data_2240252 _cell_angle_alpha 90.000 _cell_angle_beta 90.821 _cell_angle_gamma 90.000 _cell_length_a 12.9099 _cell_length_b 14.8050 _cell_length_c 14.7933 _exptl_crystal_F_000 2116.00 _reflns_d_resolution_high 0.7724 _[local]_cod_data_source_file wm5083Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' import in P 1 21/n 1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 629.17 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 35073.53 35208.42 1136.49 o 6 0 0 80307.35 96267.90 4007.73 o 8 0 0 3629.48 3517.85 251.31 o 10 0 0 37210.87 39798.59 2226.44 o 12 0 0 2303.87 4006.49 518.83 o 14 0 0 4399.97 4484.36 458.57 o 16 0 0 15.32 175.13 76.46 o 2 1 0 9142.20 8979.05 939.75 o 3 1 0 33.56 221.85 22.77 o 4 1 0 67162.38 66435.02 4936.03 o 5 1 0 2886.58 2281.52 167.35 o 6 1 0 14707.84 15668.34 844.50 o 7 1 0 8802.60 8426.92 587.30 o 8 1 0 44443.59 48233.36 1960.57 o 9 1 0 213.34 282.86 57.13 o 10 1 0 5084.69 5348.08 347.14 o 11 1 0 4604.44 5783.67 203.74 o 12 1 0 242.01 258.54 93.30 o 13 1 0 288.44 154.88 22.12 o 14 1 0 1779.02 1733.49 129.28 o 15 1 0 1240.38 1256.91 81.12 o 16 1 0 628.17 768.39 65.49 o 2 2 0 79982.57 79099.33 5459.19 o 3 2 0 116.85 259.30 22.02 o 4 2 0 11596.57 10591.71 707.32 o 5 2 0 7893.64 7788.48 387.03 o 6 2 0 89195.19 100326.85 8134.60 o 7 2 0 1887.18 2402.33 155.58 o 8 2 0 2111.55 1987.54 140.92 o 9 2 0 7756.86 8171.63 504.93 o 10 2 0 4271.18 3775.65 251.54 o 11 2 0 83.54 332.60 56.32 o 12 2 0 7673.67 8073.52 612.67 o 13 2 0 1618.46 1722.59 119.66 o 14 2 0 154.44 365.30 24.92 o 15 2 0 13.84 -14.83 44.93 o 16 2 0 4791.42 4244.31 267.52 o 1 3 0 56687.96 55320.14 2825.52 o 2 3 0 2462.34 2359.97 143.07 o 3 3 0 197873.09 204312.38 7576.08 o 4 3 0 28090.53 29985.16 1782.36 o 5 3 0 6760.55 8026.22 499.91 o 6 3 0 15188.76 15053.36 1242.70 o 7 3 0 25610.70 27697.03 1649.48 o 8 3 0 11883.05 13081.37 760.59 o 9 3 0 9715.04 12996.55 769.80 o 10 3 0 14669.49 15772.77 616.63 o 11 3 0 1467.61 2259.08 83.95 o 12 3 0 3719.66 3630.55 259.85 o 13 3 0 1965.26 2813.98 132.16 o 14 3 0 292.95 237.32 27.89 o 15 3 0 3770.25 4675.87 197.56 o 16 3 0 3.06 46.91 54.25 o 0 4 0 213260.06 197285.39 6354.54 o 1 4 0 106409.35 119536.23 3626.18 o 2 4 0 29463.47 32121.85 1441.99 o 3 4 0 38084.90 37240.89 3427.04 o 4 4 0 72815.67 79208.70 5169.46 o 5 4 0 15657.76 17989.03 677.34 o 6 4 0 6632.60 6450.71 407.95 o 7 4 0 4632.76 4578.50 376.73 o 8 4 0 41.17 299.56 67.67 o 9 4 0 10266.38 9555.66 907.76 o 10 4 0 13594.11 14461.90 1009.40 