data_2239738 _cell_angle_alpha 90.000 _cell_angle_beta 134.885 _cell_angle_gamma 90.000 _cell_length_a 31.9861 _cell_length_b 5.9668 _cell_length_c 22.6135 _exptl_crystal_F_000 1496.00 _reflns_d_resolution_high 0.6614 _cod_data_source_file sj5416Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' opd2m in C2/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 515.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 48998.68 50092.61 446.09 o 4 0 0 38285.33 38042.32 234.80 o 6 0 0 1717.17 1940.53 20.17 o 8 0 0 109.13 33.25 5.03 o 10 0 0 7447.40 7282.40 55.04 o 12 0 0 2629.32 2487.39 26.17 o 14 0 0 95.37 48.05 5.50 o 16 0 0 17260.45 18106.33 112.00 o 18 0 0 11717.90 12018.49 83.56 o 20 0 0 18541.98 18414.04 132.70 o 22 0 0 1308.82 1505.61 30.85 o 24 0 0 2422.43 2398.61 40.70 o 26 0 0 7798.74 7617.09 91.67 o 28 0 0 1664.60 1799.38 45.97 o 30 0 0 619.18 604.19 41.93 o 32 0 0 1756.99 1725.77 63.46 o 34 0 0 299.67 293.29 57.03 o 1 1 0 25635.51 25581.98 104.01 o 3 1 0 49377.63 50349.42 261.00 o 5 1 0 11097.61 11895.88 57.05 o 7 1 0 7130.43 7113.68 39.82 o 9 1 0 14691.29 16258.11 77.02 o 11 1 0 1447.77 1484.08 13.31 o 13 1 0 3283.76 3694.87 25.76 o 15 1 0 42.33 39.56 3.85 o 17 1 0 1155.17 1093.89 14.13 o 19 1 0 16.88 28.89 4.52 o 21 1 0 550.47 501.56 11.52 o 23 1 0 299.87 293.35 12.90 o 25 1 0 0.14 2.33 6.11 o 27 1 0 9.78 1.86 7.87 o 29 1 0 16.29 32.39 14.88 o 31 1 0 0.03 36.76 31.94 o 33 1 0 3.00 -16.88 15.05 o 0 2 0 142352.27 140262.48 953.18 o 2 2 0 7640.63 7119.58 37.10 o 4 2 0 23841.45 23827.26 97.89 o 6 2 0 43070.62 44529.43 199.09 o 8 2 0 16686.34 17284.12 94.70 o 10 2 0 21694.85 21268.96 101.33 o 12 2 0 7637.73 7433.58 61.23 o 14 2 0 1372.73 1073.03 13.45 o 16 2 0 11448.88 11375.58 61.80 o 18 2 0 2019.73 2074.94 22.86 o 20 2 0 1950.60 1834.35 22.50 o 22 2 0 2857.22 2962.25 31.82 o 24 2 0 1598.66 1529.31 26.51 o 26 2 0 11817.03 11740.45 94.32 o 28 2 0 1352.95 1320.47 44.59 o 30 2 0 1889.61 1880.28 51.10 o 32 2 0 2779.07 2940.76 96.08 o 1 3 0 172.12 77.01 4.63 o 3 3 0 800.83 850.76 10.81 o 5 3 0 2666.76 2836.93 18.48 o 7 3 0 4230.02 3904.68 24.49 o 9 3 0 9034.29 8682.97 43.92 o 11 3 0 1118.42 1106.02 13.88 o 13 3 0 5.90 4.76 2.70 o 15 3 0 2636.66 2476.48 26.24 o 17 3 0 3521.07 3345.19 35.79 o 19 3 0 9.03 11.04 5.36 o 21 3 0 437.09 481.20 19.63 o 23 3 0 33.62 26.54 10.42 o 25 3 0 1180.15 1166.41 32.06 o 27 3 0 139.53 133.07 28.24 o 29 3 0 47.39 38.04 13.41 o 31 3 0 36.08 44.18 13.21 o 0 4 0 18944.91 20246.20 131.20 o 2 4 0 21509.75 20990.03 96.31 o 4 4 0 6192.47 6061.63 37.88 o 6 4 0 24102.55 24149.79 116.32 o 8 4 0 9260.36 8909.33 46.12 o 10 4 0 15399.10 15549.59 78.85 o 12 4 0 8.07 18.32 4.44 o 14 4 0 140.88 144.93 9.02 o 16 4 0 3382.81 3459.20 44.22 o 18 4 0 8408.78 8083.90 74.97 o 20 4 0 2646.38 2648.16 42.73 o 22 4 0 5398.04 5348.31 73.10 o 24 4 0 681.58 667.91 22.82 o 26 4 0 4998.00 4898.85 