#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:01:17 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181901 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/01/2240142.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240142 _cell_angle_alpha 90.000 _cell_angle_beta 96.334 _cell_angle_gamma 90.000 _cell_length_a 9.4578 _cell_length_b 12.6902 _cell_length_c 30.5130 _exptl_crystal_F_000 1776.00 _reflns_d_resolution_high 0.7399 _cod_data_source_file wm5073Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' test in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 484.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 206946.31 209076.14 4242.82 o 2 0 0 14679.21 14694.56 350.62 o 3 0 0 2449.82 2446.64 140.25 o 4 0 0 8879.52 8409.17 295.82 o 5 0 0 57956.31 60297.54 1912.69 o 6 0 0 79066.52 78041.22 1856.18 o 7 0 0 22625.08 22217.92 644.90 o 8 0 0 110.73 44.14 124.66 o 9 0 0 123.26 224.48 303.27 o 10 0 0 4620.78 3837.46 545.13 o 11 0 0 3585.85 3416.18 570.85 o 12 0 0 120.19 -54.90 648.84 o 1 1 0 16.25 29.03 19.83 o 2 1 0 4554.82 4413.50 127.84 o 3 1 0 7099.10 6829.63 159.31 o 4 1 0 53823.83 54735.53 933.18 o 5 1 0 37098.24 36816.47 742.09 o 6 1 0 21809.72 20931.29 500.21 o 7 1 0 14769.03 14102.54 393.27 o 8 1 0 10990.88 11444.77 388.15 o 9 1 0 16583.11 16082.69 723.50 o 10 1 0 16123.94 17186.35 785.48 o 11 1 0 16195.37 16784.90 803.89 o 12 1 0 8635.13 8533.11 720.64 o 0 2 0 13655.08 14390.30 345.14 o 1 2 0 4344.37 4663.04 116.59 o 2 2 0 418.83 427.63 38.71 o 3 2 0 6241.56 6714.33 172.13 o 4 2 0 12391.55 12329.68 303.87 o 5 2 0 9313.05 9121.03 247.93 o 6 2 0 2184.91 2322.40 168.21 o 7 2 0 7.75 41.34 109.11 o 8 2 0 6.64 -50.73 139.28 o 9 2 0 2684.05 2518.39 295.91 o 10 2 0 442.20 668.97 261.29 o 11 2 0 1809.80 1415.22 404.27 o 12 2 0 196.44 990.73 796.08 o 1 3 0 5929.39 6102.43 142.89 o 2 3 0 1091.75 1174.03 59.89 o 3 3 0 3285.45 3393.51 98.61 o 4 3 0 561.19 466.32 64.94 o 5 3 0 4601.62 4505.38 156.92 o 6 3 0 10751.13 10769.96 360.75 o 7 3 0 9665.42 10218.61 336.26 o 8 3 0 6126.49 5669.46 298.38 o 9 3 0 1002.21 931.02 189.21 o 10 3 0 1751.45 2563.62 405.34 o 11 3 0 2692.05 2371.11 872.19 o 12 3 0 3922.13 5736.73 1230.30 o 0 4 0 5751.30 6071.25 221.49 o 1 4 0 12450.67 12824.99 305.19 o 2 4 0 85584.08 87991.60 1377.01 o 3 4 0 30164.56 29452.68 536.99 o 4 4 0 63475.89 64109.85 1057.64 o 5 4 0 9444.14 9385.18 247.05 o 6 4 0 196.66 191.22 95.41 o 