data_2239605 _cell_angle_alpha 90.000 _cell_angle_beta 113.266 _cell_angle_gamma 90.000 _cell_length_a 12.4336 _cell_length_b 22.9278 _cell_length_c 13.3267 _exptl_crystal_F_000 1656.00 _reflns_d_resolution_high 0.7387 _cod_data_source_file fj2673Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ZnAmSH in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 453.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2113.55 1963.66 26.87 o 6 0 0 56.65 128.57 21.72 o 8 0 0 2195.02 2409.07 68.85 o 10 0 0 1601.75 1786.85 141.94 o 12 0 0 460.07 317.64 129.15 o 14 0 0 8.22 -12.84 146.39 o 3 1 0 9154.93 8732.51 43.61 o 4 1 0 1636.74 1403.67 21.21 o 5 1 0 988.50 871.09 17.91 o 6 1 0 108.34 87.91 12.90 o 7 1 0 772.79 785.79 39.03 o 8 1 0 489.37 515.22 35.84 o 9 1 0 7743.39 7751.94 85.80 o 10 1 0 29.78 12.10 60.33 o 11 1 0 904.99 866.69 88.51 o 12 1 0 162.78 147.95 86.96 o 13 1 0 29.06 -16.90 94.53 o 14 1 0 1.39 94.70 104.76 o 15 1 0 76.36 295.23 125.20 o 2 2 0 3631.58 4004.67 84.07 o 3 2 0 4225.25 4636.64 33.70 o 4 2 0 22.27 77.37 16.66 o 5 2 0 33.40 40.21 13.51 o 6 2 0 488.39 568.09 25.09 o 7 2 0 1093.80 915.21 30.67 o 8 2 0 1555.12 1573.83 43.70 o 9 2 0 1577.11 1630.25 61.07 o 10 2 0 2998.34 3112.82 76.29 o 11 2 0 1861.98 2090.05 99.80 o 12 2 0 4.17 31.03 88.73 o 13 2 0 9.58 50.80 91.97 o 14 2 0 99.35 66.53 100.62 o 15 2 0 77.98 -14.14 135.30 o 1 3 0 19688.49 15768.13 36.28 o 2 3 0 84.11 88.94 35.04 o 3 3 0 919.01 678.54 18.99 o 4 3 0 2443.44 2141.55 21.84 o 5 3 0 162.44 232.46 15.43 o 6 3 0 523.63 514.03 22.43 o 7 3 0 447.88 627.92 29.65 o 8 3 0 5300.97 5050.53 68.28 o 9 3 0 971.56 968.69 56.64 o 10 3 0 173.91 203.61 55.36 o 11 3 0 1032.81 1051.36 77.05 o 12 3 0 1251.13 1217.36 101.66 o 13 3 0 224.74 195.49 95.34 o 14 3 0 15.40 -0.32 97.79 o 15 3 0 19.61 -26.67 141.21 o 0 4 0 15617.28 15987.78 95.66 o 1 4 0 47066.02 46205.18 294.57 o 2 4 0 232.74 258.35 18.16 o 3 4 0 12992.75 14265.54 53.16 o 4 4 0 276.94 401.20 17.71 o 5 4 0 7755.30 6727.20 44.89 o 6 4 0 118.02 120.10 20.44 o 7 4 0 7573.68 7141.38 65.46 o 8 4 0 407.89 365.63 40.15 o 9 4 0 769.66 895.92 56.36 o 10 4 0 1239.10 1287.64 65.52 o 11 4 0 516.70 742.13 75.65 o 12 4 0 552.48 499.24 92.55 o 13 4 0 0.65 27.48 92.65 o 14 4 0 282.43 191.84 99.81 o 15 4 0 205.01 98.69 194.93 o 1 5 0 178.86 101.82 19.69 o 2 5 0 18337.56 15832.77 57.79 o 3 5 0 8503.86 7962.88 57.98 o 4 5 0 164.17 127.44 16.34 o 5 5 0 31.39 47.79 18.32 o 6 5 0 1427.28 1541.06 31.49 o 7 5 0 1448.38 