data_2240381 _cell_angle_alpha 77.812 _cell_angle_beta 76.924 _cell_angle_gamma 88.367 _cell_length_a 11.0165 _cell_length_b 13.2508 _cell_length_c 16.4285 _exptl_crystal_F_000 1120.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file wm5107Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' off' _shelx_refln_list_code 4 _shelx_f_calc_maximum 316.69 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6699.84 6889.64 327.49 o 3 0 0 3082.15 3268.91 161.44 o 4 0 0 18092.71 19512.65 1293.07 o 5 0 0 5134.89 5448.58 281.43 o 6 0 0 20.23 35.46 16.28 o 7 0 0 1615.31 1950.10 213.08 o 8 0 0 2188.08 2292.14 149.11 o 9 0 0 89.10 66.17 24.70 o 10 0 0 29.00 16.10 11.99 o 11 0 0 447.33 459.35 55.43 o 12 0 0 377.44 336.64 44.78 o 13 0 0 74.55 61.72 22.79 o -13 1 0 511.57 478.55 102.29 o -12 1 0 107.35 78.48 42.62 o -11 1 0 254.16 253.15 38.75 o -10 1 0 367.61 363.85 47.85 o -9 1 0 983.62 964.87 68.20 o -8 1 0 2.82 4.75 6.88 o -7 1 0 232.69 266.78 29.51 o -6 1 0 675.72 1308.15 79.50 o -5 1 0 4284.76 4921.78 261.07 o -4 1 0 322.35 731.33 54.11 o -3 1 0 6178.60 6301.91 316.34 o -2 1 0 499.81 369.59 27.67 o 2 1 0 5672.57 9243.53 490.07 o 3 1 0 17472.23 19619.28 1262.95 o 4 1 0 3802.40 3474.19 150.42 o 5 1 0 766.29 569.59 30.09 o 6 1 0 344.54 292.56 24.05 o 7 1 0 1655.46 1580.06 85.00 o 8 1 0 336.61 395.35 47.94 o 9 1 0 1038.62 900.95 150.76 o 10 1 0 636.01 605.92 63.95 o 11 1 0 0.17 -0.55 6.25 o 12 1 0 145.88 144.16 25.96 o 13 1 0 170.90 127.05 51.03 o -13 2 0 7.03 -1.59 11.22 o -12 2 0 318.78 295.08 77.12 o -11 2 0 90.41 77.80 40.53 o -10 2 0 10.03 -4.85 18.54 o -9 2 0 0.09 -4.97 10.46 o -8 2 0 55.36 78.97 22.71 o -7 2 0 636.56 633.05 83.87 o -6 2 0 1667.60 1409.27 73.76 o -5 2 0 3183.96 3345.19 545.56 o -4 2 0 767.45 806.08 88.83 o -3 2 0 1524.77 1694.86 103.09 o -1 2 0 1951.50 2648.73 164.92 o 0 2 0 5362.04 5653.95 238.05 o 1 2 0 1289.97 1148.45 50.59 o 2 2 0 6666.89 7346.39 359.52 o 3 2 0 8179.38 11159.88 595.41 o 4 2 0 156.42 291.77 27.94 o 5 2 0 24.74 66.58 42.33 o 6 2 0 997.16 920.41 59.92 o 7 2 0 5291.24 5316.19 300.95 o 8 2 0 1052.87 1057.31 68.01 o 9 2 0 524.44 554.96 79.73 o 10 2 0 31.45 36.69 19.73 o 11 2 0 2.92 11.23 9.08 o 12 2 0 96.37 78.48 23.15 o 13 2 0 0.07 -3.35 11.12 o -13 3 0 174.37 164.96 66.54 o -12 3 0 304.22 312.75 86.06 o -11 3 0 1.68 3.03 11.07 o -10 3 0 30.67 25.48 17.36 o -9 3 0 8.21 11.34 22.67 o -8 3 0 773.47 715.89 64.49 o -7 3 0 641.96 765.10 103.96 o -6 3 0 1796.62 1821.53 132.81 o -5 3 0 7531.82 8134.70 639.61 o -4 3 0 3074.45 3134.10 211.29 o -3 3 0 572.36 806.92 95.69 o -1 3 0 1170.98 992.45 235.84 o 0 3 0 284.54 531.30 41.91 o 1 3 0 4754.81 