7 4 0 121.03 26.10 129.31 o 8 4 0 1497.33 1467.79 202.58 o 9 4 0 1751.35 1989.00 262.80 o 10 4 0 432.56 282.02 309.74 o 11 4 0 541.43 607.23 627.50 o 12 4 0 2469.12 578.96 900.89 o 1 5 0 4818.23 4994.64 162.07 o 2 5 0 15640.92 15789.59 312.69 o 3 5 0 11798.24 12205.98 279.71 o 4 5 0 4547.52 4462.76 192.35 o 5 5 0 8592.25 8634.70 284.14 o 6 5 0 10870.14 10874.51 389.57 o 7 5 0 6472.14 5457.63 271.28 o 8 5 0 15059.32 14885.47 558.05 o 9 5 0 12931.09 12055.61 651.94 o 10 5 0 4600.90 4742.28 752.84 o 11 5 0 4056.13 3570.86 1103.03 o 12 5 0 3391.04 5519.62 1359.82 o 0 6 0 5846.93 4944.66 269.67 o 1 6 0 8435.96 8966.93 246.34 o 2 6 0 75.80 -2.96 65.93 o 3 6 0 162.53 228.85 79.87 o 4 6 0 39.26 -11.07 90.89 o 5 6 0 24.47 150.73 100.45 o 6 6 0 2565.63 2602.65 158.20 o 7 6 0 2579.10 2708.98 510.21 o 8 6 0 25.97 -169.37 169.37 o 9 6 0 95.89 78.53 327.78 o 10 6 0 713.47 1263.38 931.96 o 11 6 0 820.68 177.18 870.94 o 1 7 0 698.52 689.26 102.93 o 2 7 0 11428.97 11412.33 237.86 o 3 7 0 10801.79 10766.10 412.15 o 4 7 0 1013.34 1037.74 129.75 o 5 7 0 5165.91 4929.78 265.72 o 6 7 0 3034.03 2620.83 355.04 o 7 7 0 513.62 752.73 215.00 o 8 7 0 10166.77 10183.28 541.96 o 9 7 0 12679.22 10497.28 1104.58 o 10 7 0 3659.54 3788.33 825.90 o 11 7 0 2268.08 1274.97 1065.59 o 0 8 0 54281.40 53108.63 1584.10 o 1 8 0 54419.67 54241.52 1076.99 o 2 8 0 49421.05 48880.10 813.09 o 3 8 0 24277.10 24075.33 487.36 o 4 8 0 20120.57 20546.34 551.01 o 5 8 0 5095.17 5219.67 331.44 o 6 8 0 10869.80 10851.41 429.88 o 7 8 0 7339.11 6482.31 442.13 o 8 8 0 2309.57 2271.31 342.37 o 9 8 0 22.22 -407.29 407.29 o 10 8 0 1236.42 184.67 898.39 o 11 8 0 2402.52 3862.59 1299.92 o 1 9 0 1442.95 1531.21 162.00 o 2 9 0 70.92 114.86 76.59 o 3 9 0 5009.61 4702.89 187.51 o 4 9 0 30764.89 30184.25 753.66 o 5 9 0 23367.27 22494.21 659.58 o 6 9 0 19903.57 19186.82 756.60 o 7 9 0 27930.42 28983.25 1289.41 o 8 9 0 9467.27 9717.47 806.53 o 9 9 0 8236.32 9713.35 1176.52 o 10 9 0 15588.21 16249.17 2250.72 o 0 10 0 2229.53 2075.14 274.71 o 1 10 0 6698.73 7367.49 348.26 o 2 10 0 19254.39 19665.67 428.54 o 3 10 0 19632.85 20240.23 530.94 o 4 10 0 3892.13 4116.96 278.51 o 5 10 0 2048.99 2286.19 229.34 o 6 10 0 78.36 -104.76 253.58 o 7 10 0 460.80 636.48 301.03 o 8 10 0 534.19 227.38 443.57 o 9 10 0 299.94 257.04 841.00 o 10 10 0 10.92 294.47 910.87 o 1 11 0 1572.45 1644.68 181.44 o 2 11 0 6345.59 6131.99 286.60 o 3 11 0 5.41 80.60 152.87 