data_2240436 _cell_angle_alpha 98.228 _cell_angle_beta 95.860 _cell_angle_gamma 97.183 _cell_length_a 8.9597 _cell_length_b 12.5586 _cell_length_c 20.0796 _exptl_crystal_F_000 996.00 _reflns_d_resolution_high 0.7287 _[local]_cod_data_source_file rz5149Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' ND12 IN P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 273.25 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 143.74 200.29 71.44 o 2 0 0 25251.28 24986.02 877.35 o 3 0 0 6113.59 6104.16 351.49 o 4 0 0 15149.64 15124.88 1468.06 o 5 0 0 768.63 791.99 57.78 o 6 0 0 3242.64 3198.79 127.01 o 7 0 0 29.34 63.92 64.88 o 8 0 0 7362.26 6973.72 409.05 o 9 0 0 286.63 279.35 53.69 o 10 0 0 5311.23 5179.12 202.83 o 11 0 0 33.74 86.26 75.79 o 12 0 0 1888.29 1652.62 247.26 o -12 1 0 19.95 56.45 90.93 o -11 1 0 1941.61 1749.40 130.03 o -10 1 0 708.23 727.23 59.56 o -9 1 0 5017.49 4787.37 167.75 o -8 1 0 158.98 186.06 67.49 o -7 1 0 7899.33 7707.85 218.90 o -6 1 0 574.50 576.71 49.35 o -5 1 0 9499.69 9670.83 328.57 o -4 1 0 2667.78 2904.53 126.42 o -3 1 0 18077.40 17667.39 1214.45 o -2 1 0 5570.04 6079.39 218.16 o -1 1 0 36028.84 37397.55 328.03 o 0 1 0 6879.86 7553.97 141.23 o 1 1 0 53675.50 45285.39 3169.86 o 2 1 0 17734.26 17471.46 622.18 o 3 1 0 19673.73 19686.55 814.64 o 4 1 0 5267.05 5315.18 226.85 o 5 1 0 7637.27 7375.66 367.44 o 6 1 0 404.15 445.24 57.59 o 7 1 0 6870.88 6387.04 258.57 o 8 1 0 1652.95 1604.73 73.54 o 9 1 0 2391.40 2255.79 99.87 o 10 1 0 297.68 301.21 62.98 o 11 1 0 3614.52 3379.29 211.33 o -12 2 0 1415.38 1308.76 103.35 o -11 2 0 29.03 51.86 68.89 o -10 2 0 3775.60 3606.18 147.38 o -9 2 0 137.96 159.53 45.64 o -8 2 0 2706.78 2720.86 104.61 o -7 2 0 1442.69 1442.09 54.26 o -6 2 0 7868.03 8146.93 228.07 o -5 2 0 2682.05 2932.68 86.69 o -4 2 0 4811.12 5012.88 411.37 o 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4718.14 5110.43 308.92 o 6 3 0 5421.33 5642.18 250.55 o 7 3 0 4472.22 4447.83 91.17 o 8 3 0 1854.79 1713.19 100.13 o 9 3 0 1004.89 1043.14 71.58 o 10 3 0 965.56 957.01 80.62 o 11 3 0 952.65 961.34 91.69 o -12 4 0 802.97 642.57 80.32 o -11 4 0 817.63 780.23 66.77 o -10 4 0 3560.25 3402.54 172.26 o -9 4 0 2318.43 2381.96 140.26 o -8 4 0 1730.82 1688.55 63.94 o -7 4 0 1067.89 1043.14 53.12 o -6 4 0 8155.96 7788.41 304.59 o -5 4 0 7480.42 7794.32 163.13 o -4 4 0 110.98 120.41 42.53 o -3 4 0 1445.65 1427.49 45.61 o -2 4 0 5905.13 5834.63 132.06 o -1 4 0 29362.00 29184.42 196.51 o 0 4 0 111.28 127.51 47.84 o 1 4 0 7650.12 7540.13 383.77 o 2 4 0 11197.04 11207.16 305.32 o 3 4 0 21362.02 21617.28 572.38 o 4 4 0 897.02 902.04 45.74 o 5 4 0 4118.90 3939.87 134.38 o 6 4 0 2066.00 2079.23 63.80 o 7 4 0 3666.40 3742.40 74.29 o 8 4 0 250.38 278.87 66.30 o 9 4 0 891.19 937.09 75.50 o 10 4 0 1028.26 1055.82 86.21 o 11 4 0 2024.46 2072.48 135.31 o -12 5 0 774.79 699.14 80.40 o -11 5 0 1046.44 964.72 90.21 o -10 5 0 1507.20 1481.50 65.45 o -9 5 0 1761.96 1753.21 155.34 o -8 5 0 2268.62 2160.26 66.11 o -7 5 0 2031.11 