data_2239781 _cell_angle_alpha 87.163 _cell_angle_beta 85.001 _cell_angle_gamma 66.509 _cell_length_a 10.0618 _cell_length_b 10.1653 _cell_length_c 27.0304 _exptl_crystal_F_000 1116.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file wm0007Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SHELXL INS file, from DIRDIF ouP-1 r S92' _shelx_refln_list_code 4 _shelx_f_calc_maximum 441.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 100037.98 97587.93 8481.83 o 3 0 0 719.42 630.07 132.31 o 4 0 0 1804.77 1662.18 87.30 o 5 0 0 337.59 676.99 96.20 o 6 0 0 2953.14 2720.85 293.11 o 7 0 0 1231.48 1590.82 268.01 o 8 0 0 405.86 517.13 140.03 o 9 0 0 104.21 25.39 146.09 o 11 0 0 4.89 169.20 157.70 o -10 1 0 91.50 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