data_2239613 _cell_angle_alpha 90.000 _cell_angle_beta 103.362 _cell_angle_gamma 90.000 _cell_length_a 8.2346 _cell_length_b 15.1469 _cell_length_c 13.7410 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.6984 _cod_data_source_file xu5792Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gul12 in P2(1)/c (compound ZN2)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 210.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2266.79 2385.72 18.25 o 2 0 0 11077.13 11843.96 119.60 o 3 0 0 1202.06 1068.80 9.84 o 4 0 0 276.30 333.63 3.25 o 5 0 0 466.16 358.21 3.39 o 6 0 0 2.28 2.39 0.33 o 7 0 0 315.69 279.40 3.62 o 8 0 0 0.54 0.00 0.52 o 9 0 0 166.85 138.70 2.60 o 10 0 0 325.14 342.32 9.92 o 11 0 0 12.45 9.34 1.21 o 1 1 0 247.64 238.42 1.45 o 2 1 0 2613.56 2740.42 17.24 o 3 1 0 914.03 951.58 5.90 o 4 1 0 50.12 67.90 0.93 o 5 1 0 781.79 733.06 4.99 o 6 1 0 359.19 393.03 2.96 o 7 1 0 1454.30 1356.71 9.44 o 8 1 0 21.52 15.83 0.62 o 9 1 0 6.40 5.09 0.58 o 10 1 0 12.92 12.99 0.95 o 11 1 0 20.82 17.91 0.97 o 0 2 0 910.83 910.46 7.60 o 1 2 0 292.01 296.34 1.70 o 2 2 0 4206.75 4260.27 27.23 o 3 2 0 1120.90 1037.37 6.67 o 4 2 0 2917.49 3188.84 18.92 o 5 2 0 2350.26 2407.37 15.82 o 6 2 0 688.06 642.83 4.34 o 7 2 0 571.75 544.82 4.18 o 8 2 0 485.63 480.97 6.15 o 9 2 0 0.24 0.69 0.56 o 10 2 0 233.32 234.46 3.01 o 11 2 0 90.29 81.93 1.62 o 1 3 0 1438.86 1471.14 7.78 o 2 3 0 475.84 560.80 3.21 o 3 3 0 539.43 479.88 3.29 o 4 3 0 2158.94 2544.22 17.45 o 5 3 0 541.34 498.20 3.46 o 6 3 0 51.49 43.39 0.60 o 7 3 0 2.18 0.70 0.40 o 8 3 0 166.59 154.57 1.88 o 9 3 0 34.93 36.19 1.05 o 10 3 0 2.85 3.53 0.66 o 11 3 0 10.80 10.02 0.79 o 0 4 0 15607.17 13116.67 256.44 o 1 4 0 4469.76 4744.34 29.50 o 2 4 0 1200.55 1226.26 7.06 o 3 4 0 548.13 574.58 3.84 o 4 4 0 2469.15 2582.41 16.30 o 5 4 0 0.37 0.57 0.24 o 6 4 0 19.97 21.43 0.47 o 7 4 0 255.58 282.67 2.52 o 8 4 0 544.63 518.91 5.04 o 9 4 0 236.38 230.98 2.98 o 10 4 0 110.93 108.92 1.99 o 11 4 0 4.66 5.33 0.71 o 1 5 0 9194.40 9305.74 103.29 o 2 5 0 172.02 140.83 0.94 o 3 5 0 2317.71 2448.37 14.86 o 4 5 0 47.65 36.87 0.45 o 5 5 0 149.70 182.06 1.37 o 6 5 0 240.45 211.29 1.66 o 7 5 0 1177.05 1131.64 9.35 o 8 5 0 18.62 16.97 0.63 o 9 5 0 0.28 0.19 0.53 o 10 5 0 82.91 103.27 2.11 o 11 5 0 3.60 0.00 0.94 o 0 6 0 468.81 