79.55 o 28 4 0 1761.35 1758.19 49.27 o 30 4 0 1472.51 1540.29 49.06 o 1 5 0 849.34 731.80 11.95 o 3 5 0 5243.66 5354.30 37.78 o 5 5 0 141.06 131.77 6.51 o 7 5 0 0.28 -3.96 3.48 o 9 5 0 25.31 29.88 4.84 o 11 5 0 3272.04 3223.32 37.58 o 13 5 0 1121.19 1144.74 27.48 o 15 5 0 600.24 536.80 18.53 o 17 5 0 1658.19 1706.15 34.74 o 19 5 0 770.26 779.72 25.16 o 21 5 0 1.32 0.13 8.19 o 23 5 0 62.93 46.09 12.80 o 25 5 0 716.22 758.95 36.83 o 27 5 0 38.75 33.21 13.42 o 0 6 0 8171.42 8846.34 73.13 o 2 6 0 8993.82 8894.63 51.82 o 4 6 0 4781.66 4882.28 38.06 o 6 6 0 3187.66 3260.87 34.09 o 8 6 0 3658.34 3593.85 45.83 o 10 6 0 1387.51 1418.70 28.59 o 12 6 0 2379.77 2300.17 41.31 o 14 6 0 1877.38 1833.69 38.98 o 16 6 0 3000.47 3018.96 60.92 o 18 6 0 3164.99 3068.46 50.81 o 20 6 0 1249.07 1191.18 33.91 o 22 6 0 2703.74 2865.76 56.95 o 24 6 0 1307.28 1387.32 44.70 o 1 7 0 127.72 171.18 12.13 o 3 7 0 802.11 759.50 20.05 o 5 7 0 480.31 507.44 18.86 o 7 7 0 65.57 51.84 9.86 o 9 7 0 55.73 36.32 8.18 o 11 7 0 89.61 112.82 12.66 o 13 7 0 50.63 43.83 9.69 o 15 7 0 402.22 359.84 22.76 o 17 7 0 977.63 982.62 35.68 o 19 7 0 166.91 188.02 20.88 o 21 7 0 25.84 39.79 14.08 o 2 8 0 1797.03 1944.41 54.31 o 4 8 0 2269.26 2253.99 67.89 o 6 8 0 759.25 825.44 42.91 o 8 8 0 4758.72 4869.70 94.36 o 10 8 0 347.34 295.73 18.84 o 12 8 0 3111.15 3332.74 60.27 o 14 8 0 565.34 554.18 41.65 o 1 9 0 84.68 100.48 16.29 o -35 1 1 1234.38 1217.13 55.66 o -33 1 1 3352.90 3365.08 65.28 o -31 1 1 5184.55 5135.35 67.07 o -29 1 1 1759.66 1864.08 38.04 o -27 1 1 4648.45 4586.41 50.89 o -25 1 1 10.46 12.32 6.19 o -23 1 1 4169.14 4409.63 38.43 o -21 1 1 13521.78 13115.51 70.76 o -19 1 1 2693.02 2864.60 24.19 o -17 1 1 14960.61 14789.16 70.70 o -15 1 1 7168.70 6935.31 39.79 o -13 1 1 12126.19 12224.63 59.07 o -11 1 1 35972.74 36042.50 153.80 o -9 1 1 2165.03 2757.61 19.98 o -7 1 1 5587.09 5706.98 36.24 o -5 1 1 33433.62 34068.17 218.88 o -3 1 1 15636.55 16584.67 64.56 o -1 1 1 55258.58 55254.66 225.78 o 1 1 1 4758.02 4637.60 24.59 o 3 1 1 112085.35 111879.55 483.01 o 5 1 1 265986.50 256738.98 3128.36 o 7 1 1 24636.89 25518.86 111.57 o 9 1 1 46214.65 45974.71 193.26 o 11 1 1 274.77 198.19 6.96 o 13 1 1 2877.28 2700.13 21.23 o 15 1 1 8527.27 8471.68 46.14 o 17 1 1 2640.74 2668.93 22.93 o 19 1 1 2151.32 2082.60 21.82 o 21 1 1 12408.44 12530.71 83.36 o 23 1 1 516.25 534.33 17.74 o 25 1 1 5313.31 5299.43 59.24 o 27 1 1 985.60 1095.59 29.28 o 29 1 1 2073.51 2077.90 57.69 o 31 1 1 4521.88 4459.79 81.00 o 33 1 1 1002.65 927.96 39.93 o -34 2 1 79.59 45.20 20.06 o -32 2 1 39.33 57.44 27.28 o -30 2 1 309.50 279.76 18.63 o -28 2 1 437.77 493.35 24.55 o -26 2 1 140.42 130.59 10.47 o -24 2 1 28.97 20.72 6.05 o -22 2 1 260.31 255.68 10.29 o -20 2 1 63.50 50.75 5.38 o -18 2 1 3767.56 3516.24 28.86 o -16 2 1 1954.93 1850.77 18.72 o -14 2 1 541.56 549.36 9.68 o -12 2 1 