#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:00:21 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181900 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/00/2240037.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240037 _cell_angle_alpha 90.000 _cell_angle_beta 104.577 _cell_angle_gamma 90.000 _cell_length_a 11.2244 _cell_length_b 6.8288 _cell_length_c 11.6641 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.8219 _cod_data_source_file sj5429Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PY34_0m in P2(1)/c (RT)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5355.74 4600.29 69.50 o 2 0 0 1096.41 1097.57 16.58 o 3 0 0 2406.47 2338.66 43.96 o 4 0 0 16.68 20.79 0.55 o 5 0 0 1345.02 1375.85 19.84 o 6 0 0 63.11 62.53 1.72 o 7 0 0 390.40 346.19 8.96 o 9 0 0 11.12 13.85 2.53 o 10 0 0 4.07 4.27 0.55 o 11 0 0 304.98 330.78 8.47 o 12 0 0 150.90 149.19 3.98 o 13 0 0 2.70 1.66 0.24 o 1 1 0 550.41 531.71 5.29 o 2 1 0 262.18 261.16 2.82 o 3 1 0 2182.39 2239.35 28.43 o 4 1 0 1546.35 1650.93 17.26 o 5 1 0 74.44 80.28 1.35 o 6 1 0 415.52 449.45 7.31 o 7 1 0 1.58 2.84 0.50 o 8 1 0 7.95 7.91 0.95 o 9 1 0 527.59 541.40 8.39 o 10 1 0 415.13 386.29 9.14 o 11 1 0 60.89 61.99 1.43 o 12 1 0 2.07 3.72 0.28 o 13 1 0 5.65 6.01 0.40 o 0 2 0 3560.07 3140.36 37.10 o 1 2 0 836.28 816.74 7.55 o 2 2 0 30.38 24.75 0.38 o 3 2 0 3624.35 3882.60 37.88 o 4 2 0 804.15 942.85 10.94 o 5 2 0 637.48 680.60 9.28 o 6 2 0 15.41 18.10 0.84 o 7 2 0 595.52 603.52 19.39 o 8 2 0 285.24 265.03 11.74 o 9 2 0 138.76 130.95 2.98 o 10 2 0 3.39 2.93 0.40 o 11 2 0 44.43 47.21 1.66 o 12 2 0 26.61 28.02 1.03 o 1 3 0 1202.44 1261.72 12.44 o 2 3 0 709.10 772.14 8.62 o 3 3 0 1870.30 1988.79 24.27 o 4 3 0 116.98 102.49 3.33 o 5 3 0 205.27 209.82 3.68 o 6 3 0 486.09 471.30 10.97 o 7 3 0 2.88 3.56 1.36 o 8 3 0 53.15 57.96 1.41 o 9 3 0 6.70 5.97 0.67 o 10 3 0 0.15 0.63 0.24 o 11 3 0 39.27 41.58 1.43 o 12 3 0 4.72 7.59 0.47 o 0 4 0 137.55 123.91 4.73 o 1 4 0 64.15 45.41 1.40 o 2 4 0 334.70 322.60 4.95 o 3 4 0 98.41 128.31 2.62 o 4 4 0 0.45 1.44 0.30 o 5 4 0 227.16 234.04 7.89 o 6 4 0 19.60 17.83 0.69 o 7 4 0 302.42 287.41 5.11 o 8 4 0 9.50 11.18 2.02 o 9 4 0 39.69 40.89 2.69 o 10 4 0 98.81 