#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:00:21 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181900 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/00/2240055.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240055 _cell_angle_alpha 72.754 _cell_angle_beta 75.891 _cell_angle_gamma 89.551 _cell_length_a 12.9784 _cell_length_b 13.0834 _cell_length_c 16.7340 _exptl_crystal_F_000 1408.00 _reflns_d_resolution_high 0.7689 _cod_data_source_file bg2536Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 05105 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 427.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4.03 -4.28 4.28 o 2 0 0 72843.29 71679.61 1044.00 o 3 0 0 964.71 1214.38 32.32 o 4 0 0 3622.85 3582.52 69.54 o 5 0 0 22501.41 22368.50 340.99 o 6 0 0 6508.99 6439.59 119.53 o 7 0 0 35422.87 35206.40 533.98 o 8 0 0 4679.36 4642.53 114.70 o 9 0 0 854.74 772.10 68.57 o 10 0 0 1249.44 1293.10 55.65 o 11 0 0 2465.51 2617.02 79.81 o 12 0 0 495.07 408.06 81.87 o 13 0 0 841.29 865.31 75.92 o 14 0 0 478.78 597.01 127.69 o 15 0 0 179.74 41.31 92.01 o -14 1 0 105.70 58.49 71.35 o -13 1 0 5996.96 5923.83 161.71 o -12 1 0 4865.42 5001.24 120.79 o -11 1 0 19068.96 21134.30 420.46 o -10 1 0 1586.00 1462.94 62.07 o -9 1 0 14913.24 15138.45 257.75 o -8 1 0 8241.22 8159.88 152.60 o -7 1 0 5462.54 5464.94 109.27 o -6 1 0 1263.86 1368.10 80.50 o -5 1 0 18141.43 18558.44 287.38 o -4 1 0 9693.45 9428.42 153.96 o -3 1 0 5230.81 5300.68 106.41 o -2 1 0 23992.56 23234.38 438.56 o -1 1 0 5808.32 5484.94 145.62 o 0 1 0 0.95 -3.79 3.79 o 1 1 0 119444.39 113847.19 1860.96 o 2 1 0 264.86 263.34 21.95 o 3 1 0 1379.81 1466.59 37.39 o 4 1 0 8905.03 8445.19 179.15 o 5 1 0 1777.42 1915.36 60.73 o 6 1 0 13571.54 14290.26 232.11 o 7 1 0 1223.51 1115.64 41.93 o 8 1 0 5539.48 5840.94 119.10 o 9 1 0 1247.87 1065.45 47.56 o 10 1 0 379.27 330.86 60.28 o 11 1 0 10818.34 10608.23 201.80 o 12 1 0 9.46 -16.90 54.45 o 13 1 0 3068.61 3201.96 199.98 o 14 1 0 1479.93 1430.22 95.16 o 15 1 0 448.55 465.52 125.81 o 16 1 0 195.14 116.42 108.91 o -14 2 0 9.22 -0.60 61.79 o -13 2 0 396.87 421.74 68.34 o -12 2 0 19.82 90.71 53.86 o -11 2 0 3689.85 3675.83 149.61 o -10 2 0 3777.69 3975.07 98.80 o -9 2 0 3111.24 2940.99 86.73 o -8 2 0 13750.45 14157.14 336.35 o -7 2 0 1675.03 1697.11 51.34 o -6 2 0 9483.86 9249.47 159.50 o -5 2 0 53.06 76.69 20.73 o -4 2 0 4036.74 3563.66 134.97 o -3 2 0 