1105.39 1216.09 14.85 o -10 2 1 1497.66 1659.88 16.34 o -8 2 1 211.78 173.80 5.82 o -6 2 1 1319.65 1259.90 11.51 o -4 2 1 14856.00 15024.73 64.73 o -2 2 1 4503.64 4053.22 23.92 o 0 2 1 541.78 428.84 7.08 o 2 2 1 5871.79 6286.57 31.66 o 4 2 1 2100.05 2138.74 15.30 o 6 2 1 1971.80 2622.79 19.77 o 8 2 1 3495.42 4269.90 26.79 o 10 2 1 6056.74 6376.99 40.39 o 12 2 1 106.64 116.14 5.19 o 14 2 1 5530.05 5824.37 37.22 o 16 2 1 471.05 349.20 9.52 o 18 2 1 563.76 535.54 12.48 o 20 2 1 1397.73 1467.15 20.73 o 22 2 1 1579.27 1493.27 25.39 o 24 2 1 385.80 409.85 18.13 o 26 2 1 121.10 112.79 12.03 o 28 2 1 10.94 10.05 9.37 o 30 2 1 538.80 503.96 37.05 o 32 2 1 28.60 26.76 18.75 o -33 3 1 791.10 785.13 34.72 o -31 3 1 1016.73 1003.83 38.26 o -29 3 1 1819.89 1820.10 51.93 o -27 3 1 4683.32 4676.57 81.49 o -25 3 1 2280.27 2342.65 44.19 o -23 3 1 5127.59 5214.98 57.39 o -21 3 1 19213.98 18013.48 177.01 o -19 3 1 1614.52 1543.78 23.25 o -17 3 1 5182.83 5488.48 45.29 o -15 3 1 96.32 75.80 5.52 o -13 3 1 7519.18 7582.33 46.72 o -11 3 1 6654.80 6203.87 41.63 o -9 3 1 5211.29 4665.46 29.51 o -7 3 1 6851.97 6920.48 38.78 o -5 3 1 25544.27 25174.45 107.37 o -3 3 1 13325.76 13838.00 69.35 o -1 3 1 81348.41 85160.54 376.96 o 1 3 1 4844.82 3982.80 26.33 o 3 3 1 39325.96 40212.47 163.69 o 5 3 1 28558.12 29370.77 119.82 o 7 3 1 6702.13 5989.38 33.68 o 9 3 1 13703.50 13286.41 63.34 o 11 3 1 16852.96 17000.98 84.52 o 13 3 1 7038.74 7178.42 48.43 o 15 3 1 7127.23 7387.40 55.30 o 17 3 1 348.03 236.72 11.77 o 19 3 1 468.00 510.60 23.05 o 21 3 1 4463.02 4564.99 56.69 o 23 3 1 4610.95 4523.10 76.57 o 25 3 1 4189.73 4083.19 62.28 o 27 3 1 2063.66 2005.68 49.46 o 29 3 1 1102.05 1107.69 35.68 o 31 3 1 2200.08 2089.22 54.08 o -30 4 1 0.05 14.45 12.49 o -28 4 1 285.33 240.96 27.77 o -26 4 1 1.09 -0.69 8.29 o -24 4 1 42.58 38.63 9.06 o -22 4 1 69.85 52.79 9.08 o -20 4 1 2708.63 2563.85 38.61 o -18 4 1 83.71 42.04 6.79 o -16 4 1 3077.25 3130.15 29.94 o -14 4 1 194.90 149.57 8.83 o -12 4 1 15457.93 14935.92 91.85 o -10 4 1 264.93 237.70 6.89 o -8 4 1 6244.23 6399.69 43.67 o -6 4 1 258.12 266.35 7.58 o -4 4 1 1198.13 981.88 12.31 o -2 4 1 1295.74 1090.01 13.63 o 0 4 1 6542.90 6851.99 40.69 o 2 4 1 342.57 343.81 8.26 o 4 4 1 54.96 55.46 4.29 o 6 4 1 180.91 230.78 6.83 o 8 4 1 3859.22 3737.65 33.05 o 10 4 1 1717.57 1647.03 24.08 o 12 4 1 0.73 -6.55 5.39 o 14 4 1 0.37 -7.20 3.62 o 16 4 1 551.00 576.15 21.32 o 18 4 1 0.59 -6.01 6.94 o 20 4 1 14.60 10.90 9.03 o 22 4 1 488.63 518.28 22.15 o 24 4 1 616.48 641.78 28.06 o 26 4 1 38.12 49.77 12.65 o 28 4 1 255.48 314.21 27.83 o -29 5 1 2050.77 2014.35 74.08 o -27 5 1 2935.75 2939.04 77.46 o -25 5 1 714.89 761.42 33.32 o -23 5 1 2013.89 1989.56 50.24 o -21 5 1 1811.61 1839.15 47.05 o -19 5 1 1886.58 1853.80 38.51 o -17 5 1 4139.32 4197.81 51.97 o -15 5 1 4307.32 4113.74 48.80 o -13 5 1 17060.80 16874.55 