data_2239583 _cell_angle_alpha 90.000 _cell_angle_beta 98.930 _cell_angle_gamma 90.000 _cell_length_a 13.0859 _cell_length_b 11.8258 _cell_length_c 27.5040 _exptl_crystal_F_000 1616.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file lh5704Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelx P 21/n R = 0.06' _shelx_refln_list_code 4 _shelx_f_calc_maximum 328.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 417.90 433.51 14.35 o 4 0 0 3192.99 3279.74 62.57 o 6 0 0 1436.24 1342.64 40.03 o 8 0 0 2035.34 2205.86 90.90 o 10 0 0 731.32 713.64 46.47 o 12 0 0 138.95 144.03 48.36 o 14 0 0 3567.03 3682.04 157.21 o 1 1 0 299.70 40.85 29.94 o 2 1 0 41196.21 43987.29 476.95 o 3 1 0 735.25 752.93 29.59 o 4 1 0 16130.20 17137.50 192.45 o 5 1 0 700.39 652.32 25.43 o 6 1 0 6496.54 6425.85 81.66 o 7 1 0 5.24 -3.00 13.44 o 8 1 0 3874.52 3619.74 60.17 o 9 1 0 47.51 12.73 19.39 o 10 1 0 1050.07 1052.53 48.06 o 11 1 0 38.95 22.57 27.31 o 12 1 0 2694.94 2567.84 71.16 o 13 1 0 2.45 117.71 51.50 o 14 1 0 12.78 -74.87 49.95 o 15 1 0 2.47 -43.32 53.75 o 16 1 0 135.86 256.49 95.25 o 0 2 0 87056.97 108542.40 1658.13 o 1 2 0 504.33 523.63 11.14 o 2 2 0 18369.44 19683.33 231.74 o 3 2 0 161.57 142.66 14.15 o 4 2 0 5335.94 5150.71 64.61 o 5 2 0 24.41 34.34 10.89 o 6 2 0 1449.39 1195.61 41.74 o 7 2 0 4.02 -0.78 13.20 o 8 2 0 1775.88 1636.98 37.75 o 9 2 0 206.87 277.82 23.64 o 10 2 0 277.27 269.54 26.99 o 11 2 0 12.59 12.92 29.32 o 12 2 0 187.60 194.65 46.42 o 13 2 0 33.92 58.21 48.77 o 14 2 0 2437.66 2593.92 104.40 o 15 2 0 0.40 -20.23 58.81 o 16 2 0 162.81 199.98 64.97 o 1 3 0 7580.19 8011.63 93.77 o 2 3 0 357.69 344.98 16.54 o 3 3 0 967.22 1079.10 23.96 o 4 3 0 4349.94 4675.28 60.56 o 5 3 0 707.09 636.48 19.87 o 6 3 0 1540.79 1239.64 28.84 o 7 3 0 9.96 18.96 14.81 o 8 3 0 6014.80 5991.80 88.03 o 9 3 0 1850.85 1827.25 44.48 o 10 3 0 0.02 -24.32 28.76 o 11 3 0 1.96 11.37 33.34 o 12 3 0 2342.13 2318.85 97.92 o 13 3 0 30.74 102.01 66.82 o 14 3 0 78.16 50.47 50.72 o 15 3 0 184.16 223.01 60.07 o 16 3 0 469.83 421.33 73.37 o 0 4 0 10350.01 12037.64 195.91 o 1 4 0 717.85 845.06 22.68 o 2 4 0 273.48 212.06 10.70 o 3 4 0 18.84 33.95 10.92 o 4 4 0 244.80 162.02 13.55 o 5 4 0 2336.61 2511.16 40.77 o 6 4 0 767.72 728.26 23.40 o 7 4 0 1196.03 1118.10 32.92 o 8 4 0 792.15 