10 o 1 4 0 60313.99 65566.20 906.08 o 2 4 0 17537.65 19215.98 271.47 o 3 4 0 9.74 18.90 6.87 o 4 4 0 55558.52 58236.49 802.01 o 5 4 0 2968.23 2937.12 119.00 o 6 4 0 2651.23 2549.59 76.12 o 7 4 0 494.11 510.79 40.95 o 8 4 0 1074.93 1080.20 68.18 o 9 4 0 1991.16 2017.11 81.39 o 10 4 0 954.43 985.98 67.77 o 11 4 0 779.33 833.34 130.16 o 12 4 0 365.06 575.19 91.73 o 13 4 0 18.12 -49.59 49.59 o 1 5 0 15096.21 15582.82 249.06 o 2 5 0 15789.55 16531.76 236.64 o 3 5 0 279.98 380.73 27.14 o 4 5 0 6980.12 6943.29 138.50 o 5 5 0 2187.75 2229.48 52.70 o 6 5 0 2028.77 2134.00 84.00 o 7 5 0 3209.05 3064.07 83.05 o 8 5 0 12535.74 12088.98 209.23 o 9 5 0 137.90 132.83 32.48 o 10 5 0 14329.33 13470.46 289.01 o 11 5 0 85.26 153.71 57.02 o 12 5 0 1994.64 2037.95 148.76 o 13 5 0 34.28 37.19 57.02 o 0 6 0 68667.22 71259.10 1194.62 o 1 6 0 867.81 745.80 21.47 o 2 6 0 42948.38 45131.79 622.63 o 3 6 0 8474.24 9486.44 147.77 o 4 6 0 6081.28 5947.36 103.34 o 5 6 0 4392.08 4872.49 91.86 o 6 6 0 208.72 175.29 22.62 o 7 6 0 3631.15 3643.67 82.32 o 8 6 0 2463.94 2279.08 88.39 o 9 6 0 983.16 932.09 58.99 o 10 6 0 35.25 61.71 31.55 o 11 6 0 232.94 304.95 71.90 o 12 6 0 40.11 71.90 57.02 o 13 6 0 250.71 225.61 74.38 o 1 7 0 8249.38 8134.65 113.07 o 2 7 0 2136.91 2410.09 51.37 o 3 7 0 6453.58 7258.14 127.07 o 4 7 0 9472.52 9762.74 156.29 o 5 7 0 259.96 274.12 21.51 o 6 7 0 10509.41 10250.92 171.55 o 7 7 0 10020.44 9780.39 169.51 o 8 7 0 6880.93 6827.93 133.83 o 9 7 0 58.46 38.18 24.75 o 10 7 0 6474.80 6616.35 175.66 o 11 7 0 2252.34 2451.99 156.19 o 12 7 0 1383.88 1279.30 131.40 o 0 8 0 48874.80 49811.85 849.34 o 1 8 0 338.92 351.08 21.47 o 2 8 0 9701.98 9067.82 144.47 o 3 8 0 11.44 37.87 10.91 o 4 8 0 2046.87 2086.69 70.91 o 5 8 0 14942.31 15582.01 240.75 o 6 8 0 4006.21 4240.18 127.54 o 7 8 0 66.37 129.93 20.05 o 8 8 0 2621.37 2714.77 74.81 o 9 8 0 2038.14 2137.84 87.48 o 10 8 0 2497.60 2737.10 158.67 o 11 8 0 213.51 188.42 61.98 o 12 8 0 4735.24 5308.10 250.41 o 1 9 0 1324.98 1369.89 34.87 o 2 9 0 285.66 271.31 19.94 o 3 9 0 1601.48 1900.17 57.60 o 4 9 0 13656.71 13529.72 320.91 o 5 9 0 454.24 519.10 30.02 o 6 9 0 25627.44 25077.49 374.83 o 7 9 0 829.09 769.53 43.60 o 8 9 0 1110.81 1172.75 64.91 o 9 9 0 386.01 347.49 45.18 o 10 9 0 15.48 19.83 49.59 o 11 9 0 128.29 203.30 69.42 o 12 9 0 1082.83 1053.69 128.92 o 0 10 0 3816.43 3133.57 121.48 o 1 10 0 881.42 949.11 29.92 o 2 10 0 31896.41 33195.55 474.73 o 3 10 0 296.65 295.68 22.06 o 4 10 0 2975.85 2943.38 67.25 o 5 10 0 2143.59 