35997.11 35860.54 529.23 o -2 2 0 37081.46 34671.92 1038.41 o -1 2 0 24062.17 23068.11 401.15 o 0 2 0 16425.83 18456.12 670.57 o 1 2 0 21032.58 19710.03 332.58 o 2 2 0 346.44 365.07 25.29 o 3 2 0 748.85 828.79 44.62 o 4 2 0 6355.93 6097.67 109.32 o 5 2 0 23047.19 24899.74 381.54 o 6 2 0 1366.28 1496.43 46.23 o 7 2 0 12652.35 12600.00 213.94 o 8 2 0 1436.45 1391.33 50.40 o 9 2 0 15661.12 14860.58 255.86 o 10 2 0 525.16 506.06 66.16 o 11 2 0 1041.11 1194.57 62.77 o 12 2 0 2734.48 2773.35 95.17 o 13 2 0 376.50 278.12 106.09 o 14 2 0 579.96 467.50 81.46 o 15 2 0 3032.87 2909.40 198.10 o 16 2 0 189.44 56.33 110.79 o -15 3 0 2018.03 2296.48 247.86 o -14 3 0 369.15 123.37 134.26 o -13 3 0 757.85 722.40 72.27 o -12 3 0 10.40 19.72 42.25 o -11 3 0 3406.19 3411.24 110.81 o -10 3 0 19.34 32.50 25.88 o -9 3 0 0.01 9.71 23.37 o -8 3 0 4076.91 4112.03 93.76 o -7 3 0 28741.39 27358.59 422.75 o -6 3 0 1589.33 1525.54 46.00 o -5 3 0 1690.66 1694.85 46.01 o -4 3 0 68833.93 64755.70 1248.36 o -3 3 0 988.21 959.63 59.33 o -2 3 0 14639.51 14255.08 272.90 o -1 3 0 17549.83 17976.81 321.72 o 0 3 0 137.01 178.30 27.10 o 1 3 0 6553.52 5874.04 168.31 o 2 3 0 14195.13 13208.76 236.71 o 3 3 0 5966.01 5914.75 127.06 o 4 3 0 5348.40 4969.60 160.03 o 5 3 0 442.70 460.97 27.58 o 6 3 0 571.06 561.85 31.67 o 7 3 0 4126.38 3957.80 91.61 o 8 3 0 4060.06 5108.97 109.87 o 9 3 0 4032.70 3921.40 107.62 o 10 3 0 12579.42 12958.23 264.71 o 11 3 0 6757.12 7075.99 170.38 o 12 3 0 664.54 521.58 55.54 o 13 3 0 2048.59 2053.46 108.78 o 14 3 0 561.44 417.75 82.19 o 15 3 0 2910.48 2754.94 149.28 o -16 4 0 360.46 805.55 238.47 o -15 4 0 902.58 968.92 208.43 o -14 4 0 400.64 436.33 93.47 o -13 4 0 5587.91 5573.94 234.38 o -12 4 0 1655.41 1737.00 83.94 o -11 4 0 1581.81 1554.23 85.10 o -10 4 0 100.15 246.14 57.61 o -9 4 0 1419.22 1299.20 65.14 o -8 4 0 15228.75 16342.93 272.77 o -7 4 0 27591.66 26556.22 413.15 o -6 4 0 47836.27 46655.89 695.60 o -5 4 0 6332.76 5985.81 249.89 o -4 4 0 3929.50 3503.96 90.03 o -3 4 0 45001.73 45170.12 780.73 o -2 4 0 67093.15 66287.16 1125.20 o -1 4 0 6450.45 6213.82 108.53 o 0 4 0 126588.14 130998.20 3888.18 o 1 4 0 3506.48 3269.98 67.86 o 2 4 0 155.07 173.74 29.44 o 3 4 0 4945.46 4542.31 105.72 o 4 4 0 7783.87 7722.37 160.91 o 5 4 0 18110.12 18674.05 660.97 o 6 4 0 2581.48 2775.31 93.83 o 7 4 0 603.20 584.45 54.77 o 8 4 0 47.50 75.96 40.08 o 9 4 0 64.33 148.70 76.21 o 10 4 0 1925.29 2162.68 