data_2240006 _cell_angle_alpha 91.593 _cell_angle_beta 95.322 _cell_angle_gamma 104.705 _cell_length_a 9.8969 _cell_length_b 11.8004 _cell_length_c 14.2020 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.7584 _[local]_cod_data_source_file cv5469Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' shelxl in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 200.82 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3178.14 2840.11 36.33 o 2 0 0 566.87 540.74 10.92 o 3 0 0 6239.10 5700.54 102.57 o 4 0 0 5338.19 5053.36 106.01 o 5 0 0 6279.22 5780.85 171.44 o 6 0 0 439.51 420.97 18.03 o 7 0 0 3.16 4.44 9.99 o 8 0 0 202.42 154.00 28.65 o 9 0 0 594.42 597.76 176.90 o 10 0 0 151.68 97.00 52.05 o 11 0 0 251.07 168.31 97.54 o 12 0 0 17.79 21.28 49.91 o -12 1 0 19.01 16.82 34.31 o -11 1 0 158.74 147.26 121.53 o -10 1 0 100.85 70.73 51.52 o -9 1 0 362.36 396.34 31.30 o -8 1 0 120.91 150.86 48.75 o -7 1 0 254.94 326.40 25.22 o -6 1 0 365.56 342.86 16.79 o -5 1 0 154.28 173.38 10.67 o -4 1 0 1.82 4.12 5.97 o -3 1 0 5.65 7.43 4.91 o -2 1 0 123.42 111.04 4.00 o -1 1 0 54.49 61.46 2.43 o 0 1 0 12.74 14.40 3.88 o 1 1 0 149.34 126.78 5.72 o 2 1 0 105.93 128.70 7.02 o 3 1 0 1131.11 1179.50 28.47 o 4 1 0 1040.64 1189.75 28.95 o 5 1 0 9.87 19.90 13.65 o 6 1 0 107.28 135.38 29.43 o 7 1 0 36.77 32.21 18.78 o 8 1 0 67.58 83.06 38.73 o 9 1 0 257.12 261.49 33.12 o 10 1 0 41.37 8.72 26.33 o 11 1 0 12.29 2.55 34.27 o 12 1 0 37.71 -20.82 68.42 o -12 2 0 151.34 71.16 104.71 o -11 2 0 31.28 22.07 17.11 o -10 2 0 1.63 5.96 15.20 o -9 2 0 96.23 96.66 42.20 o -8 2 0 1699.68 1748.31 61.85 o -7 2 0 1686.32 1570.60 98.57 o -6 2 0 84.31 61.72 19.94 o -5 2 0 737.97 697.50 34.21 o -4 2 0 2846.81 2535.00 61.00 o -3 2 0 17702.31 15774.09 130.23 o -2 2 0 283.68 336.83 15.02 o -1 2 0 13629.05 11836.70 159.25 o 1 2 0 80.54 99.47 4.94 o 2 2 0 18901.99 16960.91 570.39 o 3 2 0 1192.36 1133.87 25.01 o 4 2 0 420.02 465.76 18.33 o 5 2 0 701.33 749.84 28.93 o 6 2 0 3308.14 3662.51 103.46 o 7 2 0 1802.16 2041.52 77.69 o 8 2 0 53.83 87.21 34.51 o 9 2 0 229.83 94.64 51.13 o 10 2 0 5.83 12.58 32.69 o 11 2 0 79.41 53.01 43.11 o -12 3 0 7.81 30.48 48.86 o -11 3 0 67.98 81.17 39.08 o -10 3 0 493.02 523.06 67.63 o -9 3 0 13.36 7.47 11.64 o -8 3 0 104.93 65.46 20.99 o -7 3 0 314.97 318.70 16.88 o -6 3 0 358.19 358.92 26.85 o -5 3 0 286.54 269.78 12.43 o -4 3 0 2427.97 2546.15 31.60 o -3 3 0 63.01 69.87 10.69 o -2 3 0 2383.24 2339.01 46.16 o -1 3 0 173.18 198.37 7.44 o 0 3 0 740.59 802.24 