1412.54 39.87 o 8 5 0 7144.83 6605.99 77.69 o 9 5 0 1205.29 1109.26 58.30 o 10 5 0 666.32 758.93 62.81 o 11 5 0 268.58 300.66 62.46 o 12 5 0 86.44 170.75 75.08 o 13 5 0 1213.58 1190.60 105.33 o 14 5 0 59.03 -66.70 99.70 o 15 5 0 1.04 -164.48 185.19 o 0 6 0 7313.71 6794.74 61.41 o 1 6 0 2730.64 2429.81 28.97 o 2 6 0 3399.77 3150.03 41.33 o 3 6 0 6331.52 6956.19 43.61 o 4 6 0 4313.02 3933.20 34.17 o 5 6 0 1413.65 1406.04 34.03 o 6 6 0 1723.62 1438.31 33.88 o 7 6 0 3766.58 3470.80 51.98 o 8 6 0 439.82 469.62 43.73 o 9 6 0 478.44 475.20 55.12 o 10 6 0 274.62 209.69 57.80 o 11 6 0 1809.45 2012.73 78.84 o 12 6 0 886.14 972.28 86.23 o 13 6 0 83.22 53.96 94.07 o 14 6 0 153.33 101.55 99.40 o 1 7 0 16.34 31.19 24.95 o 2 7 0 6805.58 6381.34 45.94 o 3 7 0 26111.06 24897.05 91.41 o 4 7 0 14461.50 18089.66 135.96 o 5 7 0 90.27 15.92 21.67 o 6 7 0 1663.19 1741.80 38.72 o 7 7 0 2957.95 2685.98 56.29 o 8 7 0 4705.91 4853.09 73.04 o 9 7 0 114.64 67.93 52.46 o 10 7 0 787.34 766.03 63.84 o 11 7 0 2.20 -2.38 63.18 o 12 7 0 1435.35 1393.59 91.12 o 13 7 0 796.80 912.66 89.01 o 14 7 0 48.76 53.98 121.44 o 0 8 0 3955.58 3146.43 45.25 o 1 8 0 2979.14 3374.68 37.01 o 2 8 0 3953.61 3457.25 38.68 o 3 8 0 15381.49 18310.53 68.57 o 4 8 0 13150.93 12912.62 88.21 o 5 8 0 5342.08 5708.26 50.03 o 6 8 0 3655.59 3020.88 46.71 o 7 8 0 475.80 424.44 45.14 o 8 8 0 187.11 181.98 47.54 o 9 8 0 132.04 117.84 57.37 o 10 8 0 1791.10 1517.07 77.02 o 11 8 0 341.82 320.48 69.93 o 12 8 0 108.98 83.82 86.82 o 13 8 0 463.61 491.71 122.40 o 14 8 0 63.91 115.60 156.44 o 1 9 0 61.80 39.60 22.06 o 2 9 0 409.58 457.47 27.03 o 3 9 0 16223.51 14684.29 68.83 o 4 9 0 8125.71 8435.51 52.09 o 5 9 0 549.43 548.01 28.40 o 6 9 0 11498.11 12004.14 91.78 o 7 9 0 116.89 58.07 37.99 o 8 9 0 18.03 38.49 47.73 o 9 9 0 565.87 602.86 64.56 o 10 9 0 132.53 109.99 63.87 o 11 9 0 222.43 146.89 85.18 o 12 9 0 1293.12 1032.40 99.88 o 13 9 0 2.96 79.52 113.51 o 14 9 0 307.42 375.49 120.41 o 0 10 0 17850.68 17409.62 174.62 o 1 10 0 1791.84 2040.99 40.95 o 2 10 0 3118.48 2862.70 36.04 o 3 10 0 2179.21 2402.64 35.32 o 4 10 0 457.63 341.74 23.48 o 5 10 0 15339.97 15364.24 83.01 o 6 10 0 1161.08 1008.17 43.86 o 7 10 0 19.00 -13.08 38.43 o 8 10 0 16.93 67.59 49.93 o 9 10 0 638.39 608.30 68.43 o 10 10 0 34.80 12.85 79.77 o 11 10 0 75.26 23.37 84.60 o 12 10 0 60.57 36.08 89.00 o 13 10 0 566.77 774.26 160.10 o 14 10 0 5.00 193.19 149.38 o 1 11 0 986.35 849.20 32.95 o 2 11 0 471.87 614.89 29.79 