data_2240337 _cell_angle_alpha 90.000 _cell_angle_beta 102.360 _cell_angle_gamma 90.000 _cell_length_a 12.0578 _cell_length_b 14.5824 _cell_length_c 22.2754 _exptl_crystal_F_000 1632.00 _reflns_d_resolution_high 0.7438 _cod_data_source_file nk2228Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Mes_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 365.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 133826.81 126836.44 2164.18 o 2 0 0 11344.62 10508.84 151.77 o 3 0 0 90619.54 86239.58 1439.82 o 4 0 0 690.33 1106.32 33.41 o 5 0 0 2966.17 3830.94 72.64 o 6 0 0 16672.09 17057.16 292.95 o 7 0 0 199.30 233.77 18.63 o 8 0 0 67.31 147.30 33.41 o 9 0 0 25.54 101.52 32.13 o 10 0 0 420.88 642.84 116.94 o 11 0 0 1829.79 1929.74 56.73 o 12 0 0 942.36 1013.34 70.04 o 13 0 0 920.61 1056.33 59.11 o 14 0 0 1331.11 1445.71 71.96 o 15 0 0 362.06 343.11 46.26 o 1 1 0 1288.34 1278.24 26.45 o 2 1 0 13340.53 13116.57 182.09 o 3 1 0 20848.46 20221.37 246.18 o 4 1 0 3237.48 2918.44 35.92 o 5 1 0 5619.59 5037.60 73.21 o 6 1 0 12551.11 11938.20 147.50 o 7 1 0 11366.61 11147.21 140.03 o 8 1 0 5572.34 5343.53 73.86 o 9 1 0 3338.98 3054.44 48.99 o 10 1 0 4564.28 4574.27 76.45 o 11 1 0 1514.79 1583.31 48.49 o 12 1 0 1100.60 1145.35 36.36 o 13 1 0 671.60 744.85 32.76 o 14 1 0 67.71 122.89 26.35 o 15 1 0 2.19 -16.06 25.44 o 0 2 0 60886.66 63258.97 1440.57 o 1 2 0 1904.50 1906.46 34.07 o 2 2 0 3318.28 3167.79 41.69 o 3 2 0 903.51 733.17 13.92 o 4 2 0 949.41 1097.06 18.43 o 5 2 0 1998.29 1732.87 26.96 o 6 2 0 7317.07 7099.55 91.95 o 7 2 0 44.06 50.54 10.06 o 8 2 0 23.84 30.15 11.21 o 9 2 0 70.93 60.66 13.09 o 10 2 0 7.31 25.87 14.40 o 11 2 0 5.13 -7.00 15.51 o 12 2 0 8.50 9.63 17.82 o 13 2 0 17.39 7.71 24.70 o 14 2 0 7.25 1.21 21.47 o 15 2 0 1.72 14.14 37.27 o 1 3 0 16232.17 16637.15 268.51 o 2 3 0 375.77 346.80 11.01 o 3 3 0 150.86 96.12 8.72 o 4 3 0 3926.33 3245.65 44.53 o 5 3 0 7209.07 6407.33 83.33 o 6 3 0 8020.74 7869.84 101.51 o 7 3 0 22398.45 21307.33 294.11 o 8 3 0 18679.99 18209.99 254.13 o 9 3 0 11139.01 11514.93 167.19 o 10 3 0 7499.62 7227.59 117.44 o 11 3 0 3008.73 3066.07 64.24 o 12 3 0 1064.75 1190.51 37.48 o 13 3 0 350.91 420.07 28.44 o 14 3 0 322.22 306.92 39.84 o 15 3 0 49.92 43.69 39.84 o 0 4 0 97994.44 100664.86 2287.43 o 1 4 0 31076.96 31299.20 