100.66 2.38 o 11 4 0 25.11 27.08 0.95 o 1 5 0 316.89 330.26 11.36 o 3 5 0 462.29 440.88 6.41 o 4 5 0 50.30 40.61 1.52 o 5 5 0 2.01 2.25 0.58 o 6 5 0 43.58 44.57 2.85 o 7 5 0 10.05 12.35 1.57 o 8 5 0 13.27 9.81 1.35 o 9 5 0 38.86 42.69 2.93 o 10 5 0 0.18 0.40 0.95 o 0 6 0 8.15 7.67 0.79 o 1 6 0 1.29 1.30 0.45 o 2 6 0 5.81 5.58 0.63 o 3 6 0 0.08 0.01 0.87 o 4 6 0 22.14 21.85 2.18 o 5 6 0 24.43 23.87 1.92 o 6 6 0 1.96 3.09 0.89 o 7 6 0 139.96 131.86 4.45 o 8 6 0 6.38 7.59 1.42 o 1 7 0 9.17 6.49 1.17 o 2 7 0 24.76 27.76 1.96 o 3 7 0 19.48 18.78 1.46 o 4 7 0 1.01 1.37 0.75 o 5 7 0 4.08 4.85 0.95 o 6 7 0 23.42 25.07 2.10 o 7 7 0 6.36 4.75 0.95 o 0 8 0 100.60 100.55 3.49 o 1 8 0 33.18 29.30 2.06 o 2 8 0 0.57 0.47 0.95 o 3 8 0 14.00 16.30 1.58 o -13 1 1 0.95 0.68 0.17 o -12 1 1 14.52 17.03 0.56 o -11 1 1 111.77 110.61 2.27 o -10 1 1 224.50 222.01 4.17 o -9 1 1 88.10 89.71 2.09 o -8 1 1 227.18 260.12 8.93 o -7 1 1 758.32 800.64 16.24 o -6 1 1 124.76 143.63 3.18 o -5 1 1 84.20 80.35 1.26 o -4 1 1 124.98 142.67 1.80 o -3 1 1 626.42 627.01 5.73 o -2 1 1 1.56 6.99 0.18 o -1 1 1 630.90 607.00 5.70 o 0 1 1 1753.89 1662.00 15.80 o 1 1 1 1122.15 1210.61 12.76 o 2 1 1 2367.89 2497.51 33.63 o 3 1 1 954.36 1106.38 11.99 o 4 1 1 683.54 773.22 8.97 o 5 1 1 123.33 130.56 1.89 o 6 1 1 19.95 18.33 0.79 o 7 1 1 216.69 228.22 5.26 o 8 1 1 2.90 2.57 0.43 o 9 1 1 111.73 109.57 2.00 o 10 1 1 1.11 0.40 0.24 o 11 1 1 54.05 57.29 1.32 o 12 1 1 23.96 22.53 0.70 o -13 2 1 41.27 39.94 1.27 o -12 2 1 11.86 11.79 0.63 o -11 2 1 0.09 0.91 1.07 o -10 2 1 191.19 197.08 6.84 o -9 2 1 58.12 58.13 1.21 o -8 2 1 350.39 314.56 4.85 o -7 2 1 196.17 205.54 7.48 o -6 2 1 669.24 715.58 10.48 o -5 2 1 125.83 121.38 2.07 o -4 2 1 20.27 28.45 0.73 o -3 2 1 729.33 821.78 7.63 o -2 2 1 4811.11 4890.88 49.32 o -1 2 1 1645.82 1728.71 15.31 o 0 2 1 0.54 1.31 0.13 o 1 2 1 1350.43 1433.05 11.98 o 2 2 1 1.40 3.98 0.15 o 3 2 1 818.44 964.15 12.63 o 4 2 1 326.82 353.84 5.01 o 5 2 1 505.32 539.54 8.11 o 6 2 1 108.78 124.93 3.55 o 7 2 1 33.38 28.98 1.17 o 8 2 1 67.77 65.94 1.73 o 9 2 1 6.53 6.73 0.47 o 10 2 1 28.01 25.57 1.11 o 11 2 1 0.94 1.27 0.26 o 12 2 1 4.51 4.59 0.40 o -12 3 1 2.64 2.69 0.32 o -11 3 1 0.90 1.19 0.32 o -10 3 1 2.40 2.11 0.38 o -9 3 1 9.01 7.04 0.59 o -8 3 1 1.67 3.10 1.23 o -7 3 1 22.45 24.55 1.10 o -6 3 1 9.13 7.33 0.72 o -5 3 1 226.07 227.25 3.81 o -4 3 1 132.86 183.80 3.08 o -3 3 1 3.78 6.53 0.35 o -2 3 1 2128.21 2412.91 25.01 o -1 3 1 338.84 345.45 3.74 o 0 3 1 105.81 119.64 1.55 o 1 3 1 28.17 21.88 0.72 o 2 3 1 75.89 77.89 1.20 o 3 3 1 2434.07 2715.43 34.62 o 4 3 1 20.05 24.10 0.68 o 5 3 1 9.10 9.67 0.66 o 6 3 1 372.93 368.76 8.75 o 7 3 1 50.89 52.31 1.33 o 8 3 1 96.00 97.71 2.35 o 9 3 1 1.26 1.27 0.32 o 10 3 1 11.90 12.50 0.71 o 11 3 1 20.40 21.05 0.87 o 12 3 1 10.43 11.16 0.47 o -11 4 1 46.89 50.67 1.29 o -10 4 1 1.82 1.22 0.30 o -9 4 1 6.49 5.26 1.54 o -8 4 1 212.53 210.88 6.05 o -7 4 1 34.23 36.61 1.11 o -6 4 1 119.86 109.84 2.82 o -5 4 1 478.66 492.71 11.45 o -4 4 1 57.64 49.59 1.36 o -3 4 1 284.76 273.02 4.54 o -2 4 1 2.93 5.03 0.39 o -1 4 1 112.98 100.22 1.73 o 0 4 1 276.23 291.51 7.82 o 1 4 1 117.67 123.42 2.60 o 2 4 1 469.29 517.37 10.35 o 3 4 1 230.68 243.65 6.46 o 4 4 1 112.70 116.78 2.81 o 5 4 1 6.51 4.67 0.54 o 6 4 1 36.82 23.82 0.75 o 7 4 1 177.66 164.00 3.44 o 8 4 1 8.06 10.52 0.64 o 9 4 1 32.49 32.30 2.81 o 10 4 1 11.25 11.47 0.63 o 11 4 1 15.41 14.17 0.63 o -10 5 1 48.51 51.11 2.54 o -9 5 1 103.05 126.37 4.05 o -8 5 1 21.02 17.96 2.22 o -7 5 1 50.18 55.72 4.28 o -6 5 1 36.11 29.65 0.97 o -5 5 1 128.49 108.57 2.44 o -4 5 1 90.89 76.68 2.02 o -3 5 1 26.40 25.81 0.92 o -1 5 1 135.24 120.22 4.61 o 0 5 1 2.38 2.92 0.42 o 1 5 1 431.81 417.08 9.96 o 2 5 1 49.36 54.03 3.76 o 3 5 1 44.61 45.51 2.32 o 4 5 1 208.69 209.70 4.59 o 5 5 1 48.95 39.15 2.45 o 6 5 1 131.92 130.99 3.40 o 7 5 1 0.19 0.47 0.93 o 8 5 1 0.34 1.03 1.11 o 9 5 1 100.48 94.47 3.73 o -9 6 1 2.38 2.77 0.87 o -8 6 1 104.39 104.89 3.97 o -7 6 1 14.28 9.25 1.26 o -6 6 1 11.53 11.42 1.34 o -5 6 1 47.23 47.67 2.63 o -4 6 1 0.60 0.58 0.51 o -3 6 1 164.23 160.29 2.68 o -2 6 1 26.62 29.17 1.28 o -1 6 1 156.58 156.57 3.36 o 0 6 1 924.03 898.84 11.40 o 1 6 1 1001.19 1034.54 17.65 o 2 6 1 2.48 2.54 1.00 o 3 6 1 118.85 105.38 3.30 o 4 6 1 86.04 93.60 2.80 o 5 6 1 96.22 97.34 3.44 o 6 6 1 1.68 4.81 0.99 o 7 6 1 64.66 67.74 3.96 o 8 6 1 26.33 24.31 1.58 o -7 7 1 48.90 43.04 2.38 o -6 7 1 74.53 