#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:55:16 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181896 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/96/2239614.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2239614 _cell_angle_alpha 105.786 _cell_angle_beta 92.858 _cell_angle_gamma 110.436 _cell_length_a 12.7485 _cell_length_b 13.6973 _cell_length_c 17.3623 _exptl_crystal_F_000 1216.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file tk5315Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BRIE13' _shelx_refln_list_code 4 _shelx_f_calc_maximum 281.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -7 1 0 2342.57 2053.94 119.23 o -6 1 0 230.13 286.86 46.77 o -5 1 0 5552.08 5026.75 83.74 o -4 1 0 1594.28 1408.60 48.65 o -3 1 0 16464.89 14262.24 131.92 o -2 1 0 16.35 42.26 45.50 o -1 1 0 52874.30 49959.36 6601.88 o 0 1 0 5440.51 5988.84 158.40 o 1 1 0 2104.43 2071.54 73.78 o 2 1 0 1304.64 2440.70 347.73 o -9 2 0 217.37 270.55 50.79 o -8 2 0 1671.09 1634.72 83.38 o -7 2 0 179.04 282.83 41.39 o -6 2 0 555.27 529.54 41.63 o -5 2 0 9.98 52.98 34.23 o -4 2 0 12048.58 12189.06 92.91 o -3 2 0 13939.83 14975.08 324.84 o -2 2 0 22059.43 22989.95 1577.34 o -1 2 0 881.37 461.35 70.80 o 0 2 0 49.07 76.15 35.25 o 1 2 0 27194.71 26776.05 456.20 o 2 2 0 123.91 201.10 36.84 o 3 2 0 3519.33 3337.94 79.24 o 4 2 0 467.74 415.15 48.47 o -11 3 0 1490.02 1489.46 93.09 o -10 3 0 21.33 212.55 46.23 o -9 3 0 1387.95 1511.36 48.63 o -8 3 0 837.44 788.77 37.75 o -7 3 0 676.70 676.68 36.19 o -6 3 0 1161.86 1283.56 51.30 o -5 3 0 2362.99 2513.49 98.19 o -4 3 0 52330.30 52426.45 274.49 o -3 3 0 25414.84 24244.56 262.85 o -2 3 0 17492.34 16252.58 244.22 o -1 3 0 7589.54 6942.90 69.12 o 0 3 0 14782.61 14448.59 180.42 o 1 3 0 14715.30 14706.31 90.76 o 2 3 0 4148.13 4238.80 276.37 o 3 3 0 1291.92 1538.75 47.29 o 4 3 0 2526.02 2346.50 56.72 o 5 3 0 140.97 83.52 44.60 o 6 3 0 2227.11 2077.90 90.59 o -13 4 0 50.84 59.73 57.59 o -12 4 0 30.78 58.42 45.97 o -11 4 0 48.14 52.13 40.05 o -10 4 0 1861.88 1745.27 45.04 o -9 4 0 1877.68 1691.27 74.78 o -8 4 0 42.31 87.67 32.64 o -7 4 0 3806.48 3842.63 51.33 o -6 4 0 36.17 75.57 33.92 o -5 4 0 13612.09 12601.73 434.08 o -4 4 0 4913.09 5183.96 160.92 o -3 4 0 3916.54 