#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:54:21 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181895 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/95/2239584.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2239584 _cell_angle_alpha 107.774 _cell_angle_beta 109.045 _cell_angle_gamma 99.504 _cell_length_a 8.7600 _cell_length_b 13.3270 _cell_length_c 13.3870 _exptl_crystal_F_000 670.00 _reflns_d_resolution_high 0.6860 _cod_data_source_file rk2424Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' elech_slim_0m in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 214.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1750.75 1729.11 23.41 o 2 0 0 5809.99 6181.40 68.73 o 3 0 0 1305.18 1277.99 20.67 o 4 0 0 337.87 395.92 16.98 o 5 0 0 17.38 26.44 7.32 o 6 0 0 131.56 138.70 10.82 o 7 0 0 583.05 593.50 23.64 o 8 0 0 670.75 663.05 22.40 o 9 0 0 4.20 4.53 30.77 o 10 0 0 7.69 0.35 22.54 o 11 0 0 2.42 24.78 37.12 o -11 1 0 162.82 173.19 28.70 o -10 1 0 36.64 69.95 23.41 o -9 1 0 46.91 57.44 19.93 o -8 1 0 131.81 122.18 14.83 o -7 1 0 13.99 8.82 11.03 o -6 1 0 158.94 185.44 21.93 o -5 1 0 1764.77 1663.52 24.16 o -4 1 0 4572.93 4802.38 48.82 o -3 1 0 7393.16 7923.78 88.90 o -2 1 0 5246.20 5528.66 61.68 o -1 1 0 2152.84 2086.29 25.05 o 0 1 0 648.45 706.60 7.76 o 1 1 0 833.85 859.36 12.05 o 2 1 0 6207.38 6124.57 68.43 o 3 1 0 7733.86 7696.67 71.27 o 4 1 0 242.49 263.13 9.33 o 5 1 0 9471.36 9159.59 87.90 o 6 1 0 276.51 282.07 12.45 o 7 1 0 618.00 581.63 30.21 o 8 1 0 73.29 87.72 18.67 o 9 1 0 10.54 -2.70 19.83 o 10 1 0 8.67 -3.53 32.71 o 11 1 0 9.23 15.13 38.68 o -11 2 0 11.64 -12.42 24.61 o -10 2 0 134.37 199.25 25.81 o -9 2 0 0.21 -2.95 15.36 o -8 2 0 278.85 295.54 17.12 o -7 2 0 39.12 41.68 10.72 o -6 2 0 3628.92 3533.43 42.44 o -5 2 0 2994.85 2972.84 35.29 o -4 2 0 146.22 168.56 7.74 o -3 2 0 6451.12 6800.76 63.69 o -2 2 0 16136.91 17030.97 179.68 o -1 2 0 349.40 339.38 7.08 o 0 2 0 3783.95 4025.62 33.64 o 1 2 0 379.53 430.58 10.09 o 2 2 0 5591.34 5754.50 65.01 o 3 2 0 30292.31 30918.94 269.08 o 4 2 0 166.13 154.05 11.53 o 5 2 0 487.94 483.60 22.12 o 6 2 0 221.49 212.91 11.65 o 7 2 0 824.60 818.89 67.62 o 8 2 0 10.61 48.42 17.79 o 9 2 0 41.03 40.74 30.90 o 10 2 0 186.72 182.79 