#------------------------------------------------------------------------------
#$Date: 2016-04-06 17:01:17 +0300 (Wed, 06 Apr 2016) $
#$Revision: 181901 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/01/2240185.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2240185
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   7.0701
_cell_length_b                   7.0701
_cell_length_c                   9.7631
_exptl_crystal_F_000             356.00
_reflns_d_resolution_high        0.7253
_cod_data_source_file            hb7297Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' '
_shelx_refln_list_code           4
_shelx_f_calc_maximum            151.78
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z+1/2'
'-y, x-y, z'
'y, -x+y, z+1/2'
'-x+y, -x, z'
'x-y, x, z+1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 1 -13 8.25 6.84 2.84 o
-1 2 -13 0.36 3.67 2.91 o
0 2 -13 10.66 12.95 2.54 o
0 0 -12 504.48 514.71 5.87 o
0 1 -12 1176.64 1310.43 9.43 o
-1 2 -12 66.30 65.85 3.54 o
0 2 -12 910.35 936.99 8.62 o
-2 3 -12 1364.46 1370.35 10.39 o
-1 3 -12 847.93 838.42 8.27 o
0 3 -12 13.19 9.05 3.09 o
-3 4 -12 650.27 615.55 6.89 o
-2 4 -12 23.70 22.56 2.85 o
-1 4 -12 687.95 659.19 7.31 o
0 1 -11 9.18 10.17 3.22 o
-1 2 -11 1.89 2.04 3.33 o
0 2 -11 15.58 16.45 3.29 o
-2 3 -11 19.54 19.14 3.00 o
-1 3 -11 89.47 86.72 3.69 o
0 3 -11 41.40 41.82 3.52 o
-3 4 -11 33.06 31.61 3.13 o
-2 4 -11 3.04 4.38 2.84 o
-1 4 -11 5.97 4.21 3.03 o
0 4 -11 9.54 8.37 2.97 o
-4 5 -11 1.60 4.35 2.63 o
-3 5 -11 16.64 17.79 2.90 o
-2 5 -11 5.18 7.83 2.90 o
-1 5 -11 5.76 7.53 2.68 o
0 0 -10 844.52 832.67 7.79 o
0 1 -10 1056.68 1180.00 10.46 o
-1 2 -10 962.85 965.22 9.16 o
0 2 -10 1355.43 1500.77 11.17 o
-2 3 -10 1369.90 1456.46 10.44 o
-1 3 -10 1080.45 1144.23 9.46 o
0 3 -10 725.96 739.25 7.41 o
-3 4 -10 544.86 575.48 6.67 o
-2 4 -10 442.72 428.41 5.67 o
-1 4 -10 1002.86 1051.78 8.34 o
0 4 -10 659.59 706.31 6.90 o
-4 5 -10 300.50 299.20 5.02 o
-3 5 -10 469.41 464.59 6.10 o
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0 5 -10 369.19 391.06 5.72 o
-5 6 -10 307.49 308.84 5.33 o
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-3 6 -10 166.89 173.14 4.34 o
-2 6 -10 410.49 403.66 5.75 o
-1 6 -10 355.81 349.82 5.61 o
0 1 -9 57.85 56.89 3.72 o
-1 2 -9 54.62 53.31 3.37 o
0 2 -9 683.71 690.57 7.75 o
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-1 3 -9 311.82 307.46 5.20 o
0 3 -9 13.20 15.75 2.99 o
-3 4 -9 548.45 554.50 6.33 o
-2 4 -9 86.74 83.63 3.66 o
-1 4 -9 245.34 252.99 4.58 o
0 4 -9 127.88 139.75 3.95 o
-4 5 -9 0.22 2.49 2.76 o
-3 5 -9 178.27 183.64 4.26 o