82.16 o 11 4 0 3407.07 3491.41 127.63 o 12 4 0 1597.35 1566.66 83.06 o 13 4 0 292.60 213.33 56.14 o 14 4 0 1636.42 1774.93 163.36 o 15 4 0 410.19 179.01 69.47 o -15 5 0 1323.21 1706.87 232.84 o -14 5 0 559.05 645.94 195.29 o -13 5 0 2394.33 2568.67 105.75 o -12 5 0 6465.22 6139.48 169.75 o -11 5 0 2500.37 2854.23 174.81 o -10 5 0 295.62 389.93 91.77 o -9 5 0 1139.92 1349.83 69.03 o -8 5 0 16265.39 16510.36 428.13 o -7 5 0 20243.51 19112.63 368.79 o -6 5 0 86.71 625.71 50.69 o -5 5 0 29979.38 28591.66 517.99 o -4 5 0 67.44 72.63 39.69 o -3 5 0 75.71 270.24 51.75 o -2 5 0 267.65 193.43 33.80 o -1 5 0 4717.23 4897.44 103.80 o 0 5 0 55.62 76.23 15.51 o 1 5 0 49877.39 47634.44 706.48 o 2 5 0 20.36 12.38 14.87 o 3 5 0 18302.16 17228.84 317.18 o 4 5 0 11631.24 10854.51 249.35 o 5 5 0 4990.07 4717.77 139.21 o 6 5 0 15542.95 15375.33 298.06 o 7 5 0 454.24 445.44 45.04 o 8 5 0 200.55 164.31 31.35 o 9 5 0 4837.21 4492.28 172.00 o 10 5 0 472.93 474.33 51.75 o 11 5 0 23940.63 24278.79 462.22 o 12 5 0 2024.39 1798.96 181.20 o 13 5 0 1588.40 1699.18 107.16 o 14 5 0 166.52 220.65 64.70 o 15 5 0 389.62 162.69 72.14 o -15 6 0 740.17 630.92 221.57 o -14 6 0 1561.72 1789.49 232.84 o -13 6 0 669.41 659.21 76.26 o -12 6 0 368.62 479.66 79.91 o -11 6 0 3069.86 3046.33 110.69 o -10 6 0 3764.92 3653.52 119.32 o -9 6 0 1556.62 1701.46 80.43 o -8 6 0 12342.64 13173.85 280.76 o -7 6 0 24778.67 22497.35 430.16 o -6 6 0 3190.60 3243.71 101.85 o -5 6 0 9626.46 9424.99 239.30 o -4 6 0 4016.26 3983.55 109.25 o -3 6 0 9153.90 8669.67 187.15 o -2 6 0 35029.96 33408.02 607.65 o -1 6 0 656.59 539.19 30.98 o 0 6 0 24714.46 25725.33 398.95 o 1 6 0 487.19 384.91 32.24 o 2 6 0 1325.55 1160.63 42.79 o 3 6 0 16327.82 15693.67 338.26 o 4 6 0 1879.83 1693.68 68.26 o 5 6 0 7047.25 6876.43 173.90 o 6 6 0 5471.26 5419.48 142.15 o 7 6 0 5592.57 5268.38 139.95 o 8 6 0 1290.23 1358.03 68.89 o 9 6 0 5339.80 5146.98 182.37 o 10 6 0 584.38 498.53 56.39 o 11 6 0 214.75 217.50 41.34 o 12 6 0 5916.05 5741.92 196.98 o 13 6 0 313.53 220.90 63.90 o 14 6 0 35.87 95.76 99.52 o -15 7 0 996.19 891.93 223.45 o -14 7 0 971.85 972.67 215.94 o -13 7 0 107.89 86.05 58.94 o -12 7 0 690.06 629.29 73.38 o -11 7 0 10324.91 10254.19 246.70 o -10 7 0 3457.67 3285.22 115.27 o -9 7 0 134.38 269.30 73.06 o -8 7 0 118.35 163.62 37.03 o -7 7 0 19252.91 17719.88 357.96 o -6 7 0 906.63 976.41 100.91 o -5 7 0 140.66 222.22 68.45 o -4 7 0 10410.46 