o 3 11 0 41.08 3.61 22.12 o 4 11 0 6588.76 5567.85 48.57 o 5 11 0 1.56 11.80 28.21 o 6 11 0 7111.70 7235.41 78.64 o 7 11 0 712.05 717.39 53.19 o 8 11 0 2363.16 2471.93 81.91 o 9 11 0 695.23 739.39 71.73 o 10 11 0 4045.86 3965.40 121.21 o 11 11 0 267.51 251.77 89.02 o 12 11 0 75.58 42.70 95.41 o 13 11 0 38.23 115.38 120.85 o 14 11 0 294.17 545.81 208.34 o 0 12 0 241.94 183.38 44.39 o 1 12 0 18.69 21.95 30.39 o 2 12 0 173.01 167.20 23.56 o 3 12 0 53.25 24.52 22.99 o 4 12 0 451.02 471.88 30.63 o 5 12 0 13197.00 12867.88 94.36 o 6 12 0 486.02 513.07 50.71 o 7 12 0 417.71 466.90 53.91 o 8 12 0 35.43 20.88 63.39 o 9 12 0 1530.52 1538.42 81.20 o 10 12 0 735.03 735.41 89.61 o 11 12 0 7.29 19.64 92.81 o 12 12 0 2.85 60.11 94.64 o 13 12 0 364.80 466.59 99.49 o 1 13 0 386.83 478.63 34.64 o 2 13 0 78.75 92.62 31.63 o 3 13 0 2895.61 2834.27 48.41 o 4 13 0 6474.95 5932.74 66.99 o 5 13 0 6.31 17.01 37.55 o 6 13 0 4786.56 4782.95 82.90 o 7 13 0 821.91 843.69 59.95 o 8 13 0 805.57 799.78 72.64 o 9 13 0 89.65 121.62 71.78 o 10 13 0 498.95 575.24 94.82 o 11 13 0 578.18 534.78 98.25 o 12 13 0 266.49 267.84 95.96 o 13 13 0 2.25 58.48 103.21 o 0 14 0 201.09 104.52 50.46 o 1 14 0 340.05 261.87 35.27 o 2 14 0 1419.40 1444.86 41.70 o 3 14 0 756.48 842.18 39.78 o 4 14 0 883.22 802.77 42.91 o 5 14 0 9705.85 9954.93 99.47 o 6 14 0 543.08 589.67 56.48 o 7 14 0 126.20 97.78 55.69 o 8 14 0 7.21 11.56 68.03 o 9 14 0 604.09 618.13 76.56 o 10 14 0 1474.47 1221.09 104.50 o 11 14 0 31.83 116.37 96.91 o 12 14 0 7.40 34.11 93.88 o 13 14 0 51.75 14.25 107.65 o 1 15 0 209.24 308.77 42.26 o 2 15 0 554.71 699.26 42.02 o 3 15 0 5614.35 5304.28 65.99 o 4 15 0 7732.55 8254.16 83.15 o 5 15 0 804.12 891.22 48.37 o 6 15 0 172.07 179.28 54.41 o 7 15 0 17.31 17.75 57.65 o 8 15 0 22.90 0.85 70.10 o 9 15 0 779.35 602.40 77.96 o 10 15 0 1.38 100.77 80.40 o 11 15 0 62.70 65.17 97.94 o 12 15 0 30.07 45.71 99.66 o 13 15 0 212.62 196.28 146.49 o 0 16 0 1.00 46.61 58.31 o 1 16 0 60.70 59.13 40.95 o 2 16 0 3594.21 3505.48 61.02 o 3 16 0 2285.10 2396.41 54.60 o 4 16 0 2509.44 2477.15 59.21 o 5 16 0 886.74 926.72 50.42 o 6 16 0 699.94 796.37 64.04 o 7 16 0 47.81 22.10 60.64 o 8 16 0 779.05 681.60 79.10 o 9 16 0 10.30 62.68 75.64 o 10 16 0 1407.57 1131.41 91.11 o 11 16 0 80.03 87.99 99.84 o 12 16 0 525.57 596.40 112.97 o 13 16 0 69.16 63.35 196.15 o 1 17 0 753.20 837.29 48.02 o 2 17 0 863.26 904.96 48.64 o 3 17 0 6093.62 6140.92 83.37 o 4 17 0 656.19 850.68 50.52 o 5 