o 11 4 0 5732.91 6388.30 637.55 o 12 4 0 84.76 153.91 40.54 o 13 4 0 1775.44 2313.81 122.56 o 14 4 0 3896.55 4238.63 309.34 o 15 4 0 150.07 189.52 34.62 o 16 4 0 742.92 615.51 61.66 o 1 5 0 789.58 449.36 41.45 o 2 5 0 7649.03 4679.11 318.22 o 3 5 0 42416.62 42916.29 2362.78 o 4 5 0 12624.62 9935.74 601.02 o 5 5 0 3796.59 3285.54 145.54 o 6 5 0 31081.45 30201.77 1682.31 o 7 5 0 52126.80 54351.38 2777.25 o 8 5 0 546.82 175.62 28.57 o 9 5 0 1507.31 1360.99 48.73 o 10 5 0 2909.87 2973.01 162.46 o 11 5 0 11956.97 15526.33 1015.05 o 12 5 0 31.18 98.11 57.68 o 13 5 0 146.86 65.28 45.79 o 14 5 0 404.22 364.35 34.94 o 15 5 0 724.32 850.55 63.63 o 16 5 0 180.31 92.60 53.60 o 0 6 0 76405.08 73074.64 3955.18 o 1 6 0 17049.81 14464.78 745.90 o 2 6 0 245288.98 265554.78 11576.89 o 3 6 0 10783.41 9670.09 666.01 o 4 6 0 82109.63 84993.32 4789.37 o 5 6 0 8255.19 7915.10 392.35 o 6 6 0 59252.50 60760.33 2446.73 o 7 6 0 15513.75 15171.70 587.99 o 8 6 0 7916.02 7922.83 440.69 o 9 6 0 48.35 6.12 43.89 o 10 6 0 3787.59 3672.79 157.62 o 11 6 0 13.03 -36.95 36.95 o 12 6 0 993.42 813.26 90.34 o 13 6 0 1137.58 1350.46 154.21 o 14 6 0 215.03 293.41 37.95 o 15 6 0 2030.08 1950.33 128.19 o 1 7 0 14951.31 15327.84 652.85 o 2 7 0 1541.24 1419.41 91.92 o 3 7 0 7547.32 7233.49 556.90 o 4 7 0 4974.67 5490.50 292.25 o 5 7 0 34991.66 31776.09 1623.44 o 6 7 0 0.54 -32.05 32.05 o 7 7 0 20279.54 20075.51 626.15 o 8 7 0 364.23 338.02 40.31 o 9 7 0 10202.70 11659.39 432.85 o 10 7 0 1477.25 1256.11 54.26 o 11 7 0 240.05 322.51 43.12 o 12 7 0 1367.06 1745.62 119.27 o 13 7 0 819.30 902.68 50.40 o 14 7 0 687.98 524.47 59.41 o 15 7 0 13.12 59.38 39.83 o 0 8 0 7337.53 9407.36 224.41 o 1 8 0 79662.43 77438.01 3762.52 o 2 8 0 27945.61 27856.88 1560.02 o 3 8 0 53553.96 47650.42 3478.18 o 4 8 0 9976.10 9560.05 522.95 o 5 8 0 840.55 736.66 44.16 o 6 8 0 990.18 1212.79 43.41 o 7 8 0 37.72 58.64 63.47 o 8 8 0 4364.03 3875.16 100.79 o 9 8 0 8194.52 8628.74 444.30 o 10 8 0 2283.87 1863.90 184.45 o 11 8 0 3854.18 4078.10 173.45 o 12 8 0 3192.51 3043.38 80.14 o 13 8 0 1125.25 1574.38 79.39 o 14 8 0 664.52 393.91 48.02 o 15 8 0 669.70 715.29 55.04 o 1 9 0 39765.86 40227.44 2365.45 o 2 9 0 1686.53 1569.00 117.19 o 3 9 0 2336.34 3073.54 79.44 o 4 9 0 3112.09 3079.21 251.98 o 5 9 0 31659.18 28501.31 1081.69 o 6 9 0 181.73 244.54 42.69 o 7 9 0 7635.84 8362.31 446.53 o 8 9 0 6.35 -24.65 27.36 o 9 9 0 799.76 675.96 38.60 o 10 9 0 183.06 361.73 63.09 o 11 9 0 7734.08 9705.25 289.91 o 