786.44 38.00 o 9 4 0 138.15 176.58 39.36 o 10 4 0 9.21 20.75 30.05 o 11 4 0 505.17 540.24 50.90 o 12 4 0 730.30 752.99 62.36 o 13 4 0 385.02 271.57 56.92 o 14 4 0 813.14 871.85 81.83 o 15 4 0 17.01 -19.71 55.89 o 16 4 0 4.41 13.11 68.39 o 1 5 0 1438.18 1418.30 27.90 o 2 5 0 6785.37 6846.76 85.47 o 3 5 0 146.54 176.26 16.72 o 4 5 0 367.80 323.26 19.05 o 5 5 0 2201.45 2026.20 40.41 o 6 5 0 1637.22 1662.65 47.09 o 7 5 0 826.29 832.00 41.88 o 8 5 0 4520.29 4338.05 84.18 o 9 5 0 26.36 2.51 32.29 o 10 5 0 111.43 75.62 30.66 o 11 5 0 14.34 84.59 35.39 o 12 5 0 217.19 198.90 50.73 o 13 5 0 76.34 69.20 47.45 o 14 5 0 18.04 20.95 53.78 o 15 5 0 47.14 -32.94 57.94 o 0 6 0 23465.39 23512.51 377.15 o 1 6 0 453.37 629.54 21.97 o 2 6 0 1050.56 1113.11 29.13 o 3 6 0 90.89 82.88 21.77 o 4 6 0 31.61 55.50 18.57 o 5 6 0 284.13 249.92 27.50 o 6 6 0 2451.01 2463.49 65.91 o 7 6 0 308.98 295.43 34.11 o 8 6 0 168.50 182.63 33.87 o 9 6 0 1.18 26.44 32.69 o 10 6 0 301.14 263.14 41.75 o 11 6 0 0.03 40.62 38.27 o 12 6 0 140.94 125.98 50.78 o 13 6 0 8.22 63.46 54.56 o 14 6 0 300.77 507.24 92.72 o 15 6 0 0.09 -63.82 60.87 o 1 7 0 242.32 217.30 19.14 o 2 7 0 1179.10 1103.09 30.59 o 3 7 0 681.11 716.50 45.56 o 4 7 0 282.42 305.60 30.70 o 5 7 0 468.53 359.01 35.87 o 6 7 0 2737.02 2413.81 64.72 o 7 7 0 299.78 391.68 46.12 o 8 7 0 501.67 603.35 43.28 o 9 7 0 144.52 166.18 35.27 o 10 7 0 136.39 173.18 39.42 o 11 7 0 14.01 -17.09 35.87 o 12 7 0 408.20 556.04 55.29 o 13 7 0 501.93 510.29 64.54 o 14 7 0 0.08 71.86 57.62 o 0 8 0 10628.65 10875.38 265.94 o 1 8 0 108.55 135.06 21.53 o 2 8 0 6.57 13.80 26.05 o 3 8 0 727.85 694.86 39.73 o 4 8 0 18.59 50.00 30.92 o 5 8 0 17.18 13.31 31.50 o 6 8 0 86.03 114.79 34.97 o 7 8 0 37.04 -13.89 31.75 o 8 8 0 1281.84 1195.86 66.03 o 9 8 0 194.57 229.39 39.74 o 10 8 0 254.86 340.50 74.97 o 11 8 0 304.07 314.61 55.08 o 12 8 0 458.90 341.74 51.86 o 13 8 0 90.98 94.21 59.29 o 14 8 0 1001.84 885.55 119.44 o 1 9 0 25.83 -21.82 29.33 o 2 9 0 4241.50 3908.79 94.64 o 3 9 0 9.27 -3.94 30.95 o 4 9 0 3.33 34.15 31.93 o 5 9 0 640.10 607.69 43.85 o 6 9 0 2489.11 2370.89 76.33 o 7 9 0 5.98 -2.81 32.71 o 8 9 0 274.33 306.33 52.65 o 9 9 0 6.49 -18.46 35.13 o 10 9 0 94.50 89.65 44.33 o 11 9 0 35.39 -13.27 42.77 o 12 9 0 250.74 246.32 54.47 o 13 9 0 172.49 163.39 65.55 