#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:06:23 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181905 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/05/2240523.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240523 _cell_angle_alpha 90.000 _cell_angle_beta 102.816 _cell_angle_gamma 90.000 _cell_length_a 10.4493 _cell_length_b 13.6989 _cell_length_c 8.0235 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8135 _cod_data_source_file hb7381Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 244.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2688.24 2722.08 10.94 o 2 0 0 882.19 1020.32 5.91 o 3 0 0 83.36 76.46 1.64 o 4 0 0 3444.14 3537.34 13.69 o 5 0 0 819.95 918.44 10.42 o 6 0 0 677.26 650.50 9.78 o 7 0 0 88.45 79.00 2.96 o 8 0 0 3069.78 2987.71 37.52 o 9 0 0 1363.79 1316.36 32.18 o 10 0 0 1400.46 1473.65 46.70 o 11 0 0 161.05 171.99 7.30 o 12 0 0 27.30 28.38 3.45 o 1 1 0 117.78 116.38 1.83 o 2 1 0 6696.18 6696.13 65.83 o 3 1 0 2266.64 2477.87 11.33 o 4 1 0 0.34 0.69 0.37 o 5 1 0 137.58 112.04 1.94 o 6 1 0 18.25 11.48 0.85 o 7 1 0 638.22 630.60 6.20 o 8 1 0 16.25 16.02 1.51 o 9 1 0 75.36 69.69 2.08 o 10 1 0 1990.66 2074.10 17.13 o 11 1 0 204.94 222.90 6.11 o 12 1 0 21.29 19.60 2.12 o 0 2 0 15863.40 14698.96 125.63 o 1 2 0 659.76 653.48 3.14 o 2 2 0 530.57 579.97 6.58 o 3 2 0 2507.54 2680.09 10.94 o 4 2 0 158.25 202.78 2.39 o 5 2 0 418.89 460.04 4.40 o 6 2 0 1122.71 1192.31 8.15 o 7 2 0 76.32 73.90 2.72 o 8 2 0 292.99 269.10 4.72 o 9 2 0 47.28 43.79 1.97 o 10 2 0 768.78 776.79 13.72 o 11 2 0 68.27 69.69 4.87 o 12 2 0 72.81 74.52 5.03 o 1 3 0 232.33 240.75 2.01 o 2 3 0 978.14 1068.85 7.39 o 3 3 0 581.60 629.08 4.32 o 4 3 0 0.41 1.52 0.48 o 5 3 0 665.69 752.67 5.52 o 6 3 0 198.33 219.73 3.49 o 7 3 0 20.78 19.20 1.53 o 8 3 0 11.36 9.48 1.12 o 9 3 0 4.59 3.51 0.89 o 10 3 0 324.53 327.99 7.99 o 11 3 0 131.15 135.62 5.73 o 12 3 0 110.12 116.76 5.66 o 0 4 0 376.85 367.57 5.77 o 1 4 0 2936.45 3198.62 25.67 o 2 4 0 6444.59 6939.68 18.77 o 3 4 0 700.46 833.38 4.82 o 4 4 0 705.33 727.28 5.36 o 5 4 0 328.79 393.33 3.99 o 6 4 0 1412.22 1439.60 17.67 o 7 4 0 472.91 467.87 6.01 o 8 4 0 97.49 90.39 3.06 o 9 4 0 389.64 363.90 5.64 o 10 4 