-2 5 -9 140.21 145.53 3.95 o
-1 5 -9 17.60 22.64 2.86 o
0 5 -9 32.86 32.90 2.92 o
-5 6 -9 164.88 182.31 4.12 o
-4 6 -9 109.82 111.33 3.69 o
-3 6 -9 7.86 7.88 2.81 o
-2 6 -9 19.25 21.22 3.07 o
-1 6 -9 73.65 86.67 3.50 o
0 6 -9 3.85 4.72 2.88 o
-5 7 -9 33.27 26.87 3.19 o
-4 7 -9 234.57 226.17 4.74 o
-3 7 -9 46.13 41.95 3.37 o
-2 7 -9 0.72 1.34 2.82 o
0 0 -8 2502.81 2803.62 16.47 o
0 1 -8 1986.69 2069.28 15.98 o
-1 2 -8 1811.25 1988.68 13.69 o
0 2 -8 1815.78 1930.22 13.11 o
-2 3 -8 1773.57 1921.68 13.02 o
-1 3 -8 1263.35 1331.70 10.25 o
0 3 -8 1298.81 1431.23 10.55 o
-3 4 -8 1043.07 1082.28 8.66 o
-2 4 -8 1039.92 1137.10 8.79 o
-1 4 -8 1162.05 1268.17 9.15 o
0 4 -8 735.11 807.09 7.06 o
-4 5 -8 906.08 960.83 7.57 o
-3 5 -8 836.01 910.62 7.91 o
-2 5 -8 750.57 812.74 7.16 o
-1 5 -8 881.20 1007.62 7.74 o
0 5 -8 464.25 489.03 5.60 o
-5 6 -8 391.62 423.29 5.28 o
-4 6 -8 538.32 571.31 6.51 o
-3 6 -8 432.62 484.36 5.76 o
-2 6 -8 457.68 493.09 5.83 o
-1 6 -8 381.95 431.17 5.44 o
0 6 -8 470.81 513.07 5.97 o
-6 7 -8 180.42 196.32 4.61 o
-5 7 -8 312.17 317.75 5.31 o
-4 7 -8 265.90 287.35 5.04 o
-3 7 -8 411.12 428.85 5.72 o
-2 7 -8 288.78 314.41 5.32 o
-1 7 -8 228.47 215.94 4.82 o
0 1 -7 775.62 795.80 9.38 o
-1 2 -7 0.04 3.11 2.78 o
0 2 -7 847.86 854.98 8.73 o
-2 3 -7 858.63 912.35 8.53 o
-1 3 -7 1987.97 2193.08 13.98 o
0 3 -7 136.84 145.13 4.03 o
-3 4 -7 1033.31 1116.21 8.89 o
-2 4 -7 21.88 26.67 2.87 o
-1 4 -7 575.25 630.45 6.52 o
0 4 -7 497.16 529.93 5.90 o
-4 5 -7 1.54 3.56 2.68 o
-3 5 -7 541.50 593.22 6.29 o
-2 5 -7 415.03 439.74 5.50 o
-1 5 -7 28.17 33.72 3.03 o
0 5 -7 402.33 445.63 5.27 o
-5 6 -7 448.36 533.43 5.72 o
-4 6 -7 362.37 381.61 5.33 o
-3 6 -7 6.71 10.75 2.68 o
-2 6 -7 380.53 423.69 5.30 o
-1 6 -7 102.24 110.88 3.40 o
0 6 -7 6.77 10.07 2.78 o
-6 7 -7 122.39 132.80 3.91 o
-5 7 -7 8.50 6.51 2.78 o
-4 7 -7 270.80 311.97 4.99 o
-3 7 -7 265.58 296.08 4.67 o
-2 7 -7 3.08 4.67 2.76 o
-1 7 -7 196.52 230.33 4.39 o
0 7 -7 247.73 272.36 4.88 o
-6 8 -7 276.36 255.12 5.08 o
-5 8 -7 235.13 247.74 5.05 o
-4 8 -7 37.55 32.61 3.41 o
-3 8 -7 131.90 142.84 4.22 o
-2 8 -7 178.44 161.37 4.57 o
0 0 -6 13981.42 17638.76 90.68 o
0 1 -6 3216.21 3444.06 22.30 o
-1 2 -6 2580.69 3046.83 18.83 o
0 2 -6 1708.52 1824.33 13.19 o
-2 3 -6 4810.93 5570.51 25.48 o
-1 3 -6 1655.51 1719.43 12.47 o
0 3 -6 989.64 1103.83 9.61 o
-3 4 -6 1348.12 1531.32 10.60 o
-2 4 -6 1267.31 1409.93 10.09 o
-1 4 -6 1443.14 1577.76 10.52 o
0 4 -6 1744.86 1967.64 11.47 o
-4 5 -6 1265.64 1502.02 10.18 o
-3 5 -6 2113.60 2447.10 12.95 o
-2 5 -6 888.22 946.04 7.75 o
-1 5 -6 1502.22 1656.59 10.21 o