4011.23 170.25 o 2 3 0 72.91 281.97 44.91 o 3 3 0 6018.91 7897.56 390.01 o 4 3 0 305.73 504.19 29.51 o 5 3 0 1901.17 3288.74 266.40 o 6 3 0 2680.69 2784.43 129.17 o 7 3 0 245.52 215.74 18.82 o 8 3 0 50.04 50.50 13.33 o 9 3 0 911.92 858.51 70.92 o 10 3 0 855.06 895.74 57.17 o 11 3 0 23.41 17.01 14.24 o 12 3 0 3.01 -3.01 6.67 o 13 3 0 164.39 135.82 34.86 o -13 4 0 7.74 18.16 35.37 o -12 4 0 69.25 60.70 27.79 o -11 4 0 538.77 657.35 123.86 o -10 4 0 102.44 87.62 47.77 o -9 4 0 67.99 26.81 17.63 o -8 4 0 1469.36 1547.00 179.60 o -7 4 0 3160.69 3654.36 289.66 o -6 4 0 487.58 522.98 54.52 o -5 4 0 156.84 232.94 62.56 o -4 4 0 10036.33 11498.26 968.28 o -2 4 0 6.33 84.62 19.60 o -1 4 0 165.15 222.53 70.42 o 0 4 0 17306.94 18220.17 1177.92 o 1 4 0 5696.87 4673.94 209.75 o 2 4 0 47.69 68.11 10.37 o 3 4 0 1196.35 1035.64 44.03 o 4 4 0 2611.08 4083.99 220.62 o 5 4 0 2781.29 3352.92 150.86 o 6 4 0 2411.44 2496.53 114.68 o 7 4 0 1903.47 2434.84 123.64 o 8 4 0 1502.04 1627.39 228.34 o 9 4 0 772.73 673.24 90.35 o 10 4 0 199.14 195.39 34.42 o 11 4 0 557.86 598.87 61.04 o 12 4 0 322.63 343.05 44.91 o 13 4 0 50.95 45.19 23.06 o -13 5 0 272.59 363.14 66.61 o -12 5 0 201.92 135.05 108.51 o -11 5 0 54.15 68.40 50.96 o -10 5 0 1006.02 1019.46 104.87 o -9 5 0 1039.87 1076.49 104.34 o -8 5 0 857.94 1079.97 108.13 o -7 5 0 2555.99 3076.97 318.67 o -6 5 0 175.47 123.90 28.89 o -5 5 0 6535.93 8397.41 706.67 o -4 5 0 7510.56 8927.61 454.50 o -3 5 0 2751.78 1955.52 138.01 o -2 5 0 1172.61 1013.25 70.75 o -1 5 0 653.92 571.39 59.52 o 0 5 0 222.70 151.17 21.88 o 1 5 0 4181.51 4327.56 263.12 o 2 5 0 13419.37 14183.33 1613.84 o 3 5 0 2583.14 3464.27 242.59 o 4 5 0 0.28 3.46 5.22 o 5 5 0 1484.75 1325.52 104.15 o 6 5 0 1860.85 1878.49 83.83 o 7 5 0 359.45 459.88 33.74 o 8 5 0 70.86 90.35 16.76 o 9 5 0 1766.26 1643.46 115.14 o 10 5 0 1793.35 1515.14 108.53 o 11 5 0 322.30 288.64 25.96 o 12 5 0 13.06 15.25 10.78 o 13 5 0 968.69 781.62 69.91 o -13 6 0 34.63 18.33 16.94 o -12 6 0 119.93 194.58 31.63 o -11 6 0 703.64 849.36 81.94 o -10 6 0 243.85 299.30 35.08 o -9 6 0 95.84 105.45 21.89 o -8 6 0 956.86 1139.72 65.41 o -7 6 0 472.26 549.68 40.36 o -6 6 0 655.25 755.94 38.40 o -5 6 0 233.01 250.62 20.22 o -4 6 0 2507.68 2031.46 149.27 o -3 6 0 25.64 19.34 24.76 o -2 6 0 289.52 283.67 33.97 o -1 6 0 36.04 48.13 8.57 o 0 6 0 15690.61 16240.31 1083.03 o 1 6 0 2084.13 1935.60 88.63 o 2 6 0 60.04 82.60 28.40 o 3 6 0 101.97 116.64 19.93 o 4 6 0 1360.57 1274.97 65.17 o 5 6 0 2647.93 2690.36 149.75 o 6 6 0 87.84 100.89 15.03 o 7 6 0 156.40 196.29 38.18 o 8 6 0 131.13 140.29 20.85 o 9 6 0 24.01 20.40 13.98 o 10 6 0 65.82 