10175.62 221.81 o -3 7 0 2884.54 2884.03 95.64 o -2 7 0 166.74 143.63 76.34 o -1 7 0 3749.01 3644.39 91.01 o 0 7 0 1.01 9.17 22.43 o 1 7 0 2974.97 3048.78 76.24 o 2 7 0 937.77 947.69 42.84 o 3 7 0 2833.89 2871.38 90.91 o 4 7 0 3445.18 3263.27 100.72 o 5 7 0 2413.53 2698.80 150.81 o 6 7 0 2473.80 2461.61 104.48 o 7 7 0 9016.50 8737.32 204.70 o 8 7 0 10894.25 11491.26 329.85 o 9 7 0 525.74 514.21 56.25 o 10 7 0 10722.22 10592.45 242.92 o 11 7 0 18.70 23.95 45.48 o 12 7 0 51.90 130.46 61.03 o 13 7 0 0.07 -1.88 95.76 o 14 7 0 184.38 89.40 71.37 o -14 8 0 1481.61 1999.80 247.86 o -13 8 0 2210.42 2078.54 340.81 o -12 8 0 1892.28 2081.86 100.55 o -11 8 0 303.48 298.85 75.62 o -10 8 0 2002.80 1739.45 88.75 o -9 8 0 2605.61 2443.14 99.17 o -8 8 0 2298.67 2344.60 95.57 o -7 8 0 2.48 16.00 43.83 o -6 8 0 17974.76 17579.33 358.27 o -5 8 0 3078.71 3221.45 107.62 o -4 8 0 7549.89 7420.86 240.77 o -3 8 0 16928.03 18089.36 626.90 o -2 8 0 2941.03 2532.79 74.26 o -1 8 0 1660.95 1577.54 53.55 o 0 8 0 1167.31 1168.00 48.52 o 1 8 0 110.69 78.05 39.03 o 2 8 0 5910.39 5953.92 146.70 o 3 8 0 10950.90 10371.64 258.68 o 4 8 0 442.61 362.56 67.75 o 5 8 0 2992.15 3048.70 123.66 o 6 8 0 2376.10 2552.12 121.21 o 7 8 0 3867.71 3659.25 119.79 o 8 8 0 946.27 980.49 65.88 o 9 8 0 83.77 70.93 75.58 o 10 8 0 1592.19 1639.64 87.28 o 11 8 0 1798.00 1599.92 124.83 o 12 8 0 593.35 610.71 88.22 o 13 8 0 210.11 154.45 73.25 o -14 9 0 378.06 424.37 180.26 o -13 9 0 246.77 446.96 183.08 o -12 9 0 1542.91 1489.66 95.57 o -11 9 0 3021.10 3077.41 122.86 o -10 9 0 1469.75 1177.40 127.69 o -9 9 0 1383.64 1509.19 106.34 o -8 9 0 5013.41 5541.70 162.79 o -7 9 0 8353.46 7873.52 201.54 o -6 9 0 1062.83 1072.85 70.26 o -5 9 0 8033.30 8066.81 199.41 o -4 9 0 3768.23 3564.13 117.86 o -3 9 0 1095.98 1124.29 67.85 o -2 9 0 988.20 906.27 84.02 o -1 9 0 8044.44 7757.42 187.08 o 0 9 0 12.30 20.93 28.61 o 1 9 0 3861.55 3477.70 158.48 o 2 9 0 30.12 16.49 51.64 o 3 9 0 5618.77 5340.06 146.28 o 4 9 0 20636.28 19983.31 458.61 o 5 9 0 6332.07 6306.37 209.13 o 6 9 0 5866.23 5838.57 162.36 o 7 9 0 2.86 -18.13 43.29 o 8 9 0 5090.04 5145.35 372.74 o 9 9 0 1953.89 1984.49 94.61 o 10 9 0 150.72 105.81 61.23 o 11 9 0 4284.41 4129.68 244.87 o 12 9 0 1099.31 991.00 99.34 o -13 10 0 926.87 1103.92 136.15 o -12 10 0 9.28 20.84 61.06 o -11 10 0 248.37 255.90 57.37 o -10 10 0 54.96 69.48 64.74 o -9 10 0 2855.31 3193.51 122.28 o -8 10 0 1930.25 