115.49 o -11 5 1 646.70 756.13 16.12 o -9 5 1 4744.35 4561.89 49.12 o -7 5 1 51.43 71.07 5.45 o -5 5 1 5366.86 5225.57 35.81 o -3 5 1 7500.28 7185.32 45.41 o -1 5 1 13645.71 14125.20 67.85 o 1 5 1 8695.81 8277.31 46.05 o 3 5 1 11234.80 11498.50 60.15 o 5 5 1 17456.77 17989.78 89.30 o 7 5 1 3658.45 3410.86 29.24 o 9 5 1 3224.32 3356.09 32.51 o 11 5 1 8862.40 8752.49 70.68 o 13 5 1 3129.54 2974.52 40.35 o 15 5 1 5661.86 5693.45 69.30 o 17 5 1 1151.83 1089.10 29.12 o 19 5 1 964.08 963.59 28.90 o 21 5 1 1150.60 1093.78 35.24 o 23 5 1 1750.74 1760.64 46.37 o 25 5 1 1808.07 1894.16 56.43 o 27 5 1 1252.96 1225.57 41.50 o -26 6 1 864.80 786.52 36.13 o -24 6 1 43.38 45.91 13.07 o -22 6 1 277.71 229.40 19.09 o -20 6 1 6.13 1.11 8.59 o -18 6 1 241.98 234.28 14.87 o -16 6 1 7.89 12.77 10.78 o -14 6 1 49.10 32.36 9.34 o -12 6 1 1134.52 1197.75 26.53 o -10 6 1 1088.41 1077.79 19.61 o -8 6 1 570.89 565.71 15.50 o -6 6 1 206.71 221.78 9.70 o -4 6 1 523.17 478.61 10.56 o -2 6 1 544.50 574.63 14.82 o 0 6 1 160.85 159.22 7.53 o 2 6 1 2387.50 2333.30 23.30 o 4 6 1 1074.30 1049.42 18.49 o 6 6 1 1097.41 991.10 21.70 o 8 6 1 3389.21 3437.68 37.70 o 10 6 1 211.37 250.24 12.70 o 12 6 1 0.14 -4.26 8.57 o 14 6 1 77.15 62.75 10.25 o 16 6 1 788.63 849.28 22.68 o 18 6 1 209.99 169.96 15.96 o 20 6 1 190.49 217.81 18.71 o 22 6 1 102.92 86.29 15.94 o 24 6 1 1017.09 1103.69 40.79 o -21 7 1 801.32 728.47 52.33 o -19 7 1 3026.82 3152.13 66.29 o -17 7 1 1020.50 1028.06 35.72 o -15 7 1 1720.45 1693.68 42.34 o -13 7 1 1658.50 1643.21 36.22 o -11 7 1 1760.67 1746.10 39.38 o -9 7 1 1342.40 1316.84 33.50 o -7 7 1 2590.51 2601.97 47.81 o -5 7 1 2261.91 2290.54 32.51 o -3 7 1 6809.08 7025.11 63.99 o -1 7 1 931.15 984.10 28.66 o 1 7 1 5920.28 6103.30 57.68 o 3 7 1 2549.20 2519.36 35.34 o 5 7 1 5602.37 5929.47 68.04 o 7 7 1 3056.19 2966.80 38.06 o 9 7 1 2729.12 2820.62 39.52 o 11 7 1 794.07 765.19 33.45 o 13 7 1 3050.65 3026.81 58.86 o 15 7 1 319.30 286.72 21.53 o 17 7 1 2407.04 2369.29 57.21 o 19 7 1 696.12 704.36 61.69 o -16 8 1 28.89 8.93 10.00 o -14 8 1 98.01 72.47 14.89 o -12 8 1 23.42 33.11 13.72 o -10 8 1 40.39 20.77 8.60 o -8 8 1 4.85 -4.83 10.44 o -6 8 1 140.56 171.09 24.44 o -4 8 1 45.30 40.73 13.58 o -2 8 1 620.30 624.60 29.87 o 2 8 1 169.81 186.43 18.79 o 4 8 1 0.03 -4.50 9.89 o 6 8 1 6.08 21.63 19.60 o 8 8 1 0.18 -5.83 7.64 o 10 8 1 83.17 76.30 14.50 o 12 8 1 20.91 21.38 10.31 o 14 8 1 413.18 442.61 26.31 o -3 9 1 1339.22 1292.65 48.88 o 1 9 1 1812.24 1928.11 59.74 o -36 0 2 309.60 271.57 57.03 o -34 0 2 1483.08 1620.05 153.98 o -32 0 2 2242.52 2265.88 48.29 o -30 0 2 2139.61 2299.33 53.08 o -28 0 2 10358.26 10243.88 101.98 o -26 0 2 4449.88 4340.91 69.83 o -24 0 2 3970.32 4127.01 53.92 o -22 0 2 23088.39 21479.75 150.48 o -20 0 2 5807.75 5828.16 53.67 o -18 0 2 25844.74 26632.86 166.01 o -16 0 2 8194.27 7806.06 60.37 o -14 0 2 