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Information card for entry 2240143
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| Coordinates | 2240143.cif |
|---|---|
| Structure factors | 2240143.hkl |
| Original IUCr paper | HTML |
| Chemical name | Decacarbonyltetra-μ~4~-oxido-hexa-μ~3~-oxido-tetrakis[μ-2,2'-(pyridine-2,6-diyl)bis(1,1-diphenylethanolato)] decatin(II)ditin(IV)dimolybdenum(O)(2 <i>Mo</i>—<i>Sn</i>) toluene heptasolvate |
|---|---|
| Formula | C191 H164 Mo2 N4 O28 Sn12 |
| Calculated formula | C191 H164 Mo2 N4 O28 Sn12 |
| Title of publication | Crystal structure of a mixed-valence μ-oxide Sn~12~ cluster |
| Authors of publication | Kireenko, Marina M.; Zaitsev, Kirill V.; Karlov, Sergey S.; Egorov, Mikhail P.; Churakov, Andrei V. |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2014 |
| Journal volume | 70 |
| Journal issue | 11 |
| Pages of publication | m378 - m379 |
| a | 15.8218 ± 0.0017 Å |
| b | 15.9933 ± 0.0017 Å |
| c | 18.806 ± 0.002 Å |
| α | 94.833 ± 0.002° |
| β | 95.014 ± 0.002° |
| γ | 110.605 ± 0.002° |
| Cell volume | 4403.4 ± 0.8 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0428 |
| Residual factor for significantly intense reflections | 0.0325 |
| Weighted residual factors for significantly intense reflections | 0.0757 |
| Weighted residual factors for all reflections included in the refinement | 0.0813 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181901 (current) | 2016-04-06 | hkl/2/24/ (antanas@echidna) Adding IUCr specific svn headers to multiple entries in subrange 2/24/01 |
2240143.cif 2240143.hkl |
| 181321 | 2016-04-03 | hkl/2/24/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/24/01. |
2240143.cif 2240143.hkl |
| 176809 | 2016-02-21 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 2. |
2240143.cif 2240143.hkl |
| 125977 | 2014-10-30 | cif/ hkl/ Adding structures of 2240143 via cif-deposit CGI script. |
2240143.cif 2240143.hkl |
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Users of the data should acknowledge the original authors of the
structural data.