o 0 10 0 16486.36 16064.69 409.36 o 1 10 0 20.80 8.43 36.38 o 2 10 0 57.47 86.16 34.09 o 3 10 0 753.86 670.95 51.27 o 4 10 0 7.06 30.19 37.40 o 5 10 0 3.86 2.37 32.14 o 6 10 0 141.19 139.92 37.79 o 7 10 0 255.56 275.85 40.78 o 8 10 0 182.94 236.50 41.60 o 9 10 0 0.07 -9.96 53.16 o 10 10 0 149.62 148.43 49.31 o 11 10 0 6.47 138.97 65.69 o 12 10 0 23.16 21.43 52.27 o 1 11 0 1124.57 1121.84 68.72 o 2 11 0 554.55 399.60 54.15 o 3 11 0 24.99 15.37 36.18 o 4 11 0 10.85 22.70 35.53 o 5 11 0 65.08 56.41 35.52 o 6 11 0 438.37 435.94 58.78 o 7 11 0 39.01 79.48 42.11 o 8 11 0 22.64 30.09 40.68 o 9 11 0 1.08 -22.47 43.09 o 10 11 0 1.97 66.38 51.51 o 11 11 0 3.46 20.90 54.71 o 0 12 0 349.74 303.00 76.12 o 1 12 0 20.73 49.12 45.47 o 2 12 0 413.76 378.57 56.06 o 3 12 0 314.17 350.68 56.87 o 4 12 0 19.05 50.50 49.92 o 5 12 0 90.35 79.99 40.45 o 6 12 0 442.77 404.12 51.41 o 7 12 0 175.60 189.03 52.54 o 8 12 0 300.43 325.46 49.33 o 9 12 0 61.89 68.28 54.35 o 10 12 0 10.38 -11.67 52.27 o 1 13 0 182.43 308.12 66.34 o 2 13 0 7.45 -13.36 57.25 o 3 13 0 100.13 51.63 53.98 o 4 13 0 170.41 199.06 55.33 o 5 13 0 609.07 640.87 69.62 o 6 13 0 188.56 288.51 54.25 o 7 13 0 0.29 6.87 46.39 o 8 13 0 3.30 115.72 53.97 o 0 14 0 79.66 147.04 94.30 o 1 14 0 54.62 29.10 61.54 o 2 14 0 20.32 26.57 55.13 o 3 14 0 14.01 36.97 56.07 o 4 14 0 91.54 210.80 70.31 o 5 14 0 8.71 73.87 80.51 o 6 14 0 126.35 43.64 63.53 o 1 15 0 15.27 72.56 64.63 o 2 15 0 542.09 699.18 113.45 o 3 15 0 335.79 468.63 156.59 o -15 0 1 2.61 -81.15 104.01 o -13 0 1 2700.21 2625.06 143.15 o -11 0 1 632.43 658.16 48.32 o -9 0 1 3322.65 3449.25 122.74 o -7 0 1 2584.26 2800.26 64.38 o -5 0 1 942.79 818.34 29.45 o -3 0 1 126.63 161.36 14.81 o 3 0 1 17000.88 17127.71 269.42 o 5 0 1 1467.48 1327.83 43.55 o 7 0 1 2264.99 1982.42 52.30 o 9 0 1 1088.18 1232.54 73.53 o 11 0 1 282.19 270.08 61.50 o 13 0 1 339.53 440.40 61.07 o 15 0 1 477.55 633.22 146.30 o -16 1 1 8.60 15.28 86.07 o -15 1 1 674.26 790.20 72.92 o -14 1 1 0.53 20.37 49.36 o -13 1 1 0.02 50.19 47.18 o -12 1 1 485.95 478.08 40.36 o -11 1 1 56.88 33.72 24.34 o -10 1 1 101.66 74.77 23.72 o -9 1 1 74.51 92.01 20.66 o -8 1 1 341.84 285.22 20.50 o -7 1 1 6557.84 6387.69 89.91 o -6 1 1 321.15 299.33 17.98 o -5 1 1 360.28 284.37 23.85 o -4 1 1 0.76 -4.71 9.04 o -3 1 