#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:01:17 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181901 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/01/2240188.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240188 _cell_angle_alpha 90.000 _cell_angle_beta 98.679 _cell_angle_gamma 90.000 _cell_length_a 12.9207 _cell_length_b 19.2867 _cell_length_c 22.9773 _exptl_crystal_F_000 2232.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file is5379Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 226.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 123.70 143.89 2.98 o 4 0 0 1751.36 1491.20 31.50 o 6 0 0 800.38 774.81 14.32 o 8 0 0 7997.37 7293.57 59.65 o 10 0 0 10215.64 10971.70 142.29 o 12 0 0 1171.16 1111.54 46.83 o 14 0 0 695.78 683.27 63.18 o 16 0 0 1544.91 1605.81 79.70 o 2 1 0 4733.70 4185.94 22.88 o 3 1 0 55.47 42.19 5.42 o 4 1 0 204.96 200.33 3.72 o 5 1 0 137.27 177.62 3.27 o 6 1 0 5030.61 4924.44 73.16 o 7 1 0 1153.20 907.93 9.68 o 8 1 0 1245.51 1495.93 19.57 o 9 1 0 798.57 922.56 11.44 o 10 1 0 608.58 686.47 14.66 o 11 1 0 2820.61 2977.61 47.38 o 12 1 0 165.33 138.99 13.60 o 13 1 0 834.19 803.71 26.14 o 14 1 0 13.57 12.44 9.32 o 15 1 0 911.41 970.01 36.70 o 16 1 0 109.63 71.65 36.49 o 2 2 0 417.16 457.25 7.20 o 3 2 0 13797.98 12842.18 76.33 o 4 2 0 5130.46 4824.77 27.32 o 5 2 0 411.14 477.96 6.31 o 6 2 0 69.17 105.61 3.61 o 7 2 0 390.72 341.73 7.70 o 8 2 0 3896.66 3864.69 93.09 o 9 2 0 10346.65 10292.32 79.34 o 10 2 0 1135.30 1277.02 17.01 o 11 2 0 337.56 357.70 13.17 o 12 2 0 20.40 16.72 9.02 o 13 2 0 6.04 8.81 8.21 o 14 2 0 971.49 971.83 27.83 o 15 2 0 116.79 82.17 34.09 o 16 2 0 191.06 150.82 19.43 o 1 3 0 1317.24 1252.58 40.00 o 2 3 0 3509.55 3267.55 21.45 o 3 3 0 2124.47 2165.14 28.28 o 4 3 0 1163.97 1143.74 20.99 o 5 3 0 287.13 272.97 6.71 o 6 3 0 12120.67 11736.26 69.54 o 7 3 0 1123.27 994.54 11.79 o 8 3 0 3781.48 3903.91 66.12 o 9 3 0 6.29 10.99 5.60 o 10 3 0 3513.58 3702.85 50.13 o 11 3 0 2013.93 2103.79 34.05 o 12 3 0 4678.53 4929.03 55.07 o 13 3 0 451.00 473.72 18.42 o 14 3 0 63.67 47.45 29.59 o 15 3 0 214.90 221.22 16.02 o 16 3 0 2590.28 2595.03 91.22 o 0 4 0 1243.38 1164.48 29.94 o 1 4 0 24441.07 22574.45 372.91 o 2 4 0 427.84 489.77 8.76 o 3 4 0 19.97 6.74 2.94 o 4 4 0 1905.25 1865.89 22.91 o 5 4 0 10441.22 9947.33 65.59 o 6 4 0 1125.49 1150.22 18.20 o 7 4 0 564.59 564.09 10.11 o 8 4 0 5.05 5.09 