o 4 11 0 7986.14 8094.35 516.56 o 5 11 0 3085.57 3044.24 518.65 o 6 11 0 145.37 173.24 283.89 o 7 11 0 312.59 146.74 321.67 o 8 11 0 1245.46 -426.74 728.70 o 9 11 0 667.56 826.02 985.74 o 0 12 0 38562.66 36704.50 1380.42 o 1 12 0 17480.79 16949.99 569.27 o 2 12 0 6031.08 6296.90 368.65 o 3 12 0 1589.69 1999.43 250.01 o 4 12 0 4025.83 4365.65 417.33 o 5 12 0 6499.92 7689.43 810.05 o 6 12 0 5813.14 4875.58 537.38 o 7 12 0 2568.90 2856.87 475.86 o 8 12 0 100.34 -114.79 948.30 o 9 12 0 179.17 142.25 958.29 o 1 13 0 96.60 -200.94 216.27 o 2 13 0 2198.14 2771.08 360.63 o 3 13 0 4689.61 3885.31 418.62 o 4 13 0 4747.12 4471.89 588.82 o 5 13 0 9870.05 10289.79 758.28 o 6 13 0 5218.76 5012.47 567.72 o 7 13 0 2547.85 2415.22 808.56 o 8 13 0 8500.80 10450.30 2048.58 o 0 14 0 5025.13 5502.58 641.79 o 1 14 0 7048.30 6837.74 531.02 o 2 14 0 3458.92 4488.93 612.40 o 3 14 0 3919.81 3583.65 692.33 o 4 14 0 3280.83 3650.47 613.44 o 5 14 0 2553.15 2228.66 548.52 o 6 14 0 1117.52 1443.26 526.32 o 7 14 0 666.85 -184.67 1018.18 o 1 15 0 1418.73 1718.59 525.93 o 2 15 0 3510.33 5159.76 878.03 o 3 15 0 304.27 497.22 597.79 o 4 15 0 1957.26 3231.47 1212.83 o 5 15 0 1122.63 1354.83 1220.32 o 6 15 0 1.89 -187.17 1038.14 o 2 16 0 12756.15 11640.42 2006.16 o 3 16 0 8960.85 6352.88 1584.41 o 4 16 0 6809.14 7925.07 1838.96 o -12 1 1 1144.97 1935.57 566.36 o -11 1 1 7267.83 7290.28 977.10 o -10 1 1 9623.20 10246.31 577.16 o -9 1 1 12493.26 11764.66 640.36 o -8 1 1 6155.37 6295.03 262.05 o -7 1 1 2074.80 2173.71 153.65 o -6 1 1 6694.61 6141.00 263.23 o -5 1 1 7046.97 7400.63 255.33 o -4 1 1 593.99 613.55 87.04 o -3 1 1 679.12 998.01 63.30 o -2 1 1 991.39 974.64 48.91 o -1 1 1 826.29 866.60 36.99 o 0 1 1 56961.97 59421.19 821.54 o 1 1 1 98266.29 100344.23 1206.78 o 2 1 1 18218.77 18135.21 309.35 o 3 1 1 14254.57 14037.10 260.87 o 4 1 1 7605.59 7669.31 183.18 o 5 1 1 2694.58 2731.95 118.10 o 6 1 1 25472.53 26673.86 479.41 o 7 1 1 29258.43 29280.95 671.42 o 8 1 1 3916.03 3892.86 197.07 o 9 1 1 12221.95 12664.04 638.00 o 10 1 1 1022.24 716.82 273.16 o 11 1 1 24.77 9.15 283.61 o 12 1 1 8.28 -51.42 382.29 o -12 2 1 1694.47 633.87 761.14 o -11 2 1 4801.68 5971.79 584.63 o -10 2 1 12816.51 13751.75 1068.24 o -9 2 1 5843.22 6525.69 423.21 o -8 2 1 14010.62 13763.26 483.79 o -7 2 1 28373.99 28140.39 728.16 o -6 2 1 38458.43 39250.80 964.26 o -5 2 1 43901.30 43138.43 892.86 o -4 2 1 66471.71 66281.52 