1898.44 121.23 o -6 5 0 3021.39 2873.41 53.32 o -5 5 0 4173.30 4152.15 101.00 o -4 5 0 7849.58 7860.32 191.75 o -3 5 0 305.83 246.19 36.25 o -2 5 0 10272.12 10026.02 158.68 o -1 5 0 2494.71 2514.25 55.07 o 0 5 0 3487.54 3371.39 74.27 o 1 5 0 1939.99 1793.05 72.14 o 2 5 0 12962.36 13280.62 195.71 o 3 5 0 1566.26 1509.70 70.62 o 4 5 0 3506.95 3471.66 91.90 o 5 5 0 271.52 290.77 58.37 o 6 5 0 4108.52 4142.79 86.67 o 7 5 0 130.96 146.93 59.39 o 8 5 0 1480.11 1520.04 76.91 o 9 5 0 62.88 126.98 80.89 o 10 5 0 2234.83 2282.37 116.89 o 11 5 0 42.91 33.44 105.58 o -11 6 0 1503.69 1423.37 114.15 o -10 6 0 1055.76 1104.12 89.76 o -9 6 0 3788.38 3597.32 93.63 o -8 6 0 671.10 682.90 71.81 o -7 6 0 5031.84 4871.59 127.87 o -6 6 0 2377.46 2394.16 69.36 o -5 6 0 7807.69 7582.82 243.24 o -4 6 0 2382.10 2362.46 63.29 o -3 6 0 1716.01 1593.22 46.56 o -2 6 0 1686.65 1680.22 45.64 o -1 6 0 1712.56 1528.74 46.23 o 0 6 0 28.81 61.14 48.17 o 1 6 0 6781.78 6568.24 80.66 o 2 6 0 1467.32 1506.14 73.58 o 3 6 0 6644.25 6520.20 102.11 o 4 6 0 775.93 709.43 72.43 o 5 6 0 6596.36 6555.49 73.69 o 6 6 0 10.30 1.63 64.13 o 7 6 0 1411.69 1430.80 71.49 o 8 6 0 129.47 166.19 78.23 o 9 6 0 1447.46 1509.93 88.65 o 10 6 0 6.43 67.59 103.12 o -11 7 0 485.68 398.62 84.30 o -10 7 0 3623.96 3607.46 161.01 o -9 7 0 74.50 100.46 61.19 o -8 7 0 3649.91 3386.85 152.73 o -7 7 0 444.64 423.55 43.39 o -6 7 0 4267.14 4402.81 98.36 o -5 7 0 6.23 56.98 46.36 o -4 7 0 5014.25 4891.00 102.64 o -3 7 0 747.70 785.96 50.22 o -2 7 0 7077.56 6685.95 131.92 o -1 7 0 6.90 34.86 42.45 o 0 7 0 9893.72 9678.57 262.34 o 1 7 0 7012.91 7261.58 76.87 o 2 7 0 18207.79 18056.72 185.20 o 3 7 0 823.54 844.87 57.78 o 4 7 0 2075.64 2087.55 76.10 o 5 7 0 652.80 622.49 77.10 o 6 7 0 5635.77 5852.15 217.75 o 7 7 0 1.74 -3.84 93.78 o 8 7 0 1067.95 1172.28 74.44 o 9 7 0 73.34 106.60 97.75 o 10 7 0 1864.63 1888.16 131.63 o -11 8 0 2194.04 2090.64 96.23 o -10 8 0 17.62 74.66 92.82 o -9 8 0 2790.76 2622.29 198.08 o -8 8 0 12.38 44.74 50.27 o -7 8 0 5463.70 5087.53 147.78 o -6 8 0 1.27 36.36 49.26 o -5 8 0 2869.20 2794.23 111.55 o -4 8 0 484.07 564.18 46.80 o -3 8 0 12358.22 12225.31 300.83 o -2 8 0 127.60 126.34 40.44 o -1 8 0 4502.82 4665.37 106.35 o 0 8 0 283.23 276.75 41.07 o 1 8 0 8855.30 8886.05 376.87 o 2 8 0 682.98 683.08 66.76 o 3 8 0 6572.77 6530.95 71.64 o 4 8 0 42.55 33.22 72.12 o 5 8 0 8262.99 8560.65 101.46 o 6 8 0 313.16 364.91 84.59 o 7 8 0 3010.01 3216.32 174.69 o 8 8 0 49.07 107.91 108.20 o 9 8 0 2781.04 2801.31 246.76 o -11 9 0 139.75 167.07 89.25 o -10 9 0 2647.43 2463.73 110.54 o -9 9 0 24.42 111.26 63.38 o -8 9 0 3388.18 3048.94 77.01 o -7 9 0 57.89 84.02 61.01 o -6 9 0 1079.37 1116.90 54.08 o -5 9 0 454.38 436.32 45.62 o -4 9 0 4787.23 4659.21 174.61 o -3 9 0 796.29 766.80 46.77 o -2 9 0 7982.55 8300.56 358.05 o -1 9 0 1343.64 1384.50 50.57 o 0 9 0 9716.78 9571.48 84.38 o 1 9 0 258.45 261.00 59.87 o 2 9 0 8076.57 7926.33 80.55 o 3 9 0 539.98 540.93 52.86 o 4 9 0 5575.40 5503.45 88.59 o 5 9 0 35.26 80.47 