38.24 o 11 2 0 48.80 9.35 42.16 o -11 3 0 24.98 55.77 37.65 o -10 3 0 180.41 179.73 31.84 o -9 3 0 63.01 42.34 16.42 o -8 3 0 2968.46 3028.53 43.39 o -7 3 0 49.10 63.29 11.62 o -6 3 0 15.31 4.07 8.75 o -5 3 0 1136.04 1111.45 19.17 o -4 3 0 18.73 26.08 5.89 o -3 3 0 326.26 349.46 9.56 o -2 3 0 636.71 562.28 8.82 o 0 3 0 8949.70 9138.82 69.16 o 1 3 0 354.55 367.78 9.49 o 2 3 0 2257.33 2131.59 28.32 o 3 3 0 1721.98 1489.14 18.15 o 4 3 0 10.82 6.46 5.30 o 5 3 0 2835.28 2706.52 32.50 o 6 3 0 2200.73 2041.05 38.32 o 7 3 0 15.33 3.87 14.71 o 8 3 0 1284.66 1280.11 52.49 o 9 3 0 80.65 64.73 32.95 o 10 3 0 44.15 49.41 35.55 o -12 4 0 6.65 13.17 40.25 o -11 4 0 66.53 47.55 37.17 o -10 4 0 288.24 341.64 29.48 o -9 4 0 16.44 -14.98 14.98 o -8 4 0 250.90 244.89 16.42 o -7 4 0 343.17 354.62 15.74 o -6 4 0 328.26 328.37 13.20 o -5 4 0 3467.13 3427.11 39.30 o -4 4 0 0.27 -6.06 6.06 o -3 4 0 33974.61 34101.34 295.92 o -2 4 0 4613.50 4865.37 48.36 o -1 4 0 1628.94 1631.85 13.95 o 0 4 0 1446.27 1345.70 13.92 o 1 4 0 7565.97 7556.90 101.78 o 2 4 0 698.00 734.32 13.08 o 3 4 0 629.90 628.23 15.58 o 4 4 0 3.20 15.14 7.97 o 5 4 0 1025.56 1009.01 44.44 o 6 4 0 545.61 532.27 23.11 o 7 4 0 81.39 71.73 24.58 o 8 4 0 63.69 26.64 27.08 o 9 4 0 9.29 60.42 34.96 o 10 4 0 163.26 143.13 39.66 o -12 5 0 14.31 -22.52 40.05 o -11 5 0 2.69 -6.15 30.24 o -10 5 0 12.19 -9.58 22.04 o -9 5 0 169.48 146.71 22.01 o -8 5 0 69.95 77.07 13.59 o -7 5 0 1137.02 1141.02 24.04 o -6 5 0 1068.97 987.21 20.67 o -5 5 0 13357.95 13591.51 125.77 o -4 5 0 86.12 93.27 7.05 o -3 5 0 40.68 61.32 9.52 o -2 5 0 33.11 42.03 4.94 o -1 5 0 6705.27 6843.03 49.93 o 0 5 0 3973.03 3995.95 30.58 o 1 5 0 39.87 49.95 4.47 o 2 5 0 15545.90 15219.77 138.59 o 3 5 0 308.36 276.97 13.68 o 4 5 0 262.33 259.03 21.62 o 5 5 0 492.48 480.01 19.85 o 6 5 0 292.83 227.74 25.80 o 7 5 0 111.88 83.49 26.15 o 8 5 0 9.70 36.63 28.74 o 9 5 0 29.00 68.31 33.74 o 10 5 0 37.37 51.76 39.91 o -12 6 0 0.13 3.72 40.74 o -11 6 0 1.68 4.24 26.01 o -10 6 0 1.96 29.00 22.71 o -9 6 0 11.80 51.49 20.56 o -8 6 0 339.00 351.79 22.65 o -7 6 0 403.47 384.74 16.03 o -6 6 0 340.09 357.16 13.93 o -5 6 0 1546.27 1497.35 42.26 o -4 6 0 650.67 615.40 17.52 o -3 6 0 3703.87 3641.69 47.28 o -2 6 0 9191.24 9145.52 87.11 o -1 6 