18242.90 19657.07 130.00 o -12 0 2 18688.87 18246.78 120.25 o -10 0 2 7737.65 7312.45 53.54 o -8 0 2 16248.44 16187.10 109.52 o -6 0 2 5833.98 5095.78 48.36 o -4 0 2 5803.57 5840.57 57.63 o -2 0 2 83287.92 78947.10 1662.75 o 0 0 2 13626.82 13875.99 108.59 o 2 0 2 182267.38 174451.14 1179.34 o 4 0 2 45387.38 45171.53 418.48 o 6 0 2 4905.03 4146.73 59.80 o 8 0 2 25449.54 24140.88 147.56 o 10 0 2 41222.19 41501.62 516.42 o 12 0 2 1634.21 1656.32 22.50 o 14 0 2 45433.35 45337.81 247.47 o 16 0 2 6170.60 6241.18 52.42 o 18 0 2 1420.27 1447.79 24.68 o 20 0 2 5175.57 5314.88 61.55 o 22 0 2 1370.13 1355.18 30.57 o 24 0 2 5992.43 5890.72 77.66 o 26 0 2 2985.54 3090.55 73.20 o 28 0 2 4.76 7.23 9.43 o 30 0 2 1540.38 1557.68 76.90 o 32 0 2 63.73 65.18 40.73 o -35 1 2 7.32 -19.32 14.21 o -33 1 2 507.50 444.25 28.13 o -31 1 2 2.89 6.60 7.12 o -29 1 2 635.32 635.34 20.96 o -27 1 2 176.59 190.47 11.44 o -25 1 2 6.48 1.92 5.32 o -23 1 2 20.93 16.01 4.65 o -21 1 2 2179.07 2045.25 21.30 o -19 1 2 6.77 6.57 3.70 o -17 1 2 95.04 84.99 5.04 o -15 1 2 31.83 7.27 2.75 o -13 1 2 1685.38 1532.64 14.21 o -11 1 2 8667.04 9387.51 49.24 o -9 1 2 10386.62 10648.70 59.18 o -7 1 2 414.30 420.84 8.65 o -5 1 2 33230.14 35570.39 189.14 o -3 1 2 133.51 206.37 3.36 o -1 1 2 3.25 -2.16 1.08 o 1 1 2 1989.65 1781.60 12.39 o 3 1 2 3078.99 3572.98 18.59 o 5 1 2 26688.89 27372.74 108.01 o 7 1 2 2142.50 2796.01 19.18 o 9 1 2 1014.92 1172.70 11.79 o 11 1 2 7000.42 8054.05 42.65 o 13 1 2 2134.64 2109.35 18.33 o 15 1 2 188.98 212.32 7.40 o 17 1 2 1668.90 1702.15 18.92 o 19 1 2 463.16 510.83 13.31 o 21 1 2 284.48 309.42 11.75 o 23 1 2 0.67 -5.67 6.83 o 25 1 2 1825.96 1788.37 36.05 o 27 1 2 290.35 280.58 19.52 o 29 1 2 259.62 273.34 22.93 o 31 1 2 183.80 144.65 21.27 o -34 2 2 4479.18 4397.10 88.94 o -32 2 2 1882.25 1834.50 50.67 o -30 2 2 1545.48 1690.81 34.04 o -28 2 2 4566.77 4547.04 52.23 o -26 2 2 1391.42 1361.02 23.78 o -24 2 2 3653.25 3810.65 38.68 o -22 2 2 6441.13 6086.84 43.49 o -20 2 2 129.69 168.72 7.74 o -18 2 2 17793.12 17310.23 86.57 o -16 2 2 13805.77 13373.37 68.24 o -14 2 2 8107.37 7511.97 45.40 o -12 2 2 16796.31 16535.21 82.49 o -10 2 2 9344.11 8959.02 50.63 o -8 2 2 19033.14 20058.84 108.22 o -6 2 2 11786.13 11184.29 52.93 o -4 2 2 251.67 162.33 4.73 o -2 2 2 16177.17 16066.33 72.30 o 0 2 2 13556.83 13131.90 67.14 o 2 2 2 16561.39 16254.00 76.42 o 4 2 2 53365.20 53903.06 230.39 o 6 2 2 8584.02 7789.23 41.26 o 8 2 2 100494.68 101953.84 463.69 o 10 2 2 47906.38 48884.66 220.23 o 12 2 2 6523.94 6326.07 37.71 o 14 2 2 12457.19 11873.67 63.64 o 16 2 2 640.78 628.16 12.67 o 18 2 2 1994.79 1879.85 22.77 o 20 2 2 2256.84 2250.24 29.14 o 22 2 2 35.47 19.59 7.49 o 24 2 2 3139.44 3097.26 44.07 o 26 2 2 4868.82 4999.24 62.62 o 28 2 2 3542.87 3475.29 68.79 o 30 2 2 3566.97 3637.27 79.60 o -33 3 2 0.15 11.95 14.21 o -31 3 2 149.81 101.46 