data_2239557 _cell_angle_alpha 90.000 _cell_angle_beta 121.875 _cell_angle_gamma 90.000 _cell_length_a 12.8657 _cell_length_b 26.2810 _cell_length_c 13.9710 _exptl_crystal_F_000 1768.00 _reflns_d_resolution_high 0.7453 _[local]_cod_data_source_file hb7222Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' cus in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 411.04 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4441.14 4506.31 129.35 o 3 0 0 2021.19 2935.27 564.32 o 4 0 0 6769.97 6423.39 489.27 o 5 0 0 8349.61 8035.24 736.91 o 6 0 0 223.93 499.97 225.33 o 7 0 0 6620.39 6284.17 377.27 o 8 0 0 2561.25 2359.22 302.70 o 9 0 0 828.71 824.30 333.72 o 10 0 0 92.46 437.87 446.13 o 11 0 0 2347.46 1968.73 589.08 o 12 0 0 1159.42 1135.76 538.43 o 2 1 0 537.44 668.28 76.26 o 3 1 0 350.58 541.57 86.78 o 4 1 0 2807.28 2896.73 180.67 o 5 1 0 3393.09 3183.22 104.09 o 6 1 0 3107.74 2903.75 120.89 o 7 1 0 2808.61 3171.57 191.84 o 8 1 0 2080.88 2284.46 230.62 o 9 1 0 982.99 886.61 246.09 o 10 1 0 1510.62 1473.53 272.60 o 11 1 0 967.01 858.29 327.84 o 12 1 0 74.39 495.65 487.77 o 2 2 0 5132.11 5141.17 103.18 o 3 2 0 14834.95 14731.89 402.22 o 4 2 0 697.63 791.20 101.47 o 5 2 0 108.96 331.49 100.60 o 6 2 0 115.26 280.34 111.59 o 7 2 0 690.57 681.29 230.73 o 8 2 0 79.88 700.81 256.20 o 9 2 0 56.74 429.89 265.22 o 10 2 0 374.55 329.29 262.82 o 11 2 0 358.26 192.67 301.13 o 12 2 0 334.84 306.17 574.82 o 13 2 0 361.51 603.34 789.44 o 1 3 0 6867.50 6299.41 153.84 o 2 3 0 1145.68 1150.44 86.81 o 3 3 0 1009.70 1397.01 108.74 o 4 3 0 9.35 350.36 96.94 o 5 3 0 8277.21 8424.45 160.20 o 6 3 0 9056.81 8863.27 171.46 o 7 3 0 412.77 508.31 175.60 o 8 3 0 281.96 650.14 232.14 o 9 3 0 1480.90 1665.43 309.65 o 10 3 0 582.58 604.12 311.66 o 11 3 0 467.87 695.07 362.61 o 12 3 0 251.29 595.29 419.34 o 13 3 0 594.57 1303.86 776.31 o 1 4 0 1590.95 1655.45 90.26 o 2 4 0 1989.56 7384.38 3060.28 o 3 4 0 16486.23 15926.82 597.95 o 4 4 0 11583.88 11338.32 158.51 o 5 4 0 9960.50 9664.93 349.71 o 6 4 0 570.48 874.91 145.19 o 7 4 0 7346.10 7715.21 268.67 o 8 4 0 3055.34 2788.37 267.69 o 9 4 0 238.98 448.68 232.84 o 10 4 0 905.01 721.15 279.46 o 11 4 0 2837.80 2702.15 492.01 o 12 4 0 3059.17 4017.92 598.47 o 13 4 0 3.75 589.36 498.00 o 1 5 0 30354.80 29105.23 456.32 o 2 5 0 4292.32 4229.28 106.71 o 3 5 0 7017.10 6469.13 189.50 o 4 5 0 2507.28 2659.97 159.07 o 5 5 0 2252.36 2534.57 180.89 o 6 5 0 4168.47 4261.83 159.23 o 7 5 0 2312.21 2228.65 232.88 o 8 5 0 