0 2604.43 2698.38 22.33 o 0 6 0 10261.98 9918.56 118.34 o 1 6 0 60.41 60.00 7.70 o 2 6 0 33.62 36.88 8.60 o 3 6 0 395.67 407.23 13.14 o 4 6 0 10.06 14.21 13.59 o 5 6 0 0.79 4.05 15.30 o 6 6 0 370.18 366.56 25.06 o 7 6 0 339.48 341.38 31.66 o 8 6 0 10.84 -3.43 24.71 o 9 6 0 53.36 30.64 28.36 o -12 7 0 0.43 53.12 31.19 o -11 7 0 134.12 168.71 30.22 o -10 7 0 23.22 0.52 23.82 o -9 7 0 109.81 86.40 21.47 o -8 7 0 195.39 241.16 21.35 o -7 7 0 480.47 491.94 24.23 o -6 7 0 12.26 4.43 12.79 o -5 7 0 0.64 -1.00 6.59 o -4 7 0 45.86 64.48 10.22 o -3 7 0 1251.57 1193.15 19.44 o -2 7 0 8808.81 8659.65 63.75 o -1 7 0 4673.55 4750.04 36.98 o 0 7 0 1606.75 1506.82 15.37 o 1 7 0 2.16 -1.22 5.51 o 2 7 0 3486.05 3345.41 59.49 o 3 7 0 2600.42 2440.50 42.29 o 4 7 0 166.11 154.52 17.21 o 5 7 0 1617.86 1614.35 42.62 o 6 7 0 251.60 197.87 29.50 o 7 7 0 62.13 79.11 24.97 o 8 7 0 38.90 56.38 27.86 o 9 7 0 24.32 35.65 30.83 o -11 8 0 7.30 -13.02 26.44 o -10 8 0 66.01 64.68 32.42 o -9 8 0 79.07 33.16 21.52 o -8 8 0 227.27 207.50 21.27 o -7 8 0 79.36 74.03 16.91 o -6 8 0 1510.88 1561.50 42.53 o -5 8 0 119.43 137.53 14.07 o -4 8 0 1313.08 1286.96 28.28 o -3 8 0 183.00 185.77 9.87 o -2 8 0 2181.98 2069.74 30.26 o -1 8 0 2538.27 2497.82 22.45 o 0 8 0 19.70 14.44 4.67 o 1 8 0 1926.49 1840.66 24.22 o 2 8 0 363.30 337.77 20.37 o 3 8 0 765.00 766.76 44.44 o 4 8 0 1388.41 1322.79 34.80 o 5 8 0 474.66 460.84 26.44 o 6 8 0 3.23 -23.03 40.30 o 7 8 0 210.80 263.22 28.31 o 8 8 0 7.74 -20.47 28.76 o -11 9 0 11.03 16.34 28.11 o -10 9 0 183.45 208.21 27.38 o -9 9 0 53.18 40.75 21.29 o -8 9 0 1059.60 1126.95 48.57 o -7 9 0 263.05 200.81 19.52 o -6 9 0 124.07 123.07 15.28 o -5 9 0 99.39 93.55 13.15 o -4 9 0 44.82 39.65 11.07 o -3 9 0 843.87 865.92 32.69 o -2 9 0 239.81 249.10 19.48 o -1 9 0 3446.38 3372.37 29.36 o 0 9 0 124.20 122.01 9.29 o 1 9 0 2232.10 2311.56 29.33 o 2 9 0 287.58 265.93 16.61 o 3 9 0 722.21 700.64 26.09 o 4 9 0 320.23 326.73 22.18 o 5 9 0 36.50 30.29 20.55 o 6 9 0 100.33 75.01 23.13 o 7 9 0 28.76 73.81 31.61 o 8 9 0 63.01 1.77 38.61 o -11 10 0 27.45 41.80 30.34 o -10 10 0 278.33 264.56 53.42 o -9 10 0 0.68 -3.29 29.75 o -8 10 0 135.96 133.28 21.42 o -7 10 0 455.17 416.69 25.49 o -6 10 0 771.33 805.67 27.70 o -5 10 0 691.56 644.88 24.43 