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Information card for entry 2240229
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| Coordinates | 2240229.cif |
|---|---|
| Structure factors | 2240229.hkl |
| Original IUCr paper | HTML |
| Chemical name | Tricarbonyl(<i>N</i>-diphenylphosphanyl-<i>N</i>,<i>N</i>'-diisopropyl-<i>P</i>-phenylphosphonous diamide-κ^2^<i>P</i>,<i>P</i>')cobalt(I) tetracarbonylcobaltate(-I) toluene 0.25-solvate |
|---|---|
| Formula | C32.75 H32 Co2 N2 O7 P2 |
| Calculated formula | C32.75 H32 Co2 N2 O7 P2 |
| Title of publication | Crystal structure of tricarbonyl(<i>N</i>-diphenylphosphanyl-<i>N</i>,<i>N</i>'-diisopropyl-<i>P</i>-phenylphosphonous diamide-κ^2^<i>P</i>,<i>P</i>')cobalt(I) tetracarbonylcobaltate({-}I) toluene 0.25-solvate |
| Authors of publication | Dura, Laura; Spannenberg, Anke; Beweries, Torsten |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2014 |
| Journal volume | 70 |
| Journal issue | 12 |
| Pages of publication | 533 - 535 |
| a | 22.1602 ± 0.0006 Å |
| b | 12.973 ± 0.0003 Å |
| c | 24.7883 ± 0.0006 Å |
| α | 90° |
| β | 103.933 ± 0.0012° |
| γ | 90° |
| Cell volume | 6916.6 ± 0.3 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0431 |
| Residual factor for significantly intense reflections | 0.0381 |
| Weighted residual factors for significantly intense reflections | 0.0964 |
| Weighted residual factors for all reflections included in the refinement | 0.0997 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.031 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181902 (current) | 2016-04-06 | hkl/2/24/ (antanas@echidna) Adding IUCr specific svn headers to multiple entries in subrange 2/24/02 |
2240229.cif 2240229.hkl |
| 181322 | 2016-04-03 | hkl/2/24/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/24/02. |
2240229.cif 2240229.hkl |
| 176809 | 2016-02-21 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 2. |
2240229.cif 2240229.hkl |
| 127504 | 2014-11-19 | cif/ hkl/ Adding structures of 2240229 via cif-deposit CGI script. |
2240229.cif 2240229.hkl |
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Users of the data should acknowledge the original authors of the
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