12 9 0 335.04 359.40 37.98 o 13 9 0 1312.62 1761.68 98.51 o 14 9 0 364.08 442.84 58.23 o 0 10 0 22379.12 22165.74 2748.47 o 1 10 0 1961.80 1911.83 117.21 o 2 10 0 16931.26 16587.73 933.56 o 3 10 0 21153.80 19183.93 691.35 o 4 10 0 16611.28 17402.79 721.26 o 5 10 0 3789.60 3464.83 205.80 o 6 10 0 3735.14 3737.29 248.78 o 7 10 0 4172.57 3683.51 150.73 o 8 10 0 11062.66 13192.18 921.00 o 9 10 0 79.92 114.79 31.96 o 10 10 0 3339.83 3971.53 120.51 o 11 10 0 215.60 359.12 41.50 o 12 10 0 2392.33 2551.39 137.13 o 13 10 0 156.92 58.62 34.34 o 14 10 0 2039.39 2100.20 158.90 o 1 11 0 7567.30 7120.07 546.09 o 2 11 0 16446.82 16276.41 855.79 o 3 11 0 2835.93 2825.37 85.25 o 4 11 0 713.04 599.02 45.74 o 5 11 0 7110.72 6147.44 129.67 o 6 11 0 14753.38 14947.70 819.81 o 7 11 0 321.75 430.11 54.14 o 8 11 0 393.82 326.51 43.12 o 9 11 0 5236.94 5563.39 268.57 o 10 11 0 690.02 1081.67 78.59 o 11 11 0 524.12 323.69 60.96 o 12 11 0 349.33 328.57 45.30 o 13 11 0 1786.48 1989.14 148.06 o 0 12 0 8899.08 11624.44 1194.16 o 1 12 0 11291.27 12022.12 702.80 o 2 12 0 72752.38 79659.13 4210.07 o 3 12 0 5552.38 5105.80 296.22 o 4 12 0 11111.56 10575.82 433.32 o 5 12 0 300.07 353.66 38.04 o 6 12 0 9964.29 9314.37 465.86 o 7 12 0 14.67 48.35 38.40 o 8 12 0 8708.75 8477.93 379.58 o 9 12 0 188.02 194.72 39.38 o 10 12 0 1249.46 1694.86 105.07 o 11 12 0 712.78 540.12 66.48 o 12 12 0 382.39 198.14 44.19 o 1 13 0 438.78 758.62 88.40 o 2 13 0 1213.46 1491.42 123.28 o 3 13 0 3984.19 4269.88 202.69 o 4 13 0 34.67 55.35 33.96 o 5 13 0 1610.26 1901.60 95.58 o 6 13 0 2237.59 2016.42 126.97 o 7 13 0 5579.34 5103.52 167.14 o 8 13 0 445.60 536.26 44.19 o 9 13 0 19.09 4.43 40.54 o 10 13 0 926.21 641.15 55.39 o 11 13 0 34.09 10.76 51.47 o 12 13 0 501.30 542.94 50.78 o 0 14 0 2566.18 3217.31 235.59 o 1 14 0 1924.57 2110.65 149.88 o 2 14 0 461.52 580.30 39.93 o 3 14 0 75.82 34.58 36.59 o 4 14 0 2953.57 3043.16 220.97 o 5 14 0 1940.81 1991.50 128.98 o 6 14 0 110.32 138.66 36.89 o 7 14 0 191.23 164.42 38.71 o 8 14 0 4139.74 3662.67 131.23 o 9 14 0 631.74 601.93 71.34 o 10 14 0 75.25 44.88 40.15 o 11 14 0 156.60 194.74 53.62 o 1 15 0 3464.59 4065.16 277.84 o 2 15 0 33.92 0.84 34.59 o 3 15 0 35.70 110.86 38.86 o 4 15 0 1466.17 1417.48 81.35 o 5 15 0 1717.66 1543.94 59.11 o 6 15 0 2100.54 2018.04 102.67 o 7 15 0 703.22 601.89 44.01 o 8 15 0 700.70 653.97 63.45 o 9 15 0 1314.52 1355.73 78.62 o 10 15 0 216.00 154.46 53.16 o 0 16 0 17.55 155.97 44.24 o 1 16 0 175.09 187.55 33.05 o 