2193.19 58.60 o 6 10 0 1813.46 1823.84 70.92 o 7 10 0 718.92 671.17 39.46 o 8 10 0 3164.81 3246.88 108.72 o 9 10 0 5122.57 5446.93 233.05 o 10 10 0 1354.74 1306.57 133.88 o 11 10 0 1119.09 1405.74 141.32 o 12 10 0 4148.75 4980.83 252.88 o 1 11 0 55.94 66.77 12.30 o 2 11 0 966.48 965.56 44.15 o 3 11 0 7046.14 7038.48 126.24 o 4 11 0 2009.32 1936.22 97.57 o 5 11 0 29.11 36.80 15.66 o 6 11 0 7478.67 7518.23 165.64 o 7 11 0 4260.77 4259.09 368.17 o 8 11 0 8158.41 7890.19 389.24 o 9 11 0 487.81 609.90 91.73 o 10 11 0 4577.10 4750.26 230.57 o 11 11 0 983.05 999.14 123.96 o 0 12 0 20876.99 20024.02 392.96 o 1 12 0 1732.59 1678.77 43.88 o 2 12 0 17915.09 17643.35 272.37 o 3 12 0 2075.32 2065.84 56.81 o 4 12 0 4548.19 4824.59 99.65 o 5 12 0 95.29 107.70 19.43 o 6 12 0 94.85 110.40 20.60 o 7 12 0 187.12 151.07 31.55 o 8 12 0 853.72 1082.52 68.30 o 9 12 0 2902.87 3287.50 185.94 o 10 12 0 146.53 240.49 74.38 o 11 12 0 559.41 726.42 111.57 o 1 13 0 758.84 793.09 42.23 o 2 13 0 3513.91 3289.97 76.87 o 3 13 0 2696.93 2620.70 67.75 o 4 13 0 1029.74 990.25 42.36 o 5 13 0 2720.95 2737.23 72.27 o 6 13 0 170.47 199.95 33.88 o 7 13 0 557.96 712.82 86.77 o 8 13 0 12866.45 13050.83 426.43 o 9 13 0 456.77 476.02 89.25 o 10 13 0 8337.16 8236.10 332.22 o 11 13 0 277.59 411.56 96.69 o 0 14 0 724.34 789.84 48.00 o 1 14 0 1.30 14.92 15.73 o 2 14 0 5874.13 5688.80 113.75 o 3 14 0 2272.90 1975.93 94.66 o 4 14 0 15693.81 15502.08 252.04 o 5 14 0 5560.68 5950.13 123.05 o 6 14 0 2551.13 2495.83 92.80 o 7 14 0 310.36 350.04 63.22 o 8 14 0 1264.51 1802.42 141.32 o 9 14 0 398.40 485.94 94.21 o 10 14 0 241.30 141.32 76.86 o 11 14 0 24.61 4.96 64.46 o 1 15 0 9328.43 8419.09 134.75 o 2 15 0 11771.95 11051.93 231.85 o 3 15 0 1288.17 1139.62 47.19 o 4 15 0 7818.33 7775.25 148.35 o 5 15 0 3.86 -20.17 20.17 o 6 15 0 5796.53 6032.88 163.07 o 7 15 0 759.07 932.20 111.57 o 8 15 0 659.17 783.45 106.61 o 9 15 0 226.98 277.68 79.34 o 10 15 0 1224.69 1529.70 166.11 o 0 16 0 10418.74 9168.15 206.78 o 1 16 0 3278.02 3232.68 72.73 o 2 16 0 5595.09 5566.84 153.90 o 3 16 0 2336.81 2228.69 78.27 o 4 16 0 2097.35 2282.81 69.77 o 5 16 0 2802.78 2798.57 102.72 o 6 16 0 4048.72 4014.66 129.54 o 7 16 0 913.69 1120.63 123.96 o 8 16 0 483.77 560.31 104.13 o 9 16 0 1021.39 1105.75 131.40 o 10 16 0 1274.98 1353.68 158.67 o 1 17 0 5273.33 4904.70 96.23 o 2 17 0 740.11 597.74 56.16 o 3 17 0 81.71 99.87 22.54 o 4 17 0 3376.29 3198.96 135.12 o 5 17 0 550.26 638.07 58.91 o 6 17 0 7141.44 7254.32 290.07 o 7 17 