data_2240538 _cell_angle_alpha 87.307 _cell_angle_beta 81.801 _cell_angle_gamma 70.819 _cell_length_a 9.8413 _cell_length_b 13.8246 _cell_length_c 16.1670 _exptl_crystal_F_000 1012.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file is53923sup4.hkl _[local]_cod_data_source_block 3 _shelx_title ' suzuki17' _shelx_refln_list_code 4 _shelx_f_calc_maximum 283.32 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2852.38 2656.14 94.68 o 3 0 0 5138.78 5260.05 87.36 o 4 0 0 848.16 812.64 27.26 o 5 0 0 1409.37 1307.74 60.38 o 6 0 0 203.33 159.90 17.53 o 7 0 0 6.67 -6.02 10.04 o 8 0 0 4849.48 5129.60 225.13 o 9 0 0 537.68 615.85 47.03 o 10 0 0 31.66 32.29 36.93 o 11 0 0 566.05 648.02 60.71 o -11 1 0 267.87 195.98 130.16 o -10 1 0 133.20 134.05 32.13 o -9 1 0 1942.36 2084.32 144.23 o -8 1 0 781.77 744.02 48.60 o -7 1 0 101.02 79.55 18.44 o -6 1 0 279.38 295.09 37.82 o -5 1 0 193.03 255.80 31.46 o -4 1 0 876.92 710.08 26.81 o -3 1 0 7473.93 7329.65 172.24 o -2 1 0 6289.25 6405.99 163.90 o -1 1 0 11965.15 10268.09 207.49 o 2 1 0 6362.45 6275.85 98.65 o 3 1 0 2487.47 2509.44 47.91 o 4 1 0 2627.19 2414.19 45.07 o 5 1 0 2445.95 2436.14 44.66 o 6 1 0 30.41 40.94 10.89 o 7 1 0 1599.43 1586.45 83.19 o 8 1 0 672.99 660.40 40.65 o 9 1 0 0.69 -14.84 26.72 o 10 1 0 923.82 1088.05 68.62 o 11 1 0 58.00 73.71 46.37 o 12 1 0 118.88 127.76 61.50 o -11 2 0 25.08 28.24 23.71 o -10 2 0 545.26 447.25 284.94 o -9 2 0 624.34 431.61 46.13 o -8 2 0 67.10 57.51 11.31 o -7 2 0 514.62 520.61 40.91 o -6 2 0 131.92 107.14 29.79 o -5 2 0 634.53 623.82 28.57 o -4 2 0 140.31 63.03 23.91 o -3 2 0 1001.71 1053.92 26.44 o -2 2 0 530.37 603.39 11.61 o -1 2 0 25.05 20.27 4.23 o 0 2 0 1240.61 1188.53 19.09 o 1 2 0 2505.92 2492.57 37.64 o 2 2 0 1932.24 2246.35 39.58 o 3 2 0 1712.18 1941.58 31.87 o 4 2 0 3492.96 3790.81 75.99 o 5 2 0 895.61 765.18 46.70 o 6 2 0 21.23 16.61 10.77 o 7 2 0 11.83 -2.96 13.66 o 8 2 0 4.42 10.56 11.49 o 9 2 0 796.67 858.14 80.29 o 10 2 0 1307.03 1392.21 73.88 o 11 2 0 0.54 -11.55 29.62 o 12 2 0 26.78 24.01 22.46 o -11 3 0 6.03 3.66 14.37 o -10 3 0 235.49 257.62 54.71 o -9 3 0 1.15 -9.12 15.74 o -8 3 0 457.69 425.37 264.59 o -7 3 0 1023.73 1111.05 56.20 o -6 3 0 204.24 153.12 6.63 o -5 3 0 49.81 51.92 7.74 o -4 3 0 12.14 8.44 4.68 o -3 3 0 72.87 60.18 5.79 o -2 3 0 260.65 