2 16 0 13894.29 17197.85 1151.06 o 3 16 0 37.01 58.39 48.87 o 4 16 0 633.12 779.24 90.34 o 5 16 0 741.68 662.30 50.25 o 6 16 0 1415.18 1416.46 106.77 o 7 16 0 70.53 40.15 36.82 o 8 16 0 4172.60 4031.32 247.07 o 9 16 0 524.95 441.70 105.98 o 1 17 0 592.39 679.28 73.23 o 2 17 0 51.37 119.19 44.93 o 3 17 0 2607.42 2812.65 237.46 o 4 17 0 3688.05 3995.13 295.70 o 5 17 0 1.65 -42.91 42.91 o 6 17 0 13.03 54.74 47.40 o 7 17 0 618.80 679.12 73.03 o 0 18 0 7157.61 8868.71 896.41 o 1 18 0 98.07 74.41 40.98 o 2 18 0 5909.99 6417.19 465.27 o 3 18 0 142.36 158.99 67.95 o 4 18 0 5319.33 5559.01 391.19 o 5 18 0 132.38 134.48 60.46 o 1 19 0 42.39 75.89 84.79 o 2 19 0 78.65 15.17 80.97 o -15 0 1 10.99 -5.10 111.72 o -13 0 1 4775.40 5817.54 978.46 o -11 0 1 1045.78 1316.07 94.42 o -9 0 1 4383.64 6444.30 458.03 o -7 0 1 19976.80 19202.28 1764.17 o -5 0 1 1227.64 1566.13 67.81 o -3 0 1 4587.86 3840.88 131.48 o 3 0 1 357.34 1122.18 45.56 o 5 0 1 3345.71 3435.29 816.44 o 7 0 1 13483.61 12909.49 881.34 o 9 0 1 433.63 1140.26 196.17 o 11 0 1 505.00 548.28 50.51 o 13 0 1 4007.80 4229.90 133.16 o 15 0 1 33.60 -2.19 105.60 o -16 1 1 437.06 517.09 75.96 o -15 1 1 6.16 58.76 57.38 o -14 1 1 23.16 35.69 65.91 o -13 1 1 12.51 28.67 59.18 o -12 1 1 364.69 348.95 61.21 o -11 1 1 1081.11 1339.40 126.10 o -10 1 1 2834.63 4383.32 109.76 o -9 1 1 10826.20 12837.03 721.37 o -8 1 1 2475.81 3627.03 332.19 o -7 1 1 16359.21 17787.04 651.54 o -6 1 1 6646.35 7587.22 316.90 o -5 1 1 8468.71 7606.76 216.77 o -4 1 1 524.76 3258.46 133.66 o -3 1 1 14277.46 12624.00 372.40 o -2 1 1 11474.04 9187.74 332.91 o 2 1 1 19526.13 16023.27 1419.88 o 3 1 1 16163.06 14928.85 953.99 o 4 1 1 15574.51 19090.99 1232.20 o 5 1 1 6799.41 7238.77 232.59 o 6 1 1 1061.21 2239.22 132.39 o 7 1 1 13954.19 14160.27 572.70 o 8 1 1 12838.36 11370.07 590.20 o 9 1 1 12202.21 13049.78 470.17 o 10 1 1 1240.69 1569.55 46.55 o 11 1 1 269.14 499.67 49.86 o 12 1 1 1101.52 946.21 75.47 o 13 1 1 52.93 116.57 31.12 o 14 1 1 152.26 200.58 55.40 o 15 1 1 100.44 76.12 19.70 o 16 1 1 328.89 260.27 69.12 o -16 2 1 125.60 192.16 77.02 o -15 2 1 2750.32 2264.95 149.39 o -14 2 1 9.57 -43.44 56.37 o -13 2 1 103.21 103.62 26.62 o -12 2 1 17.10 88.86 38.18 o -11 2 1 8158.65 9409.91 452.76 o -10 2 1 5880.76 7029.33 489.27 o -9 2 1 8571.67 7850.37 636.70 o -8 2 1 9032.49 10453.09 457.32 o -7 2 1 10569.83 13922.12 730.04 o -6 2 1 6974.60 7763.00 323.25 o -5 2 1 39231.07 40887.55 906.34 o -4 2 1 10786.71 8541.22 226.72 o -3 2 1 11939.27 13263.87 234.56 o -2 2 1 1957.22 1830.42 41.19 o -1 2 1 41202.68 33101.75 1127.66 o 1 2 1 46531.83 36282.33 8758.72 o 2 2 1 434.18 709.06 44.42 o 3 2 1 35862.53 39291.85 2598.86 o 4 2 1 8309.46 7766.65 460.42 o 5 2 1 57321.93 52331.96 3766.61 o 6 2 1 5187.59 6371.57 217.80 o 7 2 1 28139.84 31042.01 1303.99 o 8 2 1 6635.87 6745.35 184.44 o 9 2 1 10642.80 11945.32 736.71 o 10 2 1 6820.23 7261.38 271.99 o 11 2 1 12072.64 11963.58 652.48 o 12 2 1 209.18 228.12 35.63 o 13 2 1 125.95 89.04 59.97 o 14 2 1 14.47 83.85 71.96 o 15 2 1 2257.36 1992.79 71.55 o 16 2 1 182.22 77.98 45.99 o -16 3 1 2965.78 3130.07 207.37 o -15 3 1 118.28 73.55 54.81 o -14 3 1 2709.28 3136.04 205.85 o -13 3 1 0.81 57.21 40.64 o -12 3 1 4563.27 6283.93 294.16 o -11 3 1 1748.19 2056.66 63.28 o -10 3 1 23190.38 29157.46 2684.33 o -9 3 1 8964.78 9392.90 440.32 o -8 3 1 3139.89 3669.36 93.08 o -7 3 1 5218.71 5218.46 232.22 o -6 3 1 33836.89 32389.24 1558.31 o -5 3 1 617.69 1013.43 56.62 o -4 3 1 7135.86 5340.97 147.52 o -3 3 1 8.72 54.68 15.12 o -2 3 1 169.16 996.13 162.46 o -1 3 1 3379.23 2547.21 133.02 o 0 3 1 11811.17 9724.59 697.72 o 1 3 1 2504.19 2465.20 248.18 o 2 3 1 5401.99 4593.80 499.98 o 3 3 1 187.62 187.36 29.98 o 4 3 1 2761.45 3084.97 229.95 o 5 3 1 3432.26 3503.84 167.23 o 6 3 1 8011.62 11414.47 711.95 o 7 3 1 2641.57 3140.21 203.39 o 8 3 1 845.19 1306.80 77.33 o 9 3 1 4699.69 5192.73 378.42 o 10 3 1 13839.17 15858.74 878.89 o 11 3 1 848.75 1144.16 65.56 o 12 3 1 2979.64 3172.30 154.12 o 13 3 1 147.61 151.48 25.82 o 14 3 1 2317.54 2623.34 172.22 o 15 3 1 254.84 202.04 40.50 o 16 3 1 2158.01 1866.61 102.94 o -16 4 1 9.56 27.06 61.91 o -15 4 1 1765.87 1577.04 79.80 o -14 4 1 85.03 63.33 36.15 o -13 4 1 598.17 434.89 34.31 o -12 4 1 2312.55 2874.37 132.69 o -11 4 1 4328.36 4038.27 150.60 o -10 4 1 773.04 987.58 100.43 o -9 4 1 4103.93 3935.64 252.91 o -8 4 1 1473.87 1687.68 109.55 o -7 4 1 2244.88 2281.31 89.00 o -6 4 1 33365.83 31664.70 1013.99 o -5 4 1 33970.67 37155.56 672.90 o -4 4 1 623.67 1404.07 65.80 o -3 4 1 18306.74 18387.08 1281.60 o -2 4 1 21858.50 19044.83 1324.91 o -1 4 1 24395.37 29931.21 1381.87 o 0 4 1 2626.42 2965.23 326.84 o 1 4 1 68943.42 71370.95 6996.74 o 2 4 1 10913.98 11622.26 944.70 o 3 4 1 13850.34 15040.16 756.31 o 4 4 1 1766.23 2449.82 175.48 o 5 4 1 76287.68 73764.95 5245.33 o 6 4 1 37168.65 42181.65 1929.73 o 7 4 1 4505.27 4653.40 242.96 o 8 4 1 879.90 1131.34 56.67 o 9 4 1 7263.89 6994.77 383.46 o 10 4 1 