data_2239597 _cell_angle_alpha 90.000 _cell_angle_beta 109.529 _cell_angle_gamma 90.000 _cell_length_a 10.9360 _cell_length_b 8.7080 _cell_length_c 13.7940 _exptl_crystal_F_000 608.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file pk2524Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' A in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 133.45 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1332.51 1207.41 25.19 o 2 0 0 500.54 472.03 6.43 o 3 0 0 8920.01 8255.82 109.66 o 4 0 0 333.17 377.01 5.41 o 5 0 0 752.94 864.20 11.84 o 6 0 0 88.91 81.50 1.76 o 7 0 0 42.11 47.00 1.31 o 8 0 0 99.34 90.50 2.10 o 9 0 0 1361.13 1410.72 19.57 o 10 0 0 39.11 42.78 1.48 o 11 0 0 16.18 14.74 1.08 o 12 0 0 101.60 99.86 2.67 o 1 1 0 685.47 597.97 6.56 o 2 1 0 3647.57 3679.34 27.73 o 3 1 0 868.19 859.62 7.99 o 4 1 0 221.48 281.78 2.55 o 5 1 0 2616.21 2670.54 22.13 o 6 1 0 2115.90 2065.43 17.49 o 7 1 0 440.77 447.57 4.75 o 8 1 0 702.55 691.80 7.12 o 9 1 0 278.45 283.74 5.48 o 10 1 0 6.79 7.18 0.58 o 11 1 0 66.37 71.51 1.70 o 12 1 0 48.36 50.92 1.55 o 0 2 0 638.05 643.78 7.87 o 1 2 0 6856.19 6576.31 65.96 o 2 2 0 30.98 27.48 0.42 o 3 2 0 558.50 523.21 4.05 o 4 2 0 900.20 908.48 6.92 o 5 2 0 6.19 7.84 0.41 o 6 2 0 62.86 53.69 0.88 o 7 2 0 676.83 649.55 6.66 o 8 2 0 0.84 1.61 0.30 o 9 2 0 652.53 622.39 7.71 o 10 2 0 131.15 138.32 2.51 o 11 2 0 42.33 39.07 1.30 o 12 2 0 83.66 76.55 1.92 o 1 3 0 407.88 484.06 3.78 o 2 3 0 283.06 294.81 2.68 o 3 3 0 459.68 496.12 4.88 o 4 3 0 98.11 69.18 0.98 o 5 3 0 747.53 747.76 5.82 o 6 3 0 57.30 72.18 0.96 o 7 3 0 547.85 550.93 5.61 o 8 3 0 1.14 0.16 0.46 o 9 3 0 431.31 433.65 5.76 o 10 3 0 70.79 68.09 1.86 o 11 3 0 181.51 187.79 3.22 o 0 4 0 3118.79 3223.47 80.17 o 1 4 0 1309.47 1244.05 9.43 o 2 4 0 167.94 146.80 4.23 o 3 4 0 681.96 729.65 6.28 o 4 4 0 33.75 16.81 0.52 o 5 4 0 35.99 30.67 0.60 o 6 4 0 382.06 372.58 4.01 o 7 4 0 86.53 77.10 1.28 o 8 4 0 21.01 20.87 1.00 o 9 4 0 291.44 289.59 5.06 o 10 4 0 2.10 4.03 0.68 o 11 4 0 169.11 175.03 3.16 o 1 5 0 98.89 90.41 0.97 o 2 5 0 45.04 48.14 1.35 o 3 5 0 971.59 985.03 8.43 o 4 5 0 1432.24 1387.18 11.67 o 5 5 0 1.31 2.98 0.34 o 6 5 0 514.02 553.77 5.75 o 7 5 0 1220.37 1210.30 11.99 o 8 5 0 24.04 18.42 0.86 o 9 5 0 223.96 218.53 3.44 o 10 5 0 277.84 290.85 4.43 o 0 6 0 608.63 586.78 