62.78 28.09 o 11 6 0 204.07 169.99 19.94 o 12 6 0 132.74 132.00 22.20 o -12 7 0 185.56 206.34 39.26 o -11 7 0 6.64 9.46 9.77 o -10 7 0 241.85 216.33 46.53 o -9 7 0 542.58 572.88 108.98 o -8 7 0 90.40 126.91 15.94 o -7 7 0 485.81 561.97 29.26 o -6 7 0 141.81 151.72 18.12 o -5 7 0 2374.09 2315.47 263.01 o -4 7 0 0.34 19.34 26.01 o -3 7 0 0.80 0.80 11.79 o -2 7 0 443.73 484.16 68.55 o -1 7 0 324.66 327.29 28.85 o 0 7 0 985.41 1003.46 139.88 o 1 7 0 60.04 61.49 13.07 o 2 7 0 1972.42 1470.31 75.87 o 3 7 0 2.27 -2.26 8.05 o 4 7 0 91.65 155.62 40.38 o 5 7 0 0.63 -2.62 7.57 o 6 7 0 98.35 129.26 24.91 o 7 7 0 81.18 92.94 17.06 o 8 7 0 445.10 428.59 69.69 o 9 7 0 725.18 642.07 66.94 o 10 7 0 653.88 687.34 72.60 o 11 7 0 20.58 41.75 19.51 o 12 7 0 49.98 50.45 23.94 o -12 8 0 165.34 199.19 80.42 o -11 8 0 386.31 484.81 78.58 o -10 8 0 359.99 408.29 40.13 o -9 8 0 97.25 123.43 16.53 o -8 8 0 703.02 786.70 73.56 o -7 8 0 989.18 1258.21 185.47 o -6 8 0 585.16 560.54 149.82 o -5 8 0 352.30 400.35 49.53 o -4 8 0 1633.28 1586.05 170.92 o -3 8 0 1608.68 1414.03 108.05 o -2 8 0 1083.00 885.02 103.05 o -1 8 0 1315.46 1233.87 54.07 o 0 8 0 424.09 430.39 101.84 o 1 8 0 298.68 246.25 25.27 o 2 8 0 875.47 928.57 53.77 o 3 8 0 522.18 409.75 26.12 o 4 8 0 1043.54 867.53 103.45 o 5 8 0 359.16 293.57 28.51 o 6 8 0 822.19 696.06 67.96 o 7 8 0 537.73 608.07 101.87 o 8 8 0 485.96 476.18 60.30 o 9 8 0 421.75 353.09 35.98 o 10 8 0 5.46 0.81 13.40 o 11 8 0 710.66 710.50 111.86 o 12 8 0 231.25 249.20 38.69 o -11 9 0 8.99 4.50 19.89 o -10 9 0 241.09 365.03 96.00 o -9 9 0 165.89 178.38 59.87 o -8 9 0 52.68 104.69 40.36 o -7 9 0 238.89 341.93 53.69 o -6 9 0 356.42 439.46 101.82 o -5 9 0 1500.83 1233.33 114.16 o -4 9 0 338.37 309.49 72.04 o -3 9 0 366.04 330.84 43.56 o -2 9 0 1407.09 1228.71 136.15 o -1 9 0 340.77 309.98 34.62 o 0 9 0 245.59 227.55 30.52 o 1 9 0 50.08 54.68 12.81 o 2 9 0 2737.20 2663.43 144.24 o 3 9 0 44.22 66.34 21.95 o 4 9 0 342.50 305.09 29.72 o 5 9 0 557.44 449.59 54.25 o 6 9 0 1058.84 890.45 72.47 o 7 9 0 198.64 170.05 21.96 o 8 9 0 24.74 12.18 12.62 o 9 9 0 865.29 712.85 98.69 o 10 9 0 500.73 436.33 66.92 o 11 9 0 111.39 80.71 26.43 o -11 10 0 256.00 416.98 119.75 o -10 10 0 125.31 104.58 48.31 o -9 10 0 4.39 6.77 12.78 o -8 10 0 149.09 198.66 34.15 o -7 10 0 481.87 571.37 174.74 o -6 10 0 288.29 243.34 63.33 o -5 10 0 0.65 2.12 10.99 o -4 10 0 905.90 800.55 84.47 o -3 10 0 3319.51 3022.68 244.43 o -2 10 0 653.29 625.96 102.56 o -1 10 0 965.80 1233.21 179.16 o 0 10 0 614.20 756.36 69.45 o 1 10 0 734.12 783.13 72.51 o 2 10 0 20.28 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