0 103.86 109.75 4.76 o 11 4 0 436.82 463.12 10.13 o 12 4 0 7.18 7.68 1.99 o 1 5 0 5187.47 5716.04 23.96 o 2 5 0 195.15 201.29 2.26 o 3 5 0 413.95 411.74 3.77 o 4 5 0 378.02 454.50 4.38 o 5 5 0 1009.84 1005.07 7.10 o 6 5 0 449.86 463.97 5.87 o 7 5 0 190.03 165.25 3.80 o 8 5 0 249.71 240.58 3.79 o 9 5 0 402.63 357.10 7.81 o 10 5 0 83.49 94.54 5.32 o 11 5 0 271.12 283.01 7.06 o 0 6 0 81.86 51.90 1.77 o 1 6 0 2044.66 2348.55 9.87 o 2 6 0 367.52 333.83 3.49 o 3 6 0 44.41 43.28 1.31 o 4 6 0 2387.99 2554.17 14.18 o 5 6 0 853.20 840.26 7.69 o 6 6 0 69.25 62.57 2.40 o 7 6 0 115.74 120.29 3.47 o 8 6 0 944.16 924.98 8.11 o 9 6 0 462.26 440.30 9.27 o 10 6 0 5.68 3.68 1.50 o 11 6 0 183.86 180.39 5.02 o 1 7 0 2741.42 3227.79 18.81 o 2 7 0 13.88 14.94 0.95 o 3 7 0 101.53 120.61 3.12 o 4 7 0 38.79 40.29 1.46 o 5 7 0 937.24 928.76 7.93 o 6 7 0 209.06 210.50 4.20 o 7 7 0 183.58 158.74 2.90 o 8 7 0 24.73 17.88 1.37 o 9 7 0 366.47 331.07 6.94 o 10 7 0 4.79 4.71 1.42 o 11 7 0 91.34 87.45 3.12 o 0 8 0 1328.67 1490.86 10.07 o 1 8 0 16.04 24.93 1.45 o 2 8 0 19.85 33.01 1.63 o 3 8 0 12.54 10.73 1.17 o 4 8 0 194.86 193.95 3.86 o 5 8 0 103.91 103.30 3.68 o 6 8 0 564.93 593.95 7.81 o 7 8 0 69.39 63.53 1.97 o 8 8 0 42.33 37.56 2.07 o 9 8 0 0.20 1.06 0.99 o 10 8 0 8.50 6.51 1.45 o 11 8 0 30.51 29.81 3.45 o 1 9 0 81.40 62.76 2.11 o 2 9 0 57.51 66.08 2.20 o 3 9 0 205.58 191.74 3.53 o 4 9 0 213.48 204.91 3.85 o 5 9 0 227.49 228.91 4.96 o 6 9 0 119.56 112.99 2.58 o 7 9 0 4.64 4.46 0.83 o 8 9 0 163.93 158.03 3.56 o 9 9 0 1.22 2.66 0.89 o 10 9 0 48.25 46.19 2.51 o 0 10 0 123.56 113.49 5.73 o 1 10 0 118.04 104.68 3.29 o 2 10 0 1285.10 1297.97 13.82 o 3 10 0 115.55 109.36 3.00 o 4 10 0 188.40 181.68 4.24 o 5 10 0 79.54 78.34 2.17 o 6 10 0 1219.86 1177.90 11.86 o 7 10 0 460.21 455.03 6.62 o 8 10 0 100.34 94.52 2.87 o 9 10 0 15.90 17.07 1.71 o 10 10 0 86.18 83.59 3.43 o 1 11 0 911.00 832.70 9.10 o 2 11 0 0.11 -0.35 0.95 o 3 11 0 87.91 86.54 1.98 o 4 11 0 938.53 928.56 6.99 o 5 11 0 106.45 102.49 2.67 o 6 11 0 81.95 76.31 3.05 o 7 11 0 384.95 379.29 6.30 o 8 11 0 50.74 50.78 2.18 o 9 11 0 455.81 520.02 7.12 o 0 12 0 83.14 88.93 3.65 o 1 12 0 290.10 238.01 4.17 o 2 12 0 139.31 143.44 2.94 o 3 12 0 50.74 