16.74 o -29 3 2 363.04 334.31 23.38 o -27 3 2 819.22 854.18 28.19 o -25 3 2 5.99 14.53 11.30 o -23 3 2 0.27 -7.49 5.63 o -21 3 2 727.59 678.86 16.19 o -19 3 2 535.01 437.17 14.30 o -17 3 2 188.05 203.85 11.95 o -15 3 2 87.84 79.20 5.56 o -13 3 2 2025.56 1806.65 19.61 o -11 3 2 7112.85 6940.62 41.01 o -9 3 2 3093.21 3003.38 22.59 o -7 3 2 288.00 284.82 6.82 o -5 3 2 3135.32 3411.67 26.16 o -3 3 2 1094.11 936.05 11.77 o -1 3 2 46.77 20.32 2.81 o 1 3 2 1635.98 1519.29 14.46 o 3 3 2 3337.01 2950.84 18.53 o 5 3 2 7512.25 6886.19 34.92 o 7 3 2 5738.08 5749.88 36.37 o 9 3 2 184.94 228.70 9.27 o 11 3 2 209.92 277.57 8.09 o 13 3 2 2.95 4.14 3.60 o 15 3 2 2629.17 2637.20 32.52 o 17 3 2 734.97 726.58 19.22 o 19 3 2 108.71 86.25 10.23 o 21 3 2 138.95 106.51 10.71 o 23 3 2 1085.85 1047.54 30.55 o 25 3 2 291.66 310.58 20.76 o 27 3 2 89.77 78.77 13.49 o 29 3 2 53.60 46.29 18.73 o -32 4 2 2599.17 2623.63 63.72 o -30 4 2 1465.79 1501.84 42.83 o -28 4 2 943.30 865.52 29.34 o -26 4 2 877.64 843.91 25.15 o -24 4 2 6060.11 6126.50 67.39 o -22 4 2 4456.63 4259.43 55.78 o -20 4 2 4710.18 4714.04 61.33 o -18 4 2 5358.28 5270.72 49.62 o -16 4 2 6363.34 6185.69 55.22 o -14 4 2 2487.10 2364.70 27.32 o -12 4 2 8560.07 8998.25 59.41 o -10 4 2 191.67 179.69 6.10 o -8 4 2 14903.96 15590.42 96.89 o -6 4 2 8069.32 7988.51 47.93 o -4 4 2 14243.57 13476.19 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2 27 577.47 711.59 33.43 o -40 2 27 40.68 20.70 19.38 o -38 2 27 171.43 167.17 22.36 o -36 2 27 45.29 39.23 13.15 o -34 2 27 127.09 177.12 16.69 o -32 2 27 254.44 217.06 16.38 o -30 2 27 2.11 22.10 11.79 o -28 2 27 15.47 7.73 7.29 o -26 2 27 88.64 146.15 13.45 o -24 2 27 14.54 33.87 10.97 o -22 2 27 83.85 75.99 14.33 o -20 2 27 1129.29 1219.41 44.21 o -18 2 27 143.37 77.92 17.82 o -16 2 27 4.89 4.45 13.77 o -14 2 27 180.20 127.75 20.99 o -12 2 27 2.18 2.81 14.35 o -10 2 27 76.84 37.15 17.16 o -8 2 27 187.26 203.29 30.64 o -43 3 27 2522.16 2749.84 60.27 o -41 3 27 2680.20 2645.38 54.35 o -39 3 27 2040.87 2060.24 44.44 o -37 3 27 654.75 782.59 28.43 o -35 3 27 4291.09 3846.00 63.86 o -33 3 27 864.36 946.67 32.04 o -31 3 27 1158.75 1159.39 29.96 o -29 3 27 340.97 247.93 15.96 o -27 3 27 2053.50 2367.40 41.80 o -25 3 27 3828.40 3774.75 53.16 o -23 3 27 5790.12 5820.37 60.25 o -21 3 27 3023.02 3360.77 47.89 o -19 3 27 2142.64 2001.86 41.16 o -17 3 27 3289.29 3519.82 75.31 o -15 3 27 3617.27 3715.92 86.89 o -13 3 27 3231.38 3027.81 71.76 o -11 3 27 2200.29 2335.45 62.85 o -40 4 27 193.87 214.20 27.05 o -38 4 27 50.77 32.61 14.69 o -36 4 27 16.97 4.81 10.82 o -34 4 27 84.90 51.92 12.48 o -32 4 27 224.56 237.75 29.07 o -30 4 27 29.04 12.90 9.62 o -28 4 27 84.23 94.11 13.08 o -26 4 27 371.08 254.79 18.80 o -24 4 27 34.29 67.19 10.74 o -22 4 27 42.61 27.23 9.05 o -20 4 27 69.54 42.75 12.56 o -18 4 27 13.02 12.63 9.28 o -16 4 27 37.85 10.96 