2303.32 2437.50 67.71 o 11 4 1 6376.00 5855.31 317.45 o 12 4 1 1623.39 1728.40 75.24 o 13 4 1 283.05 259.70 37.00 o 14 4 1 30.92 53.06 33.82 o 15 4 1 2201.54 1972.27 82.54 o 16 4 1 15.00 23.38 67.01 o -16 5 1 142.11 59.73 47.92 o -15 5 1 856.58 676.30 74.29 o -14 5 1 175.66 110.76 44.30 o -13 5 1 265.91 322.92 38.65 o -12 5 1 676.43 567.71 40.49 o -11 5 1 2598.74 3439.96 256.13 o -10 5 1 45.60 212.36 41.35 o -9 5 1 391.70 495.12 33.03 o -8 5 1 1677.18 2712.98 111.39 o -7 5 1 14551.92 15109.17 690.20 o -6 5 1 56.69 250.50 30.78 o -5 5 1 10915.83 8964.73 285.69 o -4 5 1 1042.14 1709.71 138.08 o -3 5 1 831.85 1238.71 55.07 o -2 5 1 22481.45 21446.99 721.22 o -1 5 1 9226.54 7215.71 375.55 o 0 5 1 21575.33 23646.38 3272.58 o 1 5 1 2277.64 2384.64 136.09 o 2 5 1 31346.98 29429.84 2444.29 o 3 5 1 15.20 565.66 40.31 o 4 5 1 3064.26 2245.04 253.24 o 5 5 1 3350.87 4242.16 351.78 o 6 5 1 1409.62 1497.28 81.47 o 7 5 1 26153.72 26320.32 1392.56 o 8 5 1 9317.58 9925.61 420.05 o 9 5 1 227.23 519.52 37.02 o 10 5 1 217.05 455.56 56.68 o 11 5 1 6302.47 6469.54 297.30 o 12 5 1 1471.50 1306.44 102.08 o 13 5 1 31.59 23.95 48.28 o 14 5 1 542.67 566.85 40.26 o 15 5 1 579.14 581.18 73.58 o 16 5 1 121.66 226.94 53.47 o -15 6 1 67.13 125.27 36.20 o -14 6 1 1456.90 1608.31 123.56 o -13 6 1 2137.96 2513.27 131.27 o -12 6 1 342.68 440.66 41.53 o -11 6 1 55.95 201.76 41.77 o -10 6 1 981.47 1483.35 94.30 o -9 6 1 2874.51 3019.90 141.23 o -8 6 1 89.71 155.26 31.47 o -7 6 1 1118.96 1171.96 63.13 o -6 6 1 928.29 1116.42 59.35 o -5 6 1 3577.37 4060.57 155.63 o -4 6 1 9918.72 8990.24 400.21 o -3 6 1 1264.48 3636.13 181.49 o -2 6 1 293.55 519.29 46.77 o -1 6 1 17004.21 17866.46 1281.78 o 0 6 1 24.26 112.64 16.12 o 1 6 1 4521.97 5805.57 548.91 o 2 6 1 356.97 686.81 70.85 o 3 6 1 20312.03 18874.39 2146.60 o 4 6 1 6413.53 7383.86 365.75 o 5 6 1 4912.48 5365.21 283.01 o 6 6 1 976.61 1797.62 80.23 o 7 6 1 434.06 751.22 38.56 o 8 6 1 335.54 311.26 29.61 o 9 6 1 911.62 1018.48 46.82 o 10 6 1 1348.62 1710.13 48.49 o 11 6 1 205.15 240.05 43.57 o 12 6 1 913.21 773.11 49.22 o 13 6 1 1014.64 1115.77 68.36 o 14 6 1 1564.16 1913.40 158.89 o 15 6 1 404.63 349.08 38.56 o -15 7 1 106.65 204.83 38.18 o -14 7 1 18.39 -11.48 33.62 o -13 7 1 846.00 777.12 55.11 o -12 7 1 120.82 508.66 78.14 o -11 7 1 345.92 494.72 50.22 o -10 7 1 464.65 817.76 45.26 o -9 7 1 16688.51 17032.53 959.56 o -8 7 1 16.08 399.31 37.61 o -7 7 1 1549.81 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