569.20 5.55 o 1 6 0 842.40 878.91 5.73 o 2 6 0 995.17 1012.99 6.68 o 3 6 0 128.08 133.13 0.96 o 4 6 0 937.54 975.17 6.22 o 5 6 0 219.78 245.03 1.78 o 6 6 0 2.28 1.81 0.29 o 7 6 0 46.77 38.55 0.74 o 8 6 0 92.38 102.05 1.40 o 9 6 0 172.78 173.14 2.23 o 10 6 0 324.94 341.78 4.18 o 11 6 0 18.81 23.36 1.03 o 1 7 0 1443.11 1456.79 9.33 o 2 7 0 2421.58 2601.03 17.33 o 3 7 0 554.28 677.90 4.35 o 4 7 0 870.77 884.12 5.54 o 5 7 0 47.47 30.57 0.46 o 6 7 0 1386.68 1288.02 10.29 o 7 7 0 238.44 179.76 1.89 o 8 7 0 159.73 163.52 1.95 o 9 7 0 207.79 196.93 2.46 o 10 7 0 38.84 33.58 1.62 o 0 8 0 793.15 925.79 8.35 o 1 8 0 93.80 83.94 0.66 o 2 8 0 0.29 1.78 0.30 o 3 8 0 128.12 126.50 0.99 o 4 8 0 420.79 408.59 2.55 o 5 8 0 530.69 582.22 4.20 o 6 8 0 254.36 244.89 2.40 o 7 8 0 90.50 93.48 1.26 o 8 8 0 9.29 8.70 0.54 o 9 8 0 35.55 37.77 0.96 o 10 8 0 103.93 105.40 1.72 o 1 9 0 411.75 355.50 2.35 o 2 9 0 173.44 184.46 1.43 o 3 9 0 1354.66 1306.53 8.45 o 4 9 0 1014.64 990.41 6.83 o 5 9 0 150.74 135.95 1.43 o 6 9 0 81.44 64.22 0.92 o 7 9 0 18.87 19.30 0.64 o 8 9 0 8.88 9.80 0.54 o 9 9 0 567.56 533.10 6.28 o 10 9 0 28.41 38.05 1.37 o 0 10 0 39.39 28.65 0.52 o 1 10 0 58.09 62.02 0.57 o 2 10 0 89.43 109.49 0.92 o 3 10 0 4.25 3.92 0.29 o 4 10 0 21.24 19.13 0.51 o 5 10 0 443.89 475.12 4.38 o 6 10 0 0.32 0.73 0.39 o 7 10 0 248.46 250.07 2.88 o 8 10 0 423.71 418.86 4.60 o 9 10 0 37.52 36.25 1.10 o 10 10 0 11.26 11.76 0.90 o 1 11 0 327.85 322.07 2.38 o 2 11 0 58.59 61.93 0.65 o 3 11 0 837.36 864.94 6.90 o 4 11 0 702.42 663.48 6.06 o 5 11 0 394.58 346.59 3.51 o 6 11 0 2.58 3.09 0.45 o 7 11 0 0.39 0.00 0.44 o 8 11 0 53.71 58.11 1.17 o 9 11 0 301.79 321.94 3.77 o 0 12 0 1077.54 1186.78 11.92 o 1 12 0 75.80 81.88 0.81 o 2 12 0 1129.89 1121.87 7.97 o 3 12 0 100.20 100.20 1.00 o 4 12 0 36.50 38.87 0.81 o 5 12 0 289.90 304.08 3.49 o 6 12 0 142.35 132.94 2.20 o 7 12 0 2.40 1.95 0.53 o 8 12 0 1.80 0.48 0.84 o 9 12 0 24.40 22.90 1.34 o 1 13 0 96.73 76.98 0.80 o 2 13 0 110.15 117.22 1.19 o 3 13 0 139.03 133.94 1.45 o 4 13 0 289.05 291.94 3.76 o 5 13 0 5.92 8.72 1.03 o 6 13 0 104.33 97.01 2.09 o 7 13 0 62.54 59.34 1.90 o 8 13 0 0.21 0.09 0.78 o 9 13 0 0.28 0.83 0.92 o 0 14 0 128.93 129.54 2.08 o 1 14 0 18.81 17.44 0.47 o 2 14 0 1445.98 1433.46 14.05 o 3 14 0 2.75 2.24 0.40 o 4 14 0 312.54 