4125.33 190.10 o -2 4 0 2034.91 1587.37 192.26 o -1 4 0 320.60 255.22 25.55 o 0 4 0 2337.42 2041.51 37.88 o 1 4 0 297.84 231.34 27.74 o 2 4 0 7294.21 7536.19 143.06 o 3 4 0 236.15 357.96 35.83 o 4 4 0 1578.26 1603.48 48.11 o 5 4 0 458.33 574.71 41.16 o 6 4 0 727.51 654.30 48.77 o 7 4 0 79.15 75.51 72.16 o -14 5 0 239.83 238.45 56.27 o -13 5 0 227.63 194.84 44.18 o -12 5 0 33.25 31.00 38.74 o -11 5 0 1.72 17.90 36.17 o -10 5 0 1.18 12.77 32.04 o -9 5 0 149.64 117.08 34.34 o -8 5 0 2262.61 2306.58 119.05 o -7 5 0 2791.39 2673.93 43.49 o -6 5 0 1802.70 1561.80 36.48 o -5 5 0 1858.99 1644.45 37.92 o -4 5 0 8958.10 8316.06 79.99 o -3 5 0 480.54 432.65 30.86 o -2 5 0 413.05 468.06 30.72 o -1 5 0 820.12 824.05 49.24 o 0 5 0 1209.47 1230.20 42.11 o 1 5 0 3648.90 3940.72 74.68 o 2 5 0 5006.83 5273.08 56.11 o 3 5 0 990.92 1022.78 35.42 o 4 5 0 1125.37 1101.41 39.95 o 5 5 0 383.85 322.87 41.04 o 6 5 0 14.48 54.78 38.41 o 7 5 0 0.96 0.00 76.04 o -15 6 0 408.01 324.00 82.89 o -14 6 0 3.12 28.25 44.67 o -13 6 0 629.42 619.78 43.54 o -12 6 0 262.40 229.93 40.67 o -11 6 0 80.23 125.21 32.68 o -10 6 0 119.77 109.90 30.78 o -9 6 0 1805.46 1804.36 35.93 o -8 6 0 1147.66 1201.94 101.51 o -7 6 0 9.61 19.09 27.60 o -6 6 0 735.92 802.74 29.18 o -5 6 0 2432.79 2233.18 110.67 o -4 6 0 1674.15 1949.51 37.40 o -3 6 0 2724.24 2865.13 42.70 o -2 6 0 102.83 79.02 29.00 o -1 6 0 499.81 540.06 31.64 o 0 6 0 1702.28 1775.52 37.84 o 1 6 0 255.68 359.64 28.64 o 2 6 0 1269.73 1202.42 39.35 o 3 6 0 132.80 123.57 28.72 o 4 6 0 1669.61 1624.86 40.11 o 5 6 0 8.43 38.79 33.20 o 6 6 0 269.04 317.99 43.17 o 7 6 0 111.13 141.54 46.58 o 8 6 0 826.09 868.13 79.19 o -15 7 0 6.06 0.14 49.73 o -14 7 0 196.16 207.23 43.56 o -13 7 0 61.77 40.11 38.19 o -12 7 0 700.65 814.49 40.96 o -11 7 0 144.12 168.03 31.30 o -10 7 0 210.82 199.39 28.10 o -9 7 0 1621.09 1575.93 73.21 o -8 7 0 48.69 26.64 25.13 o -7 7 0 3471.10 3279.66 37.93 o -6 7 0 839.27 861.08 28.59 o -5 7 0 66.50 18.43 25.23 o -4 7 0 717.42 695.39 54.16 o -3 7 0 3228.15 3158.92 43.17 o -2 7 0 40.27 51.49 31.94 o -1 7 0 3730.85 3440.66 40.69 o 0 7 0 23.25 44.15 25.79 o 1 7 0 826.06 663.16 29.57 o 2 7 0 213.41 278.11 26.93 o 3 7 0 96.96 73.98 37.18 o 4 7 0 55.78 73.10 29.08 o 5 7 0 86.60 177.55 35.21 