8.40 o 9 4 0 17709.41 17798.93 165.70 o 10 4 0 995.27 998.28 21.62 o 11 4 0 916.52 982.51 25.17 o 12 4 0 197.29 197.67 17.80 o 13 4 0 1379.25 1338.19 44.33 o 14 4 0 294.20 246.66 25.70 o 15 4 0 213.97 221.92 28.64 o 16 4 0 74.15 61.27 34.13 o 1 5 0 5834.70 5507.22 37.38 o 2 5 0 4052.93 3804.74 47.36 o 3 5 0 1791.22 1643.00 25.21 o 4 5 0 126.75 104.03 12.80 o 6 5 0 10868.10 10167.77 38.86 o 7 5 0 3833.13 3987.35 61.99 o 8 5 0 5271.24 5278.53 111.00 o 9 5 0 1031.61 1082.38 30.35 o 10 5 0 2786.53 2942.94 57.11 o 11 5 0 435.29 433.65 14.04 o 12 5 0 5915.78 6543.38 100.61 o 13 5 0 164.15 158.74 29.83 o 14 5 0 454.28 404.95 28.46 o 15 5 0 243.06 212.83 15.61 o 16 5 0 2004.57 2144.98 74.08 o 0 6 0 12281.13 10982.65 191.53 o 1 6 0 22592.61 20543.61 101.90 o 2 6 0 203.56 164.81 4.79 o 3 6 0 313.58 375.86 7.93 o 4 6 0 20896.44 19478.63 103.06 o 5 6 0 6512.76 6417.03 44.51 o 6 6 0 1829.10 2006.29 31.75 o 7 6 0 542.55 521.13 13.51 o 8 6 0 6000.50 6232.88 65.52 o 9 6 0 4514.05 4648.05 86.78 o 10 6 0 274.32 271.94 12.74 o 11 6 0 359.12 373.16 15.69 o 12 6 0 740.04 721.55 30.45 o 13 6 0 50.63 44.54 12.94 o 14 6 0 2139.99 2270.00 87.18 o 15 6 0 26.29 24.06 8.72 o 16 6 0 80.43 50.14 26.12 o 1 7 0 581.41 885.76 16.01 o 2 7 0 6811.04 6794.50 75.78 o 3 7 0 16023.93 15165.08 198.45 o 4 7 0 4043.22 4070.19 55.99 o 5 7 0 5809.81 5618.70 113.81 o 6 7 0 3333.49 3436.36 162.34 o 7 7 0 6497.51 5971.47 56.08 o 8 7 0 61.28 30.30 18.45 o 9 7 0 1164.57 1245.13 28.76 o 10 7 0 38.62 30.17 18.42 o 11 7 0 1358.76 1443.61 37.50 o 12 7 0 40.51 32.98 9.29 o 13 7 0 88.56 84.04 19.51 o 14 7 0 173.00 168.33 19.73 o 15 7 0 1593.88 1599.30 51.78 o 0 8 0 30754.16 27831.12 204.92 o 1 8 0 5422.89 5550.20 50.03 o 2 8 0 726.81 601.64 12.00 o 3 8 0 16.26 -1.05 5.16 o 4 8 0 7311.04 7108.84 107.15 o 5 8 0 38.29 20.45 5.84 o 6 8 0 1835.78 1987.81 60.62 o 7 8 0 1.21 2.50 1.78 o 8 8 0 10989.07 10619.36 149.49 o 9 8 0 52.81 61.91 24.56 o 10 8 0 3679.33 3886.38 55.97 o 11 8 0 37.86 39.93 17.21 o 12 8 0 80.77 57.46 16.39 o 13 8 0 15.10 8.23 6.87 o 14 8 0 1097.05 1012.53 59.06 o 15 8 0 106.01 73.97 30.06 o 1 9 0 3708.31 3271.84 88.55 o 2 9 0 2027.61 1792.29 45.72 o 3 9 0 4501.22 4176.47 57.40 o 4 9 0 2358.67 2774.86 30.11 o 5 9 0 1331.14 1288.06 29.12 o 6 9 0 7080.90 6627.72 99.49 o 7 9 0 5123.50 5414.21 133.23 o 8 9 0 29.90 27.20 6.90 o 9 9 0 16.52 16.58 7.72 o 10 9 0 1787.69 1918.77 34.98 o 11 9 0 5295.54 5386.81 