2335.61 103.84 o -7 10 0 9404.36 9072.60 229.22 o -6 10 0 156.18 518.53 75.75 o -5 10 0 2131.46 2182.93 95.42 o -4 10 0 1022.69 1025.96 69.05 o -3 10 0 702.63 767.27 65.50 o -2 10 0 4700.40 4218.19 137.83 o -1 10 0 1503.49 1477.23 78.43 o 0 10 0 1.85 35.41 36.05 o 1 10 0 2034.72 1820.92 76.91 o 2 10 0 926.26 1011.65 65.46 o 3 10 0 12852.87 12347.56 437.83 o 4 10 0 10622.97 10754.26 246.97 o 5 10 0 0.08 37.81 47.30 o 6 10 0 5849.45 6130.14 213.93 o 7 10 0 136.22 94.71 43.44 o 8 10 0 501.66 478.76 68.96 o 9 10 0 722.16 728.44 75.91 o 10 10 0 155.28 96.55 54.34 o 11 10 0 388.04 424.08 125.81 o 12 10 0 1476.32 1470.12 117.23 o -12 11 0 841.38 532.43 160.55 o -11 11 0 697.38 624.59 114.35 o -10 11 0 1668.83 1545.31 96.01 o -9 11 0 1761.21 1705.21 96.22 o -8 11 0 862.55 1279.27 85.97 o -7 11 0 8415.49 7903.57 214.99 o -6 11 0 13.12 75.78 43.44 o -5 11 0 798.41 863.54 89.35 o -4 11 0 2290.03 2356.99 102.88 o -3 11 0 726.20 757.51 68.34 o -2 11 0 4611.83 4363.81 210.69 o -1 11 0 36.67 105.89 42.33 o 0 11 0 140.59 112.13 45.57 o 1 11 0 3600.30 3616.44 148.78 o 2 11 0 5114.14 5201.96 187.63 o 3 11 0 2248.11 2239.91 156.73 o 4 11 0 20288.50 19991.69 404.89 o 5 11 0 2390.91 2394.92 189.68 o 6 11 0 2581.93 2462.07 147.91 o 7 11 0 1279.92 1321.45 140.86 o 8 11 0 1775.11 1938.91 101.01 o 9 11 0 2638.73 2682.46 162.63 o 10 11 0 1272.17 1221.96 157.90 o 11 11 0 1669.43 1369.74 181.20 o -11 12 0 0.63 13.91 67.50 o -10 12 0 541.58 819.92 108.59 o -9 12 0 1697.68 1724.07 101.57 o -8 12 0 345.18 430.04 68.62 o -7 12 0 3920.88 3706.40 137.48 o -6 12 0 2633.81 2657.24 113.89 o -5 12 0 4198.58 4021.68 225.83 o -4 12 0 1074.09 745.12 72.72 o -3 12 0 1029.24 1157.23 77.99 o -2 12 0 4.12 -39.43 56.33 o -1 12 0 1366.10 1280.24 111.73 o 0 12 0 5835.94 5724.76 200.71 o 1 12 0 1177.05 1270.42 93.38 o 2 12 0 2282.69 2141.60 118.64 o 3 12 0 1967.99 2016.77 119.49 o 4 12 0 543.12 585.22 69.48 o 5 12 0 760.04 804.95 76.02 o 6 12 0 307.64 197.94 52.57 o 7 12 0 854.48 1035.74 84.86 o 8 12 0 301.40 193.75 57.83 o 9 12 0 0.89 18.76 60.75 o 10 12 0 428.97 200.59 66.10 o -10 13 0 162.85 138.30 74.07 o -9 13 0 797.27 940.35 96.12 o -8 13 0 0.87 72.59 65.79 o -7 13 0 784.34 857.90 113.69 o -6 13 0 39.13 108.91 76.99 o -5 13 0 525.31 659.14 75.06 o -4 13 0 17.29 33.25 48.56 o -3 13 0 1880.41 2060.42 116.40 o -2 13 0 1228.67 1373.87 97.45 o -1 13 0 1739.99 1689.68 160.55 o 0 13 0 85.60 41.14 51.43 o 1 13 0 815.50 