53.20 1.65 o 4 12 0 29.98 25.51 1.64 o 5 12 0 73.55 76.56 3.43 o 6 12 0 101.47 98.91 3.28 o 7 12 0 79.37 76.65 2.71 o 8 12 0 31.37 31.01 1.52 o 1 13 0 506.86 435.75 5.03 o 2 13 0 25.44 30.30 1.82 o 3 13 0 79.22 85.92 2.70 o 4 13 0 223.97 209.59 4.82 o 5 13 0 0.80 1.61 1.08 o 6 13 0 59.08 58.94 2.69 o 7 13 0 89.38 89.45 2.85 o 0 14 0 6.59 2.73 1.50 o 1 14 0 83.83 73.91 2.45 o 2 14 0 187.87 181.44 3.49 o 3 14 0 4.16 6.00 1.21 o 4 14 0 16.73 17.26 1.62 o 5 14 0 0.05 1.29 0.93 o 6 14 0 71.66 76.11 2.60 o 1 15 0 5.29 9.96 1.02 o 2 15 0 0.14 1.21 0.75 o 3 15 0 23.41 22.55 1.49 o 4 15 0 7.77 7.90 1.12 o 5 15 0 235.77 247.08 4.25 o 0 16 0 82.03 95.35 3.41 o 1 16 0 35.82 36.78 1.48 o 2 16 0 331.38 309.43 5.35 o 3 16 0 119.47 135.55 3.12 o -12 1 1 153.67 157.56 5.46 o -11 1 1 82.42 82.86 4.78 o -10 1 1 0.31 0.31 1.54 o -9 1 1 270.02 252.60 3.80 o -8 1 1 11.20 8.83 1.30 o -7 1 1 89.79 92.84 2.42 o -6 1 1 77.89 71.67 1.74 o -5 1 1 1150.59 1276.09 6.74 o -4 1 1 1708.73 1843.01 11.72 o -3 1 1 92.77 109.01 1.42 o -2 1 1 1.46 2.95 0.33 o -1 1 1 361.46 382.84 3.13 o 0 1 1 887.40 988.49 3.69 o 1 1 1 526.64 574.68 5.06 o 2 1 1 159.37 140.72 1.65 o 3 1 1 553.39 556.72 3.40 o 4 1 1 639.17 685.35 5.05 o 5 1 1 207.56 242.24 3.22 o 6 1 1 7.26 5.50 1.01 o 7 1 1 107.36 101.19 2.94 o 8 1 1 153.79 137.18 3.88 o 9 1 1 27.06 23.95 1.49 o 10 1 1 390.38 387.36 7.40 o 11 1 1 10.63 8.93 1.28 o 12 1 1 15.83 16.57 1.72 o -12 2 1 5.37 4.80 1.83 o -11 2 1 34.73 38.77 3.41 o -10 2 1 9.60 8.54 1.81 o -9 2 1 1154.10 1159.22 8.35 o -8 2 1 25.60 23.17 1.58 o -7 2 1 334.89 303.19 4.60 o -6 2 1 294.09 306.84 3.86 o -5 2 1 41.51 41.73 1.49 o -4 2 1 1669.15 1843.13 12.72 o -3 2 1 1738.71 1863.05 9.70 o -2 2 1 496.37 482.31 6.35 o -1 2 1 37.00 25.80 0.69 o 0 2 1 748.21 819.98 2.89 o 1 2 1 628.57 702.89 3.74 o 2 2 1 43.15 53.60 0.97 o 3 2 1 387.63 385.47 2.80 o 4 2 1 700.15 756.20 4.86 o 5 2 1 1309.55 1322.82 10.70 o 6 2 1 1585.10 1724.43 12.46 o 7 2 1 246.12 248.99 4.92 o 8 2 1 16.26 18.42 1.95 o 9 2 1 26.04 24.30 1.55 o 10 2 1 210.62 216.08 5.51 o 11 2 1 26.80 31.76 2.42 o 12 2 1 179.09 195.23 15.10 o -12 3 1 156.27 162.47 5.30 o -11 3 1 135.69 135.83 5.92 o -10 3 1 177.37 179.39 5.80 o -9 3 1 377.11 