o -4 10 0 261.12 224.16 12.56 o -3 10 0 1232.87 1264.52 21.68 o -2 10 0 219.13 244.44 10.17 o -1 10 0 1110.39 1059.15 17.47 o 0 10 0 19.61 15.67 10.42 o 1 10 0 3.66 2.19 12.14 o 2 10 0 13.27 3.63 14.36 o 3 10 0 28.69 42.09 15.88 o 4 10 0 128.11 121.15 20.35 o 5 10 0 1.97 -20.93 20.93 o 6 10 0 161.37 183.93 28.27 o 7 10 0 133.34 112.83 28.98 o -11 11 0 0.13 2.20 28.11 o -10 11 0 22.03 14.61 41.08 o -9 11 0 48.13 12.25 22.97 o -8 11 0 0.22 17.04 19.96 o -7 11 0 221.00 237.90 21.44 o -6 11 0 231.18 229.40 35.50 o -5 11 0 2024.51 1961.46 82.90 o -4 11 0 1305.40 1279.37 24.49 o -3 11 0 291.31 302.13 12.31 o -2 11 0 55.13 55.72 9.08 o -1 11 0 314.43 320.49 18.54 o 0 11 0 1137.64 1149.10 43.58 o 1 11 0 2.94 7.47 12.68 o 2 11 0 426.84 425.32 22.78 o 3 11 0 75.40 91.32 19.75 o 4 11 0 566.66 591.10 30.68 o 5 11 0 126.15 104.06 25.31 o 6 11 0 1.14 22.41 27.61 o 7 11 0 66.30 75.18 31.89 o -11 12 0 0.73 0.93 29.41 o -10 12 0 1.68 -7.13 26.98 o -9 12 0 3.09 16.99 24.07 o -8 12 0 38.66 47.03 25.14 o -7 12 0 578.76 572.21 34.57 o -6 12 0 32.34 46.07 16.85 o -5 12 0 302.89 372.51 25.57 o -4 12 0 730.91 702.85 18.90 o -3 12 0 188.29 221.74 12.34 o -2 12 0 705.76 671.13 24.07 o -1 12 0 15.02 22.92 9.58 o 0 12 0 391.28 390.61 20.49 o 1 12 0 1109.51 1144.06 62.46 o 2 12 0 19.17 -1.84 17.63 o 3 12 0 27.81 8.38 19.71 o 4 12 0 224.82 244.37 35.35 o 5 12 0 45.20 23.70 45.98 o 6 12 0 11.07 -14.92 28.38 o -10 13 0 25.82 22.68 43.63 o -9 13 0 36.87 -1.08 24.83 o -8 13 0 0.21 0.47 21.39 o -7 13 0 5.43 -22.99 22.99 o -6 13 0 3.18 20.66 15.08 o -5 13 0 8.60 -11.35 13.41 o -4 13 0 13.92 10.14 11.84 o -3 13 0 56.93 82.93 11.68 o -2 13 0 1872.21 1861.59 27.44 o -1 13 0 298.30 332.86 17.32 o 0 13 0 615.45 630.44 24.97 o 1 13 0 314.04 361.74 22.75 o 2 13 0 8.01 23.07 19.24 o 3 13 0 19.92 5.90 39.49 o 4 13 0 2.39 8.99 26.32 o 5 13 0 3.46 -15.75 26.47 o -10 14 0 36.77 -3.55 28.34 o -9 14 0 46.64 88.40 50.36 o -8 14 0 24.38 21.11 23.37 o -7 14 0 0.39 11.11 28.05 o -6 14 0 25.99 29.32 18.07 o -5 14 0 120.87 118.60 16.33 o -4 14 0 514.04 523.28 19.81 o -3 14 0 26.03 13.33 11.82 o -2 14 0 3.84 28.57 23.96 o -1 14 0 20.78 32.47 25.46 o 0 14 0 4.77 35.26 29.09 o 1 14 0 0.45 -7.53 18.71 o 2 14 0 16.98 4.20 38.05 o 3 14 0 303.60 368.49 29.22 o 4 14 0 