o 6 7 0 911.30 997.22 78.41 o 7 7 0 1344.06 1291.56 75.41 o 8 7 0 166.04 120.01 57.39 o -14 8 0 52.52 47.49 40.79 o -13 8 0 211.77 215.15 38.18 o -12 8 0 284.49 235.53 33.34 o -11 8 0 677.77 687.75 34.31 o -10 8 0 488.23 488.09 30.19 o -9 8 0 539.09 526.30 29.08 o -8 8 0 848.86 915.77 32.23 o -7 8 0 163.84 165.49 25.30 o -6 8 0 660.05 560.90 51.75 o -5 8 0 420.31 324.23 30.26 o -4 8 0 575.39 515.47 25.93 o -3 8 0 1896.04 1987.57 93.93 o -2 8 0 4830.58 4529.90 61.40 o -1 8 0 1979.21 1919.68 33.33 o 0 8 0 5307.28 4937.24 228.12 o 1 8 0 934.09 936.55 32.95 o 2 8 0 1072.52 959.53 33.14 o 3 8 0 193.97 182.22 29.03 o 4 8 0 1355.33 1371.16 39.03 o 5 8 0 2.40 9.03 34.82 o 6 8 0 237.03 198.23 37.02 o 7 8 0 103.48 77.85 39.95 o 8 8 0 41.00 25.72 74.15 o -14 9 0 37.75 27.76 41.68 o -13 9 0 431.78 465.49 46.30 o -12 9 0 12.98 18.59 36.25 o -11 9 0 1440.88 1406.56 38.15 o -10 9 0 35.24 56.35 30.20 o -9 9 0 1941.77 2017.19 36.94 o -8 9 0 47.59 63.95 27.74 o -7 9 0 1463.29 1381.61 30.91 o -6 9 0 259.01 267.86 28.03 o -5 9 0 1698.47 1481.93 49.45 o -4 9 0 289.05 251.21 26.99 o -3 9 0 1881.15 1836.70 153.16 o -2 9 0 941.91 956.25 54.30 o -1 9 0 3666.69 3525.06 99.35 o 0 9 0 281.80 328.43 64.58 o 1 9 0 15.39 19.25 27.99 o 2 9 0 76.19 43.99 31.97 o 3 9 0 744.66 671.45 36.66 o 4 9 0 431.41 403.31 34.26 o 5 9 0 42.79 35.67 33.49 o 6 9 0 295.87 341.53 43.47 o 7 9 0 0.54 1.93 40.60 o 8 9 0 276.99 234.75 78.00 o -14 10 0 156.08 154.63 41.36 o -13 10 0 0.30 11.57 34.49 o -12 10 0 313.26 297.88 37.32 o -11 10 0 153.64 183.02 30.02 o -10 10 0 422.90 579.21 48.22 o -9 10 0 743.87 710.66 33.68 o -8 10 0 438.14 503.95 30.15 o -7 10 0 1233.54 1209.41 34.66 o -6 10 0 189.62 165.36 25.69 o -5 10 0 766.26 887.04 45.11 o -4 10 0 557.37 612.06 52.14 o -3 10 0 2754.30 2813.45 36.79 o -2 10 0 1095.48 1144.32 31.10 o -1 10 0 1194.20 1262.33 58.95 o 0 10 0 120.81 133.07 28.41 o 1 10 0 1072.57 1088.33 53.32 o 2 10 0 249.43 224.63 32.25 o 3 10 0 763.85 789.50 36.57 o 4 10 0 63.80 58.65 36.39 o 5 10 0 333.89 315.53 39.12 o 6 10 0 15.24 44.02 39.91 o 7 10 0 298.72 265.85 48.85 o -14 11 0 14.08 13.07 39.24 o -13 11 0 273.65 286.39 35.53 o -12 11 0 267.88 334.35 36.19 o -11 11 0 249.29 256.80 31.38 o -10 11 0 942.73 905.40 36.16 o -9 11 0 61.73 60.83 