361.11 5.59 o -8 3 1 24.48 17.72 1.46 o -7 3 1 84.58 70.57 2.63 o -6 3 1 676.10 671.61 8.18 o -5 3 1 4444.44 5090.10 18.39 o -4 3 1 3042.21 3257.38 20.11 o -3 3 1 851.06 909.64 4.60 o -2 3 1 557.84 604.72 3.60 o -1 3 1 18.40 14.48 0.60 o 0 3 1 1614.52 1774.16 13.46 o 1 3 1 3.51 12.72 0.57 o 2 3 1 487.29 527.74 3.26 o 3 3 1 149.87 140.33 2.11 o 4 3 1 3326.51 3523.73 22.69 o 5 3 1 476.01 569.67 5.40 o 6 3 1 367.93 349.18 5.39 o 7 3 1 136.75 127.00 3.55 o 8 3 1 239.28 225.17 3.58 o 9 3 1 49.44 46.21 2.33 o 10 3 1 464.56 492.60 9.44 o 11 3 1 62.77 69.39 3.25 o -12 4 1 106.91 107.68 4.22 o -11 4 1 59.32 54.12 3.77 o -10 4 1 311.47 294.68 6.40 o -9 4 1 103.35 96.46 2.77 o -8 4 1 70.10 66.69 2.68 o -7 4 1 248.87 213.09 4.30 o -6 4 1 9.87 9.22 0.79 o -5 4 1 265.12 244.00 3.05 o -4 4 1 102.85 166.02 2.10 o -3 4 1 4088.34 4457.02 11.58 o -2 4 1 510.74 517.51 3.30 o -1 4 1 39.68 50.91 0.87 o 0 4 1 1467.52 1511.57 6.22 o 1 4 1 4052.46 4294.03 16.08 o 2 4 1 132.13 130.82 1.70 o 3 4 1 60.02 55.56 1.26 o 4 4 1 63.78 68.26 1.69 o 5 4 1 1425.89 1498.73 11.65 o 6 4 1 2779.49 3019.95 25.10 o 7 4 1 15.95 15.75 2.00 o 8 4 1 53.89 49.72 1.90 o 9 4 1 221.82 195.27 4.43 o 10 4 1 200.90 208.96 6.13 o 11 4 1 66.59 66.04 5.35 o -12 5 1 15.31 16.38 2.63 o -11 5 1 67.20 63.65 3.57 o -10 5 1 23.50 19.58 1.87 o -9 5 1 50.26 44.69 2.24 o -8 5 1 319.98 279.47 4.01 o -7 5 1 15.16 12.19 1.27 o -6 5 1 1.87 1.17 0.64 o -5 5 1 1155.87 1379.90 9.91 o -4 5 1 1636.03 1902.47 8.17 o -3 5 1 108.30 127.90 1.97 o -2 5 1 185.35 188.28 2.16 o -1 5 1 0.81 1.38 0.42 o 0 5 1 1529.54 1686.28 8.20 o 1 5 1 784.63 894.00 4.95 o 2 5 1 1.84 2.68 0.46 o 3 5 1 3.50 8.04 1.39 o 4 5 1 382.94 389.35 4.23 o 5 5 1 8.68 16.01 1.22 o 6 5 1 104.22 86.76 3.14 o 7 5 1 13.77 13.54 1.60 o 8 5 1 18.86 13.94 1.24 o 9 5 1 7.26 7.60 1.28 o 10 5 1 1.10 0.73 1.32 o 11 5 1 355.39 369.75 11.13 o -11 6 1 98.93 96.74 3.66 o -10 6 1 318.09 283.53 7.23 o -9 6 1 0.30 2.12 1.19 o -8 6 1 24.38 23.95 1.38 o -7 6 1 15.40 15.53 1.44 o -6 6 1 22.44 25.08 1.40 o -5 6 1 1.85 4.03 0.64 o -4 6 1 225.97 268.95 3.24 o -3 6 1 595.69 602.18 4.43 o -2 6 1 645.29 693.14 4.68 o -1 6 1 13.00 14.38 0.73 o 0 6 1 26.19 49.11 1.28 o 1 6 1 91.50 130.51 2.45 o 2 6 1 