294.83 7.92 o -1 3 0 835.83 839.83 28.05 o 0 3 0 124.94 179.44 16.52 o 1 3 0 14517.29 14113.85 251.96 o 2 3 0 24.64 25.63 5.41 o 3 3 0 692.87 759.52 26.42 o 4 3 0 50.38 60.90 5.82 o 5 3 0 1378.23 1399.97 30.77 o 6 3 0 544.46 623.95 22.39 o 7 3 0 789.50 730.19 28.21 o 8 3 0 35.11 17.22 12.15 o 9 3 0 1618.36 1818.91 75.49 o 10 3 0 566.83 613.51 76.94 o 11 3 0 10.87 23.93 19.02 o 12 3 0 10.38 10.95 31.71 o -10 4 0 158.87 163.89 29.67 o -9 4 0 39.57 62.67 34.37 o -8 4 0 1446.08 1618.91 94.15 o -7 4 0 53.00 57.43 18.81 o -6 4 0 2.57 6.32 8.15 o -5 4 0 15.83 25.60 8.86 o -4 4 0 139.25 142.06 14.29 o -3 4 0 4869.18 5101.53 158.04 o -2 4 0 3719.61 3636.83 125.70 o -1 4 0 1326.96 1341.17 24.85 o 0 4 0 18394.64 17816.62 482.03 o 1 4 0 14665.60 14359.19 320.50 o 2 4 0 2730.18 2807.79 42.11 o 3 4 0 49.65 64.00 7.14 o 4 4 0 100.64 86.90 10.35 o 5 4 0 87.63 62.07 11.38 o 6 4 0 671.67 576.00 21.41 o 7 4 0 1926.38 1866.76 120.60 o 8 4 0 2599.26 2711.80 89.16 o 9 4 0 1550.73 1569.60 66.14 o 10 4 0 77.84 87.54 40.45 o 11 4 0 391.73 465.70 72.88 o 12 4 0 61.89 75.66 27.30 o -10 5 0 196.70 236.24 42.84 o -9 5 0 245.32 284.56 40.15 o -8 5 0 706.14 861.41 57.13 o -7 5 0 52.48 36.55 18.32 o -6 5 0 2.59 8.76 11.24 o -5 5 0 88.59 63.99 14.57 o -4 5 0 1882.84 1809.43 48.76 o -3 5 0 1254.35 529.97 431.68 o -2 5 0 636.73 513.32 31.50 o -1 5 0 205.61 177.90 14.33 o 0 5 0 6107.82 5976.37 148.04 o 1 5 0 31.80 45.02 4.59 o 2 5 0 5489.94 5504.65 147.04 o 3 5 0 2688.14 2750.55 63.91 o 4 5 0 1718.17 1842.63 38.18 o 5 5 0 219.97 230.57 11.89 o 6 5 0 2967.71 3117.78 111.14 o 7 5 0 13.39 9.04 13.54 o 8 5 0 3377.44 3534.64 205.12 o 9 5 0 86.22 76.87 17.21 o 10 5 0 786.11 813.14 81.74 o 11 5 0 1157.88 1243.26 110.54 o 12 5 0 6.95 25.27 20.86 o -9 6 0 558.95 735.54 90.38 o -8 6 0 66.34 37.44 17.78 o -7 6 0 1087.45 1110.31 107.59 o -6 6 0 597.68 605.34 51.86 o -5 6 0 23.23 30.46 18.78 o -4 6 0 329.31 401.22 19.82 o -3 6 0 2129.45 2110.67 47.95 o -2 6 0 2034.41 2175.85 44.82 o -1 6 0 1564.77 1317.56 31.58 o 0 6 0 3635.78 3715.22 101.08 o 1 6 0 6139.47 6460.56 113.30 o 2 6 0 10056.92 9995.21 351.79 o 3 6 0 466.35 492.83 10.40 o 4 6 0 9.92 13.99 6.43 o 5 6 0 946.23 913.73 54.34 o 6 6 0 168.05 149.89 16.58 o 7 6 0 922.19 882.73 91.17 o 8 6 0 1754.54 2020.98 99.37 o 9 6 0 406.81 404.42 28.33 o 10 6 0 3299.25 