318.89 4.18 o 5 14 0 255.00 230.41 3.85 o 6 14 0 115.45 128.53 2.60 o 7 14 0 1.86 1.19 0.78 o 8 14 0 80.54 81.59 2.18 o 1 15 0 1.13 1.32 0.34 o 2 15 0 0.65 1.38 0.47 o 3 15 0 71.92 80.91 1.42 o 4 15 0 972.83 968.41 11.29 o 5 15 0 0.49 0.97 0.70 o 6 15 0 23.23 22.86 1.54 o 7 15 0 3.47 1.93 1.02 o 8 15 0 27.54 29.15 2.17 o 0 16 0 644.76 625.17 8.23 o 1 16 0 88.76 81.06 1.36 o 2 16 0 1059.31 1067.33 14.44 o 3 16 0 2057.86 2008.85 20.71 o 4 16 0 95.00 92.07 1.83 o 5 16 0 17.12 17.12 1.12 o 6 16 0 0.06 0.17 0.78 o 7 16 0 0.74 1.88 2.29 o 1 17 0 794.64 797.72 7.88 o 2 17 0 5.77 4.45 0.45 o 3 17 0 800.94 786.38 8.44 o 4 17 0 2.65 3.37 0.67 o 5 17 0 590.67 591.81 8.08 o 6 17 0 137.77 140.62 2.92 o 7 17 0 37.54 42.04 3.14 o 0 18 0 1020.41 1016.33 13.09 o 1 18 0 4.37 7.06 0.52 o 2 18 0 25.42 27.56 0.78 o 3 18 0 87.03 85.57 1.41 o 4 18 0 79.13 76.54 1.71 o 5 18 0 117.68 121.14 2.55 o 6 18 0 248.78 240.83 7.50 o 1 19 0 189.87 192.89 2.28 o 2 19 0 180.48 175.86 2.32 o 3 19 0 95.82 98.60 1.65 o 4 19 0 66.04 62.95 2.93 o 5 19 0 111.72 107.30 4.35 o 0 20 0 259.73 264.34 5.54 o 1 20 0 22.13 22.42 0.76 o 2 20 0 89.90 89.83 1.63 o 3 20 0 4.89 4.74 0.60 o 4 20 0 43.54 48.56 3.14 o 1 21 0 163.15 178.12 3.05 o 2 21 0 39.51 43.97 2.90 o -11 1 1 0.61 0.18 0.72 o -10 1 1 21.73 16.92 0.94 o -9 1 1 121.49 123.92 1.84 o -8 1 1 127.56 112.52 1.49 o -7 1 1 3580.53 3535.52 24.14 o -6 1 1 1233.51 1267.35 8.74 o -5 1 1 1.63 2.86 0.25 o -4 1 1 1795.48 1783.13 10.52 o -3 1 1 6225.52 6775.03 47.22 o -2 1 1 2461.57 2442.65 14.39 o -1 1 1 4123.13 4363.58 25.91 o 0 1 1 2179.16 2360.71 19.66 o 1 1 1 3024.07 3122.80 16.25 o 2 1 1 514.26 503.29 3.54 o 3 1 1 11.79 12.37 0.30 o 4 1 1 2478.93 2830.10 17.68 o 5 1 1 70.10 65.97 0.67 o 6 1 1 1758.73 1618.77 10.57 o 7 1 1 821.71 810.12 6.18 o 8 1 1 357.38 369.48 3.70 o 9 1 1 250.45 245.97 2.83 o 10 1 1 101.41 105.06 1.73 o 11 1 1 85.33 82.73 1.84 o -11 2 1 1.23 0.10 0.65 o -10 2 1 30.01 32.90 1.54 o -9 2 1 2.98 2.22 0.56 o -8 2 1 49.83 50.62 1.04 o -7 2 1 28.04 28.98 0.73 o -6 2 1 81.43 71.22 0.95 o -5 2 1 7.73 8.23 0.25 o -4 2 1 265.61 252.25 1.88 o -3 2 1 25.00 13.74 0.29 o -2 2 1 13442.30 12227.47 85.99 o -1 2 1 1741.94 1730.11 9.37 o 0 2 1 80.09 61.18 0.61 o 1 2 1 4646.48 5038.03 34.11 o 2 2 1 3614.92 3570.79 20.14 o 3 2 1 1179.49 1303.09 