502.05 o 2 4 0 20575.32 20617.27 336.72 o 3 4 0 16136.92 15350.15 251.41 o 4 4 0 3352.00 2918.61 41.63 o 5 4 0 3904.46 3691.46 51.48 o 6 4 0 5524.10 5480.38 73.58 o 7 4 0 2609.11 2519.52 45.07 o 8 4 0 445.76 461.93 20.13 o 9 4 0 24.42 19.43 12.87 o 10 4 0 2607.10 2500.73 50.25 o 11 4 0 1359.44 1343.68 65.85 o 12 4 0 524.38 547.75 42.48 o 13 4 0 679.52 671.06 87.38 o 14 4 0 437.14 381.49 37.28 o 1 5 0 638.93 661.17 19.02 o 2 5 0 1510.89 1693.45 31.11 o 3 5 0 2577.86 2734.36 45.41 o 4 5 0 56.43 62.06 7.37 o 5 5 0 873.20 891.13 19.88 o 6 5 0 1385.53 1390.68 26.18 o 7 5 0 584.07 531.56 31.09 o 8 5 0 233.81 221.39 20.68 o 9 5 0 519.23 476.23 21.01 o 10 5 0 16.42 -1.98 14.26 o 11 5 0 0.44 -15.77 15.77 o 12 5 0 79.84 86.53 26.54 o 13 5 0 0.77 -22.87 25.88 o 14 5 0 28.31 22.33 29.23 o 0 6 0 11249.85 10933.40 255.73 o 1 6 0 23296.54 22668.68 520.45 o 2 6 0 14976.36 14722.11 228.31 o 3 6 0 9035.59 8867.11 135.42 o 4 6 0 2948.94 2654.88 46.17 o 5 6 0 3780.20 3510.64 51.32 o 6 6 0 3827.05 3688.44 54.16 o 7 6 0 3894.15 3806.75 63.51 o 8 6 0 1189.34 1229.99 31.39 o 9 6 0 1279.95 1113.68 31.28 o 10 6 0 70.09 99.98 17.16 o 11 6 0 3.46 14.73 22.50 o 12 6 0 512.11 514.08 36.73 o 13 6 0 599.47 556.50 54.62 o 14 6 0 348.89 432.19 87.38 o 1 7 0 510.02 542.41 19.99 o 2 7 0 1317.39 1314.65 28.67 o 3 7 0 1812.86 1545.38 31.89 o 4 7 0 5508.75 5301.59 83.09 o 5 7 0 12992.11 13091.51 167.26 o 6 7 0 5741.19 5580.38 77.67 o 7 7 0 10008.04 9755.50 143.01 o 8 7 0 6662.39 6379.69 99.09 o 9 7 0 3658.92 3664.14 64.78 o 10 7 0 2303.92 2360.07 64.04 o 11 7 0 2410.88 2329.72 66.23 o 12 7 0 953.48 971.85 70.68 o 13 7 0 291.35 352.86 35.20 o 0 8 0 9428.37 9256.38 221.03 o 1 8 0 2159.54 2090.72 44.06 o 2 8 0 2435.38 2341.60 106.66 o 3 8 0 560.45 508.75 19.46 o 4 8 0 5.48 -19.71 25.95 o 5 8 0 6.66 -15.85 15.85 o 6 8 0 145.80 117.64 14.28 o 7 8 0 590.55 477.55 21.96 o 8 8 0 122.03 133.09 22.49 o 9 8 0 2381.21 2353.98 63.30 o 10 8 0 1524.21 1587.74 53.24 o 11 8 0 68.18 60.12 25.01 o 12 8 0 50.06 68.11 27.78 o 13 8 0 90.68 128.54 41.12 o 1 9 0 327.98 329.33 34.05 o 2 9 0 692.26 680.50 24.67 o 3 9 0 3922.72 4100.69 69.24 o 4 9 0 3655.89 3676.34 63.77 o 5 9 0 5102.24 5082.68 103.03 o 6 9 0 3756.75 3695.08 91.29 o 7 9 0 2327.00 2326.69 61.07 o 8 9 0 716.65 702.53 62.33 o 9 9 0 2180.80 