1 10302.83 10762.55 130.79 o -2 1 1 1429.76 1366.41 19.45 o -1 1 1 35765.43 43149.05 1717.92 o 1 1 1 4.70 -7.45 3.73 o 2 1 1 107.35 73.77 6.75 o 3 1 1 5299.11 5546.83 66.99 o 4 1 1 6792.69 6931.29 83.21 o 5 1 1 363.27 441.52 17.52 o 6 1 1 1720.58 1618.80 31.48 o 7 1 1 13484.04 13512.39 160.22 o 8 1 1 5.25 3.35 15.71 o 9 1 1 5.87 -41.97 25.46 o 10 1 1 117.55 94.90 23.80 o 11 1 1 2853.86 2834.34 72.53 o 12 1 1 342.93 418.16 40.23 o 13 1 1 1023.60 1106.22 68.56 o 14 1 1 106.85 96.74 50.11 o 15 1 1 64.74 161.86 58.87 o 16 1 1 0.45 -159.92 161.16 o -16 2 1 0.61 -82.10 61.70 o -15 2 1 2.14 -22.89 51.35 o -14 2 1 5.19 5.78 47.83 o -13 2 1 992.61 1005.00 67.18 o -12 2 1 2.80 11.83 41.08 o -11 2 1 30.07 34.89 26.70 o -10 2 1 686.14 620.68 32.72 o -9 2 1 3622.64 3422.78 81.00 o -8 2 1 8.79 -0.36 15.93 o -7 2 1 2564.24 2771.33 45.71 o -6 2 1 115.13 111.31 13.74 o -5 2 1 6160.32 6492.42 80.79 o -4 2 1 3956.60 3922.60 51.51 o -3 2 1 6045.10 6156.68 73.89 o -2 2 1 2003.92 1827.62 29.55 o -1 2 1 3294.70 3465.01 42.10 o 0 2 1 1927.50 1935.97 26.48 o 1 2 1 35312.50 36301.88 394.87 o 2 2 1 20.89 4.91 9.70 o 3 2 1 16682.95 18077.82 202.04 o 4 2 1 3314.05 3446.89 46.93 o 5 2 1 17242.36 17214.90 196.15 o 6 2 1 1178.58 1127.88 34.97 o 7 2 1 73.70 110.07 15.94 o 8 2 1 4262.92 4193.17 64.45 o 9 2 1 1426.98 1405.87 49.14 o 10 2 1 19.45 -2.77 22.99 o 11 2 1 723.97 865.28 51.42 o 12 2 1 709.04 720.54 58.42 o 13 2 1 998.82 987.69 68.43 o 14 2 1 73.78 99.96 51.91 o 15 2 1 732.80 1004.79 77.07 o 16 2 1 7.35 46.25 66.43 o -16 3 1 9.45 23.28 63.52 o -15 3 1 401.82 457.90 67.90 o -14 3 1 459.84 444.61 62.10 o -13 3 1 139.21 106.05 48.26 o -12 3 1 20.18 21.00 34.97 o -11 3 1 1028.78 1055.22 53.41 o -10 3 1 95.50 93.81 29.62 o -9 3 1 28.35 -2.49 20.11 o -8 3 1 112.09 122.74 19.81 o -7 3 1 5409.65 5362.35 73.74 o -6 3 1 526.45 472.20 19.04 o -5 3 1 8178.05 8742.41 113.50 o -4 3 1 108.93 176.63 15.82 o -3 3 1 1313.68 1276.82 27.69 o -2 3 1 320.81 323.88 18.32 o -1 3 1 10179.58 10659.56 122.04 o 0 3 1 4923.42 5095.97 63.07 o 1 3 1 7496.00 7969.67 93.57 o 2 3 1 3072.25 2902.93 46.63 o 3 3 1 0.04 49.97 14.15 o 4 3 1 1037.15 991.47 28.41 o 5 3 1 10518.62 10724.97 135.22 o 6 3 1 68.35 39.90 16.19 o 7 3 1 16872.16 17304.23 202.39 o 8 3 1 1185.37 1285.24 42.28 o 9 3 1 1376.70 1397.50 39.88 