8.16 o 4 2 1 2318.68 2485.48 14.44 o 5 2 1 40.76 44.69 0.48 o 6 2 1 386.98 332.95 2.45 o 7 2 1 48.95 33.72 0.72 o 8 2 1 2.10 0.19 0.40 o 9 2 1 22.25 19.71 0.98 o 10 2 1 125.75 129.13 2.01 o 11 2 1 4.49 2.57 0.71 o -11 3 1 80.42 76.87 1.58 o -10 3 1 27.62 26.18 1.11 o -9 3 1 52.09 58.98 1.26 o -8 3 1 194.08 179.13 2.08 o -7 3 1 141.16 140.58 1.41 o -6 3 1 160.73 176.30 1.78 o -5 3 1 341.46 358.73 2.71 o -4 3 1 660.97 675.31 4.34 o -3 3 1 4437.46 4839.60 31.75 o -2 3 1 769.94 793.25 4.73 o -1 3 1 1930.14 2045.35 13.97 o 0 3 1 3627.92 3819.91 36.61 o 1 3 1 1108.92 1131.69 7.33 o 2 3 1 51.35 58.30 0.45 o 3 3 1 405.24 385.26 2.80 o 4 3 1 751.67 867.58 5.48 o 5 3 1 1821.10 1852.97 11.54 o 6 3 1 7.53 11.64 0.34 o 7 3 1 243.75 244.65 2.35 o 8 3 1 51.33 39.21 1.06 o 9 3 1 208.30 216.37 2.86 o 10 3 1 58.29 64.61 1.54 o 11 3 1 261.03 257.55 3.33 o -11 4 1 33.86 30.23 1.12 o -10 4 1 218.21 247.50 3.50 o -9 4 1 5.49 2.71 0.54 o -8 4 1 50.35 46.06 0.95 o -7 4 1 194.71 181.06 1.69 o -6 4 1 141.14 132.27 1.18 o -5 4 1 3.99 6.80 0.30 o -4 4 1 353.07 359.28 2.47 o -3 4 1 376.37 333.69 2.27 o -2 4 1 133.93 147.18 0.96 o -1 4 1 16477.82 14615.09 112.89 o 0 4 1 16038.25 14121.92 216.09 o 1 4 1 3905.40 4257.97 26.38 o 2 4 1 2.94 14.62 0.22 o 3 4 1 564.26 667.44 4.38 o 4 4 1 620.08 757.29 5.19 o 5 4 1 171.52 205.47 1.60 o 6 4 1 12.65 9.04 0.33 o 7 4 1 180.19 176.52 1.82 o 8 4 1 1.06 0.30 0.43 o 9 4 1 133.46 143.97 2.12 o 10 4 1 65.13 65.79 1.56 o 11 4 1 287.26 297.69 3.72 o -11 5 1 58.83 55.37 1.47 o -10 5 1 96.56 104.27 1.96 o -9 5 1 9.10 9.66 0.61 o -8 5 1 43.54 37.07 0.82 o -7 5 1 1147.09 1058.02 8.77 o -6 5 1 163.91 146.29 1.28 o -5 5 1 87.02 87.19 0.80 o -4 5 1 109.17 134.30 1.07 o -3 5 1 146.82 132.49 0.96 o -2 5 1 783.61 747.10 4.68 o -1 5 1 529.02 599.61 3.82 o 0 5 1 125.60 104.70 0.68 o 1 5 1 92.24 66.47 0.51 o 2 5 1 2333.31 2401.95 14.90 o 3 5 1 429.15 400.55 2.57 o 4 5 1 1690.36 1827.08 11.27 o 5 5 1 405.75 355.41 2.96 o 6 5 1 7.91 3.11 0.29 o 7 5 1 82.61 71.52 1.08 o 8 5 1 15.74 15.37 0.59 o 9 5 1 2.38 3.49 0.64 o 10 5 1 84.88 77.02 1.56 o 11 5 1 73.92 71.04 3.14 o -11 6 1 13.90 12.00 1.08 o -10 6 1 3.76 2.74 0.79 o -9 6 1 45.70 46.02 1.07 o -8 6 1 875.72 852.91 7.49 o -7 6 1 229.72 244.10 2.32 o -6 6 1 3012.43 2893.95 20.63 o -5 6 1 2729.69 2885.46 18.94 o -4 6 1 737.61 814.67 5.47 o -3 6 1 954.58 885.48 5.37 o -2 6 1 2669.45 2854.80 18.51 o -1 6 1 1615.81 1715.16 10.64 o 0 6 1 314.11 293.25 2.03 o 1 6 1 302.95 326.07 2.20 o 2 6 1 370.82 450.98 3.05 o 3 6 1 250.12 325.88 2.36 o 4 6 1 377.27 410.13 2.58 o 5 6 1 119.07 99.93 0.82 o 6 6 1 595.74 599.04 4.74 o 7 6 1 1405.33 1361.17 11.60 o 8 6 1 331.88 313.02 3.25 o 9 6 1 190.49 191.05 2.59 o 10 6 1 205.16 216.72 2.89 o -10 7 1 11.01 9.25 0.73 o -9 7 1 10.74 6.92 0.58 o -8 7 1 53.76 57.06 1.02 o -7 7 1 0.55 2.68 0.39 o -6 7 1 402.29 383.77 3.25 o -5 7 1 110.79 106.91 0.94 o -4 7 1 59.41 66.36 0.58 o -3 7 1 2444.94 2632.92 16.53 o -2 7 1 102.22 113.27 0.92 o -1 7 1 2.37 13.73 0.31 o 0 7 1 3884.03 4149.36 25.67 o 1 7 1 103.90 139.20 0.98 o 2 7 1 36.13 41.09 0.69 o 3 7 1 16.71 12.10 0.34 o 4 7 1 35.26 38.01 0.43 o 5 7 1 4.85 6.04 0.23 o 6 7 1 51.73 48.05 0.77 o 7 7 1 349.82 322.74 3.07 o 8 7 1 49.02 63.04 1.25 o 9 7 1 22.43 26.29 0.95 o 10 7 1 136.25 151.64 2.23 o -10 8 1 78.59 67.86 1.41 o -9 8 1 0.30 0.00 0.48 o -8 8 1 369.98 363.41 3.46 o -7 8 1 2.55 0.93 0.34 o -6 8 1 60.16 54.87 0.95 o -5 8 1 1717.45 1686.08 12.98 o -4 8 1 326.87 308.18 2.00 o -3 8 1 4295.72 4510.88 29.33 o -2 8 1 0.55 0.44 0.19 o -1 8 1 4464.59 4645.95 29.66 o 0 8 1 1057.23 1040.65 6.90 o 1 8 1 2771.82 2883.44 18.60 o 2 8 1 4631.83 4885.22 31.89 o 3 8 1 6.50 5.52 0.34 o 4 8 1 1970.53 2045.35 13.71 o 5 8 1 578.26 534.51 4.22 o 6 8 1 164.06 170.87 1.76 o 7 8 1 122.52 123.10 1.63 o 8 8 1 15.38 11.54 0.55 o 9 8 1 305.20 313.60 3.50 o 10 8 1 57.86 52.51 1.49 o -10 9 1 36.06 39.47 1.08 o -9 9 1 8.20 6.47 0.57 o -8 9 1 52.25 49.90 0.91 o -7 9 1 39.18 28.87 0.73 o -6 9 1 353.09 342.37 3.23 o -5 9 1 26.04 27.67 0.53 o -4 9 1 497.83 525.86 3.44 o -3 9 1 1.64 3.45 0.38 o -2 9 1 654.75 726.36 4.89 o -1 9 1 298.97 327.63 2.19 o 0 9 1 855.35 903.33 6.08 o 1 9 1 1152.97 1306.69 8.94 o 2 9 1 798.24 861.82 5.45 o 3 9 1 25.53 28.60 0.41 o 4 9 1 253.00 239.07 2.01 o 5 9 1 1.25 0.11 0.30 o 6 9 1 217.73 218.60 2.65 o 7 9 1 51.16 47.01 1.48 o 8 9 1 77.22 75.14 1.37 o 9 9 1 0.21 1.82 0.62 o 10 9 1 55.86 57.69 1.61 o -10 10 1 149.46 157.07 2.43 o -9 10 1 918.30 933.25 10.47 o -8 10 1 340.29 348.00 3.32 o -7 10 1 137.80 128.33 1.53 o -6 10 1 12.21 9.61 0.40 o -5 10 1 940.75 906.60 7.19 o -4 10 1 926.47 943.06 