9.80 o -14 4 27 41.60 7.63 10.10 o -35 5 27 1829.86 1671.20 239.78 o -33 5 27 880.76 847.55 41.52 o -31 5 27 1665.26 1796.14 46.00 o -29 5 27 888.14 675.44 27.46 o -27 5 27 3072.39 3313.64 57.26 o -25 5 27 1421.59 1381.06 64.78 o -23 5 27 2741.04 2710.74 57.12 o -21 5 27 1384.12 1575.57 53.18 o -19 5 27 1795.76 1699.76 45.48 o -46 0 28 3185.91 2984.50 130.35 o -44 0 28 3634.84 4008.37 113.28 o -42 0 28 1823.39 1501.34 57.33 o -40 0 28 3574.79 3525.12 68.27 o -38 0 28 2918.50 3336.74 58.75 o -36 0 28 4584.91 4096.72 71.34 o -34 0 28 276.57 334.87 23.37 o -32 0 28 740.34 616.07 32.85 o -30 0 28 1725.46 1448.70 48.46 o -28 0 28 1345.09 1791.83 60.28 o -26 0 28 1954.46 1686.76 85.54 o -24 0 28 1978.72 2109.42 66.88 o -22 0 28 4590.52 5072.15 124.92 o -20 0 28 4635.68 4116.93 119.49 o -18 0 28 5561.04 6029.64 122.85 o -16 0 28 1983.02 1865.63 65.20 o -14 0 28 2948.31 2841.81 81.59 o -12 0 28 4449.50 5085.67 113.30 o -10 0 28 2505.18 2494.60 75.83 o -47 1 28 5.41 -25.93 12.96 o -45 1 28 113.73 85.06 15.00 o -43 1 28 34.73 9.80 10.96 o -41 1 28 2.43 -19.64 9.82 o -39 1 28 9.69 -0.41 8.92 o -37 1 28 4.69 6.29 9.37 o -35 1 28 8.03 -4.05 8.48 o -33 1 28 0.04 0.84 8.59 o -31 1 28 22.03 5.68 9.78 o -29 1 28 66.62 48.41 12.28 o -27 1 28 45.48 39.09 12.69 o -25 1 28 51.52 59.69 13.51 o -23 1 28 482.83 405.17 24.57 o -21 1 28 22.17 16.42 11.10 o -19 1 28 34.22 29.55 10.07 o -17 1 28 34.53 22.50 11.37 o -15 1 28 14.32 0.65 12.69 o -13 1 28 12.95 0.63 14.84 o -11 1 28 105.95 86.02 20.97 o -9 1 28 284.08 254.05 29.81 o -46 2 28 2129.55 1862.86 62.60 o -44 2 28 3573.00 3941.96 97.02 o -42 2 28 1054.46 794.33 31.72 o -40 2 28 1640.22 1626.39 43.53 o -38 2 28 2795.48 2609.18 347.84 o -36 2 28 3952.35 3511.06 66.88 o -34 2 28 1751.58 1842.58 47.82 o -32 2 28 391.00 343.74 21.85 o -30 2 28 1453.28 1201.14 34.80 o -28 2 28 977.68 1277.84 30.81 o -26 2 28 5070.39 4589.67 67.65 o -24 2 28 2532.46 2581.74 49.35 o -22 2 28 1720.57 1940.36 55.45 o -20 2 28 2672.09 2389.68 61.75 o -18 2 28 3460.92 3643.82 77.22 o -16 2 28 2583.04 2479.80 64.20 o -14 2 28 2614.97 2458.52 64.47 o -12 2 28 1575.83 1718.05 54.80 o -10 2 28 2051.49 1982.96 86.60 o -43 3 28 69.97 97.74 19.23 o -41 3 28 15.75 10.80 13.86 o -39 3 28 33.62 25.84 12.17 o -37 3 28 1222.49 1017.93 32.76 o -35 3 28 48.01 88.28 14.60 o -33 3 28 578.94 646.04 29.10 o -31 3 28 1.28 -1.55 8.93 o -29 3 28 14.35 9.63 9.05 o -27 3 28 79.87 60.60 12.19 o -25 3 28 3.82 -1.35 9.16 o -23 3 28 31.35 27.53 11.27 o -21 3 28 74.99 77.45 15.99 o -19 3 28 203.82 271.02 29.95 o -17 3 28 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-25 1 29 294.10 264.82 21.78 o -23 1 29 1738.85 1971.90 46.66 o -21 1 29 1506.02 1207.73 45.87 o -19 1 29 2609.93 2867.97 51.36 o -17 1 29 2161.29 2237.76 52.96 o -15 1 29 4343.70 4224.60 74.73 o -13 1 29 2109.87 2402.92 66.36 o -44 2 29 832.63 915.67 45.69 