797.45 85.21 o 2 13 0 928.97 908.20 91.68 o 3 13 0 391.22 408.04 74.59 o 4 13 0 1599.45 1588.09 113.20 o 5 13 0 1111.25 1125.84 103.17 o 6 13 0 40.61 47.02 64.96 o 7 13 0 30.53 -12.51 65.94 o 8 13 0 1789.17 1699.66 108.18 o -9 14 0 441.47 665.66 103.79 o -8 14 0 180.76 349.03 84.48 o -7 14 0 113.30 164.32 80.68 o -6 14 0 7.96 -4.72 58.11 o -5 14 0 19.84 -3.51 60.00 o -4 14 0 730.58 667.74 92.03 o -3 14 0 340.21 363.00 123.93 o -2 14 0 235.66 163.34 59.04 o -1 14 0 1715.15 1766.91 116.40 o 0 14 0 2333.90 2590.08 138.38 o 1 14 0 1455.32 1444.49 108.16 o 2 14 0 1457.65 1643.58 114.44 o 3 14 0 3519.62 3717.06 170.99 o 4 14 0 2231.28 2244.18 138.52 o 5 14 0 574.27 704.54 102.46 o 6 14 0 829.87 807.70 110.44 o 7 14 0 949.24 1016.52 171.81 o -7 15 0 708.61 689.12 100.02 o -6 15 0 213.93 163.66 70.78 o -5 15 0 81.31 143.24 69.44 o -4 15 0 4523.52 4703.23 194.58 o -3 15 0 988.78 1005.48 106.35 o -2 15 0 1965.10 2031.85 129.33 o -1 15 0 1.70 88.69 131.44 o 0 15 0 2.81 15.56 63.09 o 1 15 0 0.30 30.14 64.86 o 2 15 0 3294.74 3672.29 174.15 o 3 15 0 38.37 117.06 73.47 o 4 15 0 5521.15 5987.61 391.51 o 5 15 0 308.33 369.92 140.83 o -3 16 0 2691.12 2668.27 195.29 o -2 16 0 28.54 151.68 112.66 o -1 16 0 1353.37 1469.13 199.04 o 0 16 0 1074.44 1115.93 120.18 o -4 -15 1 3.92 -9.39 138.95 o -3 -15 1 1262.11 1242.15 174.63 o -2 -15 1 1078.20 1237.55 115.80 o -1 -15 1 12.66 7.22 67.60 o 0 -15 1 84.04 49.38 68.12 o 1 -15 1 3.77 30.70 91.07 o 2 -15 1 2886.47 3005.71 156.10 o 3 -15 1 420.78 466.76 132.38 o 4 -15 1 42.36 107.29 67.60 o 5 -15 1 731.49 1080.67 151.16 o 6 -15 1 1556.46 1662.27 122.27 o -6 -14 1 2.52 -7.12 72.25 o -5 -14 1 1885.94 1877.61 142.71 o -4 -14 1 18.28 23.37 77.93 o -3 -14 1 1714.34 1799.85 232.84 o -2 -14 1 0.35 -9.39 101.40 o -1 -14 1 169.90 180.06 60.89 o 0 -14 1 1.30 -54.45 93.89 o 1 -14 1 1475.14 1467.27 109.62 o 2 -14 1 1498.76 1452.46 111.41 o 3 -14 1 7683.22 7992.91 525.77 o 4 -14 1 9.25 -6.03 59.53 o 5 -14 1 435.97 414.10 125.81 o 6 -14 1 531.02 468.74 76.57 o 7 -14 1 3.83 26.47 67.60 o 8 -14 1 962.10 929.31 99.67 o 9 -14 1 3.03 52.58 144.59 o -8 -13 1 924.97 824.55 104.06 o -7 -13 1 20.16 34.79 61.42 o -6 -13 1 969.72 1154.20 114.60 o -5 -13 1 46.65 79.32 62.87 o -4 -13 1 436.27 499.83 150.22 o -3 -13 1 318.51 383.46 74.81 o -2 -13 1 2074.28 1854.29 257.25 o -1 -13 1 6453.19 6578.44 298.56 o 0 -13 1 1.14 -31.67 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