#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:06:23 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181905 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/05/2240536.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240536 _cell_angle_alpha 90.000 _cell_angle_beta 91.820 _cell_angle_gamma 90.000 _cell_length_a 9.0293 _cell_length_b 15.2154 _cell_length_c 13.7936 _exptl_crystal_F_000 976.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file is53921sup2.hkl _cod_data_source_block 1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' suzuki0712off' _shelx_refln_list_code 4 _shelx_f_calc_maximum 251.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5328.16 4299.49 640.70 o 6 0 0 17321.66 16763.02 509.85 o 8 0 0 3973.60 4180.56 129.03 o 2 1 0 36704.85 37377.31 1080.82 o 3 1 0 6.15 6.63 4.46 o 4 1 0 6169.90 5881.03 118.51 o 5 1 0 359.80 424.14 17.90 o 6 1 0 400.97 355.43 12.77 o 7 1 0 666.28 709.28 35.32 o 8 1 0 1940.69 1978.29 56.79 o 9 1 0 330.68 301.00 19.46 o 10 1 0 1344.68 1484.83 82.46 o 11 1 0 145.58 155.40 50.39 o 1 2 0 9022.04 9528.30 93.52 o 2 2 0 35565.37 38069.75 686.11 o 3 2 0 13706.09 14197.77 195.35 o 4 2 0 4598.33 4490.78 66.13 o 5 2 0 9457.02 9889.94 201.88 o 6 2 0 9867.27 10012.79 158.46 o 7 2 0 836.17 757.80 28.65 o 8 2 0 2821.33 2766.44 93.23 o 9 2 0 2253.09 2314.92 58.64 o 10 2 0 105.09 92.13 29.50 o 11 2 0 839.18 866.95 47.09 o 1 3 0 4736.36 4435.39 41.07 o 2 3 0 2835.36 2638.99 32.87 o 3 3 0 624.45 648.79 11.48 o 4 3 0 14743.10 14870.25 223.11 o 5 3 0 905.22 871.09 19.55 o 6 3 0 478.41 440.27 19.05 o 7 3 0 2170.69 2060.09 36.40 o 8 3 0 1248.97 1125.28 39.10 o 9 3 0 326.13 330.95 24.63 o 10 3 0 1428.97 1605.51 56.10 o 11 3 0 0.50 7.90 12.46 o 0 4 0 339.73 459.43 10.52 o 1 4 0 3.57 17.30 3.20 o 2 4 0 33.17 123.89 7.39 o 3 4 0 22468.51 23090.41 381.77 o 4 4 0 1921.18 1802.71 28.94 o 5 4 0 4999.69 4884.54 88.59 o 6 4 0 1021.06 995.24 27.65 o 7 4 0 135.46 167.72 23.58 o 8 4 0 21.61 17.24 5.90 o 9 4 0 4110.09 3826.61 191.50 o 10 4 0 3.81 4.12 8.10 o 11 4 0 1413.80 1567.05 185.10 o 1 5 0 20401.78 21643.09 326.41 o 2 5 0 13995.48 15168.49 216.97 o 3 5 0 5904.91 6450.27 89.61 o 4 5 0 2147.27 2211.31 39.87 o 5 5 0 10370.69 10564.05 173.49 o 6 5 0 214.57 232.80 15.44 o 7 5 0 2159.06 2220.70 65.17 o 8 5 0 1129.51 1112.60 38.03 o 9 5 0 703.78 671.27 40.56 o 10 5 0 159.24 170.25 19.89 o 11 5 0 602.30 769.03 90.51 o 0 6 0 218.84 259.48 