2109.91 60.93 o 10 9 0 412.90 470.43 33.63 o 11 9 0 1118.51 1168.97 49.94 o 12 9 0 1214.48 1400.75 71.96 o 13 9 0 120.89 120.60 54.62 o 0 10 0 21830.09 21617.49 502.46 o 1 10 0 22145.60 21836.74 358.47 o 2 10 0 17341.04 17488.48 285.01 o 3 10 0 9637.21 9355.01 184.49 o 4 10 0 3521.62 3302.89 59.99 o 5 10 0 1572.72 1631.88 50.87 o 6 10 0 178.96 129.99 21.30 o 7 10 0 468.76 509.03 52.69 o 8 10 0 210.73 198.97 25.60 o 9 10 0 1.02 -8.25 21.58 o 10 10 0 305.93 335.76 31.79 o 11 10 0 307.99 329.46 33.85 o 12 10 0 1149.04 1279.47 55.79 o 1 11 0 3.24 -11.33 11.33 o 2 11 0 1614.72 1632.18 39.08 o 3 11 0 1639.44 1705.12 53.88 o 4 11 0 3703.69 3727.04 89.38 o 5 11 0 3414.10 3405.30 83.40 o 6 11 0 222.16 246.10 25.61 o 7 11 0 2299.89 2101.09 60.49 o 8 11 0 1140.47 1146.00 47.18 o 9 11 0 168.75 188.61 27.78 o 10 11 0 184.60 169.88 30.19 o 11 11 0 117.76 136.96 49.48 o 12 11 0 96.07 30.43 30.26 o 0 12 0 473.84 696.51 42.41 o 1 12 0 30.60 54.69 13.99 o 2 12 0 1605.83 1681.06 74.53 o 3 12 0 1139.17 1222.70 71.96 o 4 12 0 1956.98 1785.29 58.17 o 5 12 0 2922.21 2682.42 73.44 o 6 12 0 260.46 303.38 28.69 o 7 12 0 619.58 656.54 37.65 o 8 12 0 562.73 558.44 37.05 o 9 12 0 684.51 769.95 43.36 o 10 12 0 883.55 844.24 46.47 o 11 12 0 106.97 78.20 39.84 o 1 13 0 15.81 9.94 20.11 o 2 13 0 217.07 170.75 24.55 o 3 13 0 415.10 431.86 32.13 o 4 13 0 1181.05 1178.24 49.93 o 5 13 0 4434.00 4338.76 104.12 o 6 13 0 2764.89 2780.54 73.78 o 7 13 0 2204.83 2267.55 86.74 o 8 13 0 1257.01 1304.72 53.71 o 9 13 0 1293.41 1405.71 90.60 o 10 13 0 786.73 941.51 59.76 o 11 13 0 266.51 312.27 59.11 o 0 14 0 2141.80 2701.22 158.06 o 1 14 0 1498.09 1619.42 90.41 o 2 14 0 1074.79 1017.59 48.25 o 3 14 0 1877.12 1925.92 85.46 o 4 14 0 842.48 738.24 59.76 o 5 14 0 31.10 9.00 28.27 o 6 14 0 1403.43 1398.73 107.30 o 7 14 0 715.83 667.15 41.37 o 8 14 0 143.68 202.28 31.78 o 9 14 0 112.24 116.07 30.87 o 10 14 0 741.28 917.92 51.96 o 1 15 0 154.67 79.03 52.05 o 2 15 0 488.38 359.65 57.23 o 3 15 0 75.23 62.25 25.88 o 4 15 0 128.20 105.33 28.49 o 5 15 0 177.53 124.65 34.70 o 6 15 0 69.19 66.82 33.41 o 7 15 0 96.19 103.32 35.98 o 8 15 0 40.23 40.97 29.33 o 9 15 0 57.76 56.04 33.41 o 0 16 0 496.59 570.57 96.38 o 1 16 0 1343.57 1370.59 89.84 o 2 16 0 3113.83 3207.99 129.90 o 3 16 0 260.21 347.26 76.46 o 