o 10 3 1 144.84 182.12 35.18 o 11 3 1 193.41 181.23 37.01 o 12 3 1 275.66 327.46 49.79 o 13 3 1 256.57 229.43 53.27 o 14 3 1 50.39 28.32 51.53 o 15 3 1 5.08 -41.58 56.87 o 16 3 1 25.82 85.27 68.15 o -16 4 1 25.18 -1.29 63.02 o -15 4 1 175.74 152.49 61.08 o -14 4 1 19.01 -72.48 48.66 o -13 4 1 245.25 245.92 54.19 o -12 4 1 226.01 281.73 41.52 o -11 4 1 920.21 999.92 53.92 o -10 4 1 128.19 77.59 31.73 o -9 4 1 1473.08 1363.34 49.47 o -8 4 1 1007.06 893.73 80.00 o -7 4 1 3.80 27.11 16.08 o -6 4 1 381.18 380.20 17.99 o -5 4 1 9160.95 9901.72 119.10 o -4 4 1 526.22 666.60 26.96 o -3 4 1 2454.53 2583.75 47.80 o -2 4 1 185.62 251.56 11.50 o -1 4 1 1056.27 1592.97 65.83 o 0 4 1 217.68 191.48 12.42 o 1 4 1 2423.86 2221.05 34.46 o 2 4 1 3100.04 3081.93 47.92 o 3 4 1 7763.23 8551.21 118.47 o 4 4 1 11.19 15.52 13.00 o 5 4 1 1825.77 1404.28 29.71 o 6 4 1 2.17 15.06 14.26 o 7 4 1 8.29 -1.85 16.31 o 8 4 1 0.31 -23.76 20.81 o 9 4 1 1171.52 1176.23 49.14 o 10 4 1 1786.45 1837.11 67.63 o 11 4 1 403.32 452.14 43.49 o 12 4 1 8.97 74.12 47.89 o 13 4 1 2072.83 2091.82 124.89 o 14 4 1 49.83 66.09 52.61 o 15 4 1 235.76 292.82 68.69 o 16 4 1 11.38 78.08 69.59 o -15 5 1 776.85 948.90 81.82 o -14 5 1 129.01 128.35 71.44 o -13 5 1 10.19 10.64 52.63 o -12 5 1 121.66 193.82 41.92 o -11 5 1 1142.72 1123.87 56.72 o -10 5 1 0.21 -11.47 30.08 o -9 5 1 975.62 871.35 47.25 o -8 5 1 17.24 15.16 26.43 o -7 5 1 4708.70 4473.60 83.14 o -6 5 1 481.21 392.17 28.16 o -5 5 1 105.26 126.78 21.69 o -4 5 1 634.17 631.64 32.12 o -3 5 1 203.10 354.30 18.73 o -2 5 1 7297.80 7736.09 94.86 o -1 5 1 161.39 230.28 14.14 o 0 5 1 4085.44 4021.50 55.53 o 1 5 1 0.85 31.65 11.61 o 2 5 1 988.84 1025.39 36.78 o 3 5 1 1341.74 1764.43 80.84 o 4 5 1 4816.31 4779.67 71.45 o 5 5 1 1645.64 1865.74 39.72 o 6 5 1 863.03 947.94 49.89 o 7 5 1 3694.09 3629.78 73.37 o 8 5 1 156.75 63.21 29.39 o 9 5 1 979.74 997.08 46.60 o 10 5 1 0.93 3.36 46.86 o 11 5 1 226.67 238.27 46.80 o 12 5 1 79.65 72.16 46.84 o 13 5 1 599.75 674.47 101.13 o 14 5 1 50.72 44.25 58.73 o 15 5 1 145.37 167.92 72.26 o -15 6 1 8.61 -34.53 60.60 o -14 6 1 0.36 39.31 54.14 o -13 6 1 206.32 191.52 53.89 o -12 6 1 303.24 320.47 47.08 o -11 6 1 2081.31 1832.50 98.33 o -10 6 1 159.06 158.81 38.01 o -9 6 1 934.48 896.96 48.30 o -8 6 1 1335.80 1371.49 