108.74 359.22 220.20 o 9 5 0 7.53 283.79 232.08 o 10 5 0 616.66 836.25 439.56 o 11 5 0 1453.38 1353.63 419.61 o 12 5 0 6321.57 6891.81 578.07 o 13 5 0 2294.70 2613.41 562.86 o 14 5 0 5.80 373.33 584.58 o 0 6 0 2593.30 2808.75 187.79 o 1 6 0 7380.68 7482.63 118.02 o 2 6 0 913.71 1104.18 100.79 o 3 6 0 10837.51 10667.05 480.70 o 4 6 0 442.37 556.27 108.16 o 5 6 0 3256.23 3283.33 154.13 o 6 6 0 241.09 477.55 148.64 o 7 6 0 658.76 921.27 216.85 o 8 6 0 3749.78 3391.68 275.13 o 9 6 0 385.73 681.35 258.95 o 10 6 0 103.47 449.14 343.84 o 11 6 0 23.67 393.30 417.94 o 12 6 0 471.15 275.36 392.72 o 13 6 0 1598.16 1491.66 503.52 o 14 6 0 43.93 313.54 500.40 o 1 7 0 12403.17 11406.74 151.81 o 2 7 0 2553.51 2305.00 103.23 o 3 7 0 1333.50 1414.34 117.72 o 4 7 0 2.82 324.73 83.49 o 5 7 0 6459.51 6764.62 171.61 o 6 7 0 28796.52 27939.34 513.21 o 7 7 0 1237.54 1108.51 188.94 o 8 7 0 2094.87 2665.62 279.69 o 9 7 0 691.17 916.98 341.23 o 10 7 0 1514.16 1610.46 435.02 o 11 7 0 1776.15 1671.49 412.53 o 12 7 0 88.05 325.86 473.92 o 13 7 0 226.12 711.49 546.68 o 14 7 0 218.04 646.33 512.82 o 0 8 0 4688.62 5254.33 194.24 o 1 8 0 14902.87 15240.53 394.38 o 2 8 0 37.50 1284.00 380.95 o 3 8 0 4429.41 4610.62 218.73 o 4 8 0 2540.45 2875.40 104.83 o 5 8 0 19.13 249.35 87.31 o 6 8 0 1955.40 1772.42 174.70 o 7 8 0 11241.16 11180.59 237.04 o 8 8 0 8.57 345.87 217.37 o 9 8 0 200.97 193.30 288.00 o 10 8 0 3110.42 3538.56 431.93 o 11 8 0 2229.66 2367.17 508.38 o 12 8 0 1535.09 1958.04 557.04 o 13 8 0 492.55 488.73 422.83 o 14 8 0 1405.58 1182.03 590.96 o 1 9 0 6203.24 6453.14 130.01 o 2 9 0 3604.09 3877.58 112.21 o 3 9 0 1039.56 1224.59 131.38 o 4 9 0 1442.80 1581.32 144.49 o 5 9 0 1720.78 1620.74 118.80 o 6 9 0 384.12 382.86 187.03 o 7 9 0 1127.61 1254.92 178.18 o 8 9 0 2503.48 2024.36 308.74 o 9 9 0 7766.94 8188.64 485.85 o 10 9 0 439.88 599.66 372.28 o 11 9 0 499.44 608.73 386.82 o 12 9 0 702.40 1181.69 470.39 o 13 9 0 267.05 810.77 517.58 o 0 10 0 11223.14 11150.06 222.85 o 1 10 0 4027.56 4352.15 149.69 o 2 10 0 52.15 441.38 88.95 o 3 10 0 3.43 246.86 131.33 o 4 10 0 80.88 458.32 118.70 o 5 10 0 266.15 443.72 109.90 o 6 10 0 366.12 496.96 151.94 o 7 10 0 16.31 373.64 208.05 o 8 10 0 459.43 509.75 301.12 o 9 10 0 5.02 650.56 373.87 o 10 10 0 449.26 476.69 413.29 o 11 10 0 7.61 250.12 421.73 o 12 10 0 53.49 150.49 441.80 o 13 10 0 36.36 657.22 559.19 o 1 11 0 11943.53 12582.60 325.52 o 2 11 0 15124.14 14525.16 1622.11 o 3 11 0 5197.07 5822.42 156.00 o 4 11 0 