83.15 2.60 o -5 7 1 37.37 30.43 1.54 o -4 7 1 188.66 183.34 4.39 o -3 7 1 1.97 1.63 0.87 o -2 7 1 112.74 116.70 4.92 o -1 7 1 15.91 17.29 1.57 o 0 7 1 177.38 172.68 4.30 o 1 7 1 228.63 234.81 4.44 o 2 7 1 15.58 12.13 1.14 o 3 7 1 107.39 113.47 3.41 o 4 7 1 19.90 20.38 1.32 o 5 7 1 16.62 19.78 1.14 o 6 7 1 40.88 44.91 1.71 o -3 8 1 53.66 64.85 2.77 o -2 8 1 0.66 0.95 0.87 o -1 8 1 55.58 50.02 2.46 o 0 8 1 28.32 28.43 2.06 o 1 8 1 16.22 15.18 1.12 o 2 8 1 16.62 14.56 1.58 o 3 8 1 67.17 70.78 2.94 o -13 0 2 26.83 26.52 0.95 o -12 0 2 91.05 95.29 2.78 o -11 0 2 64.86 68.16 2.22 o -10 0 2 27.28 24.54 1.19 o -9 0 2 10.56 8.54 0.83 o -8 0 2 745.70 813.78 25.90 o -7 0 2 293.24 259.63 5.92 o -6 0 2 187.91 264.07 5.93 o -5 0 2 3485.21 3771.84 58.09 o -4 0 2 349.92 409.42 5.06 o -3 0 2 2101.50 2198.68 26.61 o -2 0 2 100.38 139.75 2.20 o -1 0 2 3821.63 3343.44 46.84 o 0 0 2 1327.11 1264.54 37.80 o 1 0 2 9399.58 8683.24 131.36 o 2 0 2 688.47 770.17 13.49 o 3 0 2 1361.56 1403.90 21.32 o 4 0 2 1358.46 1311.69 19.62 o 5 0 2 14.22 26.72 0.88 o 6 0 2 239.29 243.36 4.55 o 8 0 2 27.70 22.24 1.03 o 9 0 2 209.16 184.26 4.94 o 10 0 2 360.82 376.23 9.52 o 11 0 2 355.49 347.93 8.73 o 12 0 2 8.15 7.28 0.47 o -13 1 2 0.07 0.02 0.13 o -12 1 2 94.01 97.14 1.99 o -11 1 2 2.48 2.06 0.28 o -10 1 2 771.93 753.26 11.51 o -9 1 2 10.91 10.91 0.88 o -8 1 2 7.98 5.54 0.79 o -7 1 2 901.63 950.09 18.30 o -6 1 2 28.98 33.68 1.10 o -5 1 2 2914.73 2906.57 34.86 o -4 1 2 387.05 382.12 3.95 o -3 1 2 2524.79 2589.62 24.89 o -2 1 2 6175.72 5913.35 51.05 o -1 1 2 974.25 1011.98 8.48 o 0 1 2 35.78 34.28 0.41 o 1 1 2 13284.88 13258.49 166.34 o 2 1 2 8792.82 9127.65 103.13 o 3 1 2 4.44 5.18 0.19 o 4 1 2 511.74 571.48 7.04 o 5 1 2 1726.28 1749.39 19.26 o 6 1 2 294.80 316.59 5.10 o 8 1 2 101.17 93.48 2.78 o 9 1 2 14.76 8.07 0.63 o 10 1 2 57.72 54.83 1.82 o 11 1 2 40.45 34.37 1.27 o 12 1 2 10.28 11.35 0.45 o -12 2 2 7.85 9.57 0.44 o -11 2 2 0.61 0.75 0.22 o -10 2 2 23.87 21.12 1.46 o -9 2 2 54.31 53.27 0.97 o -8 2 2 1081.88 1017.30 17.92 o -7 2 2 96.98 103.45 2.68 o -6 2 2 850.65 833.08 12.27 o -5 2 2 427.49 432.57 6.20 o -4 2 2 382.58 424.30 5.67 o -3 2 2 270.81 271.87 3.31 o -2 2 2 0.32 0.81 0.13 o -1 2 2 1379.86 