7.96 o -3 10 1 3324.48 3363.89 23.57 o -2 10 1 701.76 655.43 4.45 o -1 10 1 394.96 383.36 2.71 o 0 10 1 5.44 11.55 0.38 o 1 10 1 1988.20 1982.81 14.01 o 2 10 1 1521.39 1517.47 10.93 o 3 10 1 85.63 107.56 0.96 o 4 10 1 768.02 720.15 6.08 o 5 10 1 664.62 631.03 6.10 o 6 10 1 75.25 77.28 1.24 o 7 10 1 184.48 188.99 2.38 o 8 10 1 46.00 42.99 1.75 o 9 10 1 495.53 517.32 5.64 o 10 10 1 819.71 838.52 10.44 o -10 11 1 3.71 5.07 2.17 o -9 11 1 1.60 2.62 0.80 o -8 11 1 8.93 8.32 0.55 o -7 11 1 32.95 28.34 0.86 o -6 11 1 504.32 472.94 5.28 o -5 11 1 90.80 91.54 1.32 o -4 11 1 5.12 7.52 0.37 o -3 11 1 0.57 0.67 0.23 o -2 11 1 116.76 125.75 1.09 o -1 11 1 0.23 1.54 0.18 o 0 11 1 105.12 110.94 0.94 o 1 11 1 629.68 670.76 4.77 o 2 11 1 0.02 0.22 0.21 o 3 11 1 60.19 54.79 0.82 o 4 11 1 460.55 437.11 3.80 o 5 11 1 0.04 0.46 0.34 o 6 11 1 346.38 314.58 3.70 o 7 11 1 1.80 0.84 0.53 o 8 11 1 6.23 3.34 0.56 o 9 11 1 7.65 7.92 0.68 o -9 12 1 66.47 68.92 1.80 o -8 12 1 164.45 167.67 3.71 o -7 12 1 138.03 151.37 2.50 o -6 12 1 337.66 341.60 4.58 o -5 12 1 23.23 17.02 0.73 o -4 12 1 346.92 320.99 3.36 o -3 12 1 1089.35 1071.13 7.99 o -2 12 1 130.09 130.52 1.13 o -1 12 1 1169.47 1132.29 7.93 o 0 12 1 164.47 138.41 1.15 o 1 12 1 89.98 96.45 1.20 o 2 12 1 1895.80 1840.91 14.75 o 3 12 1 250.85 237.24 2.28 o 4 12 1 239.08 219.51 2.74 o 5 12 1 25.52 27.57 1.28 o 6 12 1 52.72 54.04 1.20 o 7 12 1 41.56 47.82 1.20 o 8 12 1 86.98 86.46 1.76 o 9 12 1 24.49 22.58 1.03 o -9 13 1 103.67 93.63 3.62 o -8 13 1 4.14 3.92 0.92 o -7 13 1 55.96 50.19 1.62 o -6 13 1 26.32 23.59 1.02 o -5 13 1 100.92 97.00 1.96 o -4 13 1 597.18 623.30 8.05 o -3 13 1 496.50 477.94 4.15 o -2 13 1 1988.74 2052.84 15.15 o -1 13 1 24.47 26.61 0.48 o 0 13 1 557.86 554.85 4.29 o 1 13 1 24.00 23.55 0.45 o 2 13 1 102.32 102.62 1.45 o 3 13 1 490.42 527.98 4.68 o 4 13 1 0.39 1.28 0.42 o 5 13 1 481.42 540.49 9.16 o 6 13 1 185.77 177.60 3.90 o 7 13 1 52.28 47.36 1.53 o 8 13 1 407.73 405.45 6.50 o -8 14 1 76.70 79.26 4.35 o -7 14 1 29.19 25.03 1.71 o -6 14 1 119.86 128.63 3.25 o -5 14 1 101.08 93.42 2.56 o -4 14 1 18.17 20.87 0.82 o -3 14 1 42.36 36.41 0.80 o -2 14 1 74.67 66.11 0.94 o -1 14 1 169.96 143.32 1.43 o 0 14 1 182.39 175.01 1.64 o 1 14 1 245.79 232.65 2.07 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