3787.96 198.54 o 11 6 0 577.37 632.43 81.43 o 12 6 0 207.75 209.91 59.18 o -9 7 0 310.25 323.39 39.09 o -8 7 0 138.05 131.72 30.94 o -7 7 0 1209.95 1418.82 71.51 o -6 7 0 29.88 17.68 14.75 o -5 7 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14.16 o 9 8 0 247.49 286.09 24.02 o 10 8 0 121.00 130.01 18.43 o 11 8 0 194.25 174.10 48.19 o 12 8 0 194.77 114.28 47.49 o -8 9 0 101.12 98.20 25.93 o -7 9 0 0.90 -12.61 14.29 o -6 9 0 78.40 104.43 20.13 o -5 9 0 20.20 17.03 14.11 o -4 9 0 357.39 321.27 27.50 o -3 9 0 76.31 85.24 12.22 o -2 9 0 447.86 422.56 23.45 o -1 9 0 472.20 509.22 31.06 o 0 9 0 744.95 722.18 39.82 o 1 9 0 447.07 509.28 23.34 o 2 9 0 2382.54 2525.22 55.05 o 3 9 0 1454.75 1518.26 30.38 o 4 9 0 70.11 71.06 10.23 o 5 9 0 96.48 114.24 12.85 o 6 9 0 21.31 17.79 6.75 o 7 9 0 335.30 342.83 27.64 o 8 9 0 130.67 151.13 21.76 o 9 9 0 92.96 95.64 22.02 o 10 9 0 30.15 39.76 19.90 o 11 9 0 157.21 114.14 21.53 o 12 9 0 11.41 3.50 22.87 o -7 10 0 93.97 85.36 27.73 o -6 10 0 206.89 244.50 46.85 o -5 10 0 2.43 -1.41 10.23 o -4 10 0 4.15 -7.86 11.07 o -3 10 0 54.25 27.06 8.73 o -2 10 0 43.13 30.64 9.46 o -1 10 0 759.33 831.12 32.91 o 0 10 0 1742.13 1893.05 62.33 o 1 10 0 279.65 257.07 13.46 o 2 10 0 1799.60 1778.32 55.41 o 3 10 0 253.13 234.74 16.37 o 4 10 0 17.94 11.64 7.54 o 5 10 0 96.49 118.40 15.79 o 6 10 0 564.94 562.80 27.15 o 7 10 0 398.01 397.38 45.02 o 8 10 0 1152.30 1317.43 103.48 o 9 10 0 77.30 66.74 19.76 o 10 10 0 251.82 303.44 94.47 o 11 10 0 177.31 148.25 33.81 o 12 10 0 0.19 2.61 12.94 o -6 11 0 4.13 12.51 23.79 o -5 11 0 18.66 32.94 18.02 o -4 11 0 34.88 48.44 24.05 o -3 11 0 22.22 19.77 9.04 o -2 11 0 6.46 17.02 9.32 o -1 11 0 1559.44 1585.12 56.25 o 0 11 0 1152.96 1390.24 42.34 o 1 11 0 236.54 199.69 12.49 o 2 11 0 556.95 648.80 23.00 o 3 11 0 5.44 8.60 8.32 o 4 11 0 407.24 478.70 23.49 o 5 11 0 3.50 0.04 7.96 o 6 11 0 268.44 276.68 15.74 o 7 11 0 1183.13 1369.22 134.39 o 8 11 0 1382.50 1558.09 133.19 o 9 11 0 33.66 40.96 17.07 o 10 11 0 811.54 936.22 105.95 o 11 11 0 72.06 57.48 26.52 o -6 12 0 14.30 17.26 27.07 o -5 12 0 281.23 187.57 44.17 o -4 12 0 297.90 275.39 41.41 o -3 12 0 1.63 1.16 8.26 o -2 12 0 565.65 580.79 36.89 o -1 12 0 1825.82 1996.40 93.68 o 0 12 0 0.27 -0.63 6.74 o 1 12 0 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