6.71 o 1 6 0 198.87 184.86 2.00 o 2 6 0 895.26 854.80 7.42 o 3 6 0 192.28 189.30 2.09 o 4 6 0 47.96 47.93 0.88 o 5 6 0 7.32 6.56 0.41 o 6 6 0 0.02 0.23 0.46 o 7 6 0 5.53 4.86 0.46 o 8 6 0 38.41 40.52 1.24 o 9 6 0 31.52 33.84 1.23 o 1 7 0 291.37 295.38 3.34 o 2 7 0 744.29 748.81 6.66 o 3 7 0 17.14 24.09 0.67 o 4 7 0 143.34 155.49 1.88 o 5 7 0 716.73 711.95 7.32 o 6 7 0 34.82 39.90 1.00 o 7 7 0 8.43 5.97 0.52 o 8 7 0 90.65 100.89 2.11 o 9 7 0 18.46 19.19 1.31 o 0 8 0 25.51 32.23 5.63 o 1 8 0 110.45 110.99 1.73 o 2 8 0 82.08 72.42 1.39 o 3 8 0 794.06 754.58 11.66 o 4 8 0 22.11 24.76 0.82 o 5 8 0 0.44 0.34 0.39 o 6 8 0 162.62 156.01 2.33 o 7 8 0 6.37 8.07 0.71 o 1 9 0 52.91 46.75 1.15 o 2 9 0 227.76 233.95 3.02 o 3 9 0 32.20 29.12 0.92 o 4 9 0 0.10 1.42 0.42 o 5 9 0 38.89 46.63 1.71 o 6 9 0 21.29 19.04 1.53 o 0 10 0 720.02 717.58 18.27 o 1 10 0 369.79 363.76 4.36 o 2 10 0 1.00 1.20 0.52 o 3 10 0 199.81 199.38 3.36 o -12 1 1 1.00 0.61 0.71 o -11 1 1 661.71 644.84 8.53 o -10 1 1 135.56 145.32 2.17 o -9 1 1 26.36 27.65 0.88 o -8 1 1 653.32 613.12 6.36 o -7 1 1 70.60 69.06 1.16 o -6 1 1 59.27 65.31 0.91 o -5 1 1 223.80 310.09 2.85 o -4 1 1 58.17 37.42 0.53 o -3 1 1 925.37 908.13 8.44 o -2 1 1 2794.63 2662.84 44.87 o -1 1 1 764.19 722.74 5.98 o 0 1 1 3.14 -0.49 0.32 o 1 1 1 5777.50 5693.28 44.04 o 2 1 1 4271.72 4099.89 34.73 o 3 1 1 2968.10 2843.71 62.46 o 4 1 1 1.66 10.21 0.29 o 5 1 1 1598.76 1576.43 13.15 o 6 1 1 46.39 47.11 0.70 o 7 1 1 527.90 498.65 5.27 o 8 1 1 1077.71 1057.17 10.52 o 9 1 1 720.24 705.29 7.38 o 10 1 1 732.41 723.03 12.01 o 11 1 1 0.04 0.27 0.43 o -12 2 1 21.20 24.08 1.14 o -11 2 1 16.40 19.56 0.99 o -10 2 1 37.86 42.99 1.27 o -9 2 1 1569.91 1562.15 15.21 o -8 2 1 228.89 248.32 2.99 o -7 2 1 170.14 144.39 1.59 o -6 2 1 828.25 771.14 7.49 o -5 2 1 594.89 643.35 5.01 o -4 2 1 88.76 80.59 1.00 o -3 2 1 1746.94 1655.22 13.64 o -2 2 1 3091.85 3234.59 27.99 o -1 2 1 474.16 505.60 3.86 o 0 2 1 9703.80 8679.02 89.04 o 1 2 1 2807.20 2830.35 23.43 o 2 2 1 400.22 410.26 3.56 o 3 2 1 1526.01 1596.11 11.97 o 4 2 1 3358.56 3626.56 27.61 o 5 2 1 2572.53 2531.54 26.54 o 6 2 1 18.44 18.92 0.52 o 7 2 1 154.19 156.53 2.07 o 8 2 1 995.23 974.81 9.77 o 9 2 1 172.44 171.12 2.82 o 10 2 1 11.92 13.80 0.90 o 11 2 1 19.01 25.68 1.12 o -11 3 1 32.38 34.56 1.26 o -10 3 1 