8.57 o 1 6 0 2712.64 2780.45 35.02 o 2 6 0 4753.60 5059.13 62.25 o 3 6 0 14552.66 14531.64 232.98 o 4 6 0 209.63 312.63 12.77 o 5 6 0 3017.89 2933.00 48.99 o 6 6 0 365.45 441.76 18.22 o 7 6 0 895.23 925.68 45.73 o 8 6 0 13.94 21.53 12.39 o 9 6 0 2427.20 2310.71 146.87 o 10 6 0 216.00 234.88 34.94 o 11 6 0 1348.22 1478.22 103.16 o 1 7 0 17290.29 17217.88 270.80 o 2 7 0 68.83 46.63 11.48 o 3 7 0 447.13 535.99 15.57 o 4 7 0 164.73 195.60 11.10 o 5 7 0 1719.63 1580.16 32.36 o 6 7 0 265.81 227.93 15.79 o 7 7 0 7652.69 7849.75 183.62 o 8 7 0 159.01 204.31 24.01 o 9 7 0 369.66 298.64 76.87 o 10 7 0 457.83 496.06 64.68 o 0 8 0 3173.74 3340.20 60.28 o 1 8 0 9559.20 9890.80 140.98 o 2 8 0 237.42 245.53 8.76 o 3 8 0 3312.86 3221.55 52.30 o 4 8 0 0.43 3.81 6.69 o 5 8 0 653.47 635.42 21.25 o 6 8 0 1220.62 1252.23 36.83 o 7 8 0 12.09 5.14 4.14 o 8 8 0 1904.25 1992.16 69.55 o 9 8 0 486.08 544.64 46.68 o 10 8 0 81.12 102.51 26.22 o 1 9 0 7267.80 7304.70 102.76 o 2 9 0 907.96 953.38 19.92 o 3 9 0 9.25 14.28 4.82 o 4 9 0 1075.95 1097.40 25.51 o 5 9 0 1209.47 1289.30 38.17 o 6 9 0 693.67 644.34 29.36 o 7 9 0 1501.49 1590.36 50.88 o 8 9 0 731.45 854.49 48.15 o 9 9 0 85.93 119.13 21.82 o 10 9 0 321.29 368.86 46.78 o 0 10 0 4773.59 5059.20 104.09 o 1 10 0 45.22 66.66 6.19 o 2 10 0 471.19 534.51 18.76 o 3 10 0 702.24 781.81 25.07 o 4 10 0 20.64 36.29 7.20 o 5 10 0 23.83 47.54 11.65 o 6 10 0 3011.65 3151.24 67.36 o 7 10 0 10.76 21.23 9.57 o 8 10 0 1334.03 1460.22 65.27 o 9 10 0 32.86 50.27 15.92 o 10 10 0 2.16 10.01 10.31 o 1 11 0 523.76 569.82 21.32 o 2 11 0 3363.61 3255.56 63.05 o 3 11 0 216.25 186.43 12.49 o 4 11 0 5060.55 5173.78 93.09 o 5 11 0 2535.26 2636.31 64.70 o 6 11 0 1196.20 1225.70 48.11 o 7 11 0 116.33 134.19 18.52 o 8 11 0 788.09 864.76 48.05 o 9 11 0 100.61 106.42 18.42 o 0 12 0 4.18 12.70 6.89 o 1 12 0 165.23 160.78 11.80 o 2 12 0 1989.84 1988.23 47.45 o 3 12 0 0.59 9.29 5.35 o 4 12 0 106.74 101.64 11.87 o 5 12 0 0.20 18.58 8.24 o 6 12 0 998.93 1009.36 37.06 o 7 12 0 19.86 30.93 11.02 o 8 12 0 662.34 732.68 37.55 o 9 12 0 109.57 103.88 25.42 o 1 13 0 187.71 178.15 11.62 o 2 13 0 1604.97 1567.78 48.13 o 3 13 0 711.14 712.03 26.52 o 4 13 0 6978.29 6942.11 146.22 o 5 13 0 34.02 35.90 11.56 o 6 13 0 388.28 410.98 30.32 o 7 13 0 187.79 220.38 29.72 o 8 13 0 173.19 189.76 23.78 o 0 14 0 699.73 729.18 34.65 o 1 14 0 9.46 17.43 7.77 o 2 14 0 256.94 249.19 23.51 o 3 14 0 243.30 232.95 