78.79 o 6 9 0 3786.07 3852.90 97.16 o 7 9 0 66.92 95.80 96.61 o 8 9 0 1896.74 1927.61 115.78 o 9 9 0 428.74 400.00 129.25 o -10 10 0 126.85 43.79 73.46 o -9 10 0 1933.59 1759.15 97.52 o -8 10 0 402.79 410.93 69.09 o -7 10 0 3119.16 3023.20 80.77 o -6 10 0 1761.29 1740.93 51.70 o -5 10 0 4450.05 4449.89 125.42 o -4 10 0 1721.81 1714.81 64.88 o -3 10 0 13625.20 13308.19 315.55 o -2 10 0 677.17 653.66 53.07 o -1 10 0 3319.39 3380.11 73.69 o 0 10 0 934.00 948.44 62.02 o 1 10 0 4476.48 4471.63 311.09 o 2 10 0 655.98 648.07 60.09 o 3 10 0 5098.75 4952.30 84.41 o 4 10 0 1781.75 1763.99 81.59 o 5 10 0 3707.59 3842.99 139.15 o 6 10 0 1013.88 1024.89 92.84 o 7 10 0 5037.16 5235.82 190.70 o 8 10 0 437.67 489.76 117.53 o -10 11 0 800.01 758.49 88.70 o -9 11 0 334.46 351.42 71.52 o -8 11 0 3751.60 3636.83 78.36 o -7 11 0 2921.79 2561.15 63.91 o -6 11 0 1844.06 1836.44 85.97 o -5 11 0 847.72 794.60 59.23 o -4 11 0 1515.20 1557.83 63.00 o -3 11 0 4348.95 4362.75 136.98 o -2 11 0 1272.91 1266.02 51.31 o -1 11 0 3234.56 3212.73 70.50 o 0 11 0 6072.40 6539.28 351.65 o 1 11 0 4634.49 4413.83 170.50 o 2 11 0 2891.99 2775.27 69.98 o 3 11 0 2156.53 2187.48 84.09 o 4 11 0 4009.85 4050.66 99.11 o 5 11 0 2504.47 2541.99 75.79 o 6 11 0 1496.45 1629.73 99.26 o 7 11 0 964.59 992.25 108.10 o 8 11 0 1273.61 1402.49 155.16 o -9 12 0 1036.55 959.86 74.20 o -8 12 0 1248.07 1199.33 89.42 o -7 12 0 1087.19 1078.00 64.67 o -6 12 0 1599.94 1534.25 66.89 o -5 12 0 2423.21 2368.83 104.61 o -4 12 0 2997.48 2997.27 107.36 o -3 12 0 1972.96 1854.81 80.19 o -2 12 0 1300.05 1347.42 65.56 o -1 12 0 1202.67 1305.27 60.07 o 0 12 0 2419.80 2386.21 153.64 o 1 12 0 1203.83 1095.50 78.52 o 2 12 0 1363.47 1336.24 65.82 o 3 12 0 2196.17 2136.92 153.66 o 4 12 0 3563.45 3726.68 80.53 o 5 12 0 511.18 475.08 90.90 o 6 12 0 1435.17 1516.88 81.88 o 7 12 0 1040.86 1096.59 115.12 o -9 13 0 826.81 825.45 75.71 o 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28.23 0.03 61.46 o -3 15 0 1659.29 1643.46 76.92 o -2 15 0 131.73 139.41 63.51 o -1 15 0 1742.31 1607.92 66.78 o 0 15 0 3.73 -23.06 81.38 o 1 15 0 1786.42 1715.68 95.15 o 2 15 0 0.14 17.14 80.22 o 3 15 0 2010.65 1917.09 101.59 o 4 15 0 137.06 138.15 84.09 o -5 16 0 44.97 95.58 72.70 o -4 16 0 1602.79 1607.46 86.56 o -3 16 0 102.88 175.84 65.15 o -2 16 0 2376.23 2291.99 125.56 o -1 16 0 113.13 86.23 87.64 o 0 16 0 2082.35 1977.28 89.94 o 1 16 0 27.13 30.78 100.49 o 2 16 0 2090.42 1949.97 109.45 o -2 17 0 107.88 46.58 82.69 o -1 17 0 1161.15 1191.26 179.19 o 1 -17 1 336.15 258.65 115.70 o 2 -17 1 1191.23 1016.27 121.95 o 3 -17 1 819.57 712.76 125.13 o -2 -16 1 745.50 713.03 104.27 o -1 -16 1 1147.09 1006.35 87.36 o 0 -16 1 1032.06 846.48 282.91 o 1 -16 1 1517.25 1421.78 168.48 o 2 -16 1 735.82 715.20 69.99 o 3 -16 1 723.37 692.59 70.95 o 4 -16 1 141.39 154.73 82.56 o 5 -16 1 1475.52 1571.67 77.66 o -4 -15 1 1397.51 1274.48 92.02 o -3 -15 1 891.24 939.72 81.40 o -2 -15 1 1123.07 1052.26 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