0 5 -6 701.01 807.73 6.93 o
-5 6 -6 403.40 471.78 5.36 o
-4 6 -6 1562.70 1798.87 10.59 o
-3 6 -6 912.68 1036.59 8.18 o
-2 6 -6 329.52 366.66 5.09 o
-1 6 -6 281.31 313.62 4.66 o
0 6 -6 423.84 514.09 5.69 o
-6 7 -6 400.74 459.90 5.60 o
-5 7 -6 184.70 201.39 4.17 o
-4 7 -6 281.15 317.25 4.95 o
-3 7 -6 423.10 471.83 5.69 o
-2 7 -6 498.39 535.71 5.76 o
-1 7 -6 336.67 395.23 5.15 o
0 7 -6 343.07 382.69 5.35 o
-7 8 -6 85.61 88.86 3.80 o
-6 8 -6 197.87 224.80 4.56 o
-5 8 -6 318.20 335.27 5.46 o
-4 8 -6 105.25 111.86 3.76 o
-3 8 -6 365.98 378.96 5.57 o
-2 8 -6 378.08 387.09 5.58 o
-1 8 -6 141.41 149.80 4.29 o
0 1 -5 1762.37 1751.16 15.73 o
-1 2 -5 15.12 18.51 3.26 o
0 2 -5 1262.86 1371.75 12.14 o
-2 3 -5 833.91 858.28 8.41 o
-1 3 -5 57.81 62.01 3.37 o
0 3 -5 374.83 393.96 5.79 o
-3 4 -5 343.72 332.98 5.29 o
-2 4 -5 32.32 33.51 2.96 o
-1 4 -5 831.65 858.11 7.89 o
0 4 -5 655.44 717.04 6.88 o
-4 5 -5 2.43 4.44 2.81 o
-3 5 -5 395.58 404.53 5.48 o
-2 5 -5 771.66 823.78 7.27 o
-1 5 -5 44.65 48.22 2.97 o
0 5 -5 361.54 405.18 5.14 o
-5 6 -5 175.78 175.93 4.22 o
-4 6 -5 330.21 372.97 5.13 o
-3 6 -5 12.81 10.43 3.02 o
-2 6 -5 301.58 318.42 4.78 o
-1 6 -5 687.59 762.04 6.56 o
0 6 -5 3.82 6.98 2.43 o
-6 7 -5 310.41 357.55 4.94 o
-5 7 -5 4.41 5.82 2.97 o
-4 7 -5 277.18 314.12 4.92 o
-3 7 -5 177.90 199.46 4.18 o
-2 7 -5 3.94 6.06 2.48 o
-1 7 -5 148.05 174.42 3.92 o
0 7 -5 87.46 96.80 3.45 o
-7 8 -5 21.74 26.11 3.01 o
-6 8 -5 75.81 90.57 3.63 o
-5 8 -5 90.98 104.56 3.75 o
-4 8 -5 15.81 13.48 2.89 o
-3 8 -5 203.69 234.00 4.53 o
-2 8 -5 104.16 122.05 3.90 o
-1 8 -5 12.34 16.22 2.91 o
-5 9 -5 156.72 157.44 4.55 o
-4 9 -5 55.41 59.14 3.77 o
0 0 -4 3910.94 4032.45 36.83 o
0 1 -4 3744.12 3953.58 29.05 o
-1 2 -4 4358.40 4778.67 28.53 o
0 2 -4 5560.61 6224.05 32.39 o
-2 3 -4 5737.69 6550.69 30.04 o
-1 3 -4 3703.43 4070.79 21.99 o
0 3 -4 2757.91 2888.97 16.89 o
-3 4 -4 1627.66 1719.00 12.03 o
-2 4 -4 1429.25 1394.04 10.84 o
-1 4 -4 3498.41 3616.00 18.35 o
0 4 -4 1863.37 1985.99 12.06 o
-4 5 -4 1083.57 1182.85 8.97 o
-3 5 -4 1329.80 1423.02 10.22 o
-2 5 -4 1639.27 1621.73 10.89 o
-1 5 -4 1682.63 1622.26 10.45 o
0 5 -4 960.35 1065.44 7.92 o
-5 6 -4 778.44 885.52 7.41 o
-4 6 -4 974.03 1059.09 8.33 o
-3 6 -4 451.86 462.23 5.60 o
-2 6 -4 1115.43 1119.35 8.33 o
-1 6 -4 929.43 976.39 7.43 o
0 6 -4 794.44 857.94 6.96 o
-6 7 -4 605.34 708.77 6.58 o
-5 7 -4 423.79 461.17 5.63 o
-4 7 -4 564.00 595.17 6.37 o
-3 7 -4 1022.21 1065.54 7.97 o
-2 7 -4 407.13 425.01 5.13 o
-1 7 -4 454.20 507.22 5.60 o
0 7 -4 464.91 518.86 5.69 o
-7 8 -4 132.32 142.25 3.83 o
-6 8 -4 428.75 467.29 5.72 o