153.87 168.41 49.48 o -9 15 0 2.92 30.42 23.47 o -8 15 0 149.15 142.41 22.83 o -7 15 0 94.38 81.76 29.23 o -6 15 0 0.05 2.22 17.75 o -5 15 0 12.89 22.41 16.09 o -4 15 0 19.48 16.35 20.40 o -3 15 0 72.28 117.78 28.29 o -2 15 0 0.27 -10.99 26.30 o -1 15 0 4.68 -3.08 40.94 o 0 15 0 70.14 88.77 45.88 o 1 15 0 421.71 485.19 28.15 o 2 15 0 16.72 25.21 23.75 o 3 15 0 21.62 9.47 26.39 o -8 16 0 9.63 -2.97 23.14 o -7 16 0 74.75 108.58 24.14 o -6 16 0 39.55 49.16 19.01 o -5 16 0 51.32 58.54 26.65 o -4 16 0 21.70 -8.33 28.76 o -3 16 0 66.87 76.36 41.18 o -2 16 0 383.33 431.96 38.22 o -1 16 0 22.85 -8.81 45.15 o 0 16 0 22.99 48.97 48.38 o 1 16 0 30.41 73.79 52.00 o 2 16 0 3.64 51.71 54.60 o -7 17 0 26.93 31.36 31.08 o -6 17 0 0.20 17.41 29.38 o -5 17 0 257.82 225.39 32.50 o -4 17 0 63.69 73.15 33.06 o -3 17 0 56.22 71.67 33.07 o -2 17 0 22.72 -1.96 48.82 o -1 17 0 14.36 -41.28 48.72 o 0 17 0 8.45 52.59 52.69 o 1 17 0 3.67 96.41 58.51 o -6 18 0 0.46 -34.32 46.47 o -5 18 0 16.81 -12.39 45.59 o -4 18 0 16.02 -9.41 33.87 o -3 18 0 10.57 26.79 35.21 o -2 18 0 0.09 45.64 56.31 o -1 18 0 9.94 -16.70 57.29 o 0 -18 1 4.44 4.16 54.01 o 1 -18 1 90.50 92.40 56.65 o 2 -18 1 56.13 77.32 52.83 o 3 -18 1 17.96 -11.74 33.82 o 4 -18 1 27.56 73.64 47.40 o 5 -18 1 0.26 -23.94 45.49 o 6 -18 1 71.10 67.84 40.27 o -1 -17 1 50.93 -30.90 53.57 o 0 -17 1 3.61 -2.84 50.92 o 1 -17 1 18.54 51.66 50.43 o 2 -17 1 11.31 45.73 32.34 o 3 -17 1 121.94 167.49 33.59 o 4 -17 1 87.84 90.83 45.15 o 5 -17 1 34.27 88.54 30.36 o 6 -17 1 7.05 -19.87 29.71 o 7 -17 1 29.21 27.17 56.80 o -3 -16 1 11.25 -0.83 54.99 o -2 -16 1 4.68 7.64 51.37 o -1 -16 1 18.57 -47.59 47.59 o 0 -16 1 1.24 7.10 46.86 o 1 -16 1 683.28 745.55 63.12 o 2 -16 1 38.61 -14.09 28.90 o 3 -16 1 1.55 31.52 29.13 o 4 -16 1 102.54 123.54 23.83 o 5 -16 1 37.44 20.81 30.43 o 6 -16 1 29.40 49.40 25.51 o 7 -16 1 33.70 26.28 20.99 o 8 -16 1 41.14 52.89 22.92 o -4 -15 1 0.23 -9.36 26.81 o -3 -15 1 46.01 57.94 24.49 o -2 -15 1 233.64 249.13 25.38 o -1 -15 1 89.86 13.22 43.19 o 0 -15 1 7.28 -9.84 41.91 o 1 -15 1 25.53 11.04 26.69 o 2 -15 1 0.05 13.64 25.80 o 3 -15 1 65.28 65.60 20.03 o 4 -15 1 98.05 113.07 21.13 o 5 -15 1 26.57 10.91 18.17 o 6 -15 1 298.39 374.26 21.55 o 7 -15 1 35.58 27.10 36.78 o 8 -15 1 