3881.74 3956.49 153.11 o 5 11 0 5175.52 4612.57 160.49 o 6 11 0 15079.67 15501.34 331.35 o 7 11 0 2930.58 2708.63 506.49 o 8 11 0 3879.75 4020.89 405.57 o 9 11 0 4260.22 4623.94 472.62 o 10 11 0 936.98 681.52 464.58 o 11 11 0 263.59 430.01 448.51 o 12 11 0 1064.33 1230.16 532.48 o 13 11 0 3977.23 3654.94 668.71 o 0 12 0 3856.12 4919.03 304.14 o 1 12 0 1534.94 1502.41 82.15 o 2 12 0 3664.16 3293.57 106.03 o 3 12 0 1890.41 2014.82 137.17 o 4 12 0 2914.56 3241.56 183.16 o 5 12 0 80.05 293.33 140.27 o 6 12 0 1534.56 1750.69 254.92 o 7 12 0 3454.09 3650.67 281.00 o 8 12 0 1012.24 1048.71 298.56 o 9 12 0 1116.03 1391.24 486.38 o 10 12 0 3304.31 3725.69 445.57 o 11 12 0 2012.37 2540.37 599.05 o 12 12 0 791.53 880.00 561.88 o 13 12 0 542.28 781.54 617.26 o 1 13 0 14435.42 15051.85 563.80 o 2 13 0 6055.71 5721.07 172.19 o 3 13 0 6305.27 6095.28 218.56 o 4 13 0 163.88 339.64 114.97 o 5 13 0 1624.98 1346.72 170.75 o 6 13 0 1797.99 2044.27 268.10 o 7 13 0 1202.75 1547.90 285.21 o 8 13 0 48.30 543.98 352.50 o 9 13 0 324.37 443.71 290.28 o 10 13 0 23.56 544.77 436.21 o 11 13 0 4.76 132.48 401.93 o 12 13 0 20.15 143.60 442.48 o 13 13 0 1.48 368.94 513.32 o 0 14 0 1845.46 1942.34 124.59 o 1 14 0 3449.09 3742.73 103.42 o 2 14 0 838.35 1000.94 109.21 o 3 14 0 203.52 458.05 127.34 o 4 14 0 6.79 192.95 115.72 o 5 14 0 2134.32 2033.95 258.89 o 6 14 0 1019.88 1282.00 340.60 o 7 14 0 2884.77 2107.31 282.48 o 8 14 0 104.99 54.14 261.92 o 9 14 0 41.07 395.96 366.93 o 10 14 0 12.47 257.44 420.65 o 11 14 0 284.00 714.64 512.06 o 12 14 0 1175.39 1278.85 693.76 o 13 14 0 3.17 50.28 674.25 o 1 15 0 16489.12 15720.61 414.19 o 2 15 0 394.09 643.08 143.04 o 3 15 0 3.50 480.61 164.28 o 4 15 0 570.82 608.09 178.38 o 5 15 0 1971.76 2233.41 262.95 o 6 15 0 8141.83 7533.47 334.03 o 7 15 0 25.68 185.92 237.73 o 8 15 0 8495.66 8334.98 363.73 o 9 15 0 374.55 549.13 365.26 o 10 15 0 3172.81 3039.40 531.34 o 11 15 0 491.26 303.62 421.33 o 12 15 0 1196.93 1465.68 538.40 o 13 15 0 1281.62 1884.68 802.95 o 0 16 0 7038.72 6773.68 289.00 o 1 16 0 165.66 376.50 164.17 o 2 16 0 1298.45 1675.40 215.30 o 3 16 0 663.25 598.12 182.78 o 4 16 0 3743.20 3697.80 254.41 o 5 16 0 31.35 422.99 242.58 o 6 16 0 2074.72 2019.82 350.24 o 7 16 0 1442.06 1303.63 294.87 o 8 16 0 20.52 -94.07 279.58 o 9 16 0 43.62 349.55 395.59 o 10 16 0 106.49 311.72 436.88 o 11 16 0 1063.73 744.38 505.74 o 12 16 0 57.07 181.14 495.59 o 1 17 0 11985.13 11476.32 253.13 o 2 17 0 6388.53 6573.38 268.06 o 3 17 