138.34 o 12 9 0 3236.41 3316.43 70.51 o 13 9 0 316.99 340.23 27.39 o 14 9 0 63.99 52.19 38.37 o 15 9 0 618.25 613.80 47.79 o 0 10 0 11941.56 11074.45 137.16 o 1 10 0 23138.67 22559.33 176.43 o 2 10 0 1012.75 941.28 13.97 o 3 10 0 3445.60 3342.35 45.91 o 4 10 0 85.50 27.99 6.96 o 5 10 0 2938.05 2928.79 60.11 o 6 10 0 1495.96 1534.85 28.18 o 7 10 0 1189.38 1189.06 39.27 o 8 10 0 2294.09 2456.26 52.71 o 9 10 0 1544.06 1571.38 56.59 o 10 10 0 13083.00 13232.63 177.27 o 11 10 0 2299.07 2253.45 51.35 o 12 10 0 75.83 69.80 26.72 o 13 10 0 1427.96 1478.14 48.14 o 14 10 0 28.90 19.55 18.21 o 15 10 0 104.48 80.74 70.11 o 1 11 0 746.93 874.33 33.45 o 2 11 0 4400.14 4228.71 71.43 o 3 11 0 182.33 217.99 18.06 o 4 11 0 461.27 316.45 19.04 o 5 11 0 461.85 405.43 25.81 o 6 11 0 2400.05 2334.46 54.34 o 7 11 0 41.85 28.36 8.60 o 8 11 0 35.71 65.32 25.92 o 9 11 0 10.65 8.54 11.66 o 10 11 0 120.41 102.99 27.51 o 11 11 0 857.61 883.84 35.93 o 12 11 0 7139.08 7565.09 131.50 o 13 11 0 1189.94 1125.81 40.70 o 14 11 0 68.80 54.22 26.02 o 0 12 0 20.64 27.73 19.23 o 1 12 0 9865.19 9413.78 122.63 o 2 12 0 260.88 302.35 27.28 o 3 12 0 26.55 13.04 8.21 o 4 12 0 3785.78 4444.01 90.34 o 5 12 0 9198.41 9596.70 192.82 o 6 12 0 96.21 82.24 6.95 o 7 12 0 111.18 95.46 25.06 o 8 12 0 12725.81 13009.07 309.94 o 9 12 0 7174.31 7882.48 127.23 o 10 12 0 14.73 1.96 12.43 o 11 12 0 172.11 194.22 57.28 o 12 12 0 180.48 186.64 26.46 o 13 12 0 2509.74 2678.35 78.96 o 14 12 0 15.53 10.98 10.61 o 1 13 0 0.57 -1.11 18.16 o 2 13 0 8972.60 8551.03 101.13 o 3 13 0 1559.82 1833.07 131.31 o 4 13 0 761.47 772.16 32.82 o 5 13 0 745.58 643.19 35.42 o 6 13 0 4302.34 4570.14 163.28 o 7 13 0 113.31 112.37 53.26 o 8 13 0 109.26 111.45 35.83 o 9 13 0 45.52 37.82 20.33 o 10 13 0 473.13 526.50 32.00 o 11 13 0 1530.00 1564.70 42.97 o 12 13 0 3649.52 3767.02 82.94 o 13 13 0 19.01 15.24 8.83 o 14 13 0 218.19 198.21 23.51 o 0 14 0 9564.98 8961.06 154.35 o 1 14 0 10573.15 10479.83 127.97 o 2 14 0 221.54 261.02 36.38 o 3 14 0 384.28 355.45 22.34 o 4 14 0 3324.63 3431.18 112.66 o 5 14 0 3179.61 3268.13 125.93 o 6 14 0 1132.34 1227.49 72.69 o 7 14 0 343.32 331.88 26.56 o 8 14 0 110.00 112.88 48.91 o 9 14 0 3789.54 3999.58 98.12 o 10 14 0 1357.91 1389.99 38.44 o 11 14 0 112.70 76.26 29.38 o 12 14 0 955.43 940.50 32.47 o 13 14 0 566.03 572.59 22.58 o 1 15 0 1364.51 1435.08 45.62 o 2 15 0 1005.05 1104.39 37.72 o 3 15 0 1824.76 