-5 8 -4 587.98 652.19 6.71 o
-4 8 -4 275.30 299.72 4.81 o
-3 8 -4 428.90 460.71 5.74 o
-2 8 -4 143.43 166.23 4.01 o
-1 8 -4 151.00 152.34 4.06 o
0 8 -4 185.63 186.87 4.58 o
-6 9 -4 116.54 103.05 3.99 o
-5 9 -4 201.68 188.68 4.99 o
-4 9 -4 243.14 233.12 5.11 o
-3 9 -4 106.05 116.21 4.09 o
0 1 -3 2533.72 2645.93 25.15 o
-1 2 -3 847.76 851.66 10.61 o
0 2 -3 616.86 682.97 8.99 o
-2 3 -3 39.78 40.44 3.13 o
-1 3 -3 59.42 48.19 3.09 o
0 3 -3 65.56 63.90 3.20 o
-3 4 -3 286.31 295.50 5.29 o
-2 4 -3 711.26 745.94 7.96 o
-1 4 -3 23.64 24.09 2.80 o
0 4 -3 197.19 186.82 4.13 o
-4 5 -3 0.08 0.91 2.52 o
-3 5 -3 63.75 63.32 3.10 o
-2 5 -3 102.71 100.37 3.36 o
-1 5 -3 82.08 84.17 3.32 o
0 5 -3 510.24 543.28 5.86 o
-5 6 -3 12.22 14.10 2.68 o
-4 6 -3 79.81 92.38 3.62 o
-3 6 -3 35.69 34.69 2.90 o
-2 6 -3 600.33 627.06 6.35 o
-1 6 -3 128.37 135.43 3.58 o
0 6 -3 13.21 11.43 2.54 o
-6 7 -3 2.29 2.21 2.62 o
-5 7 -3 124.46 126.44 3.87 o
-4 7 -3 26.06 34.75 2.85 o
-3 7 -3 177.25 193.70 3.96 o
-2 7 -3 4.13 3.99 2.67 o
-1 7 -3 68.57 76.63 3.19 o
0 7 -3 64.43 68.52 3.30 o
-7 8 -3 0.53 3.76 2.57 o
-6 8 -3 39.57 40.92 3.02 o
-5 8 -3 47.57 59.80 3.37 o
-4 8 -3 38.74 46.98 3.25 o
-3 8 -3 7.32 4.63 2.91 o
-2 8 -3 8.52 12.02 2.69 o
-1 8 -3 9.67 9.87 2.79 o
0 8 -3 0.47 2.85 2.53 o
-7 9 -3 19.19 27.26 3.19 o
-6 9 -3 2.28 5.09 3.15 o
-5 9 -3 17.14 16.45 3.41 o
-4 9 -3 2.00 6.38 3.23 o
-3 9 -3 12.06 15.13 3.08 o
-2 9 -3 2.52 2.76 2.70 o
0 0 -2 15489.45 15781.30 125.92 o
0 1 -2 5836.40 6368.27 49.58 o
-1 2 -2 13185.95 13362.13 68.22 o
0 2 -2 5223.85 5174.03 33.36 o
-2 3 -2 4854.53 4960.89 28.32 o
-1 3 -2 2658.31 2447.79 17.51 o
0 3 -2 7110.38 7743.75 34.06 o
-3 4 -2 2360.59 2336.45 15.53 o
-2 4 -2 4471.93 4563.49 23.24 o
-1 4 -2 2949.09 2737.26 16.21 o
0 4 -2 1328.20 1262.70 9.88 o
-4 5 -2 2981.68 3250.22 16.80 o
-3 5 -2 1736.16 1686.13 11.70 o
-2 5 -2 1594.11 1473.64 10.81 o
-1 5 -2 4860.97 4951.24 21.24 o
0 5 -2 717.46 692.57 6.59 o
-5 6 -2 736.72 817.39 7.00 o
-4 6 -2 927.33 942.36 8.12 o
-3 6 -2 1963.48 2009.72 12.04 o
-2 6 -2 890.14 872.61 7.41 o
-1 6 -2 684.41 699.53 6.55 o
0 6 -2 2149.13 2344.13 11.79 o
-6 7 -2 251.85 281.85 4.50 o
-5 7 -2 1317.34 1491.13 9.37 o
-4 7 -2 425.39 438.20 5.63 o
-3 7 -2 807.72 809.78 7.09 o
-2 7 -2 1465.09 1594.45 9.71 o
-1 7 -2 389.44 431.10 5.16 o
0 7 -2 299.08 326.49 4.87 o
-7 8 -2 638.37 710.34 6.74 o
-6 8 -2 311.81 338.81 4.83 o
-5 8 -2 344.64 356.74 5.18 o
-4 8 -2 963.61 1006.90 8.19 o
-3 8 -2 298.35 318.63 4.80 o
-2 8 -2 173.71 180.39 3.85 o
-1 8 -2 441.30 482.64 5.59 o
0 8 -2 139.27 147.03 3.91 o
-7 9 -2 118.32 113.09 3.99 o