1190.35 o -3 2 1 86443.54 87611.06 1362.11 o -2 2 1 52402.14 52232.85 819.35 o -1 2 1 33382.32 33142.37 554.50 o 0 2 1 16088.11 16592.32 287.52 o 1 2 1 10042.42 10266.26 168.35 o 2 2 1 13530.46 13977.68 230.66 o 3 2 1 2041.58 1921.36 77.38 o 4 2 1 95.41 114.78 63.58 o 5 2 1 463.88 357.20 91.92 o 6 2 1 6196.48 5996.23 241.53 o 7 2 1 14325.64 14118.09 442.64 o 8 2 1 8075.33 7898.22 499.72 o 9 2 1 6753.57 7106.53 418.00 o 10 2 1 8432.71 8272.16 527.65 o 11 2 1 8681.12 9355.96 719.84 o 12 2 1 8677.09 6719.72 1237.78 o -12 3 1 9365.47 7984.96 1367.30 o -11 3 1 3261.51 2866.79 620.22 o -10 3 1 2566.13 2148.01 416.48 o -9 3 1 1281.85 1134.77 184.95 o -8 3 1 857.78 670.83 151.53 o -7 3 1 6839.35 6656.14 260.68 o -6 3 1 7547.45 8220.44 259.11 o -5 3 1 1462.04 1678.67 99.95 o -4 3 1 11154.24 11599.48 330.28 o -3 3 1 2714.46 2540.34 87.97 o -2 3 1 32906.15 33394.44 625.45 o -1 3 1 31991.53 33124.08 482.10 o 0 3 1 13055.32 13499.22 261.33 o 1 3 1 22177.37 22533.19 391.11 o 2 3 1 37416.11 38134.90 582.58 o 3 3 1 35907.33 37004.07 596.90 o 4 3 1 40725.89 40406.90 666.94 o 5 3 1 81276.42 81229.51 1450.72 o 6 3 1 13545.72 12864.50 420.68 o 7 3 1 7298.65 7327.22 288.94 o 8 3 1 7816.82 8110.33 389.68 o 9 3 1 2788.23 2963.66 291.89 o 10 3 1 3949.92 3446.35 459.34 o 11 3 1 6390.95 7676.83 666.09 o 12 3 1 675.91 549.02 860.96 o -12 4 1 51.14 1023.17 875.93 o -11 4 1 305.26 -75.10 479.82 o -10 4 1 58.12 -58.73 282.10 o -9 4 1 193.76 191.83 203.51 o -8 4 1 1512.34 1616.23 221.85 o -7 4 1 1380.25 1202.21 139.51 o -6 4 1 3941.48 3906.96 178.55 o -5 4 1 1189.63 1084.04 80.26 o -4 4 1 46.46 156.72 59.64 o -3 4 1 1943.26 2013.43 128.41 o -2 4 1 1471.01 1594.46 103.45 o -1 4 1 260.41 357.56 54.11 o 0 4 1 10595.68 11083.52 243.72 o 1 4 1 24671.66 25557.07 455.72 o 2 4 1 267.45 375.29 51.30 o 3 4 1 5861.03 5968.14 149.28 o 4 4 1 409.63 420.12 75.83 o 5 4 1 20.37 -22.69 72.74 o 6 4 1 3031.48 2998.02 167.44 o 7 4 1 4502.57 4365.97 226.23 o 8 4 1 136.02 113.41 152.36 o 9 4 1 3347.24 3078.12 299.39 o 10 4 1 4308.27 3286.67 646.22 o 11 4 1 446.78 -71.63 501.85 o 12 4 1 136.50 -254.54 836.00 o -12 5 1 4779.91 2829.69 1155.43 o -11 5 1 1730.27 1928.80 933.33 o -10 5 1 788.85 102.30 483.98 o -9 5 1 759.07 614.12 260.35 o -8 5 1 77.34 20.42 165.08 o -7 5 1 2220.65 1961.85 214.78 o -6 5 1 9338.11 9350.71 354.26 o -5 5 1 1746.34 1799.09 110.48 o -4 5 1 7938.22 7909.22 245.12 o -3 5 1 10008.35 9719.41 310.42 