38.72 o -8 11 0 306.06 283.25 33.65 o -7 11 0 7.38 16.51 25.03 o -6 11 0 410.44 387.37 26.13 o -5 11 0 100.07 74.41 25.91 o -4 11 0 65.36 50.39 25.30 o -3 11 0 262.34 272.23 26.90 o -2 11 0 214.32 208.26 27.66 o -1 11 0 133.52 181.76 51.54 o 0 11 0 1865.28 1786.80 36.31 o 1 11 0 262.57 241.34 30.72 o 2 11 0 1203.29 1204.01 34.96 o 3 11 0 196.38 190.97 35.14 o 4 11 0 263.86 252.72 39.57 o 5 11 0 50.94 88.56 39.31 o -13 12 0 180.74 167.98 37.07 o -12 12 0 7.28 0.00 35.48 o -11 12 0 347.42 355.68 33.48 o -10 12 0 1.40 20.86 29.65 o -9 12 0 1019.03 901.58 62.48 o -8 12 0 34.44 34.01 30.56 o -7 12 0 632.31 652.32 31.82 o -6 12 0 259.77 232.03 27.65 o -5 12 0 1762.00 1823.40 123.21 o -4 12 0 11.07 8.77 26.02 o -3 12 0 247.50 306.10 29.33 o -2 12 0 17.86 19.20 30.27 o -1 12 0 1972.85 1942.43 50.56 o 0 12 0 338.23 328.77 33.30 o 1 12 0 199.51 160.43 31.18 o 2 12 0 147.94 135.85 35.50 o 3 12 0 80.32 96.89 36.28 o 4 12 0 59.28 33.88 41.25 o -12 13 0 39.50 52.22 55.28 o -11 13 0 0.02 8.34 34.68 o -10 13 0 468.60 492.46 36.40 o -9 13 0 64.89 30.30 31.36 o -8 13 0 212.83 270.70 30.44 o -7 13 0 134.00 115.70 30.43 o -6 13 0 24.76 11.48 30.77 o -5 13 0 608.59 647.93 32.14 o -4 13 0 27.63 44.94 29.97 o -3 13 0 694.95 687.69 33.60 o -2 13 0 361.43 393.36 33.01 o -1 13 0 559.87 519.02 34.19 o 0 13 0 56.50 32.25 31.66 o 1 13 0 233.22 250.74 36.15 o 2 13 0 4.43 17.75 35.37 o 3 13 0 110.03 77.23 39.09 o -11 14 0 199.76 202.75 36.18 o -10 14 0 122.25 60.27 33.11 o -9 14 0 193.18 199.19 35.21 o -8 14 0 255.85 311.97 48.99 o -7 14 0 180.22 134.84 33.21 o -6 14 0 121.33 109.35 38.23 o -5 14 0 225.67 210.94 33.93 o -4 14 0 390.91 440.86 32.26 o -3 14 0 23.55 63.80 33.28 o -2 14 0 374.38 383.85 60.91 o -1 14 0 0.36 8.05 32.89 o 0 14 0 215.23 229.31 38.81 o 1 14 0 31.48 51.50 35.39 o -9 15 0 243.36 236.23 37.80 o -8 15 0 3.96 6.00 35.70 o -7 15 0 531.86 546.66 37.78 o -6 15 0 12.42 0.43 33.82 o -5 15 0 407.70 348.10 43.33 o -4 15 0 38.83 94.97 36.80 o -3 15 0 286.28 285.56 52.91 o -2 15 0 15.24 20.72 34.79 o 1 -15 1 94.64 70.42 36.92 o 2 -15 1 162.73 170.65 34.52 o 3 -15 1 51.37 52.00 53.08 o 4 -15 1 332.16 319.46 34.65 o 5 -15 1 186.73 153.18 40.57 o 6 -15 1 169.69 232.41 33.28 o 7 -15 1 23.81 35.44 33.53 o 8 -15 1 269.59 329.37 45.64 o 