1841.51 40.85 o 4 15 0 151.18 156.35 56.65 o 5 15 0 914.66 868.36 40.84 o 6 15 0 90.21 60.53 35.72 o 7 15 0 2621.48 2685.64 83.76 o 8 15 0 110.05 77.68 32.96 o 9 15 0 65.81 99.57 34.71 o 10 15 0 578.53 564.64 57.00 o 11 15 0 2852.21 3052.80 77.63 o 12 15 0 245.44 239.84 25.66 o 13 15 0 503.32 473.17 24.95 o 0 16 0 7490.22 8159.59 273.55 o 1 16 0 1996.57 1896.97 53.55 o 2 16 0 488.45 439.52 24.99 o 3 16 0 476.55 479.31 36.01 o 4 16 0 8136.19 9081.08 245.58 o 5 16 0 326.04 374.98 34.72 o 6 16 0 1319.39 1343.89 51.18 o 7 16 0 270.90 244.57 27.11 o 8 16 0 2374.30 2513.98 52.34 o 9 16 0 318.63 295.81 61.57 o 10 16 0 2757.25 2814.73 54.11 o 11 16 0 53.95 13.60 13.67 o 12 16 0 125.85 82.19 44.60 o 1 17 0 2228.27 2398.31 46.02 o 2 17 0 1347.71 1287.85 30.86 o 3 17 0 2111.34 2158.60 44.90 o 4 17 0 458.45 454.98 51.65 o 5 17 0 287.97 356.98 51.44 o 6 17 0 877.91 801.01 48.87 o 7 17 0 3626.09 3595.92 132.66 o 8 17 0 462.87 368.70 52.75 o 9 17 0 7.18 27.01 18.33 o 10 17 0 14.10 25.68 10.21 o 11 17 0 2098.99 2124.49 65.56 o 12 17 0 530.46 496.40 24.21 o 0 18 0 3208.92 3496.13 83.28 o 1 18 0 2297.63 2334.89 56.10 o 2 18 0 37.31 23.80 18.86 o 3 18 0 67.72 88.23 41.85 o 4 18 0 411.02 425.41 40.23 o 5 18 0 4764.29 5089.27 144.94 o 6 18 0 7.35 -20.38 26.43 o 7 18 0 486.91 387.71 47.93 o 8 18 0 432.12 488.00 31.66 o 9 18 0 1114.31 1111.36 56.16 o 10 18 0 1649.44 1547.27 49.54 o 11 18 0 41.84 53.45 26.86 o 1 19 0 1645.61 1483.81 87.03 o 2 19 0 2526.40 2712.09 69.49 o 3 19 0 1373.35 1409.05 34.10 o 4 19 0 503.93 442.82 42.80 o 5 19 0 5.84 -8.83 28.03 o 6 19 0 2501.20 2549.00 75.94 o 7 19 0 179.98 154.99 87.90 o 8 19 0 580.99 650.92 67.72 o 9 19 0 160.51 159.37 70.10 o 10 19 0 427.81 364.23 28.60 o 0 20 0 296.42 248.71 47.04 o 1 20 0 5511.84 5809.13 190.97 o 2 20 0 2.78 2.34 8.04 o 3 20 0 860.48 1020.10 69.30 o 4 20 0 518.40 500.95 43.50 o 5 20 0 2598.41 2766.84 97.25 o 6 20 0 4.59 7.38 17.63 o 7 20 0 4.83 10.21 17.14 o 8 20 0 176.67 174.70 55.07 o 9 20 0 2464.33 2328.49 107.02 o 1 21 0 12.98 16.51 17.75 o 2 21 0 3331.80 3305.07 73.51 o 3 21 0 175.28 165.18 90.57 o 4 21 0 382.70 378.10 29.99 o 5 21 0 214.53 147.38 59.69 o 6 21 0 1642.14 1819.01 90.85 o 7 21 0 246.90 194.01 32.24 o 8 21 0 156.82 128.30 69.68 o 9 21 0 373.02 342.48 47.25 o 0 22 0 2222.46 2192.09 102.49 o 1 22 0 239.99 252.90 24.17 o 2 22 0 72.82 94.39 36.47 o 3 22 0 60.70 67.40 45.18 o 4 22 0 3095.01 3208.42 109.79 o 