111.23 123.36 2.41 o 3 6 1 73.83 77.62 1.89 o 4 6 1 5.65 7.97 0.70 o 5 6 1 12.43 18.90 1.18 o 6 6 1 0.31 1.73 1.09 o 7 6 1 13.84 16.38 1.00 o 8 6 1 2.94 2.69 0.98 o 9 6 1 0.29 -0.04 1.31 o 10 6 1 18.92 21.01 2.15 o 11 6 1 5.70 4.63 1.00 o -11 7 1 96.76 102.65 3.74 o -10 7 1 81.77 79.19 3.79 o -9 7 1 66.19 72.92 3.02 o -8 7 1 179.74 177.58 4.46 o -7 7 1 427.53 387.40 4.72 o -6 7 1 139.01 157.54 3.15 o -5 7 1 117.01 115.14 2.71 o -4 7 1 220.76 213.49 3.78 o -3 7 1 16.17 21.09 1.26 o -2 7 1 498.87 516.42 4.67 o -1 7 1 1.23 3.46 0.55 o 0 7 1 4.60 3.16 0.55 o 1 7 1 74.23 96.91 2.14 o 2 7 1 1248.41 1290.61 9.66 o 3 7 1 81.51 97.22 2.87 o 4 7 1 1193.38 1227.33 17.58 o 5 7 1 503.79 492.78 6.89 o 6 7 1 614.77 574.15 8.06 o 7 7 1 59.24 55.64 1.84 o 8 7 1 20.90 19.79 1.39 o 9 7 1 9.06 11.15 1.54 o 10 7 1 17.73 21.68 1.78 o -11 8 1 286.22 305.36 6.53 o -10 8 1 215.18 230.58 4.38 o -9 8 1 58.75 78.48 3.36 o -8 8 1 4.78 5.18 1.05 o -7 8 1 33.04 35.31 1.52 o -6 8 1 692.51 679.01 7.58 o -5 8 1 3151.64 3077.19 18.60 o -4 8 1 924.78 902.22 13.28 o -3 8 1 973.12 1002.45 8.53 o -2 8 1 6.40 8.89 0.83 o -1 8 1 2458.16 2462.74 16.47 o 0 8 1 368.65 393.52 4.41 o 1 8 1 3.93 4.89 0.68 o 2 8 1 184.83 205.78 3.37 o 3 8 1 2350.28 2367.30 13.35 o 4 8 1 19.28 18.50 1.83 o 5 8 1 449.64 429.38 8.95 o 6 8 1 2.78 3.10 1.25 o 7 8 1 129.44 123.46 3.33 o 8 8 1 1012.41 985.74 10.93 o 9 8 1 135.79 137.33 4.27 o 10 8 1 7.75 10.28 1.42 o -10 9 1 186.00 180.72 5.31 o -9 9 1 1.49 2.50 1.04 o -8 9 1 338.58 321.94 6.86 o -7 9 1 788.25 731.49 8.32 o -6 9 1 7.08 7.50 0.65 o -5 9 1 25.13 25.26 1.93 o -4 9 1 1484.26 1476.24 10.99 o -3 9 1 474.92 486.90 6.94 o -2 9 1 2214.14 2142.71 15.83 o -1 9 1 36.29 51.76 2.13 o 0 9 1 252.51 211.38 3.95 o 1 9 1 22.07 23.64 1.27 o 2 9 1 797.54 805.63 7.38 o 3 9 1 9.74 13.47 1.27 o 4 9 1 604.14 593.63 8.54 o 5 9 1 2513.77 2458.48 17.75 o 6 9 1 1295.35 1250.04 9.64 o 7 9 1 733.05 723.12 8.33 o 8 9 1 35.36 31.02 1.68 o 9 9 1 33.91 35.97 1.67 o 10 9 1 3.00 4.71 1.20 o -10 10 1 28.01 34.75 1.84 o -9 10 1 7.01 4.20 1.23 o -8 10 1 88.35 76.29 3.36 o -7 10 1 106.20 102.40 3.55 o -6 10 1 493.04 468.01 5.75 o -5 10 1 867.72 833.15 6.60 o -4 10 1 3077.12 3057.13 21.11 o -3 10 1 772.63 