1341.91 11.78 o 0 2 2 29.10 32.00 0.59 o 1 2 2 98.66 111.64 1.37 o 2 2 2 2240.31 2454.13 24.15 o 3 2 2 35.20 30.96 0.73 o 4 2 2 895.37 961.45 13.47 o 5 2 2 61.41 71.66 2.10 o 6 2 2 79.26 82.41 2.65 o 7 2 2 223.57 215.02 5.66 o 8 2 2 261.48 237.31 4.98 o 9 2 2 14.94 13.61 0.79 o 10 2 2 10.80 13.54 0.61 o 11 2 2 0.87 0.85 0.79 o 12 2 2 7.42 9.18 0.47 o -12 3 2 0.46 0.24 0.24 o -11 3 2 66.66 67.44 1.82 o -10 3 2 77.17 80.50 2.19 o -9 3 2 96.25 100.87 2.45 o -8 3 2 22.26 23.00 0.68 o -7 3 2 171.22 168.03 3.57 o -6 3 2 21.78 27.53 0.99 o -5 3 2 50.17 36.06 1.01 o -4 3 2 766.78 828.17 12.61 o -3 3 2 505.79 542.31 7.35 o -2 3 2 1917.11 1901.59 22.91 o -1 3 2 422.89 489.85 6.08 o 0 3 2 77.50 76.55 1.11 o 1 3 2 21.83 21.63 0.47 o 2 3 2 114.84 127.65 1.59 o 3 3 2 1173.90 1146.67 15.01 o 4 3 2 256.25 268.20 5.00 o 5 3 2 348.92 311.90 6.14 o 6 3 2 39.19 36.80 1.70 o 7 3 2 5.79 5.23 0.58 o 8 3 2 152.13 142.97 3.15 o 9 3 2 8.24 8.15 0.59 o 10 3 2 47.16 46.50 1.58 o 11 3 2 4.33 6.64 0.47 o -11 4 2 14.81 15.27 1.35 o -10 4 2 103.29 110.41 3.81 o -9 4 2 369.46 390.85 10.17 o -8 4 2 6.01 4.97 0.77 o -7 4 2 9.60 9.44 1.07 o -6 4 2 270.97 235.86 3.86 o -5 4 2 191.90 180.54 3.93 o -4 4 2 415.26 401.41 6.71 o -3 4 2 7.55 9.59 0.46 o -2 4 2 956.84 1061.24 15.15 o -1 4 2 2456.98 2493.63 33.63 o 0 4 2 1.60 1.01 0.20 o 1 4 2 228.61 229.47 4.82 o 2 4 2 404.88 386.07 7.85 o 3 4 2 1.09 1.88 0.83 o 5 4 2 4.46 4.97 0.41 o 6 4 2 125.32 119.20 2.96 o 7 4 2 6.66 9.20 0.64 o 8 4 2 69.61 73.00 2.06 o 9 4 2 0.58 1.42 0.32 o 10 4 2 2.61 2.77 0.32 o -10 5 2 35.17 37.14 1.82 o -9 5 2 0.68 0.32 0.95 o -8 5 2 112.72 115.67 5.32 o -7 5 2 9.23 12.19 0.87 o -6 5 2 238.15 212.20 2.99 o -5 5 2 104.27 86.10 1.58 o -4 5 2 10.88 10.57 0.68 o -3 5 2 15.58 17.33 1.46 o 0 5 2 479.07 474.60 15.92 o 1 5 2 27.43 26.69 1.59 o 2 5 2 369.71 343.70 7.27 o 3 5 2 0.67 4.65 3.80 o 4 5 2 94.49 87.74 3.53 o 5 5 2 2.87 2.51 1.01 o 6 5 2 39.78 38.95 1.56 o 7 5 2 24.41 28.12 0.91 o 8 5 2 56.25 51.72 1.32 o 9 5 2 16.97 18.04 0.71 o -9 6 2 2.05 2.14 0.79 o -8 6 2 91.29 89.68 3.10 o -7 6 2 18.44 13.42 1.42 o -6 6 2 10.08 9.76 0.67 o -5 6 2 27.41 30.86 1.55 o -4 6 2 17.14 20.68 1.12 o -3 6 2 80.08 78.73 1.93 o -2 6 2 11.89 12.42 