4 16 0 1578.91 1723.02 112.44 o 5 16 0 964.49 1033.65 55.58 o 6 16 0 113.25 101.80 41.56 o 7 16 0 183.82 211.84 31.08 o 8 16 0 460.18 455.33 38.33 o 1 17 0 503.61 401.89 64.50 o 2 17 0 119.59 70.47 55.41 o 3 17 0 738.98 796.72 75.87 o 4 17 0 2268.43 2290.75 220.39 o 5 17 0 1648.40 1863.35 161.92 o 6 17 0 249.46 321.98 52.53 o 7 17 0 153.26 206.57 59.76 o 0 18 0 62.55 191.48 87.38 o 1 18 0 155.12 216.33 62.62 o 2 18 0 43.83 -9.41 56.25 o 3 18 0 48.53 -38.72 56.54 o 2 19 0 32.59 20.56 84.81 o 3 19 0 174.92 154.21 88.67 o -15 1 1 599.14 722.48 122.72 o -14 1 1 1385.10 1498.85 49.98 o -13 1 1 1460.23 1580.75 47.58 o -12 1 1 461.67 506.26 26.64 o -11 1 1 2113.54 1971.39 44.71 o -10 1 1 767.30 738.75 26.41 o -9 1 1 938.42 987.60 32.46 o -8 1 1 1819.33 1644.44 38.26 o -7 1 1 1538.18 1480.64 45.44 o -6 1 1 190.93 217.58 10.41 o -5 1 1 3.39 8.80 5.85 o -4 1 1 8361.98 8126.83 110.55 o -3 1 1 10513.45 10294.53 140.83 o -2 1 1 32967.26 33204.96 467.66 o -1 1 1 31.44 45.45 3.16 o 0 1 1 6497.62 6898.56 186.98 o 1 1 1 5584.20 5562.68 78.17 o 2 1 1 44.91 58.69 5.10 o 3 1 1 7737.11 7902.67 88.58 o 4 1 1 3277.23 3240.97 39.67 o 5 1 1 16480.56 17603.79 195.06 o 6 1 1 641.93 723.11 15.93 o 7 1 1 1.65 10.74 14.65 o 8 1 1 488.24 465.15 20.20 o 9 1 1 6.28 -1.88 10.78 o 10 1 1 2.26 -11.99 11.99 o 11 1 1 348.08 310.26 21.16 o 12 1 1 798.13 855.93 32.76 o 13 1 1 839.45 876.71 35.62 o 14 1 1 113.49 80.08 33.41 o 15 1 1 162.64 145.74 32.77 o -15 2 1 11.49 17.81 42.41 o -14 2 1 205.06 234.66 25.96 o -13 2 1 696.30 676.13 53.66 o -12 2 1 5745.91 5526.76 93.30 o -11 2 1 2609.14 2562.24 51.97 o -10 2 1 1910.94 1883.74 41.26 o -9 2 1 1566.13 1457.09 34.17 o -8 2 1 1390.92 1213.29 29.50 o -7 2 1 6941.89 6924.63 102.39 o -6 2 1 4108.63 3707.28 78.41 o -5 2 1 9642.56 9764.78 137.04 o -4 2 1 7855.90 7961.49 99.91 o -3 2 1 7688.02 7568.78 107.58 o -2 2 1 3217.38 3082.42 70.38 o -1 2 1 12783.69 13032.64 210.36 o 0 2 1 33.99 60.82 7.07 o 1 2 1 51934.12 55260.37 770.91 o 2 2 1 3609.75 3410.40 44.87 o 3 2 1 6440.66 6400.30 80.93 o 4 2 1 0.86 -4.52 4.52 o 5 2 1 906.43 919.04 20.65 o 6 2 1 748.28 878.88 30.57 o 7 2 1 297.65 199.18 12.74 o 8 2 1 8.00 -6.01 13.73 o 9 2 1 169.28 153.72 17.99 o 10 2 1 349.94 368.20 20.32 o 11 2 1 2068.98 1951.53 44.27 o 12 2 1 2313.25 2365.63 51.67 o 13 2 