787.35 9.38 o -2 10 1 205.93 204.73 4.64 o -1 10 1 0.95 0.86 0.74 o 0 10 1 70.34 64.54 2.20 o 1 10 1 379.55 360.34 5.88 o 2 10 1 21.41 18.20 1.26 o 3 10 1 697.06 689.85 8.03 o 4 10 1 914.83 899.45 6.55 o 5 10 1 1572.51 1532.33 11.69 o 6 10 1 0.17 -0.58 0.98 o 7 10 1 132.78 134.98 3.31 o 8 10 1 27.83 26.64 1.81 o 9 10 1 164.72 170.04 3.69 o -9 11 1 74.38 78.93 4.48 o -8 11 1 0.36 -0.28 1.26 o -7 11 1 30.44 30.65 2.18 o -6 11 1 225.79 230.77 4.32 o -5 11 1 43.89 43.97 1.54 o -4 11 1 207.23 195.91 3.07 o -3 11 1 1032.60 989.00 7.94 o -2 11 1 15.19 16.75 1.94 o -1 11 1 78.65 64.64 3.14 o 0 11 1 28.93 27.77 1.90 o 1 11 1 13.72 11.18 1.06 o 2 11 1 112.68 93.78 2.06 o 3 11 1 9.81 9.30 0.77 o 4 11 1 2.07 1.39 0.69 o 5 11 1 782.20 779.84 8.69 o 6 11 1 36.01 35.88 1.95 o 7 11 1 278.64 281.19 4.77 o 8 11 1 76.13 74.75 2.25 o 9 11 1 4.08 1.55 1.55 o -8 12 1 149.73 148.99 5.20 o -7 12 1 516.97 539.65 9.82 o -6 12 1 122.12 125.30 3.06 o -5 12 1 1.88 2.76 1.05 o -4 12 1 0.75 0.76 0.81 o -3 12 1 97.95 104.72 2.54 o -2 12 1 13.10 13.51 0.99 o -1 12 1 234.89 189.95 3.54 o 0 12 1 11.53 8.46 1.06 o 1 12 1 570.17 562.11 5.44 o 2 12 1 391.18 351.22 4.81 o 3 12 1 91.69 77.58 2.19 o 4 12 1 320.53 296.86 6.63 o 5 12 1 85.56 88.35 3.19 o 6 12 1 74.94 70.51 2.72 o 7 12 1 77.68 80.37 2.60 o 8 12 1 105.23 112.76 3.07 o -8 13 1 273.17 325.17 6.35 o -7 13 1 327.46 352.30 5.57 o -6 13 1 421.94 441.65 6.17 o -5 13 1 2.07 2.96 0.85 o -4 13 1 330.54 332.19 5.45 o -3 13 1 243.70 234.94 5.18 o -2 13 1 1155.36 1111.05 10.21 o -1 13 1 59.83 48.42 1.99 o 0 13 1 638.42 615.17 7.14 o 1 13 1 46.25 46.22 2.02 o 2 13 1 809.21 748.48 10.43 o 3 13 1 28.11 26.34 1.88 o 4 13 1 80.87 82.05 3.44 o 5 13 1 85.70 79.49 3.25 o 6 13 1 194.87 187.89 4.45 o 7 13 1 35.87 34.71 1.74 o -7 14 1 69.73 71.07 4.36 o -6 14 1 142.73 154.89 4.08 o -5 14 1 517.10 537.11 6.45 o -4 14 1 10.66 8.83 1.13 o -3 14 1 103.55 105.57 3.04 o -2 14 1 109.49 110.00 2.92 o -1 14 1 1175.59 1157.30 9.30 o 0 14 1 119.37 115.43 3.61 o 1 14 1 144.39 147.44 3.64 o 2 14 1 5.74 8.03 1.17 o 3 14 1 926.17 968.21 17.45 o 4 14 1 323.32 339.33 6.12 o 5 14 1 88.15 91.25 3.06 o 6 14 1 6.06 4.38 1.00 o -5 15 1 6.62 10.36 1.08 o -4 15 1 55.55 65.93 2.26 o -3 