1.03 o -1 6 2 103.62 109.74 5.16 o 0 6 2 46.02 49.38 2.91 o 1 6 2 34.45 30.08 2.18 o 2 6 2 123.60 121.35 3.41 o 3 6 2 1.11 1.67 0.95 o 4 6 2 155.28 170.25 4.87 o 5 6 2 74.27 81.60 2.94 o 6 6 2 23.58 26.79 1.93 o 7 6 2 0.10 0.53 0.76 o 8 6 2 42.18 40.11 4.04 o -6 7 2 0.60 0.60 0.68 o -5 7 2 0.03 0.12 0.67 o -4 7 2 4.30 5.54 1.03 o -3 7 2 2.09 1.58 1.27 o -2 7 2 15.55 14.32 2.06 o -1 7 2 26.19 25.59 1.82 o 0 7 2 45.99 40.95 2.46 o 1 7 2 46.32 46.00 2.43 o 2 7 2 19.36 17.79 1.21 o 3 7 2 4.74 7.00 1.02 o 4 7 2 1.01 0.83 0.74 o 5 7 2 48.56 51.86 1.88 o 6 7 2 18.31 20.38 1.12 o -3 8 2 0.00 0.24 0.79 o -2 8 2 2.68 3.48 1.03 o -1 8 2 0.40 -0.24 0.87 o 0 8 2 1.61 3.72 1.03 o 1 8 2 101.79 117.59 3.97 o -13 1 3 16.31 19.32 0.56 o -12 1 3 8.06 7.17 0.42 o -11 1 3 21.57 21.96 0.73 o -10 1 3 24.34 22.75 0.73 o -9 1 3 7.74 7.70 0.38 o -8 1 3 0.77 5.73 2.29 o -7 1 3 99.89 89.46 2.16 o -6 1 3 172.21 215.17 3.53 o -5 1 3 476.29 558.70 7.13 o -4 1 3 33.98 36.99 0.66 o -3 1 3 49.22 56.92 0.70 o -2 1 3 383.67 433.38 4.24 o -1 1 3 726.43 684.16 6.61 o 0 1 3 5516.86 5588.27 58.85 o 1 1 3 4670.54 4887.67 48.22 o 2 1 3 977.76 1074.66 11.75 o 3 1 3 242.13 258.07 3.15 o 4 1 3 338.21 354.71 4.79 o 5 1 3 51.48 43.03 1.29 o 6 1 3 106.33 116.23 3.07 o 7 1 3 106.26 82.39 2.46 o 8 1 3 15.31 12.26 0.79 o 9 1 3 1.17 0.47 0.32 o 10 1 3 31.61 27.47 1.11 o 11 1 3 0.63 1.48 0.26 o 12 1 3 26.99 24.92 0.81 o -13 2 3 16.52 16.63 0.47 o -12 2 3 16.03 16.69 0.75 o -11 2 3 22.50 21.01 1.22 o -10 2 3 19.91 20.11 0.58 o -9 2 3 487.20 508.39 6.68 o -8 2 3 1000.31 925.91 11.89 o -7 2 3 5.65 9.25 1.12 o -6 2 3 13.98 15.02 0.74 o -5 2 3 17.95 16.71 0.62 o -4 2 3 684.08 717.67 9.40 o -3 2 3 165.24 169.16 2.24 o -2 2 3 79.21 102.79 1.21 o -1 2 3 556.81 604.02 6.48 o 0 2 3 212.36 204.09 2.25 o 1 2 3 143.82 160.76 2.18 o 2 2 3 1104.29 1252.55 15.25 o 3 2 3 614.41 612.46 8.74 o 4 2 3 286.67 333.17 5.26 o 5 2 3 51.32 56.99 1.58 o 6 2 3 29.12 25.41 1.66 o 7 2 3 10.51 8.86 0.62 o 8 2 3 6.39 6.94 0.51 o 9 2 3 7.27 7.99 0.53 o 10 2 3 1.88 1.05 0.26 o 11 2 3 3.52 4.26 0.40 o -12 3 3 5.63 7.38 1.23 o -11 3 3 35.48 36.73 1.51 o -10 3 3 27.95 28.64 1.10 o -9 3 3 176.98 181.48 5.45 o -8 3 3 89.68 77.45 2.30 o -7 3 3 414.63 411.76 