5 22 0 2172.64 2248.06 100.57 o 6 22 0 612.90 628.30 36.70 o 7 22 0 419.65 444.12 44.88 o 1 23 0 850.19 933.10 35.97 o 2 23 0 20.92 6.13 18.80 o 3 23 0 1153.89 1171.45 55.44 o 4 23 0 1156.19 1103.24 58.07 o 5 23 0 813.31 867.00 44.36 o 6 23 0 40.82 12.48 12.39 o 0 24 0 2309.42 2617.79 106.98 o 1 24 0 113.67 80.67 63.28 o 2 24 0 227.29 149.80 46.80 o 3 24 0 218.35 178.29 35.34 o 4 24 0 1562.33 1521.41 79.90 o 1 25 0 606.49 596.42 35.93 o -16 0 1 32.11 15.91 18.84 o -14 0 1 1244.92 1189.65 55.44 o -12 0 1 2082.64 2101.65 50.71 o -10 0 1 4952.85 5311.90 89.42 o -8 0 1 7388.95 8141.40 63.03 o -6 0 1 48139.91 47900.17 1565.18 o -4 0 1 2967.43 2529.62 17.41 o 2 0 1 7728.75 7154.87 61.93 o 4 0 1 13937.82 14045.42 127.74 o 6 0 1 10723.35 10274.55 108.94 o 8 0 1 1359.78 1164.49 21.42 o 10 0 1 141.76 141.46 9.02 o 12 0 1 6221.38 6563.51 112.61 o 14 0 1 293.54 298.35 34.41 o 16 0 1 994.05 938.19 77.63 o -16 1 1 125.21 76.28 32.74 o -15 1 1 21.06 6.92 15.10 o -14 1 1 730.88 768.03 24.36 o -13 1 1 4129.42 4296.66 75.44 o -12 1 1 78.14 65.07 25.71 o -11 1 1 797.13 858.48 16.53 o -10 1 1 79.17 69.00 9.35 o -9 1 1 5510.61 5351.70 44.73 o -8 1 1 2199.27 2262.23 31.29 o -7 1 1 4261.23 4228.59 46.69 o -6 1 1 141.40 191.71 5.57 o -5 1 1 788.39 709.04 9.20 o -4 1 1 14888.25 13950.43 52.83 o -3 1 1 477.95 619.44 8.72 o -2 1 1 16117.88 10962.11 91.51 o 2 1 1 6.98 26.83 3.91 o 3 1 1 222.31 252.91 4.02 o 4 1 1 0.89 0.21 1.86 o 5 1 1 9400.58 8935.86 80.69 o 6 1 1 1.71 3.22 1.98 o 7 1 1 176.03 244.98 4.81 o 8 1 1 0.53 8.12 2.98 o 9 1 1 13680.38 13496.42 93.06 o 10 1 1 3659.04 3887.64 42.78 o 11 1 1 2043.34 2102.04 36.35 o 12 1 1 58.67 51.73 12.14 o 13 1 1 1947.70 2043.29 40.87 o 14 1 1 489.56 522.85 18.86 o 15 1 1 250.27 256.21 23.99 o 16 1 1 30.98 25.08 10.46 o -16 2 1 548.58 485.97 28.04 o -15 2 1 734.84 732.55 46.55 o -14 2 1 953.27 932.70 25.69 o -13 2 1 54.72 53.46 15.51 o -12 2 1 1607.45 1731.50 44.74 o -11 2 1 12.80 19.77 5.91 o -10 2 1 5140.12 5569.08 66.57 o -9 2 1 79.57 83.09 8.26 o -8 2 1 1138.88 1266.91 20.88 o -7 2 1 12475.96 12107.24 128.16 o -6 2 1 15891.23 14733.99 58.94 o -5 2 1 662.15 547.55 8.03 o -4 2 1 303.62 304.73 4.63 o -3 2 1 14574.87 13044.92 78.24 o 2 2 1 5045.93 4420.73 35.14 o 4 2 1 9778.66 8583.05 51.48 o 5 2 1 211.38 214.53 3.82 o 6 2 1 6310.43 6408.86 33.67 o 7 2 1 4530.02 4600.38 44.95 o 8 2 1 3.61 -0.65 2.38 o 9 2 1 335.63 375.16 19.74 o 10 2 1 1757.79 