o -2 5 1 34008.50 34370.46 585.24 o -1 5 1 4084.08 3773.87 133.41 o 0 5 1 168.16 212.18 60.93 o 1 5 1 2917.96 3184.19 119.42 o 2 5 1 14978.92 14784.95 307.09 o 3 5 1 14794.52 14457.91 311.03 o 4 5 1 20502.36 19622.72 453.84 o 5 5 1 32235.67 31473.43 760.58 o 6 5 1 5909.95 6291.18 324.90 o 7 5 1 5490.38 5682.33 267.23 o 8 5 1 1107.97 1076.79 202.46 o 9 5 1 1351.88 1427.00 482.60 o 10 5 1 1297.64 1319.14 568.92 o 11 5 1 3315.08 3820.16 1103.03 o 12 5 1 43.82 -87.34 855.97 o -11 6 1 992.82 566.49 823.53 o -10 6 1 1587.36 1821.80 595.75 o -9 6 1 13924.06 14371.85 727.29 o -8 6 1 39743.64 39045.74 1187.64 o -7 6 1 39069.38 37452.07 982.65 o -6 6 1 40886.98 39246.44 885.37 o -5 6 1 28974.53 28565.23 725.29 o -4 6 1 18916.11 18710.60 484.20 o -3 6 1 36012.32 35566.86 730.65 o -2 6 1 67367.56 67748.24 1075.26 o -1 6 1 42065.87 41395.09 706.01 o 0 6 1 28708.94 29217.42 557.47 o 1 6 1 17670.93 17805.51 362.65 o 2 6 1 5200.66 5844.44 181.26 o 3 6 1 640.13 800.64 87.59 o 4 6 1 276.92 295.65 100.99 o 5 6 1 176.63 224.37 99.83 o 6 6 1 620.57 475.42 106.38 o 7 6 1 2967.87 2864.67 243.29 o 8 6 1 10978.25 11744.62 635.89 o 9 6 1 11840.23 12041.88 674.03 o 10 6 1 7986.28 9197.82 2234.63 o 11 6 1 10810.20 10999.32 1776.57 o -11 7 1 6576.20 5938.87 1449.66 o -10 7 1 8061.81 9072.74 1081.50 o -9 7 1 4915.31 6488.83 881.60 o -8 7 1 10719.31 11547.38 574.88 o -7 7 1 1990.54 2072.34 264.87 o -6 7 1 579.27 310.85 163.88 o -5 7 1 74.00 91.41 119.14 o -4 7 1 3177.67 3518.12 194.90 o -3 7 1 6485.16 6392.35 238.55 o -2 7 1 11426.94 11842.98 253.94 o -1 7 1 14051.80 14733.90 355.67 o 0 7 1 32476.96 33006.04 664.98 o 1 7 1 39127.85 39360.69 719.81 o 2 7 1 71675.74 73105.09 1116.56 o 3 7 1 79234.35 79937.92 1400.91 o 4 7 1 19591.41 19564.71 582.34 o 5 7 1 10489.04 10476.44 398.10 o 6 7 1 16464.50 17175.54 665.91 o 7 7 1 28606.19 29527.98 898.30 o 8 7 1 19465.81 19448.07 800.02 o 9 7 1 11169.93 10280.24 2036.11 o 10 7 1 2945.20 1826.48 990.73 o 11 7 1 111.59 -668.80 823.53 o -11 8 1 941.49 -267.02 935.83 o -10 8 1 3348.41 3473.53 1175.40 o -9 8 1 2700.43 2828.14 1613.24 o -8 8 1 562.44 128.49 251.58 o -7 8 1 334.11 572.46 214.17 o -6 8 1 2888.28 2804.10 252.11 o -5 8 1 6547.59 6830.76 342.16 o -4 8 1 23948.45 24139.35 620.31 o -3 8 1 15629.44 15325.25 343.30 o -2 8 1 2484.62 2396.02 115.43 o -1 8 1 1657.21 1864.16 149.34 o 0 8 1 417.97 485.58 113.77 o 1 8 1 262.45 172.90 97.79 o 2 8 1 5191.07 