17 0 0.81 7.02 45.30 o 6 17 0 1076.97 1046.06 67.69 o 7 17 0 3075.09 3218.02 89.20 o 8 17 0 66.24 38.29 74.09 o 9 17 0 3137.75 2425.07 102.97 o 10 17 0 503.40 510.92 85.50 o 11 17 0 22.86 30.75 95.51 o 12 17 0 21.44 29.87 103.06 o 0 18 0 184.59 163.39 66.48 o 1 18 0 1338.89 1448.43 54.91 o 2 18 0 3074.85 3291.49 71.24 o 3 18 0 188.78 242.90 53.47 o 4 18 0 2002.56 2169.77 68.06 o 5 18 0 41.33 24.44 48.95 o 6 18 0 1412.55 1608.40 74.22 o 7 18 0 355.55 378.37 67.08 o 8 18 0 1589.82 1478.04 91.29 o 9 18 0 22.73 41.31 79.55 o 10 18 0 788.36 534.67 87.96 o 11 18 0 233.34 298.31 105.04 o 12 18 0 614.93 403.34 150.64 o 1 19 0 1805.31 1934.41 61.32 o 2 19 0 89.37 97.46 48.39 o 3 19 0 2686.17 3034.04 83.22 o 4 19 0 774.93 758.91 61.31 o 5 19 0 294.95 330.74 59.66 o 6 19 0 124.15 206.32 75.69 o 7 19 0 852.23 877.22 75.71 o 8 19 0 786.92 1001.94 86.04 o 9 19 0 354.97 239.81 85.62 o 10 19 0 102.69 120.88 88.28 o 11 19 0 805.73 809.36 115.95 o 12 19 0 0.94 -101.12 220.52 o 0 20 0 434.99 478.36 76.28 o 1 20 0 1696.41 1847.14 63.02 o 2 20 0 524.26 485.21 53.13 o 3 20 0 407.79 460.44 61.29 o 4 20 0 2387.86 2501.42 84.38 o 5 20 0 81.99 129.17 59.75 o 6 20 0 1648.67 1518.00 91.41 o 7 20 0 4.87 58.47 79.22 o 8 20 0 15.70 8.73 93.70 o 9 20 0 190.32 202.43 87.50 o 10 20 0 895.78 703.82 92.83 o 11 20 0 48.16 76.10 151.15 o 1 21 0 1045.67 1161.22 61.19 o 2 21 0 91.48 64.54 52.47 o 3 21 0 233.47 242.62 62.72 o 4 21 0 189.97 165.96 61.86 o 5 21 0 409.40 418.32 70.10 o 6 21 0 567.74 520.79 85.80 o 7 21 0 2548.31 2421.80 106.54 o 8 21 0 526.74 577.56 102.26 o 9 21 0 8.79 57.34 103.52 o 10 21 0 0.40 58.45 148.29 o 0 22 0 9560.93 9752.59 154.71 o 1 22 0 5.61 80.18 56.83 o 2 22 0 54.38 70.80 63.02 o 3 22 0 9.17 9.42 64.90 o 4 22 0 628.45 530.48 68.64 o 5 22 0 75.34 129.92 69.40 o 6 22 0 8.97 107.59 94.92 o 7 22 0 424.84 280.04 100.74 o 8 22 0 249.63 239.45 117.60 o 9 22 0 244.03 81.79 138.31 o 10 22 0 92.12 105.21 145.51 o 1 23 0 2402.84 2693.23 77.64 o 2 23 0 396.14 361.00 67.23 o 3 23 0 5.80 22.17 68.64 o 4 23 0 655.61 741.57 71.38 o 5 23 0 0.20 9.46 67.23 o 6 23 0 92.71 68.74 95.76 o 7 23 0 147.36 114.19 99.31 o 8 23 0 66.40 43.23 120.24 o 9 23 0 341.66 274.02 148.11 o 0 24 0 9427.46 10109.86 185.67 o 1 24 0 9.73 86.87 60.57 o 2 24 0 197.68 145.47 69.70 o 3 24 0 663.61 697.82 74.39 o 4 24 0 6.37 86.02 68.93 o 5 24 0 1057.61 969.90 85.77 o 6 24 0 49.78 -0.80 87.70 o 7 24 0 49.17 11.81 99.00 o 8 24 0 109.61 20.52 136.09 o 1 25 0 2081.89 