-6 9 -2 476.25 492.59 6.28 o
-5 9 -2 78.01 80.40 3.56 o
-4 9 -2 165.99 163.94 4.42 o
-3 9 -2 382.66 408.96 5.69 o
-2 9 -2 242.37 233.10 4.77 o
0 1 -1 155.88 160.94 6.20 o
-1 2 -1 32.06 30.01 3.04 o
0 2 -1 103.36 96.19 3.91 o
-2 3 -1 0.15 2.99 2.27 o
-1 3 -1 1628.33 1702.96 13.86 o
0 3 -1 831.21 880.06 8.73 o
-3 4 -1 134.17 144.36 4.00 o
-2 4 -1 82.08 85.55 3.34 o
-1 4 -1 38.21 34.49 2.64 o
0 4 -1 29.25 27.86 2.79 o
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-3 5 -1 19.14 20.67 2.40 o
-2 5 -1 99.18 95.41 3.30 o
-1 5 -1 97.26 91.44 3.22 o
0 5 -1 22.80 24.58 2.69 o
-5 6 -1 55.83 56.36 2.87 o
-4 6 -1 2.94 4.88 2.41 o
-3 6 -1 23.71 20.57 2.59 o
-2 6 -1 43.59 41.41 2.93 o
-1 6 -1 244.28 234.50 4.17 o
0 6 -1 11.63 14.31 2.44 o
-6 7 -1 50.77 53.23 2.82 o
-5 7 -1 13.03 12.76 2.61 o
-4 7 -1 28.11 28.06 2.74 o
-3 7 -1 10.57 10.93 2.84 o
-2 7 -1 5.58 6.95 2.61 o
-1 7 -1 3.43 5.55 2.29 o
0 7 -1 9.99 12.60 2.47 o
-7 8 -1 38.37 47.46 3.00 o
-6 8 -1 16.49 18.86 2.71 o
-5 8 -1 6.14 5.63 2.80 o
-4 8 -1 57.20 52.66 3.23 o
-3 8 -1 16.67 16.84 2.84 o
-2 8 -1 8.69 8.19 2.58 o
-1 8 -1 15.20 19.49 2.72 o
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-7 9 -1 17.76 14.88 2.97 o
-6 9 -1 0.68 4.76 2.91 o
-5 9 -1 12.37 9.75 2.83 o
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-2 9 -1 3.15 7.28 2.65 o
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0 2 0 182.60 169.43 5.00 o
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-1 3 0 460.45 395.45 6.34 o
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-3 7 0 146.32 157.86 3.94 o
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-1 7 0 115.77 121.67 3.38 o
0 7 0 147.39 164.89 3.54 o
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-6 8 0 43.68 55.66 2.97 o
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-4 8 0 1127.83 1185.96 8.55 o
-3 8 0 171.72 182.60 3.86 o
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-1 8 0 1152.25 1229.24 8.41 o
0 8 0 7.07 7.51 2.80 o
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-5 9 0 72.62 82.84 3.71 o
-4 9 0 2.42 2.31 2.62 o
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-2 9 0 129.62 119.28 3.68 o
0 1 1 155.19 155.49 6.01 o
-1 2 1 32.10 29.13 2.80 o
0 2 1 106.00 100.97 3.85 o
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-1 5 1 97.26 87.70 3.33 o
0 5 1 24.47 25.09 2.60 o
-5 6 1 57.69 53.42 3.06 o
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-3 6 1 23.70 22.72 2.69 o
-2 6 1 41.49 39.17 2.73 o
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-5 7 1 13.03 14.61 2.29 o
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