0 141.76 76.86 54.54 o 8 17 0 3050.04 3344.52 203.30 o 9 17 0 67.19 193.38 74.38 o 0 18 0 23318.49 22242.46 433.01 o 1 18 0 1024.85 1069.49 63.33 o 2 18 0 11187.67 10674.87 225.76 o 3 18 0 21.65 8.78 18.87 o 4 18 0 46.78 40.29 26.60 o 5 18 0 5.79 -3.90 39.67 o 6 18 0 227.09 223.13 66.94 o 7 18 0 1515.50 1842.09 166.11 o 8 18 0 77.65 66.94 64.46 o 9 18 0 581.80 696.67 121.48 o 1 19 0 222.66 287.80 42.03 o 2 19 0 574.35 639.76 45.07 o 3 19 0 1722.45 1614.06 80.83 o 4 19 0 558.50 453.27 90.49 o 5 19 0 3884.42 3909.79 205.78 o 6 19 0 3388.36 3723.85 210.74 o 7 19 0 35.22 123.96 71.90 o 8 19 0 5150.61 5818.82 282.64 o 9 19 0 363.09 565.27 114.05 o 0 20 0 3698.70 3554.39 119.06 o 1 20 0 3899.76 3776.35 133.92 o 2 20 0 3106.31 2956.59 88.59 o 3 20 0 6199.97 5599.62 164.54 o 4 20 0 2205.76 2098.16 98.11 o 5 20 0 466.57 505.77 96.69 o 6 20 0 2019.19 2018.12 163.63 o 7 20 0 19.21 -2.48 59.50 o 8 20 0 29.51 -7.44 59.50 o 1 21 0 23.28 65.22 25.26 o 2 21 0 5671.60 5314.91 160.06 o 3 21 0 3386.81 3424.42 218.17 o 4 21 0 6535.55 6352.90 250.41 o 5 21 0 805.70 676.84 109.09 o 6 21 0 832.24 922.28 131.40 o 7 21 0 46.30 49.59 69.42 o 0 22 0 145.22 166.11 54.54 o 1 22 0 693.87 675.30 79.34 o 2 22 0 2357.64 2368.87 105.79 o 3 22 0 121.32 107.43 38.03 o 4 22 0 6178.55 6743.59 292.55 o 5 22 0 71.94 168.59 74.38 o 6 22 0 1324.59 1242.11 151.23 o 7 22 0 825.45 860.30 136.36 o 1 23 0 6748.00 6716.22 189.24 o 2 23 0 1316.24 1363.02 87.48 o 3 23 0 6.15 61.98 49.59 o 4 23 0 828.32 597.50 99.17 o 5 23 0 308.22 220.65 81.82 o 6 23 0 712.22 803.28 128.92 o 0 24 0 4796.05 5104.80 230.57 o 1 24 0 354.82 404.24 59.50 o 2 24 0 4068.36 3926.48 242.97 o 3 24 0 91.16 71.90 57.02 o 4 24 0 444.37 416.52 94.21 o 5 24 0 1333.44 1033.85 131.40 o 1 25 0 809.39 761.18 91.73 o 2 25 0 55.61 2.48 49.59 o 3 25 0 720.92 885.10 114.05 o 4 25 0 523.15 540.48 106.61 o 5 25 0 20.63 -29.75 59.50 o 0 26 0 4625.84 4276.72 215.70 o 1 26 0 261.75 256.75 49.09 o 2 26 0 1998.28 2613.14 176.03 o 3 26 0 787.70 877.66 121.48 o 4 26 0 77.50 86.77 71.90 o 1 27 0 78.55 44.63 54.54 o 2 27 0 120.71 161.15 69.42 o -11 0 1 3994.54 3808.14 173.55 o -9 0 1 6394.27 6079.15 213.22 o -5 0 1 15111.26 14811.10 384.29 o -3 0 1 1903.79 2055.31 69.42 o -1 0 1 15645.90 17000.29 399.16 o 3 0 1 3.66 4.96 12.40 o 5 0 1 20272.91 18829.98 480.98 o 7 0 1 24846.87 22987.70 597.50 o 11 0 1 1985.73 1842.09 123.96 o 13 0 1 1820.22 1579.29 156.19 o -12 1 1 35.43 74.38 49.59 o -11 1 1 2143.74 1949.73 138.84 o -10 1 1 6.49 23.55 30.99 o -9 1 1 431.55 392.45 70.66 o -8 1 1 1182.06 1268.58 57.85 o -7 1 1 628.69 546.79 38.45 o -6 1 1 1089.67 1112.36 90.49 o -5 1 1 2551.84 3061.89 109.09 o -4 1 1 5576.44 5950.23 168.59 o -3 1 1 10232.04 11260.80 282.64 o -2 1 1 20371.37 22310.38 375.15 o -1 1 1 63301.91 68204.45 1611.52 o 1 1 1 48672.22 43763.72 3940.78 o 2 1 1 21613.72 22807.12 386.56 o 3 1 1 137.05 138.00 24.79 o 4 1 1 2150.39 2229.87 60.46 o 5 1 1 415.47 378.09 28.05 o 6 1 1 3343.89 3313.71 91.73 o 7 1 1 3187.41 3191.27 92.03 o 8 1 1 15.57 49.59 32.23 o 9 1 1 275.10 234.86 34.15 o 10 1 1 48.04 66.94 42.15 o 11 1 1 2163.24 1968.45 90.27 o 12 1 1 9.32 -7.17 32.11 o 13 1 1 3051.58 3624.68 198.34 o -12 2 1 84.91 76.86 54.54 o -11 2 1 709.63 606.12 56.96 o -10 2 1 895.16 864.26 62.07 o -9 2 1 5464.97 5008.12 157.43 o -8 2 1 1410.34 1444.68 65.70 o -7 2 1 11124.95 10751.30 218.21 o -6 2 1 3032.22 3002.13 81.51 o -5 2 1 21471.30 21395.79 380.37 o -4 2 1 16283.82 17519.89 311.14 o -3 2 1 10059.44 10450.04 234.29 o -2 2 1 8713.04 9644.40 170.87 o -1 2 1 3650.35 3690.55 194.85 o 1 2 1 8.49 -10.50 10.50 o 2 2 1 1731.17 1987.77 48.19 o 3 2 1 7152.72 7077.83 161.15 o 4 2 1 36162.92 40037.33 680.20 o 5 2 1 25516.90 26089.04 460.17 o 6 2 1 71.61 69.31 20.10 o 7 2 1 11572.19 10698.01 309.91 o 8 2 1 937.10 970.37 53.45 o 9 2 1 2989.45 2845.57 98.13 o 10 2 1 112.18 116.73 31.41 o 11 2 1 3341.33 3136.26 166.11 o 12 2 1 35.94 -33.47 33.47 o 13 2 1 419.67 498.33 89.25 o -12 3 1 23.92 -4.96 42.15 o -11 3 1 1462.92 1443.06 77.88 o -10 3 1 2737.21 2570.99 138.84 o -9 3 1 1272.68 1138.91 60.31 o -8 3 1 183.34 133.30 26.12 o -7 3 1 2759.77 2593.14 111.57 o -6 3 1 1576.28 1398.84 52.51 o -5 3 1 16511.18 16523.29 301.47 o -4 3 1 495.61 528.99 27.13 o -3 3 1 31680.43 34032.05 471.83 o -2 3 1 19.50 37.19 7.74 o -1 3 1 3048.02 3427.90 56.22 o 0 3 1 1187.31 1205.78 21.56 o 1 3 1 1534.56 1635.97 28.63 o 2 3 1 12364.84 13233.44 189.87 o 3 3 1 62708.22 68362.11 1136.01 o 4 3 1 169.24 162.12 18.35 o 5 3 1 15436.39 15295.64 332.22 o 6 3 1 6252.38 6443.88 148.76 o 7 3 1 3133.10 2882.38 115.29 o 8 3 1 934.29 946.95 52.59 o 9 3 1 1392.29 1321.26 67.48 o 10 3 1 985.15 1091.68 71.81 o 11 3 1 1394.52 1356.16 123.96 o 12 3 1 366.76 379.33 52.24 o 13 3 1 975.24 1041.29 123.96 o -13 4 1 565.14 741.30 104.13 o -12 4 1 366.63 322.30 74.38 o -11 4 1 2755.88 2280.92 141.32 o -10 4 1 358.94 363.36 36.01 o -9 4 1 6186.49 6458.28 160.23 o -8 4 1 4.52 -7.66 19.05 o -7 4 1 4982.67 4406.72 112.82 o -6 4 1 4823.47 4844.32 114.58 o -5 