17.40 o 4 14 0 2.57 16.32 7.78 o 5 14 0 28.91 36.34 10.94 o 6 14 0 96.76 145.57 20.86 o 7 14 0 3.34 6.72 10.84 o 8 14 0 285.50 288.00 25.26 o 1 15 0 3377.17 3292.90 92.44 o 2 15 0 487.87 508.58 27.05 o 3 15 0 78.23 75.97 15.41 o 4 15 0 203.15 232.65 20.01 o 5 15 0 1436.51 1416.25 50.75 o 6 15 0 277.34 361.76 29.28 o 7 15 0 747.42 763.63 42.58 o 0 16 0 1135.81 1158.11 54.36 o 1 16 0 6.91 19.58 7.93 o 2 16 0 19.97 18.30 10.70 o 3 16 0 661.81 688.11 32.35 o 4 16 0 73.44 97.62 23.72 o 5 16 0 231.17 239.16 23.40 o 6 16 0 213.28 217.65 25.16 o 1 17 0 2076.31 2098.06 80.29 o 2 17 0 12.99 37.92 12.24 o 3 17 0 0.13 0.34 7.03 o 4 17 0 110.68 103.19 21.87 o 5 17 0 632.87 545.76 108.52 o 0 18 0 1.41 24.96 16.93 o 1 18 0 946.41 1010.51 45.63 o 2 18 0 21.52 15.78 14.60 o 3 18 0 694.58 622.66 77.42 o 4 18 0 21.26 18.09 13.94 o 1 19 0 472.78 481.35 33.19 o 2 19 0 659.03 624.26 35.63 o 3 19 0 18.14 33.79 16.65 o -9 0 1 6329.54 6550.00 251.17 o -7 0 1 5786.90 5497.30 129.80 o -5 0 1 2099.25 1770.05 150.83 o -3 0 1 18763.67 18189.39 367.28 o 3 0 1 2961.51 2937.88 58.51 o 7 0 1 1.12 4.82 6.03 o 9 0 1 201.63 199.21 32.83 o 11 0 1 174.29 239.95 34.25 o -11 1 1 934.76 987.21 62.33 o -9 1 1 103.51 100.76 12.55 o -8 1 1 700.87 679.56 27.09 o -7 1 1 15128.00 15394.32 353.79 o -6 1 1 1514.14 1444.56 33.53 o -5 1 1 9585.66 9195.11 137.63 o -4 1 1 32.21 15.47 2.48 o -3 1 1 1365.36 1453.20 19.60 o -2 1 1 237.61 199.66 4.22 o 1 1 1 24843.01 26251.05 290.37 o 2 1 1 16812.12 16900.13 178.00 o 3 1 1 229.19 271.79 14.22 o 4 1 1 185.81 277.09 19.68 o 5 1 1 11340.42 11177.33 243.75 o 6 1 1 293.27 284.06 13.62 o 7 1 1 10322.76 10462.13 248.25 o 8 1 1 983.45 971.72 33.26 o 9 1 1 514.00 560.13 35.33 o 10 1 1 248.38 246.68 37.61 o 11 1 1 0.42 -3.27 7.73 o -11 2 1 448.67 380.30 240.79 o -10 2 1 284.39 292.81 49.24 o -9 2 1 2963.17 3088.44 77.12 o -8 2 1 10.79 10.68 2.85 o -7 2 1 877.36 855.18 28.81 o -6 2 1 999.18 937.01 36.60 o -5 2 1 6398.69 6612.53 93.81 o -4 2 1 1.74 9.43 4.15 o -3 2 1 27533.09 27497.59 465.21 o -2 2 1 6580.24 7364.53 148.59 o -1 2 1 4922.54 4887.15 52.80 o 0 2 1 17448.38 17356.17 229.21 o 1 2 1 1591.85 1905.81 21.34 o 2 2 1 3510.45 3813.29 32.18 o 3 2 1 17073.44 16742.58 219.76 o 4 2 1 346.45 352.38 13.76 o 5 2 1 2695.09 2775.45 56.25 o 6 2 1 1405.35 1392.63 37.89 o 7 2 1 42.33 58.00 9.01 o 8 2 1 382.48 394.22 25.43 o 9 2 1 747.53 710.69 27.79 o 10 2 1 82.36 83.44 16.35 o 11 2 1 658.05 690.73 