o -42 2 29 252.10 215.00 23.68 o -40 2 29 875.71 864.37 36.36 o -38 2 29 99.69 30.87 20.74 o -36 2 29 4.40 13.16 10.73 o -34 2 29 937.70 962.21 36.36 o -32 2 29 265.79 271.52 22.67 o -30 2 29 458.32 520.62 25.64 o -28 2 29 190.39 273.00 20.67 o -26 2 29 639.08 573.62 32.11 o -24 2 29 379.46 355.89 25.10 o -22 2 29 1.62 -21.20 12.49 o -20 2 29 47.80 68.69 18.14 o -18 2 29 303.71 235.31 33.32 o -16 2 29 21.40 -0.11 15.17 o -14 2 29 65.30 75.88 18.94 o -43 3 29 1021.17 958.87 41.94 o -41 3 29 3490.48 3579.62 71.15 o -39 3 29 5226.22 5570.65 97.20 o -37 3 29 3582.95 3391.56 62.19 o -35 3 29 2309.19 2484.13 52.12 o -33 3 29 2002.58 2148.51 48.23 o -31 3 29 703.95 537.02 24.17 o -29 3 29 276.23 284.94 18.59 o -27 3 29 185.28 134.87 15.31 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1480.93 1342.87 49.92 o -41 3 30 211.18 243.42 30.59 o -39 3 30 0.09 -9.45 12.44 o -37 3 30 451.24 299.10 22.72 o -35 3 30 3.85 2.56 10.89 o -33 3 30 3.85 8.55 10.20 o -31 3 30 5.30 -2.64 9.00 o -29 3 30 0.53 9.00 10.05 o -27 3 30 115.72 167.99 21.98 o -25 3 30 0.87 -15.90 12.96 o -23 3 30 0.26 -10.41 14.01 o -21 3 30 66.42 68.67 19.32 o -19 3 30 273.64 246.93 26.26 o -36 4 30 2707.63 2611.18 59.69 o -34 4 30 1632.78 1805.81 50.71 o -32 4 30 2482.78 2362.44 56.82 o -30 4 30 1815.05 1985.65 62.78 o -28 4 30 1624.44 1642.39 44.70 o -26 4 30 526.62 460.47 28.06 o -24 4 30 890.32 947.97 37.74 o -43 1 31 2414.28 2327.34 51.94 o -41 1 31 1861.03 2284.64 54.97 o -39 1 31 326.92 158.04 19.19 o -37 1 31 1085.34 1136.37 39.73 o -35 1 31 1356.79 1360.95 43.00 o -33 1 31 4974.78 4648.48 80.81 o -31 1 31 5649.01 6385.32 96.80 o -29 1 31 898.14 630.30 79.57 o -27 1 31 1191.10 936.07 153.82 o -25 1 31 2469.41 2894.94 61.71 o -23 1 31 1302.61 1061.68 48.94 o -21 1 31 559.53 576.18 38.52 o -19 1 31 564.28 586.04 40.03 o -17 1 31 1939.33 1712.16 70.07 o -42 2 31 167.07 160.09 22.37 o -40 2 31 81.14 118.82 18.53 o -38 2 31 51.39 26.49 14.05 o -36 2 31 64.61 36.36 23.91 o -34 2 31 44.52 50.93 16.14 o -32 2 31 76.33 65.89 15.47 o -30 2 31 447.79 378.66 29.88 o -28 2 31 40.64 51.91 17.45 o -26 2 31 8.65 1.79 12.37 o -24 2 31 59.45 47.11 16.20 o -22 2 31 4.30 12.18 12.69 o -20 2 31 15.20 0.39 14.43 o -39 3 31 1466.92 1370.66 49.52 o -37 3 31 1131.17 1175.31 46.55 o -35 3 31 1400.21 1524.99 46.63 o -33 3 31 2246.34 2037.39 53.55 o -31 3 31 2262.32 2547.35 58.86 o -29 3 31 842.46 831.12 35.38 o -27 3 31 2132.63 1940.27 51.36 o -25 3 31 1368.51 1575.08 52.95 o -23 3 31 2348.35 2082.08 61.08 o -44 0 32 3969.62 3687.85 143.93 o -42 0 32 1485.68 1762.46 97.76 o -40 0 32 1866.85 1547.92 89.62 o -38 0 32 3156.14 3201.75 130.35 o -36 0 32 1077.61 1192.52 48.94 o -34 0 32 24.46 -8.47 15.57 o -32 0 32 101.37 52.58 20.86 o -30 0 32 1183.51 1075.33 50.21 o -28 0 32 10066.99 10317.66 339.46 o -26 0 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