1 608.00 651.50 30.89 o 14 2 1 276.97 319.74 44.47 o 15 2 1 413.23 519.17 52.69 o -15 3 1 3.82 -9.00 37.27 o -14 3 1 3.09 -10.20 21.27 o -13 3 1 2.74 -15.88 21.92 o -12 3 1 216.70 186.57 20.71 o -11 3 1 40.95 40.37 16.40 o -10 3 1 10.87 10.11 13.47 o -9 3 1 168.32 180.76 15.55 o -8 3 1 299.32 203.40 17.79 o -7 3 1 1053.12 983.40 49.90 o -6 3 1 60.78 60.12 9.17 o -5 3 1 3931.36 4595.92 61.11 o -4 3 1 1124.25 1096.88 26.52 o -3 3 1 101.25 85.22 6.18 o -2 3 1 4.07 6.43 5.45 o -1 3 1 1568.16 1689.88 31.80 o 0 3 1 6748.91 6689.90 110.85 o 1 3 1 863.09 794.13 23.94 o 2 3 1 4019.67 4005.72 59.93 o 3 3 1 3461.93 3484.75 46.84 o 4 3 1 604.97 522.71 13.38 o 5 3 1 2863.61 2980.95 42.47 o 6 3 1 823.58 840.89 20.03 o 7 3 1 626.48 507.74 20.87 o 8 3 1 1256.17 1289.84 43.40 o 9 3 1 4.41 -5.01 12.10 o 10 3 1 725.83 703.32 27.20 o 11 3 1 0.91 23.43 19.32 o 12 3 1 81.89 138.73 20.35 o 13 3 1 78.62 117.04 21.80 o 14 3 1 6.66 53.39 35.34 o 15 3 1 27.83 74.53 39.84 o -14 4 1 236.77 252.12 34.20 o -13 4 1 314.65 312.02 25.07 o -12 4 1 572.89 595.03 28.11 o -11 4 1 648.45 667.88 29.04 o -10 4 1 703.51 661.95 31.23 o -9 4 1 2050.60 2078.03 42.73 o -8 4 1 4258.66 4003.60 74.35 o -7 4 1 3205.00 2922.42 50.05 o -6 4 1 3817.42 3564.93 50.42 o -5 4 1 7556.04 7631.64 98.67 o -4 4 1 4960.61 4922.01 65.53 o -3 4 1 3492.07 3170.49 44.32 o -2 4 1 2390.42 2471.63 45.88 o -1 4 1 10314.07 10798.46 176.28 o 0 4 1 66.89 77.65 6.77 o 1 4 1 4.15 2.97 5.02 o 2 4 1 4653.21 4452.23 67.12 o 3 4 1 1246.65 1171.33 43.17 o 4 4 1 497.64 472.79 15.58 o 5 4 1 163.49 225.25 16.69 o 6 4 1 124.80 133.48 9.07 o 7 4 1 38.56 65.41 10.80 o 8 4 1 424.32 393.81 29.85 o 9 4 1 73.29 65.61 29.67 o 10 4 1 1.91 -18.40 18.40 o 11 4 1 1585.05 1421.31 38.85 o 12 4 1 1363.35 1266.74 49.09 o 13 4 1 82.39 36.82 35.34 o 14 4 1 142.58 147.43 35.98 o -14 5 1 1345.58 1395.41 58.66 o -13 5 1 1529.59 1579.07 58.36 o -12 5 1 2100.16 2244.16 51.48 o -11 5 1 1472.17 1575.72 40.63 o -10 5 1 1195.00 1154.11 35.77 o -9 5 1 269.60 240.42 17.28 o -8 5 1 1061.83 995.37 27.46 o -7 5 1 1206.17 1124.11 27.80 o -6 5 1 321.20 282.19 11.90 o -5 5 1 361.58 288.78 12.51 o -4 5 1 2096.61 2048.07 32.64 o -3 5 1 3964.91 3923.74 61.58 o -2 5 1 4914.08 4551.77 79.51 o -1 5 1 14108.79 14096.81 229.90 o 0 5 1 1404.59 1286.80 28.13 o 1 5 1 4.74 -9.20 9.20 o 2 5 1 893.61 954.56 21.27 o 3 5 1 1676.10 1581.06 29.93 o 4 5 1 273.11 331.15 18.92 o 5 5 1 31.16 25.55 7.23 o 6 5 1 23.10 17.56 7.93 o 7 5 1 1428.32 1350.74 31.47 o 8 5 1 1527.47 1506.57 38.36 o 9 5 1 91.87 95.33 14.52 o 10 5 1 250.72 201.17 18.05 o 11 5 1 67.97 46.16 22.23 o 12 5 1 286.73 225.65 29.33 o 13 5 1 27.15 18.24 26.82 o 14 5 1 183.62 137.27 32.71 o -14 6 1 295.76 329.48 49.48 o -13 6 1 268.14 285.39 33.63 o -12 6 1 846.57 919.97 45.34 o -11 6 1 4138.27 4084.24 73.07 o -10 6 1 6031.05 6143.29 98.83 o -9 6 1 476.05 486.86 31.24 o -8 6 1 417.26 466.60 21.35 o -7 6 1 2795.50 2702.98 48.55 o -6 6 1 426.96 393.94 17.99 o -5 6 1 384.38 413.60 28.56 o -4 6 1 2361.39 2474.96 38.85 o -3 6 1 711.45 825.38 24.07 o -2 6 1 10846.46 12175.33 201.27 o -1 6 1 3287.73 3317.01 59.97 o 0 6 1 2110.24 2068.59 46.91 o 1 6 1 810.42 639.54 18.70 o 2 6 1 1718.70 1550.22 30.62 o 3 6 1 516.19 457.25 29.44 o 4 6 1 9.95 21.37 9.58 o 5 6 1 2963.28 2974.81 45.11 o 6 6 1 2376.19 2169.21 36.38 o 7 6 1 62.50 70.00 11.79 o 8 6 1 28.77 7.18 11.58 o 9 6 1 2.14 1.09 13.24 o 10 6 1 838.46 793.93 44.98 o 11 6 1 117.30 137.54 26.99 o 12 6 1 338.32 369.54 41.76 o 13 6 1 485.36 464.24 37.66 o 14 6 1 310.76 306.69 37.66 o -14 7 1 305.00 336.22 37.95 o -13 7 1 169.11 230.94 32.71 o -12 7 1 28.90 30.89 25.93 o -11 7 1 167.74 219.80 41.76 o -10 7 1 990.72 1007.62 79.03 o -9 7 1 73.56 96.63 15.55 o -8 7 1 2779.53 2636.20 50.17 o -7 7 1 976.50 969.28 28.05 o -6 7 1 876.36 914.89 53.05 o -5 7 1 1885.80 1967.96 66.40 o -4 7 1 5338.30 5136.69 88.08 o -3 7 1 1258.58 1308.14 42.41 o -2 7 1 5176.26 5704.77 99.50 o -1 7 1 556.01 477.17 19.02 o 0 7 1 0.09 -0.45 7.68 o 1 7 1 78.91 37.13 8.22 o 2 7 1 109.56 132.14 10.46 o 3 7 1 1233.05 1152.12 38.63 o 4 7 1 9177.09 9602.96 141.73 o 5 7 1 4356.89 4287.22 61.91 o 6 7 1 3070.77 2929.21 46.63 o 7 7 1 3718.22 3641.79 62.04 o 8 7 1 484.95 490.13 24.11 o 9 7 1 2389.21 2299.43 62.21 o 10 7 1 1564.90 1651.15 53.24 o 11 7 1 21.30 40.53 43.05 o 12 7 1 346.67 416.84 55.90 o 13 7 1 360.63 391.27 37.36 o -13 8 1 194.70 201.00 33.35 o -12 8 1 206.98 294.49 34.05 o -11 8 1 1378.52 1453.59 91.24 o -10 8 1 3398.89 3375.23 81.78 o -9 8 1 1541.47 1553.91 50.13 o -8 8 1 2531.54 2347.13 51.03 o 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