2141.58 78.37 o 2 25 0 231.84 291.21 73.08 o 3 25 0 33.69 2.30 75.15 o 4 25 0 939.93 765.34 77.87 o 5 25 0 19.85 18.85 90.21 o 6 25 0 825.28 769.75 105.04 o 7 25 0 9.12 -13.56 110.29 o 8 25 0 119.41 5.34 124.55 o 0 26 0 846.83 1190.91 118.35 o 1 26 0 90.53 187.99 72.64 o 2 26 0 464.99 390.59 77.46 o 3 26 0 480.14 404.17 78.49 o 4 26 0 126.23 139.11 73.79 o 5 26 0 423.91 275.93 102.08 o 6 26 0 28.34 30.42 115.75 o 7 26 0 456.66 516.91 121.87 o 1 27 0 171.76 185.83 78.27 o 2 27 0 261.40 354.87 79.77 o 3 27 0 0.09 108.39 74.65 o 4 27 0 265.80 117.46 87.88 o 5 27 0 0.42 -110.57 115.11 o 6 27 0 301.31 149.02 112.24 o 0 28 0 272.15 251.64 114.78 o 1 28 0 7.55 108.44 91.59 o 2 28 0 83.45 218.85 94.03 o 3 28 0 384.98 398.42 102.55 o 4 28 0 17.45 10.74 131.76 o 5 28 0 127.81 -197.79 137.08 o 1 29 0 86.27 190.27 115.27 o 2 29 0 42.23 162.39 122.05 o 3 29 0 75.97 227.70 127.69 o 4 29 0 226.01 -37.13 128.09 o 0 30 0 6.21 -91.38 198.59 o 1 30 0 171.43 199.57 118.12 o 2 30 0 89.73 326.78 125.23 o 3 30 0 69.83 163.26 209.55 o -15 0 1 209.58 -24.82 125.08 o -13 0 1 1044.43 1169.22 143.87 o -11 0 1 7617.24 7753.10 245.49 o -9 0 1 3847.64 3947.77 86.21 o -7 0 1 2968.18 3673.65 68.88 o -5 0 1 325.19 228.91 22.14 o 3 0 1 57.46 149.30 22.96 o 5 0 1 2173.79 2265.06 38.88 o 7 0 1 4942.22 3955.35 75.22 o 9 0 1 1748.25 1841.01 121.47 o 11 0 1 441.77 242.97 120.12 o 13 0 1 895.92 475.68 143.49 o -15 1 1 2.23 -0.35 93.91 o -14 1 1 697.51 429.08 95.07 o -13 1 1 56.64 104.66 90.68 o -12 1 1 2874.45 3055.98 111.54 o -11 1 1 1674.84 1662.93 77.08 o -10 1 1 1022.89 1026.08 52.66 o -9 1 1 81.29 97.98 36.71 o -8 1 1 5338.53 5368.73 62.18 o -7 1 1 1758.49 1655.21 33.91 o -6 1 1 6396.55 6132.84 41.99 o -5 1 1 4207.36 4766.25 43.85 o -4 1 1 7228.15 8953.34 46.15 o -3 1 1 10562.42 11681.57 75.22 o 2 1 1 8231.35 8636.41 54.34 o 3 1 1 1128.52 888.97 21.35 o 4 1 1 1060.08 900.11 13.47 o 5 1 1 834.29 695.56 17.65 o 6 1 1 5382.03 4730.99 34.12 o 7 1 1 59.83 55.31 28.81 o 8 1 1 8298.13 8880.55 86.61 o 9 1 1 1534.64 1666.01 70.97 o 10 1 1 1098.04 990.31 84.36 o 11 1 1 540.59 394.53 87.47 o 12 1 1 0.38 9.13 92.60 o 13 1 1 32.74 30.84 96.54 o 14 1 1 212.18 163.01 95.38 o -15 2 1 249.51 127.03 97.84 o -14 2 1 40.00 101.94 96.02 o -13 2 1 1330.28 1233.15 102.24 o -12 2 1 56.94 45.07 81.03 o -11 2 1 568.55 635.51 61.81 o -10 2 1 366.75 389.47 47.51 o -9 2 1 564.06 554.36 44.51 o -8 2 1 1810.24 1956.71 47.77 o -7 2 1 1711.88 2005.04 36.51 o -6 2 1 1196.07 