5019.56 247.24 o 3 8 1 5229.02 5363.86 176.94 o 4 8 1 185.53 216.98 118.72 o 5 8 1 2117.02 1778.52 196.07 o 6 8 1 8569.73 8272.85 510.19 o 7 8 1 7154.14 7202.54 622.93 o 8 8 1 1572.63 1679.66 426.16 o 9 8 1 782.56 1380.79 602.18 o 10 8 1 33.15 -494.12 768.62 o 11 8 1 2146.83 1003.20 1045.63 o -10 9 1 1593.08 2250.72 1152.94 o -9 9 1 1394.44 1519.94 878.30 o -8 9 1 1094.10 733.08 426.64 o -7 9 1 69.96 242.66 259.60 o -6 9 1 1629.69 1635.65 267.34 o -5 9 1 22.11 22.32 143.02 o -4 9 1 7.12 72.94 131.13 o -3 9 1 724.69 800.33 111.73 o -2 9 1 259.05 264.75 82.58 o -1 9 1 897.65 899.21 136.59 o 0 9 1 9363.01 9971.16 347.19 o 1 9 1 3920.65 3783.92 197.73 o 2 9 1 1948.88 1876.85 146.53 o 3 9 1 2061.57 2107.72 137.28 o 4 9 1 147.84 155.81 125.88 o 5 9 1 7371.13 6441.74 327.46 o 6 9 1 1440.20 1412.45 308.33 o 7 9 1 2746.28 2490.74 364.34 o 8 9 1 496.94 247.93 314.09 o 9 9 1 835.45 1399.75 948.30 o 10 9 1 1154.23 786.09 958.29 o -10 10 1 7214.84 5699.30 1497.07 o -9 10 1 5164.02 5991.28 1449.66 o -8 10 1 1567.84 1247.50 489.98 o -7 10 1 9130.92 9853.03 655.80 o -6 10 1 12763.75 13230.91 746.34 o -5 10 1 14861.41 15225.18 540.82 o -4 10 1 39125.74 38977.29 1124.70 o -3 10 1 23782.15 23310.78 560.33 o -2 10 1 10268.48 10419.90 306.40 o -1 10 1 3362.27 3441.40 241.44 o 0 10 1 2695.26 2723.82 213.16 o 1 10 1 1913.01 2034.24 161.80 o 2 10 1 8106.92 8197.05 230.50 o 3 10 1 6850.34 7279.75 282.91 o 4 10 1 232.73 204.98 146.84 o 5 10 1 368.23 275.64 164.67 o 6 10 1 3505.62 3104.56 419.24 o 7 10 1 7413.69 6532.54 562.93 o 8 10 1 2322.65 3557.01 603.70 o 9 10 1 1222.94 656.33 1030.66 o 10 10 1 2349.71 2218.28 1197.86 o -9 11 1 5274.03 5272.56 1462.13 o -8 11 1 2591.28 2757.32 1155.43 o -7 11 1 496.69 281.32 304.96 o -6 11 1 13.30 511.42 301.70 o -5 11 1 89.32 -147.61 252.89 o -4 11 1 1121.63 956.61 205.74 o -3 11 1 687.79 777.87 181.81 o -2 11 1 8382.97 7581.69 305.85 o -1 11 1 13048.96 13022.03 487.19 o 0 11 1 15849.55 16169.53 652.77 o 1 11 1 8312.04 8649.17 346.93 o 2 11 1 14051.36 13914.11 378.99 o 3 11 1 10823.51 11837.70 454.56 o 4 11 1 15559.61 15204.78 561.89 o 5 11 1 18236.95 20187.21 996.29 o 6 11 1 15297.27 16705.71 907.10 o 7 11 1 11539.51 12562.99 789.31 o 8 11 1 3639.06 3555.89 1210.33 o 9 11 1 3584.49 4399.13 1427.20 o -9 12 1 973.57 -84.85 1048.12 o -8 12 1 2998.65 1245.27 1118.00 o -7 12 1 2239.06 1758.12 631.75 o -6 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