547.63 535.47 6.91 o -9 3 1 1128.24 1091.37 12.73 o -8 3 1 29.04 30.88 1.19 o -7 3 1 0.40 1.93 0.30 o -6 3 1 562.96 553.02 4.94 o -5 3 1 318.27 363.40 2.99 o -4 3 1 2196.01 2427.23 18.29 o -3 3 1 597.90 667.29 5.17 o -2 3 1 7249.58 6953.67 54.23 o -1 3 1 137.86 151.36 1.32 o 0 3 1 823.79 806.25 6.15 o 1 3 1 2292.11 2252.29 16.99 o 2 3 1 0.06 0.55 0.14 o 3 3 1 3686.46 3807.33 32.29 o 4 3 1 221.10 181.07 1.64 o 5 3 1 85.29 88.56 0.94 o 6 3 1 925.64 983.15 8.48 o 7 3 1 819.97 805.51 11.61 o 8 3 1 137.39 125.74 2.26 o 9 3 1 2.09 4.39 0.54 o 10 3 1 16.75 15.45 0.90 o 11 3 1 301.74 302.31 4.55 o -11 4 1 25.70 23.87 1.11 o -10 4 1 270.08 275.94 4.15 o -9 4 1 1.94 4.75 0.56 o -8 4 1 62.59 50.99 1.27 o -7 4 1 724.64 701.66 7.06 o -6 4 1 61.81 64.93 1.10 o -5 4 1 8.11 5.06 0.36 o -4 4 1 5830.76 5917.85 51.74 o -3 4 1 15.58 7.55 0.63 o -2 4 1 96.01 134.61 1.26 o -1 4 1 1265.91 1327.03 10.05 o 0 4 1 60.51 49.86 0.67 o 1 4 1 422.08 430.28 3.46 o 2 4 1 321.68 394.42 3.57 o 3 4 1 1738.78 1823.65 16.61 o 4 4 1 47.76 46.72 0.86 o 5 4 1 26.06 25.45 0.71 o 6 4 1 720.67 730.37 7.31 o 7 4 1 128.69 105.76 3.68 o 8 4 1 0.83 -0.25 0.39 o 9 4 1 602.73 632.17 7.96 o 10 4 1 31.87 30.51 1.17 o 11 4 1 15.08 17.64 1.02 o -10 5 1 25.41 20.86 1.12 o -9 5 1 119.85 114.81 2.53 o -8 5 1 42.53 34.42 1.08 o -7 5 1 72.04 74.49 1.30 o -6 5 1 221.62 231.31 2.79 o -5 5 1 31.45 28.20 0.66 o -4 5 1 184.98 180.73 2.49 o -3 5 1 401.65 386.38 3.60 o -2 5 1 737.69 782.83 6.13 o -1 5 1 132.93 152.53 1.46 o 0 5 1 1183.72 1283.11 13.85 o 1 5 1 780.08 830.72 6.48 o 2 5 1 733.30 749.82 6.52 o 3 5 1 3.28 0.66 0.26 o 4 5 1 0.01 -0.07 0.25 o 5 5 1 251.60 265.51 2.68 o 6 5 1 2.35 4.24 0.48 o 7 5 1 26.15 17.03 0.70 o 8 5 1 3.36 5.36 0.62 o 9 5 1 1.96 1.85 0.57 o 10 5 1 1.92 1.18 0.56 o -10 6 1 152.48 156.71 3.64 o -9 6 1 151.76 157.96 3.94 o -8 6 1 21.19 14.14 1.33 o -7 6 1 313.19 357.69 4.10 o -6 6 1 957.85 937.58 9.33 o -5 6 1 20.85 19.63 0.62 o -4 6 1 964.69 963.89 8.36 o -3 6 1 909.20 924.74 8.00 o -2 6 1 193.50 224.26 2.34 o -1 6 1 511.19 501.23 4.56 o 0 6 1 846.11 936.91 8.05 o 1 6 1 86.76 107.36 1.35 o 2 6 1 595.41 597.00 6.67 o 3 6 1 2671.25 2713.40 22.37 o 4 6 1 147.36 135.42 1.87 o 5 6 1 640.37 620.43 6.39 o 6 6 1 788.99 770.45 9.15 o 7 6 1 157.72 147.86 2.21 o 8 6 1 17.59 20.47 0.93 o 9 6 1 173.41 169.41 3.00 