6.33 o -6 3 3 14.37 13.40 0.67 o -5 3 3 369.92 353.95 5.55 o -4 3 3 10.27 14.51 0.51 o -3 3 3 948.03 1011.54 13.54 o -2 3 3 4.84 8.77 0.37 o -1 3 3 28.77 17.89 0.45 o 0 3 3 189.41 182.42 2.37 o 1 3 3 94.71 90.62 1.41 o 2 3 3 98.50 105.43 1.51 o 3 3 3 602.93 563.49 7.86 o 4 3 3 221.13 257.89 4.37 o 5 3 3 9.16 7.92 0.66 o 6 3 3 73.98 69.30 2.06 o 7 3 3 75.45 65.17 1.76 o 8 3 3 104.07 97.58 2.29 o 9 3 3 14.80 14.34 1.74 o 10 3 3 0.10 0.29 0.20 o 11 3 3 25.70 28.35 0.95 o -11 4 3 25.18 23.67 1.58 o -10 4 3 19.63 28.41 2.77 o -9 4 3 38.40 39.91 2.30 o -8 4 3 23.98 27.68 1.43 o -7 4 3 299.34 298.13 4.35 o -6 4 3 65.10 59.78 1.46 o -5 4 3 70.79 75.82 2.59 o -4 4 3 55.61 62.20 1.71 o -3 4 3 104.10 96.26 1.84 o -2 4 3 28.75 28.01 0.90 o -1 4 3 480.36 460.93 6.72 o 0 4 3 308.91 319.63 4.11 o 1 4 3 35.69 40.35 0.90 o 2 4 3 247.62 235.31 7.30 o 3 4 3 58.28 55.91 1.76 o 4 4 3 298.48 266.94 4.38 o 5 4 3 0.45 0.42 0.30 o 6 4 3 42.19 37.21 1.61 o 7 4 3 6.08 5.52 0.51 o 8 4 3 23.87 22.74 1.86 o 9 4 3 0.55 0.32 0.24 o 10 4 3 6.18 6.25 0.40 o -9 5 3 109.35 112.34 5.16 o -8 5 3 15.02 12.99 0.83 o -7 5 3 41.62 42.07 1.86 o -6 5 3 21.70 16.50 1.15 o -5 5 3 152.05 137.21 2.78 o -4 5 3 4.07 3.30 0.50 o -3 5 3 241.42 215.85 5.40 o -2 5 3 179.51 163.37 4.26 o -1 5 3 0.20 0.32 1.34 o 0 5 3 488.46 475.25 8.98 o 1 5 3 199.41 179.43 5.09 o 2 5 3 728.30 692.77 12.60 o 3 5 3 25.07 25.50 1.50 o 4 5 3 38.36 33.95 1.68 o 5 5 3 234.69 254.89 4.18 o 6 5 3 13.54 13.07 0.70 o 7 5 3 13.60 15.65 0.67 o 8 5 3 71.16 67.43 2.49 o 9 5 3 0.16 0.00 0.16 o -8 6 3 22.65 26.75 2.53 o -7 6 3 24.76 21.37 2.53 o -6 6 3 61.88 58.23 1.60 o -5 6 3 54.71 46.08 1.39 o -4 6 3 209.14 200.00 3.64 o -3 6 3 74.03 71.82 2.62 o -2 6 3 119.30 123.78 2.62 o -1 6 3 58.41 54.36 2.60 o 0 6 3 68.80 79.89 3.20 o 1 6 3 30.37 26.32 2.06 o 2 6 3 6.19 2.88 1.06 o 3 6 3 7.59 9.15 1.36 o 4 6 3 74.32 67.03 3.11 o 5 6 3 0.49 1.25 0.89 o 6 6 3 26.98 30.50 1.98 o 7 6 3 17.93 13.31 1.10 o -7 7 3 111.76 107.33 3.82 o -6 7 3 184.32 162.73 3.75 o -5 7 3 11.84 14.95 1.82 o -4 7 3 3.72 2.06 1.19 o -3 7 3 38.33 41.74 1.35 o -2 7 3 97.38 95.87 2.18 o -1 7 3 15.37 15.46 0.93 o 0 7 3 92.79 90.07 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