964.12 22.16 o -5 2 1 2326.38 2492.64 31.86 o -4 2 1 3229.31 2872.10 29.11 o -3 2 1 14435.33 13637.01 92.37 o -2 2 1 20766.42 22991.24 155.95 o -1 2 1 309.67 244.89 26.80 o 1 2 1 38.42 49.95 19.37 o 2 2 1 362.98 334.39 16.96 o 3 2 1 43.63 13.73 16.91 o 4 2 1 3189.98 3812.44 31.68 o 5 2 1 1203.33 1367.15 24.49 o 6 2 1 1262.42 1141.64 22.93 o 7 2 1 6241.75 5719.69 60.23 o 8 2 1 886.87 868.20 51.30 o 9 2 1 1894.08 1895.64 75.09 o 10 2 1 2126.15 2177.75 83.11 o 11 2 1 2.65 -8.13 84.59 o 12 2 1 358.50 306.99 97.44 o 13 2 1 221.86 170.91 96.99 o 14 2 1 40.54 44.33 99.00 o -15 3 1 0.28 13.15 97.03 o -14 3 1 388.18 332.42 95.48 o -13 3 1 104.96 183.23 87.09 o -12 3 1 1289.41 1299.65 95.04 o -11 3 1 2828.99 3008.24 81.90 o -10 3 1 478.78 509.94 56.92 o -9 3 1 3455.75 3853.25 66.40 o -8 3 1 2647.45 2789.52 49.67 o -7 3 1 2992.37 2464.48 39.61 o -6 3 1 111.29 89.22 18.10 o -5 3 1 1483.33 1302.75 22.46 o -4 3 1 11020.64 13582.63 79.33 o -3 3 1 12848.32 11975.09 84.55 o -2 3 1 8819.64 7929.98 71.81 o -1 3 1 1892.57 2084.02 50.26 o 0 3 1 270.30 205.36 42.63 o 1 3 1 15461.88 17250.71 111.90 o 2 3 1 6473.81 7121.09 40.06 o 3 3 1 3474.59 3707.09 26.05 o 4 3 1 731.03 797.68 25.90 o 5 3 1 3199.83 2943.62 27.17 o 6 3 1 4918.96 4725.34 38.92 o 7 3 1 19.84 28.16 28.25 o 8 3 1 5645.49 5777.03 87.45 o 9 3 1 4421.52 4743.44 84.26 o 10 3 1 600.10 593.24 70.11 o 11 3 1 472.59 338.18 83.27 o 12 3 1 1158.08 989.27 101.80 o 13 3 1 55.92 2.81 95.07 o 14 3 1 142.83 66.50 100.68 o -15 4 1 256.80 211.24 105.87 o -14 4 1 73.88 66.40 92.01 o -13 4 1 900.99 847.63 96.28 o -12 4 1 80.11 34.82 60.97 o -11 4 1 13.68 35.78 58.27 o -10 4 1 10620.99 10946.75 117.94 o -9 4 1 133.00 160.53 41.85 o -8 4 1 358.99 548.65 36.02 o -7 4 1 4222.55 4855.62 50.59 o -6 4 1 6118.10 6493.43 46.70 o -5 4 1 1081.19 1328.78 24.45 o -4 4 1 7843.54 6939.55 31.16 o -3 4 1 1472.73 1521.89 26.61 o -2 4 1 714.31 605.11 19.12 o -1 4 1 2637.30 3252.37 36.19 o 0 4 1 6247.58 6499.54 34.83 o 1 4 1 2913.57 3678.93 41.14 o 2 4 1 1620.66 1426.45 19.54 o 3 4 1 669.36 870.54 23.07 o 4 4 1 681.51 731.10 23.22 o 5 4 1 9218.45 10161.83 55.27 o 6 4 1 3072.95 2432.33 34.38 o 7 4 1 3565.32 3900.20 60.22 o 8 4 1 2745.22 2730.38 66.63 o 9 4 1 298.21 257.20 52.40 o 10 4 1 817.60 882.74 74.19 o 11 4 1 509.59 522.15 74.99 o 12 4 1 78.29 -21.66 93.63 o 13 4 1 378.05 261.53 98.10 o 14 4 1 32.43 11.03 100.96 o -15 5 1 1.33 -31.60 118.02 o -14 5 1 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