46.92 o -11 3 1 1185.36 1376.15 77.33 o -10 3 1 1850.89 2043.90 64.73 o -9 3 1 279.96 306.52 35.89 o -8 3 1 1223.60 1157.09 26.00 o -7 3 1 2525.39 2332.26 60.23 o -6 3 1 813.26 780.19 25.48 o -5 3 1 12815.55 12720.86 219.27 o -4 3 1 14984.82 15148.68 228.02 o -3 3 1 1362.63 1270.49 19.26 o -2 3 1 63255.06 66849.19 1561.97 o -1 3 1 49716.63 52406.51 1062.32 o 0 3 1 1241.85 1411.15 15.90 o 1 3 1 16693.07 16930.19 215.42 o 2 3 1 8651.99 8663.77 97.41 o 3 3 1 262.75 296.64 7.68 o 4 3 1 8218.89 7674.17 109.45 o 5 3 1 8672.67 8496.83 139.67 o 6 3 1 1648.08 1607.11 41.88 o 7 3 1 1434.16 1390.77 44.47 o 8 3 1 567.02 524.78 28.95 o 9 3 1 1003.48 1137.15 52.94 o 10 3 1 2241.66 2374.31 68.25 o 11 3 1 595.71 653.45 50.13 o -11 4 1 755.12 1017.04 110.65 o -10 4 1 155.09 160.20 18.43 o -9 4 1 314.27 323.48 21.06 o -8 4 1 213.10 216.22 13.01 o -7 4 1 0.42 9.56 5.45 o -6 4 1 1232.38 1267.19 31.97 o -5 4 1 1619.29 1506.89 31.31 o -4 4 1 10188.30 10892.08 160.90 o -3 4 1 22798.25 23151.85 377.30 o -2 4 1 9268.77 10042.23 124.23 o -1 4 1 2817.15 3231.85 33.07 o 0 4 1 8420.23 8847.27 93.36 o 1 4 1 15779.42 17135.78 240.23 o 2 4 1 2139.76 1966.19 27.58 o 3 4 1 8286.71 8144.27 99.68 o 4 4 1 1.33 4.10 1.88 o 5 4 1 9.72 16.25 4.22 o 6 4 1 1273.90 1213.99 51.61 o 7 4 1 134.85 138.28 22.04 o 8 4 1 4629.05 4708.52 176.99 o 9 4 1 728.56 674.11 57.94 o 10 4 1 209.60 219.15 21.88 o 11 4 1 470.96 493.59 69.77 o -11 5 1 6.59 7.11 22.55 o -10 5 1 3639.81 3925.74 143.85 o -9 5 1 57.47 53.61 8.45 o -8 5 1 1763.49 1745.72 65.50 o -7 5 1 4.15 8.94 8.34 o -6 5 1 679.24 607.84 31.53 o -5 5 1 338.36 356.29 13.15 o -4 5 1 31879.45 33118.71 655.62 o -3 5 1 605.51 702.86 14.04 o -2 5 1 28457.50 30274.28 538.91 o -1 5 1 11154.24 11998.38 151.13 o 0 5 1 3464.48 3687.58 39.88 o 1 5 1 805.81 852.56 15.75 o 2 5 1 14168.34 14625.15 199.02 o 3 5 1 2010.38 2262.45 31.99 o 4 5 1 19589.66 19718.02 339.93 o 5 5 1 542.77 509.75 10.37 o 6 5 1 302.94 315.44 17.67 o 7 5 1 713.08 735.46 31.90 o 8 5 1 147.89 120.18 22.38 o 9 5 1 452.77 431.22 39.55 o 10 5 1 3250.46 3450.61 107.81 o 11 5 1 0.39 19.70 19.42 o -11 6 1 0.64 24.94 14.32 o -10 6 1 22.36 42.96 30.86 o -9 6 1 352.45 380.93 36.94 o -8 6 1 1530.35 1542.94 83.64 o -7 6 1 40.61 41.31 10.64 o -6 6 1 6982.60 7201.68 139.81 o -5 6 1 1959.55 1989.18 38.53 o -4 6 1 140.40 119.83 7.49 o -3 6 1 275.55 398.42 10.10 o -2 6 1 3582.93 3474.14 42.34 o -1 6 1 3809.39 4266.81 51.56 o 0 6 