5.39 13.35 21.20 o 9 -15 1 29.06 32.34 27.94 o -5 -14 1 79.00 81.89 29.75 o -4 -14 1 130.69 158.32 28.50 o -3 -14 1 36.92 0.50 28.96 o -2 -14 1 327.70 282.37 23.88 o -1 -14 1 33.86 60.96 27.03 o 0 -14 1 3.49 -35.89 35.89 o 1 -14 1 13.85 -10.78 23.84 o 2 -14 1 231.23 252.85 38.48 o 3 -14 1 192.72 181.65 20.33 o 4 -14 1 611.43 601.77 20.60 o 5 -14 1 73.41 62.73 15.05 o 6 -14 1 10.46 -3.20 15.82 o 7 -14 1 16.70 3.34 20.75 o 8 -14 1 83.20 62.71 23.22 o 9 -14 1 12.70 47.19 27.03 o 10 -14 1 8.38 29.41 30.14 o -6 -13 1 2.35 -30.63 30.63 o -5 -13 1 20.71 47.52 33.59 o -4 -13 1 176.99 193.48 26.25 o -3 -13 1 21.39 14.57 20.19 o -2 -13 1 5.03 -4.25 28.23 o -1 -13 1 241.85 253.91 19.00 o 0 -13 1 138.80 139.58 15.17 o 1 -13 1 366.35 372.41 27.24 o 2 -13 1 0.36 -9.21 9.21 o 3 -13 1 422.44 426.75 31.90 o 4 -13 1 35.68 28.13 12.06 o 5 -13 1 20.59 11.09 13.72 o 6 -13 1 70.54 71.90 22.43 o 7 -13 1 104.26 109.76 21.64 o 8 -13 1 0.32 35.85 27.69 o 9 -13 1 164.70 176.63 49.16 o 10 -13 1 60.23 49.25 30.90 o -6 -12 1 0.25 -19.21 26.43 o -5 -12 1 35.65 60.85 24.60 o -4 -12 1 203.59 233.79 31.36 o -3 -12 1 13.90 6.39 20.71 o -2 -12 1 1504.48 1584.83 43.24 o -1 -12 1 2.69 5.67 13.52 o 0 -12 1 2.14 6.67 10.93 o 1 -12 1 363.99 356.82 16.57 o 2 -12 1 0.03 3.77 8.23 o 3 -12 1 9.12 8.01 11.15 o 4 -12 1 754.38 710.29 20.50 o 5 -12 1 0.92 3.82 17.02 o 6 -12 1 182.32 154.65 18.46 o 7 -12 1 217.15 205.49 21.61 o 8 -12 1 142.94 144.16 23.34 o 9 -12 1 0.30 22.10 22.93 o 10 -12 1 4.78 -16.66 26.28 o -7 -11 1 14.36 37.53 30.08 o -6 -11 1 129.12 156.16 28.03 o -5 -11 1 112.28 109.41 23.24 o -4 -11 1 405.50 434.99 26.56 o -3 -11 1 127.22 90.67 18.90 o -2 -11 1 376.50 368.52 20.98 o -1 -11 1 34.21 24.44 11.74 o 0 -11 1 1055.94 1037.18 17.90 o 1 -11 1 383.68 394.70 15.63 o 2 -11 1 680.00 682.17 14.40 o 3 -11 1 2091.59 2063.47 26.93 o 4 -11 1 214.18 200.11 12.82 o 5 -11 1 14.98 20.47 12.79 o 6 -11 1 508.04 484.44 23.21 o 7 -11 1 135.29 129.40 26.86 o 8 -11 1 0.54 -14.58 23.36 o 9 -11 1 0.16 -17.67 21.79 o 10 -11 1 0.88 -13.00 24.68 o 11 -11 1 7.47 42.33 29.27 o -8 -10 1 35.14 14.68 30.84 o -7 -10 1 175.56 152.53 63.19 o -6 -10 1 7.21 -9.02 23.57 o -5 -10 1 121.92 147.19 24.56 o -4 -10 1 6.96 32.22 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