o -9 7 1 173.20 185.44 3.98 o -8 7 1 14.57 16.23 1.14 o -7 7 1 12.02 20.97 0.96 o -6 7 1 14.70 16.49 0.74 o -5 7 1 389.58 398.52 3.94 o -4 7 1 152.11 151.83 2.26 o -3 7 1 583.82 598.89 6.16 o -2 7 1 429.29 412.80 4.46 o -1 7 1 0.47 0.07 0.27 o 0 7 1 1.51 1.49 0.32 o 1 7 1 573.34 528.51 5.49 o 2 7 1 751.20 723.48 9.25 o 3 7 1 70.90 80.90 1.24 o 4 7 1 636.76 615.17 5.68 o 5 7 1 52.49 44.87 1.06 o 6 7 1 168.69 160.67 2.29 o 7 7 1 146.46 135.18 2.09 o 8 7 1 29.48 27.78 1.23 o -8 8 1 276.83 295.27 5.52 o -7 8 1 3.85 3.02 0.56 o -6 8 1 688.07 693.63 8.41 o -5 8 1 139.66 146.66 2.54 o -4 8 1 11.20 12.93 0.66 o -3 8 1 816.99 829.74 8.34 o -2 8 1 326.56 307.33 3.60 o -1 8 1 15.89 15.58 0.70 o 0 8 1 349.58 377.50 4.24 o 1 8 1 178.25 164.46 2.27 o 2 8 1 21.29 18.90 0.78 o 3 8 1 2.67 2.92 0.51 o 4 8 1 67.19 66.85 1.28 o 5 8 1 547.39 536.61 5.85 o 6 8 1 0.27 0.03 0.38 o 7 8 1 308.01 295.89 3.74 o -6 9 1 69.96 66.63 2.10 o -5 9 1 1.62 4.35 1.93 o -4 9 1 98.34 96.29 1.98 o -3 9 1 33.27 32.21 1.14 o -2 9 1 141.11 139.63 2.13 o -1 9 1 746.40 746.48 7.70 o 0 9 1 518.90 491.49 5.37 o 1 9 1 74.71 81.39 1.53 o 2 9 1 410.85 404.79 4.63 o 3 9 1 172.69 166.03 2.39 o 4 9 1 10.44 12.27 0.68 o 5 9 1 280.25 280.60 4.15 o -3 10 1 3.84 3.65 0.86 o -2 10 1 112.32 124.18 2.38 o -1 10 1 85.91 93.22 2.04 o 0 10 1 151.44 157.00 2.39 o 1 10 1 90.94 90.78 1.73 o 2 10 1 12.09 9.77 0.92 o -12 0 2 545.37 539.22 9.34 o -11 0 2 226.31 229.80 4.67 o -10 0 2 847.65 815.95 11.95 o -9 0 2 2847.93 2765.33 38.15 o -8 0 2 1708.47 1700.00 26.48 o -7 0 2 56.92 45.01 1.25 o -6 0 2 63.38 45.44 0.80 o -5 0 2 232.35 204.10 2.48 o -4 0 2 718.29 638.07 6.93 o -3 0 2 940.59 927.57 9.87 o -2 0 2 3302.27 2972.54 42.09 o 0 0 2 1393.23 1243.14 55.56 o 1 0 2 79.13 72.28 0.95 o 2 0 2 12004.26 10858.06 172.33 o 3 0 2 1.37 -0.40 0.62 o 4 0 2 0.82 2.41 0.34 o 5 0 2 7308.91 6837.72 113.40 o 6 0 2 59.13 47.57 1.31 o 7 0 2 247.48 256.99 4.32 o 8 0 2 598.07 578.96 8.65 o 9 0 2 14.98 15.54 1.02 o 10 0 2 4.88 3.30 0.68 o 11 0 2 139.86 138.05 3.18 o -12 1 2 16.88 21.01 1.08 o -11 1 2 1.05 0.25 0.38 o -10 1 2 319.51 321.59 3.84 o -9 1 2 69.67 56.60 1.16 o -8 1 2 15.38 19.48 0.66 o -7 1 2 1882.87 1969.94 16.45 o -6 1 2 3069.53 3141.93 42.41 o -5 1 2 104.01 98.07 0.94 o -4 1 2 7725.48 7188.58 55.09 o -3 1 2 965.77 961.97 7.25 o -2 1 