4 1 6684.25 6671.83 140.92 o -4 4 1 287.56 434.75 21.51 o -3 4 1 35023.75 37500.62 519.52 o -2 4 1 3291.98 3588.63 61.42 o -1 4 1 15068.40 16338.76 281.18 o 0 4 1 1075.68 1247.28 34.71 o 1 4 1 22271.12 23752.11 287.24 o 2 4 1 6062.71 6732.06 103.45 o 3 4 1 49399.44 53973.72 739.54 o 4 4 1 26.48 93.37 17.27 o 5 4 1 4281.05 3891.87 96.37 o 6 4 1 1517.37 1422.80 56.02 o 7 4 1 2243.44 1976.59 70.85 o 8 4 1 953.23 795.38 54.35 o 9 4 1 11095.50 11321.72 247.11 o 10 4 1 262.35 166.76 35.70 o 11 4 1 3005.78 3064.22 115.55 o 12 4 1 302.98 275.20 71.90 o 13 4 1 4.61 -49.59 52.06 o -13 5 1 313.24 448.75 89.25 o -12 5 1 112.32 203.30 66.94 o -11 5 1 21.13 4.96 49.59 o -10 5 1 288.92 426.15 38.10 o -9 5 1 2399.25 2373.63 71.38 o -8 5 1 1358.47 1422.84 60.13 o -7 5 1 349.19 287.46 26.22 o -6 5 1 2055.08 2070.00 54.28 o -5 5 1 8604.64 8790.98 144.44 o -4 5 1 6019.20 6812.40 113.44 o -3 5 1 23329.20 23612.30 334.87 o -2 5 1 496.73 411.73 23.42 o -1 5 1 8515.34 9423.16 142.15 o 0 5 1 13495.73 14214.96 179.71 o 1 5 1 15455.22 16083.42 200.46 o 2 5 1 16920.88 17633.03 251.89 o 3 5 1 39160.66 42199.49 584.00 o 4 5 1 1595.94 1748.98 49.76 o 5 5 1 14157.31 14813.12 226.08 o 6 5 1 1071.90 1055.32 37.36 o 7 5 1 3488.79 3422.26 141.32 o 8 5 1 14.75 80.58 26.30 o 9 5 1 626.11 626.10 42.89 o 10 5 1 817.60 833.37 63.83 o 11 5 1 5.29 10.06 30.34 o 12 5 1 1217.67 1316.49 133.88 o 13 5 1 303.93 329.74 84.29 o -13 6 1 67.74 -9.92 59.50 o -12 6 1 1364.30 1375.99 133.88 o -11 6 1 6357.07 6041.96 250.41 o -10 6 1 0.41 9.92 42.15 o -9 6 1 17453.25 16951.22 276.59 o -8 6 1 1259.92 1098.34 46.58 o -7 6 1 6081.89 6284.57 144.42 o -6 6 1 707.24 736.12 49.04 o -5 6 1 2273.27 2436.87 57.02 o -4 6 1 2711.98 2643.44 57.02 o -3 6 1 6837.95 7062.13 149.29 o -2 6 1 1283.11 1455.88 35.07 o -1 6 1 7136.83 7153.25 113.96 o 0 6 1 10735.86 11151.15 146.24 o 1 6 1 17795.53 18816.50 234.84 o 2 6 1 967.33 1201.98 34.95 o 3 6 1 1096.37 981.34 28.67 o 4 6 1 1746.94 1811.33 66.38 o 5 6 1 3150.46 3197.12 67.96 o 6 6 1 572.92 553.91 29.87 o 7 6 1 9504.31 9532.59 192.29 o 8 6 1 2204.68 2246.52 100.58 o 9 6 1 11855.92 11811.11 258.47 o 10 6 1 421.41 383.90 48.71 o 11 6 1 3782.09 3754.40 132.92 o 12 6 1 1120.67 1321.45 136.36 o -12 7 1 35.70 27.27 57.02 o -11 7 1 562.67 545.44 89.25 o -10 7 1 2308.78 2266.04 141.32 o -9 7 1 812.86 830.16 96.33 o -8 7 1 89.84 114.14 21.51 o -7 7 1 436.75 403.59 30.52 o -6 7 1 6224.00 5734.52 109.34 o -5 7 1 511.95 583.19 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