1 12681.14 13161.58 179.40 o 1 6 1 12058.55 12884.46 170.57 o 2 6 1 9739.02 9904.93 140.13 o 3 6 1 153.86 207.73 17.47 o 4 6 1 991.48 997.28 21.08 o 5 6 1 84.37 81.07 7.79 o 6 6 1 3919.51 3719.36 93.25 o 7 6 1 1008.21 1065.26 50.68 o 8 6 1 1212.95 1333.62 64.62 o 9 6 1 162.65 222.91 27.49 o 10 6 1 396.77 451.16 46.62 o 11 6 1 112.84 102.29 30.52 o -10 7 1 926.55 991.47 90.92 o -9 7 1 511.80 462.09 57.65 o -8 7 1 2212.47 2380.35 73.73 o -7 7 1 138.19 142.35 12.79 o -6 7 1 1951.09 1983.46 45.87 o -5 7 1 2094.20 2101.61 71.63 o -4 7 1 1482.23 1243.31 26.21 o -3 7 1 1581.81 1584.74 27.38 o -2 7 1 6122.60 5881.04 85.23 o -1 7 1 3538.05 3778.18 51.54 o 0 7 1 2078.47 2507.48 34.23 o 1 7 1 2654.38 2660.37 37.56 o 2 7 1 2145.25 1817.34 28.78 o 3 7 1 1923.03 1949.60 44.61 o 4 7 1 4447.90 4359.15 70.23 o 5 7 1 1868.83 1760.92 47.58 o 6 7 1 1038.34 1068.99 23.09 o 7 7 1 1972.55 2079.98 61.28 o 8 7 1 1706.04 1737.21 99.80 o 9 7 1 909.33 911.85 78.32 o 10 7 1 475.79 512.69 66.45 o -10 8 1 105.43 97.27 25.31 o -9 8 1 99.90 102.39 21.70 o -8 8 1 2152.52 2224.18 65.50 o -7 8 1 269.11 273.67 24.10 o -6 8 1 8504.27 8904.29 186.85 o -5 8 1 1459.13 1582.08 37.12 o -4 8 1 1199.86 1191.42 27.42 o -3 8 1 13.38 11.87 4.22 o -2 8 1 1567.78 1427.35 24.20 o -1 8 1 3295.78 3421.58 49.58 o 0 8 1 20388.96 20371.33 337.35 o 1 8 1 2042.06 2128.88 33.29 o 2 8 1 2349.86 2562.03 37.68 o 3 8 1 1.74 11.04 5.19 o 4 8 1 949.70 933.05 20.19 o 5 8 1 3510.68 3564.00 69.62 o 6 8 1 7312.56 7140.66 287.16 o 7 8 1 141.20 124.90 10.14 o 8 8 1 2272.48 2350.33 76.80 o 9 8 1 289.84 292.90 35.00 o 10 8 1 1.60 4.64 18.14 o -10 9 1 66.00 32.92 22.31 o -9 9 1 7.16 5.27 7.07 o -8 9 1 1084.66 1155.22 57.38 o -7 9 1 1782.57 1902.22 55.93 o -6 9 1 55.03 58.34 9.76 o -5 9 1 18.99 37.32 6.86 o -4 9 1 240.36 280.24 15.00 o -3 9 1 90.12 74.29 7.23 o -2 9 1 361.20 342.04 18.88 o -1 9 1 787.09 692.82 15.87 o 0 9 1 28.42 57.51 6.60 o 1 9 1 7891.47 8477.19 130.78 o 2 9 1 1147.34 1212.18 21.72 o 3 9 1 595.78 584.04 16.22 o 4 9 1 583.40 668.01 19.28 o 5 9 1 331.32 329.48 18.97 o 6 9 1 277.25 257.64 16.96 o 7 9 1 3383.52 3343.19 90.56 o 8 9 1 191.80 218.14 19.42 o 9 9 1 119.79 118.03 21.88 o 10 9 1 160.47 145.59 31.77 o -10 10 1 13.44 1.42 6.91 o -9 10 1 1427.53 1474.18 61.24 o -8 10 1 812.86 880.23 40.90 o -7 10 1 95.96 101.97 13.14 o -6 10 1 2011.74 2071.21 48.70 o -5 10 1 339.36 370.14 18.87 o -4 10 1 215.04 245.85 13.89 o -3 10 1 3971.53 