9 -15 1 0.47 6.26 35.53 o -1 -14 1 161.16 145.49 34.98 o 0 -14 1 0.98 0.21 34.51 o 1 -14 1 171.22 171.09 35.57 o 2 -14 1 31.88 51.71 33.60 o 3 -14 1 649.77 702.91 36.24 o 4 -14 1 309.26 326.65 50.63 o 5 -14 1 209.58 245.95 32.69 o 6 -14 1 114.26 89.36 31.48 o 7 -14 1 640.80 722.53 49.27 o 8 -14 1 29.04 17.08 33.38 o 9 -14 1 360.64 335.16 33.17 o 10 -14 1 195.87 207.24 33.84 o 11 -14 1 104.91 110.44 34.04 o -3 -13 1 10.25 16.18 38.31 o -2 -13 1 226.74 258.57 41.48 o -1 -13 1 0.03 17.37 34.54 o 0 -13 1 250.01 255.46 31.35 o 1 -13 1 216.61 206.94 30.61 o 2 -13 1 13.28 10.26 30.69 o 3 -13 1 2.98 3.24 29.97 o 4 -13 1 97.00 141.34 37.22 o 5 -13 1 46.68 66.95 27.29 o 6 -13 1 3.24 31.66 28.76 o 7 -13 1 136.95 143.27 30.38 o 8 -13 1 46.61 85.45 61.89 o 9 -13 1 631.75 606.14 79.50 o 10 -13 1 52.28 58.48 33.11 o 11 -13 1 320.35 272.16 35.83 o 12 -13 1 11.63 6.83 38.53 o -4 -12 1 68.67 84.85 40.15 o -3 -12 1 284.17 309.02 36.73 o -2 -12 1 64.16 75.29 33.03 o -1 -12 1 245.17 288.33 36.03 o 0 -12 1 477.36 481.97 37.25 o 1 -12 1 21.71 17.33 29.69 o 2 -12 1 3.74 14.84 30.16 o 3 -12 1 22.42 55.72 28.06 o 4 -12 1 505.16 537.81 29.08 o 5 -12 1 792.31 865.29 56.50 o 6 -12 1 303.71 344.63 28.02 o 7 -12 1 155.07 196.50 28.43 o 8 -12 1 514.58 535.85 33.31 o 9 -12 1 218.87 223.58 30.56 o 10 -12 1 492.11 534.41 32.84 o 11 -12 1 0.99 29.57 30.57 o 12 -12 1 163.09 181.04 64.26 o 13 -12 1 0.44 28.46 36.17 o -6 -11 1 170.75 138.93 45.25 o -5 -11 1 59.04 23.23 39.11 o -4 -11 1 97.39 112.90 38.25 o -3 -11 1 4.03 47.69 36.10 o -2 -11 1 161.16 160.57 35.00 o -1 -11 1 156.88 143.19 27.98 o 0 -11 1 155.68 136.44 29.82 o 1 -11 1 246.06 247.98 30.61 o 2 -11 1 178.33 170.75 26.76 o 3 -11 1 2166.50 2165.29 90.40 o 4 -11 1 244.71 246.64 26.34 o 5 -11 1 1152.33 1140.77 91.06 o 6 -11 1 42.10 37.33 25.99 o 7 -11 1 659.36 644.09 28.44 o 8 -11 1 24.98 24.63 27.90 o 9 -11 1 578.85 529.69 30.99 o 10 -11 1 6.17 31.90 30.32 o 11 -11 1 481.50 484.29 59.68 o 12 -11 1 54.40 95.13 33.35 o 13 -11 1 297.35 334.37 34.96 o 14 -11 1 4.76 15.96 36.19 o -7 -10 1 59.06 35.99 46.36 o -6 -10 1 163.19 179.81 40.12 o -5 -10 1 55.42 20.80 36.07 o -4 -10 1 190.40 201.01 31.39 o -3 -10 1 47.76 82.19 28.58 o -2 -10 1 20.54 17.97 28.53 o -1 -10 1 41.61 67.64 33.68 o 0 -10 1 