0 5664.16 5346.86 252.59 o 4 17 0 49.66 312.35 183.86 o 5 17 0 2520.25 2809.17 335.69 o 6 17 0 2361.21 2310.64 320.07 o 7 17 0 4277.46 4006.79 326.35 o 8 17 0 77.22 309.03 288.21 o 9 17 0 6.22 -103.31 405.32 o 10 17 0 11.45 129.09 248.13 o 11 17 0 196.80 232.80 483.05 o 12 17 0 524.37 490.98 503.20 o 0 18 0 18791.25 18342.70 535.80 o 1 18 0 81.97 418.58 165.23 o 2 18 0 34.45 343.64 158.28 o 3 18 0 24.42 330.08 185.83 o 4 18 0 540.31 797.68 219.94 o 5 18 0 707.55 874.71 270.90 o 6 18 0 2289.08 2881.22 348.98 o 7 18 0 2982.67 2926.77 339.64 o 8 18 0 420.11 464.28 340.63 o 9 18 0 1.78 37.36 500.62 o 10 18 0 62.56 428.49 496.61 o 11 18 0 64.53 319.18 495.45 o 12 18 0 912.72 1026.95 703.52 o 1 19 0 9214.11 8679.00 258.92 o 2 19 0 509.98 704.23 186.03 o 3 19 0 126.35 284.60 188.45 o 4 19 0 801.38 1189.47 245.10 o 5 19 0 54.49 480.39 281.03 o 6 19 0 100.32 345.95 268.65 o 7 19 0 553.37 960.57 318.83 o 8 19 0 1046.04 1209.14 331.71 o 9 19 0 63.34 366.44 451.75 o 10 19 0 365.28 662.12 555.69 o 11 19 0 193.21 374.18 518.73 o 0 20 0 14861.23 15092.54 1354.32 o 1 20 0 2659.90 2624.28 225.60 o 2 20 0 391.39 540.89 229.67 o 3 20 0 1902.80 2003.95 248.94 o 4 20 0 1650.16 1379.08 236.81 o 5 20 0 1743.38 1624.89 322.83 o 6 20 0 460.04 719.46 307.11 o 7 20 0 57.49 231.81 282.89 o 8 20 0 568.09 747.71 347.18 o 9 20 0 3.28 211.09 420.70 o 10 20 0 25.46 301.86 474.75 o 11 20 0 15.36 262.20 465.85 o 1 21 0 1761.52 1616.22 283.55 o 2 21 0 2319.27 1997.60 241.63 o 3 21 0 385.17 600.72 224.64 o 4 21 0 402.35 362.96 212.69 o 5 21 0 1131.97 985.04 296.68 o 6 21 0 23.68 658.48 349.39 o 7 21 0 317.97 524.89 342.39 o 8 21 0 11.20 240.40 326.88 o 9 21 0 164.39 351.91 478.37 o 10 21 0 754.94 696.74 451.16 o 11 21 0 273.98 529.80 621.72 o 0 22 0 24815.41 25469.76 480.75 o 1 22 0 623.46 785.17 253.60 o 2 22 0 2782.21 3148.41 281.93 o 3 22 0 1333.85 1483.70 235.52 o 4 22 0 10158.87 9900.56 439.65 o 5 22 0 11009.90 9734.82 381.40 o 6 22 0 564.53 852.31 354.68 o 7 22 0 1356.69 1294.06 359.76 o 8 22 0 6.52 201.23 282.38 o 9 22 0 116.19 636.10 495.53 o 10 22 0 58.02 549.97 527.83 o 11 22 0 60.08 114.81 700.89 o 1 23 0 313.37 449.00 259.24 o 2 23 0 1179.44 1249.10 265.57 o 3 23 0 31.71 442.26 257.07 o 4 23 0 123.90 216.62 224.78 o 5 23 0 2686.31 2565.90 333.70 o 6 23 0 2875.22 3347.62 478.65 o 7 23 0 262.10 594.90 410.13 o 8 23 0 14.49 21.00 368.08 o 9 23 0 750.38 664.32 517.72 o 10 23 0 7.49 543.90 549.27 o 0 24 0 1164.44 930.52 562.82 o 1 24 0 3744.77 3497.57 