54.61 o -7 6 1 2310.16 2304.72 59.93 o -6 6 1 762.52 778.63 38.87 o -5 6 1 818.74 947.03 41.49 o -4 6 1 1505.63 1550.30 45.24 o -3 6 1 1079.84 1191.10 47.86 o -2 6 1 375.72 352.54 17.60 o -1 6 1 63.10 29.59 14.45 o 0 6 1 931.21 896.02 25.42 o 1 6 1 291.43 200.72 16.47 o 2 6 1 12.82 -5.05 12.78 o 3 6 1 2792.96 2984.87 52.77 o 4 6 1 1618.13 1828.24 41.19 o 5 6 1 834.24 646.30 43.19 o 6 6 1 39.55 30.52 26.12 o 7 6 1 103.23 64.76 29.39 o 8 6 1 112.42 102.04 31.84 o 9 6 1 63.86 88.56 31.92 o 10 6 1 315.99 398.70 42.87 o 11 6 1 35.57 69.86 39.00 o 12 6 1 829.07 860.42 67.43 o 13 6 1 1581.07 1571.28 103.44 o 14 6 1 79.17 12.22 58.36 o 15 6 1 105.64 101.36 66.22 o -15 7 1 254.00 366.90 152.02 o -14 7 1 96.33 98.80 62.50 o -13 7 1 0.91 -86.17 52.25 o -12 7 1 249.40 271.94 48.51 o -11 7 1 43.82 38.54 38.51 o -10 7 1 114.19 118.36 35.29 o -9 7 1 102.38 123.83 32.88 o -8 7 1 32.41 16.99 33.54 o -7 7 1 3794.14 3527.76 85.30 o -6 7 1 709.65 712.23 41.19 o -5 7 1 2024.01 2217.89 93.39 o -4 7 1 1323.33 1371.44 49.33 o -3 7 1 2033.23 1984.61 53.16 o -2 7 1 666.94 789.51 34.78 o -1 7 1 437.93 512.53 23.07 o 0 7 1 3221.82 3340.38 71.03 o 1 7 1 1799.70 1956.17 39.38 o 2 7 1 43.09 31.13 16.16 o 3 7 1 6.41 -20.53 19.12 o 4 7 1 884.75 873.17 41.09 o 5 7 1 23.30 31.87 28.57 o 6 7 1 105.58 81.51 31.31 o 7 7 1 5590.96 5546.00 103.91 o 8 7 1 30.00 2.07 31.53 o 9 7 1 59.29 26.70 31.65 o 10 7 1 19.18 40.06 39.55 o 11 7 1 34.75 39.45 41.16 o 12 7 1 100.32 87.12 52.91 o 13 7 1 401.21 504.77 65.87 o 14 7 1 214.91 218.01 63.70 o -14 8 1 1.20 -3.68 73.90 o -13 8 1 321.16 252.02 62.32 o -12 8 1 420.49 404.34 51.09 o -11 8 1 4.63 -84.56 48.69 o -10 8 1 44.31 47.16 34.33 o -9 8 1 41.20 42.56 35.07 o -8 8 1 208.38 261.40 36.68 o -7 8 1 1565.09 1590.23 79.49 o -6 8 1 507.85 533.15 41.59 o -5 8 1 705.03 630.66 41.92 o -4 8 1 23.12 15.10 28.18 o -3 8 1 94.97 108.80 40.98 o -2 8 1 145.51 98.20 28.36 o -1 8 1 2.29 -3.76 23.68 o 0 8 1 1658.12 1562.42 58.32 o 1 8 1 6682.19 6336.69 99.31 o 2 8 1 580.06 556.32 35.81 o 3 8 1 1511.70 1522.02 52.63 o 4 8 1 247.52 293.54 34.73 o 5 8 1 2952.77 2858.41 71.88 o 6 8 1 20.90 20.75 32.59 o 7 8 1 400.04 347.24 41.95 o 8 8 1 18.94 50.41 33.76 o 9 8 1 83.67 59.69 36.24 o 10 8 1 24.10 32.90 38.86 o 11 8 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