2 1.72 2.57 0.11 o -1 1 2 1806.71 1769.15 15.48 o 0 1 2 238.48 264.09 2.10 o 1 1 2 3918.97 4073.77 35.27 o 2 1 2 4361.34 4256.47 47.88 o 3 1 2 3519.85 3501.36 26.68 o 4 1 2 1.05 1.13 0.21 o 5 1 2 18.08 9.75 0.32 o 6 1 2 14.88 18.22 0.87 o 7 1 2 1566.27 1581.07 15.27 o 8 1 2 342.55 320.12 3.74 o 9 1 2 598.48 600.40 6.46 o 10 1 2 747.34 741.40 7.88 o 11 1 2 205.33 200.44 3.37 o -12 2 2 1.09 1.31 0.58 o -11 2 2 249.07 245.84 3.81 o -10 2 2 365.12 350.24 4.83 o -9 2 2 297.85 289.56 3.42 o -8 2 2 159.68 184.81 2.35 o -7 2 2 173.77 198.71 2.06 o -6 2 2 60.91 69.03 0.84 o -5 2 2 1906.04 2012.33 18.65 o -4 2 2 25.82 12.66 0.69 o -3 2 2 474.07 535.74 12.71 o -2 2 2 2633.56 2570.91 20.33 o -1 2 2 4687.47 4310.46 33.76 o 0 2 2 17807.62 14696.81 232.69 o 1 2 2 17717.17 15469.40 190.34 o 2 2 2 610.28 789.66 6.02 o 3 2 2 1385.78 1351.31 10.20 o 4 2 2 931.19 1016.60 8.46 o 5 2 2 430.77 528.27 4.62 o 6 2 2 897.99 836.92 8.16 o 7 2 2 296.30 288.09 3.33 o 8 2 2 6.08 6.89 0.56 o 9 2 2 241.59 235.42 3.93 o 10 2 2 15.06 19.00 1.22 o 11 2 2 6.01 5.09 0.68 o -12 3 2 49.01 55.47 1.60 o -11 3 2 0.42 1.03 0.52 o -10 3 2 18.41 18.73 0.92 o -9 3 2 40.39 48.42 1.27 o -8 3 2 265.71 259.48 3.75 o -7 3 2 1.73 2.25 0.60 o -6 3 2 490.90 537.83 4.32 o -5 3 2 388.71 386.38 3.17 o -4 3 2 27.50 41.81 0.91 o -3 3 2 1789.61 1812.75 13.61 o -2 3 2 471.60 555.62 4.33 o -1 3 2 0.74 1.96 0.16 o 0 3 2 1541.76 1762.64 13.23 o 1 3 2 57.83 48.43 0.57 o 2 3 2 903.30 955.01 7.30 o 3 3 2 60.20 70.31 0.86 o 4 3 2 1062.42 1033.27 8.18 o 5 3 2 106.33 126.69 1.52 o 6 3 2 351.04 331.94 5.31 o 7 3 2 215.81 197.35 3.03 o 8 3 2 269.51 239.06 3.56 o 9 3 2 6.37 7.02 0.68 o 10 3 2 247.42 251.86 3.93 o 11 3 2 18.24 23.11 1.12 o -11 4 2 35.21 36.66 1.65 o -10 4 2 491.34 498.70 8.39 o -9 4 2 1.61 0.53 0.40 o -8 4 2 138.27 123.08 2.16 o -7 4 2 824.49 837.22 8.27 o -6 4 2 72.82 82.63 1.09 o -5 4 2 62.20 73.89 1.16 o -4 4 2 444.42 488.97 3.94 o -3 4 2 2.73 6.64 0.39 o -2 4 2 719.85 788.38 6.12 o -1 4 2 14.48 25.90 0.44 o 0 4 2 627.62 659.48 5.17 o 1 4 2 461.32 409.79 3.32 o 2 4 2 227.45 265.98 2.55 o 3 4 2 607.70 552.26 4.87 o 4 4 2 1445.56 1399.19 13.28 o 5 4 2 139.10 130.22 1.76 o 6 4 2 568.14 543.97 5.64 o 7 4 2 25.82 20.60 1.02 o 8 4 2 22.06 21.72 0.93 o 9 4 2 122.74 121.56 2.35 o 10 4 2 0.19 -0.37 0.43 o -11 5 2 58.79 62.78 