13.35 o 1 3 0 852.13 927.55 15.30 o 2 3 0 765.66 826.33 15.29 o 3 3 0 152.19 167.10 10.60 o 4 3 0 39.09 68.85 19.73 o 5 3 0 0.73 0.03 10.92 o 6 3 0 56.81 60.52 22.61 o 7 3 0 159.40 201.70 27.85 o 8 3 0 4.36 11.93 14.60 o 9 3 0 63.49 77.35 43.55 o 10 3 0 1.10 26.46 30.84 o 11 3 0 52.35 68.43 51.26 o -12 4 0 1.51 -9.03 29.25 o 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0 17.23 16.17 5.99 o 0 5 0 330.42 425.37 13.33 o 1 5 0 6.27 25.55 9.72 o 2 5 0 2109.21 2540.05 64.42 o 3 5 0 109.54 107.13 25.75 o 4 5 0 32.26 34.25 13.59 o 5 5 0 70.45 64.06 23.84 o 6 5 0 512.91 482.96 33.08 o 7 5 0 8.89 22.36 16.31 o 8 5 0 23.77 27.56 17.98 o 9 5 0 0.68 -0.93 27.70 o 10 5 0 32.30 27.63 45.79 o -12 6 0 253.35 147.02 79.14 o -11 6 0 92.27 42.95 36.50 o -10 6 0 748.37 706.69 65.82 o -9 6 0 208.50 133.80 64.31 o -8 6 0 593.57 570.34 46.46 o -7 6 0 182.82 198.57 73.74 o -6 6 0 2368.80 2562.90 120.99 o -5 6 0 2509.77 2493.59 117.39 o -4 6 0 2094.15 2173.02 62.01 o -3 6 0 7597.13 7471.98 140.29 o -2 6 0 2324.95 2592.48 63.76 o -1 6 0 3000.29 3210.60 64.05 o 0 6 0 17900.96 17531.95 196.96 o 1 6 0 1194.67 1177.27 37.61 o 2 6 0 933.76 963.29 33.44 o 3 6 0 218.18 175.78 26.96 o 4 6 0 3140.35 3288.33 184.31 o 5 6 0 3177.60 3604.78 185.35 o 6 6 0 170.76 210.97 66.18 o 7 6 0 104.38 127.87 41.21 o 8 6 0 91.60 98.59 45.68 o 9 6 0 395.68 318.51 173.89 o 10 6 0 59.87 48.65 39.71 o -12 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3711.77 256.86 o 2 8 0 3314.93 3691.46 200.51 o 3 8 0 842.95 878.94 56.51 o 4 8 0 207.22 188.24 81.11 o 5 8 0 519.72 506.38 60.61 o 6 8 0 866.00 995.02 97.57 o 7 8 0 414.44 350.81 190.43 o 8 8 0 3.47 -9.16 51.33 o 9 8 0 43.47 74.42 64.66 o -12 9 0 77.06 61.81 43.09 o -11 9 0 17.31 39.21 33.69 o -10 9 0 223.57 226.77 102.64 o -9 9 0 212.78 183.44 90.95 o -8 9 0 66.59 62.50 45.61 o -7 9 0 12.93 31.93 27.75 o -6 9 0 66.65 41.90 18.42 o -5 9 0 2437.78 2455.65 97.08 o -4 9 0 459.44 436.16 21.27 o -3 9 0 917.70 953.77 56.79 o -2 9 0 99.79 117.08 46.91 o -1 9 0 915.52 953.29 59.78 o 0 9 0 468.94 427.93 59.00 o 1 9 0 748.23 795.46 47.31 o 2 9 0 42.70 50.98 22.77 o 3 9 0 0.17 16.95 22.06 o 4 9 0 5.02 34.55 18.48 o 5 9 0 3.11 -2.29 27.51 o 6 9 0 0.70 15.59 52.02 o 7 9 0 9.38 16.16 30.77 o 8 9 0 12.10 13.77 45.61 o -11 10 0 115.33 114.99 81.45 o -10 10 0 269.03 157.29 75.27 o -9 10 0 240.18 134.10 79.23 o -8 10 0 83.76 68.33 46.79 o -7 10 0 120.83 101.30 43.92 o -6 10 0 878.58 701.27 154.52 o -5 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