385.72 o 2 24 0 104.04 530.15 288.39 o 3 24 0 2915.99 2648.73 275.24 o 4 24 0 1899.28 2171.60 301.90 o 5 24 0 4255.75 3456.64 370.42 o 6 24 0 156.89 790.39 386.25 o 7 24 0 432.62 733.07 385.90 o 8 24 0 846.87 1253.38 468.64 o 9 24 0 15.16 99.89 539.36 o 10 24 0 233.19 310.30 722.28 o 1 25 0 254.82 440.24 426.64 o 2 25 0 95.98 181.73 232.40 o 3 25 0 172.38 237.48 257.77 o 4 25 0 105.51 200.94 313.61 o 5 25 0 220.40 206.49 352.99 o 6 25 0 42.80 533.75 415.52 o 7 25 0 40.17 238.08 376.38 o 8 25 0 577.94 879.78 441.57 o 9 25 0 93.42 120.88 434.82 o 0 26 0 4381.57 4077.04 638.23 o 1 26 0 1868.24 1271.42 428.90 o 2 26 0 754.25 1298.66 389.43 o 3 26 0 197.35 648.46 275.78 o 4 26 0 273.43 348.69 349.79 o 5 26 0 202.15 275.49 368.09 o 6 26 0 41.87 305.67 388.81 o 7 26 0 2118.10 2600.38 474.37 o 8 26 0 19.07 239.91 459.16 o 9 26 0 168.62 1070.98 613.70 o 1 27 0 287.46 143.87 358.34 o 2 27 0 1491.67 1320.45 361.45 o 3 27 0 571.83 626.65 292.45 o 4 27 0 5.75 378.12 384.74 o 5 27 0 83.79 399.07 386.49 o 6 27 0 925.29 929.82 394.62 o 7 27 0 328.45 258.11 377.73 o 8 27 0 1099.82 1670.59 437.64 o 0 28 0 2798.09 2250.14 707.27 o 1 28 0 1283.59 1328.85 555.98 o 2 28 0 30.61 352.67 376.22 o 3 28 0 276.70 452.73 396.40 o 4 28 0 315.57 285.12 369.98 o 5 28 0 154.87 251.00 375.70 o 6 28 0 493.05 583.23 435.76 o 7 28 0 5408.07 5052.81 478.84 o 8 28 0 3694.56 3331.85 547.27 o 1 29 0 779.38 1162.94 383.60 o 2 29 0 1015.42 764.40 375.19 o 3 29 0 70.87 59.56 270.38 o 4 29 0 775.35 702.40 500.94 o 5 29 0 183.56 520.63 423.78 o 6 29 0 2148.20 2227.96 445.39 o 7 29 0 663.13 917.39 404.87 o 0 30 0 510.18 980.80 754.92 o 1 30 0 223.65 615.77 384.52 o 2 30 0 530.98 751.78 355.34 o 3 30 0 14.07 394.52 420.84 o 4 30 0 65.28 246.22 529.76 o 5 30 0 206.22 388.23 411.51 o 6 30 0 1.43 170.58 443.93 o 7 30 0 59.59 376.34 646.11 o 1 31 0 311.88 864.33 462.22 o 2 31 0 21.07 430.94 409.62 o 3 31 0 75.57 389.58 406.11 o 4 31 0 1225.38 1765.16 564.75 o 5 31 0 2733.48 2394.04 557.28 o 6 31 0 1791.36 1898.57 845.35 o 0 32 0 680.31 868.28 511.39 o 1 32 0 9.73 388.48 407.99 o 2 32 0 315.25 673.12 417.71 o 3 32 0 548.63 572.78 602.66 o 4 32 0 536.34 1168.57 670.34 o 1 33 0 246.52 898.18 426.88 o 2 33 0 0.16 474.18 474.35 o 0 34 0 783.99 1456.57 871.99 o 1 34 0 16.90 906.13 810.08 o 2 34 0 21.08 253.27 792.44 o -13 1 1 2583.60 2650.47 465.07 o -12 1 1 1574.58 1497.91 457.86 o -11 1 1 29.33 460.06 279.31 o -10 1 1 356.32 342.17 271.19 o -9 1 1 17.28 252.41 204.70 o -8 1 1 