15 1 41.76 48.14 2.10 o -2 15 1 68.19 73.19 2.23 o -1 15 1 20.93 22.91 1.45 o 0 15 1 42.56 51.99 2.07 o 1 15 1 5.31 3.16 0.95 o 2 15 1 412.88 410.97 6.61 o 3 15 1 29.48 28.75 1.81 o 4 15 1 206.17 225.67 5.14 o 5 15 1 4.36 2.17 0.92 o -3 16 1 182.31 208.72 3.38 o -2 16 1 33.47 39.66 1.39 o -1 16 1 26.09 29.39 1.37 o 0 16 1 44.25 49.66 1.90 o 1 16 1 0.45 1.19 0.79 o 2 16 1 2.00 2.35 0.77 o 3 16 1 134.73 145.00 3.65 o -12 0 2 23.04 24.19 2.40 o -11 0 2 296.85 275.38 9.81 o -10 0 2 87.81 89.16 4.24 o -9 0 2 2894.24 2834.46 23.75 o -8 0 2 92.77 99.17 3.63 o -7 0 2 70.49 67.47 2.87 o -6 0 2 2733.37 2741.52 19.67 o -5 0 2 205.85 210.85 5.26 o -4 0 2 47.11 32.72 2.08 o -3 0 2 749.18 799.36 6.91 o -2 0 2 11061.35 11446.95 45.30 o -1 0 2 5990.15 6428.97 59.07 o 0 0 2 1224.52 1340.84 9.24 o 1 0 2 1335.90 1467.10 29.36 o 2 0 2 120.51 74.49 1.89 o 3 0 2 7296.45 7931.01 23.99 o 4 0 2 302.19 287.72 6.12 o 5 0 2 51.13 48.89 2.28 o 6 0 2 553.92 519.07 7.91 o 7 0 2 403.46 364.30 7.58 o 8 0 2 251.98 241.16 5.29 o 9 0 2 1.63 -0.05 1.69 o 10 0 2 82.37 78.43 4.60 o 11 0 2 1481.56 1669.43 16.70 o -12 1 2 379.74 412.31 6.40 o -11 1 2 4.57 4.67 1.72 o -10 1 2 127.81 111.12 3.31 o -9 1 2 2239.64 2246.20 13.51 o -8 1 2 206.49 189.48 3.81 o -7 1 2 2559.43 2483.25 20.30 o -6 1 2 29.81 21.54 1.22 o -5 1 2 1520.59 1603.15 11.87 o -4 1 2 22.69 30.75 1.14 o -3 1 2 1200.43 1245.88 7.43 o -2 1 2 245.12 248.03 2.58 o -1 1 2 1956.36 2168.35 14.41 o 0 1 2 51.61 57.72 2.90 o 1 1 2 59909.27 54292.86 159.32 o 2 1 2 2679.22 2889.87 12.14 o 3 1 2 279.48 316.65 2.75 o 4 1 2 538.28 561.25 5.42 o 5 1 2 297.16 258.76 3.94 o 6 1 2 79.75 83.04 3.20 o 7 1 2 725.92 698.99 8.42 o 8 1 2 264.34 259.31 3.72 o 9 1 2 834.82 803.81 10.73 o 10 1 2 452.17 466.54 7.59 o 11 1 2 674.12 733.06 7.81 o -12 2 2 99.05 99.68 3.50 o -11 2 2 40.27 37.44 3.04 o -10 2 2 251.71 255.16 5.91 o -9 2 2 2320.23 2310.59 14.12 o -8 2 2 377.93 361.68 5.95 o -7 2 2 50.30 55.99 2.24 o -6 2 2 1.03 4.98 0.81 o -5 2 2 66.19 52.19 1.56 o -4 2 2 0.93 1.72 0.51 o -3 2 2 600.55 652.65 5.98 o -2 2 2 306.11 296.08 2.52 o -1 2 2 1754.70 1872.69 12.69 o 0 2 2 517.00 528.61 4.48 o 1 2 2 435.68 469.71 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