3.06 o -10 5 2 72.53 81.77 2.50 o -9 5 2 35.53 36.08 1.60 o -8 5 2 168.04 174.83 2.72 o -7 5 2 0.12 1.05 0.46 o -6 5 2 0.92 1.89 1.29 o -5 5 2 3068.22 2961.59 24.31 o -4 5 2 808.53 880.13 7.58 o -3 5 2 431.01 469.19 4.26 o -2 5 2 6282.29 6278.37 50.99 o -1 5 2 722.50 727.61 5.72 o 0 5 2 10.12 12.20 0.34 o 1 5 2 1276.47 1242.73 9.50 o 2 5 2 129.82 127.52 1.48 o 3 5 2 35.23 24.19 0.74 o 4 5 2 1058.47 1020.91 8.77 o 5 5 2 664.10 667.06 6.77 o 6 5 2 541.03 540.30 5.66 o 7 5 2 387.37 362.58 4.93 o 8 5 2 73.82 79.40 2.22 o 9 5 2 50.30 60.67 1.64 o 10 5 2 0.02 0.05 0.46 o -10 6 2 313.64 328.24 5.92 o -9 6 2 509.51 497.62 8.08 o -8 6 2 148.05 158.40 2.65 o -7 6 2 443.42 446.71 4.88 o -6 6 2 212.68 190.18 2.47 o -5 6 2 4.54 5.84 0.40 o -4 6 2 0.21 0.41 0.25 o -3 6 2 68.53 59.21 0.96 o -2 6 2 89.95 95.43 1.25 o -1 6 2 56.68 61.57 0.92 o 0 6 2 95.32 74.58 1.06 o 1 6 2 12.29 8.13 0.41 o 2 6 2 35.00 38.94 0.78 o 3 6 2 856.87 833.74 7.33 o 4 6 2 97.14 96.31 1.35 o 5 6 2 614.92 592.49 6.21 o 6 6 2 35.26 36.75 1.05 o 7 6 2 62.34 60.58 1.26 o 8 6 2 18.13 11.97 0.84 o 9 6 2 16.32 17.48 0.96 o -9 7 2 235.01 245.17 4.78 o -8 7 2 4.69 2.82 0.52 o -7 7 2 161.25 142.57 2.50 o -6 7 2 179.62 203.73 3.16 o -5 7 2 7.22 7.98 0.47 o -4 7 2 363.60 361.08 3.58 o -3 7 2 1074.55 1122.07 14.72 o -2 7 2 62.00 69.03 1.25 o -1 7 2 165.94 162.29 2.15 o 0 7 2 306.47 311.44 3.52 o 1 7 2 41.73 44.78 1.02 o 2 7 2 720.85 724.54 6.50 o 3 7 2 44.36 43.41 0.89 o 4 7 2 1001.76 1029.16 9.02 o 5 7 2 0.29 0.89 0.58 o 6 7 2 16.96 14.17 0.72 o 7 7 2 353.92 356.22 4.23 o 8 7 2 8.34 8.36 0.80 o -8 8 2 108.70 112.51 2.28 o -7 8 2 137.75 145.77 2.60 o -6 8 2 124.80 119.42 2.26 o -5 8 2 62.26 61.66 1.30 o -4 8 2 103.66 105.27 2.01 o -3 8 2 65.40 59.38 1.45 o -2 8 2 29.03 26.61 0.84 o -1 8 2 31.23 30.84 0.93 o 0 8 2 323.45 309.30 3.62 o 1 8 2 199.02 201.93 2.65 o 2 8 2 511.01 518.33 5.55 o 3 8 2 30.88 33.35 0.92 o 4 8 2 0.08 -0.16 0.29 o 5 8 2 7.86 8.42 0.60 o 6 8 2 0.23 1.36 0.42 o 7 8 2 2.01 2.36 0.50 o -6 9 2 153.93 153.54 3.41 o -5 9 2 45.63 39.74 1.65 o -4 9 2 1.37 1.33 0.49 o -3 9 2 58.43 62.79 1.79 o -2 9 2 12.68 17.10 0.93 o -1 9 2 3.49 3.79 0.58 o 0 9 2 62.04 58.07 1.27 o 1 9 2 639.45 642.84 6.80 o 2 9 2 0.68 0.04 0.38 o 3 9 2 2.00 2.00 0.40 o 4 9 2 0.13 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