1634.39 1861.03 254.70 o -7 1 1 1083.34 1562.32 199.82 o -6 1 1 7925.36 7984.62 241.40 o -5 1 1 7316.49 7286.30 202.60 o -4 1 1 9463.23 9452.18 384.51 o -3 1 1 22384.41 22524.19 374.50 o -2 1 1 260.81 298.52 85.71 o 1 1 1 15004.52 14307.50 3549.11 o 2 1 1 10709.15 10417.20 474.35 o 3 1 1 539.38 698.43 93.38 o 4 1 1 1539.80 2068.74 355.65 o 5 1 1 1294.64 1456.10 164.47 o 6 1 1 12472.15 12805.47 229.63 o 7 1 1 1674.91 1835.67 217.86 o 8 1 1 1573.09 1428.33 239.95 o 9 1 1 88.51 363.58 223.02 o 10 1 1 69.68 385.49 263.20 o 11 1 1 25.52 445.75 464.14 o -14 2 1 67.13 591.71 686.26 o -13 2 1 3007.81 3039.96 673.50 o -12 2 1 443.80 645.91 329.14 o -11 2 1 2455.38 2479.00 358.99 o -10 2 1 792.32 886.23 283.21 o -9 2 1 1.41 417.58 245.59 o -8 2 1 278.00 707.91 242.12 o -7 2 1 3634.25 3285.23 363.06 o -6 2 1 2938.62 2943.77 129.30 o -5 2 1 9889.25 9793.88 159.97 o -4 2 1 3290.88 3182.76 109.89 o -3 2 1 266.45 373.54 98.32 o -2 2 1 119.46 226.19 60.62 o 1 2 1 1789.85 1642.22 129.98 o 2 2 1 19026.17 19162.17 414.81 o 3 2 1 10431.95 9775.05 294.56 o 4 2 1 7185.21 7273.87 280.80 o 5 2 1 13370.50 13604.62 459.21 o 6 2 1 4381.09 4138.76 219.34 o 7 2 1 14381.28 14846.05 392.24 o 8 2 1 1595.61 1942.08 295.34 o 9 2 1 210.24 393.87 248.91 o 10 2 1 31.53 307.64 267.58 o 11 2 1 4126.36 4231.23 511.77 o 12 2 1 3021.53 3502.22 890.00 o -14 3 1 18.14 64.91 665.62 o -13 3 1 1667.10 888.87 693.39 o -12 3 1 689.93 833.87 347.17 o -11 3 1 816.12 815.34 330.77 o -10 3 1 8144.22 8542.73 363.23 o -9 3 1 1425.81 1190.95 261.96 o -8 3 1 3588.12 3306.29 224.26 o -7 3 1 250.68 382.54 191.39 o -6 3 1 18800.68 18863.04 615.39 o -5 3 1 29389.32 30446.21 300.42 o -4 3 1 16289.03 16593.02 293.61 o -3 3 1 3.50 218.54 95.59 o -2 3 1 234.86 318.43 80.90 o -1 3 1 18581.31 16875.47 204.49 o 1 3 1 473.95 549.15 107.75 o 2 3 1 1045.16 1056.52 178.41 o 3 3 1 10841.32 11495.90 482.12 o 4 3 1 1076.80 1551.24 161.84 o 5 3 1 3162.78 3551.72 276.54 o 6 3 1 5882.86 5622.78 185.72 o 7 3 1 339.47 398.22 189.65 o 8 3 1 92.91 303.58 201.96 o 9 3 1 1523.91 1417.33 267.93 o 10 3 1 4.55 356.72 360.03 o 11 3 1 1350.72 1488.66 508.97 o 12 3 1 12.69 419.10 422.11 o -15 4 1 32.34 296.79 832.59 o -14 4 1 695.98 626.98 762.80 o -13 4 1 912.69 1009.54 480.76 o -12 4 1 458.15 592.84 416.68 o -11 4 1 149.09 499.56 308.00 o -10 4 1 379.16 583.35 262.52 o -9 4 1 6401.75 6737.98 294.00 o -8 4 1 252.98 418.05 219.82 o -7 4 1 156.97 222.11 137.06 o 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