1052.11 986.97 32.18 o 1 -10 1 165.90 162.84 27.89 o 2 -10 1 3738.87 3640.11 50.98 o 3 -10 1 78.11 85.80 25.89 o 4 -10 1 1707.66 1653.30 31.77 o 5 -10 1 7.93 8.89 24.68 o 6 -10 1 243.51 275.10 25.84 o 7 -10 1 67.91 81.38 26.04 o 8 -10 1 84.98 112.71 27.45 o 9 -10 1 2.08 14.56 29.70 o 10 -10 1 425.88 398.58 34.25 o 11 -10 1 298.72 343.68 30.66 o 12 -10 1 253.10 209.26 33.78 o 13 -10 1 319.51 362.66 37.44 o 14 -10 1 60.76 27.43 37.97 o -8 -9 1 11.61 6.52 54.99 o -7 -9 1 274.12 261.54 44.95 o -6 -9 1 5.80 3.49 38.41 o -5 -9 1 697.34 761.37 41.07 o -4 -9 1 207.94 215.80 29.78 o -3 -9 1 292.58 278.50 33.37 o -2 -9 1 153.71 120.41 32.25 o -1 -9 1 756.19 799.51 30.65 o 0 -9 1 893.89 888.54 29.99 o 1 -9 1 4426.67 4131.90 182.90 o 2 -9 1 10.16 40.71 24.46 o 3 -9 1 1608.32 1519.06 52.91 o 4 -9 1 1226.22 1336.75 31.70 o 5 -9 1 237.51 260.58 24.95 o 6 -9 1 945.56 937.21 31.14 o 7 -9 1 252.41 286.60 26.76 o 8 -9 1 961.90 899.85 63.91 o 9 -9 1 994.52 961.23 33.48 o 10 -9 1 639.27 597.87 31.65 o 11 -9 1 1160.85 1181.55 35.51 o 12 -9 1 1272.06 1268.86 40.08 o 13 -9 1 52.15 92.22 34.63 o 14 -9 1 153.27 161.04 39.04 o -8 -8 1 355.41 379.64 54.04 o -7 -8 1 116.48 109.69 41.89 o -6 -8 1 699.20 807.83 40.93 o -5 -8 1 42.53 50.54 36.80 o -4 -8 1 106.21 137.80 33.35 o -3 -8 1 919.01 888.07 33.64 o -2 -8 1 2390.25 2432.18 54.76 o -1 -8 1 82.90 63.29 26.09 o 0 -8 1 1407.63 1524.30 35.82 o 1 -8 1 1296.90 1538.24 32.07 o 2 -8 1 508.28 588.40 29.73 o 3 -8 1 2257.37 2327.33 35.65 o 4 -8 1 3.18 13.96 25.53 o 5 -8 1 1201.18 991.14 29.20 o 6 -8 1 11.34 37.09 24.56 o 7 -8 1 1222.94 1174.03 65.52 o 8 -8 1 81.66 61.96 26.95 o 9 -8 1 2170.84 2322.70 51.26 o 10 -8 1 6.35 22.50 30.64 o 11 -8 1 5287.12 5449.49 65.59 o 12 -8 1 190.75 178.80 37.23 o 13 -8 1 394.03 395.02 36.25 o 14 -8 1 125.71 114.45 40.38 o -8 -7 1 113.58 130.27 82.05 o -7 -7 1 595.16 641.49 47.38 o -6 -7 1 110.22 35.03 42.10 o -5 -7 1 77.00 70.90 33.14 o -4 -7 1 323.46 278.99 32.43 o -3 -7 1 7.41 2.15 29.40 o -2 -7 1 2489.40 2493.18 40.89 o -1 -7 1 5.04 8.90 29.94 o 0 -7 1 6284.75 5598.27 176.82 o 1 -7 1 187.02 128.00 28.50 o 2 -7 1 6855.48 6681.05 289.23 o 3 -7 1 191.28 148.59 30.24 o 4 -7 1 1056.64 859.92 30.69 o 5 -7 1 811.07 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