1887.67 23.61 o 11 2 1 321.38 343.50 11.22 o 12 2 1 5452.93 5728.15 58.88 o 13 2 1 1616.86 1758.09 34.18 o 14 2 1 0.15 -0.10 10.78 o 15 2 1 247.05 244.70 28.83 o 16 2 1 159.05 160.54 18.51 o -16 3 1 270.51 246.00 35.77 o -15 3 1 27.09 31.51 14.58 o -14 3 1 1458.55 1478.42 38.86 o -13 3 1 572.90 541.20 19.60 o -12 3 1 33.37 21.54 12.21 o -11 3 1 145.11 126.54 23.09 o -10 3 1 7774.44 8232.76 160.99 o -9 3 1 6169.89 6172.72 98.80 o -8 3 1 6321.85 5623.50 72.05 o -7 3 1 1035.86 1009.61 17.55 o -6 3 1 204.24 168.79 6.07 o -5 3 1 446.64 539.94 13.97 o -4 3 1 10154.88 9166.54 84.74 o -3 3 1 3010.61 3061.10 41.52 o -2 3 1 74.02 71.97 5.51 o -1 3 1 12607.39 11496.24 56.48 o 1 3 1 6666.97 6449.69 47.19 o 2 3 1 7021.20 7003.27 50.57 o 3 3 1 45.76 67.78 3.88 o 4 3 1 1689.22 1614.83 22.91 o 5 3 1 3394.22 3453.76 31.81 o 6 3 1 3303.23 3087.62 44.26 o 7 3 1 4006.07 4203.27 71.05 o 8 3 1 8409.30 8327.86 147.48 o 9 3 1 2891.67 2826.21 48.84 o 10 3 1 7673.49 7799.21 180.29 o 11 3 1 1472.13 1574.30 28.86 o 12 3 1 193.90 200.96 16.59 o 13 3 1 32.49 37.32 14.81 o 14 3 1 2618.32 2766.04 62.17 o 15 3 1 165.97 132.27 36.90 o 16 3 1 11.84 7.30 6.44 o -16 4 1 273.87 276.04 25.80 o -15 4 1 1890.77 1969.35 58.65 o -14 4 1 455.80 467.99 22.49 o -13 4 1 238.84 246.48 22.81 o -12 4 1 11.21 7.97 5.52 o -11 4 1 7011.85 7277.90 262.59 o -10 4 1 46.83 46.92 13.57 o -9 4 1 3082.70 3224.35 61.78 o -8 4 1 9.59 13.53 3.92 o -7 4 1 3958.75 3824.35 93.11 o -6 4 1 0.78 1.45 3.76 o -5 4 1 7328.11 6996.14 36.60 o -4 4 1 1679.20 1740.69 12.79 o -3 4 1 17994.25 16006.14 67.59 o -2 4 1 8610.39 7845.09 35.97 o -1 4 1 2005.72 2182.13 97.41 o 0 4 1 8943.95 8275.88 38.30 o 1 4 1 421.47 463.20 12.69 o 2 4 1 27328.57 24952.37 205.16 o 3 4 1 6621.28 5879.15 35.00 o 4 4 1 587.24 592.57 7.88 o 5 4 1 111.60 120.95 3.66 o 6 4 1 33.68 30.19 3.35 o 7 4 1 9811.77 9523.62 75.71 o 8 4 1 22.63 24.18 6.38 o 9 4 1 141.85 99.26 14.85 o 10 4 1 169.30 173.03 26.79 o 11 4 1 5012.62 5361.10 73.72 o 12 4 1 1204.38 1177.32 24.81 o 13 4 1 1319.53 1527.33 30.11 o 14 4 1 7.61 8.90 10.07 o 15 4 1 202.42 191.87 26.19 o 16 4 1 19.27 12.87 8.68 o -16 5 1 412.65 364.68 20.43 o -15 5 1 18.78 16.12 12.34 o -14 5 1 237.43 245.86 27.37 o -13 5 1 1227.98 1303.55 54.26 o -12 5 1 329.99 333.68 16.60 o -11 5 1 16.70 20.80 9.34 o -10 5 1 8093.88 8169.95 143.83 o -9 5 1 678.85 611.38 17.76 o 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