3968.70 76.90 o -2 10 1 4107.27 4256.02 73.14 o -1 10 1 11360.71 11619.81 189.95 o 0 10 1 3650.15 3706.02 61.82 o 1 10 1 395.29 417.20 16.24 o 2 10 1 1192.32 1144.14 27.20 o 3 10 1 4120.50 4187.35 82.33 o 4 10 1 786.99 838.60 37.33 o 5 10 1 5504.94 5782.13 105.53 o 6 10 1 1663.83 1766.61 44.06 o 7 10 1 116.64 117.78 9.44 o 8 10 1 269.12 296.13 24.28 o 9 10 1 1784.14 1981.11 74.34 o 10 10 1 113.72 118.78 25.79 o -9 11 1 2.69 2.54 6.90 o -8 11 1 13.06 22.16 10.79 o -7 11 1 147.43 174.58 20.26 o -6 11 1 271.85 225.94 20.52 o -5 11 1 709.98 691.03 30.85 o -4 11 1 690.09 697.88 27.34 o -3 11 1 1094.05 1044.95 27.13 o -2 11 1 187.93 199.82 12.07 o -1 11 1 3005.88 3004.88 53.05 o 0 11 1 110.10 124.98 9.43 o 1 11 1 3038.03 2898.81 65.52 o 2 11 1 0.19 13.05 5.62 o 3 11 1 1889.83 2004.67 63.43 o 4 11 1 649.73 677.18 21.69 o 5 11 1 95.31 85.64 12.90 o 6 11 1 60.62 53.11 11.03 o 7 11 1 1395.71 1432.96 53.41 o 8 11 1 251.79 253.21 37.43 o 9 11 1 784.94 930.31 49.18 o -9 12 1 683.15 742.86 58.67 o -8 12 1 17.21 4.50 7.89 o -7 12 1 212.35 216.16 20.41 o -6 12 1 31.62 39.25 10.41 o -5 12 1 953.21 927.32 35.27 o -4 12 1 0.14 3.73 5.88 o -3 12 1 6551.16 6540.07 117.70 o -2 12 1 219.67 214.25 12.48 o -1 12 1 318.43 305.40 17.13 o 0 12 1 639.62 633.28 18.49 o 1 12 1 239.68 223.03 12.20 o 2 12 1 3.50 18.45 8.80 o 3 12 1 6957.27 6889.73 131.07 o 4 12 1 51.17 42.28 9.08 o 5 12 1 3112.54 3149.88 79.43 o 6 12 1 119.95 157.33 15.05 o 7 12 1 0.03 5.86 6.50 o 8 12 1 40.54 50.02 12.82 o 9 12 1 1783.39 2069.22 109.70 o -8 13 1 10.00 -1.31 9.16 o -7 13 1 184.75 196.71 26.63 o -6 13 1 0.77 2.64 8.22 o -5 13 1 2220.01 2299.31 74.15 o -4 13 1 120.23 138.18 14.41 o -3 13 1 0.16 1.12 4.65 o -2 13 1 89.99 71.82 9.27 o -1 13 1 2.18 12.84 5.85 o 0 13 1 284.23 284.83 29.22 o 1 13 1 2092.42 2134.82 45.39 o 2 13 1 160.66 147.19 14.77 o 3 13 1 1765.52 1725.24 45.40 o 4 13 1 485.09 446.78 24.96 o 5 13 1 788.29 848.70 52.54 o 6 13 1 0.72 10.61 8.78 o 7 13 1 1402.16 1500.05 76.75 o 8 13 1 1.96 12.79 11.13 o -8 14 1 446.38 475.77 31.62 o -7 14 1 20.18 34.09 12.86 o -6 14 1 564.11 621.03 35.50 o -5 14 1 374.70 431.36 27.09 o -4 14 1 113.54 133.28 15.79 o -3 14 1 1878.28 1993.32 53.86 o -2 14 1 1400.91 1397.56 48.80 o -1 14 1 527.34 567.55 25.53 o 0 14 1 254.52 231.12 15.36 o 1 14 1 411.41 437.24 29.53 o 2 14 1 1085.46 1077.19 60.89 o 3 14 1 3608.77 3745.44 86.70 o 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