data_2240542 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.3680 _cell_length_b 22.4243 _cell_length_c 6.6148 _exptl_crystal_F_000 492.00 _reflns_d_resolution_high 0.8314 _cod_data_source_file su5104Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bp1a in Pba2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 145.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -7 601.72 543.59 42.39 o 2 0 -7 24.29 10.70 15.93 o 4 0 -7 70.61 66.74 19.69 o 1 1 -7 109.70 100.39 9.07 o 2 1 -7 70.37 75.98 11.77 o 3 1 -7 21.35 21.91 11.44 o 4 1 -7 71.65 83.33 14.05 o 0 2 -7 89.71 105.42 11.41 o 1 2 -7 133.91 126.02 9.47 o 2 2 -7 67.89 71.86 10.47 o 3 2 -7 10.28 2.89 11.80 o 4 2 -7 25.44 -9.07 23.51 o 1 3 -7 54.48 59.45 9.60 o 2 3 -7 27.31 29.35 12.75 o 3 3 -7 99.62 88.01 13.17 o 4 3 -7 41.39 30.32 13.90 o 0 4 -7 24.59 22.61 11.49 o 1 4 -7 69.34 52.07 9.87 o 2 4 -7 19.95 10.57 11.06 o 3 4 -7 55.20 54.69 12.72 o 4 4 -7 6.97 23.62 15.40 o 1 5 -7 11.60 3.46 10.68 o 2 5 -7 14.16 32.86 14.56 o 3 5 -7 79.57 87.29 12.87 o 0 6 -7 72.99 69.81 15.45 o 1 6 -7 150.71 165.50 14.25 o 2 6 -7 18.06 19.66 16.69 o 3 6 -7 41.66 34.48 16.79 o 1 7 -7 7.33 14.05 13.27 o 2 7 -7 68.72 78.57 17.30 o 3 7 -7 36.72 64.52 18.37 o 0 8 -7 210.77 227.06 26.02 o 1 8 -7 0.41 -13.32 13.32 o 2 8 -7 116.59 147.16 18.12 o 3 8 -7 39.40 37.90 18.60 o 1 9 -7 14.60 23.28 17.55 o 2 9 -7 99.61 88.86 21.23 o 3 9 -7 8.70 -7.33 25.47 o 0 10 -7 23.00 43.26 24.81 o 1 10 -7 60.93 39.90 20.69 o 2 10 -7 40.98 24.36 22.83 o 1 11 -7 2.31 -16.35 21.12 o 2 11 -7 8.15 -9.22 22.05 o 0 12 -7 3.68 -35.78 35.78 o 1 12 -7 90.96 71.47 22.63 o 0 0 -6 610.25 612.39 21.93 o 2 0 -6 404.48 415.55 24.33 o 4 0 -6 32.13 60.86 12.05 o 1 1 -6 40.67 52.02 5.19 o 2 1 -6 378.23 371.77 12.27 o 3 1 -6 61.04 61.23 7.26 o 4 1 -6 154.71 171.23 9.62 o 5 1 -6 9.04 -0.88 15.81 o 0 2 -6 239.15 264.30 10.95 o 1 2 -6 668.76 648.38 13.35 o 2 2 -6 16.52 19.69 5.96 o 3 2 -6 52.38 40.89 7.43 o 4 2 -6 44.01 30.04 8.56 o 5 2 -6 98.48 98.04 14.06 o 1 3 -6 176.73 176.27 6.41 o 2 3 -6 22.90 13.12 5.59 o 3 3 -6 213.81 229.64 9.55 o 4 3 -6 55.22 42.17 8.66 o 5 3 -6 154.86 179.32 15.40 o 0 4 -6 34.83 35.93 7.26 o 1 4 -6 286.00 299.20 9.35 o 2 4 -6 152.70 140.95 6.87 o 3 4 -6 86.54 92.74 7.63 o 4 4 -6 3.80 18.27 8.51 o 5 4 -6 60.91 66.50 14.15 o 1 5 -6 35.43 33.75 5.38 o 2 5 -6 38.28 29.18 5.98 o 3 5 -6 337.52 325.66 12.09 o 4 5 -6 9.82 16.69 10.98 o 5 5 -6 139.62 156.53 15.42 o 0 6 -6 259.51 266.51 12.38 o 1 6 -6 103.03 118.33 7.51 o 2 6 -6 222.98 223.02 10.22 o 3 6 -6 49.89 42.66 9.22 o 4 6 -6 29.58 24.77 9.57 o 5 6 -6 59.48 72.46 16.57 o 1 7 -6 11.96 11.31 7.47 o 2 7 -6 176.87 168.37 9.76 o 3 7 -6 50.36 41.40 10.29 o 4 7 -6 176.24 167.81 14.36 o 5 7 -6 15.07 27.03 16.35 o 0 8 -6 469.57 461.92 27.31 o 1 8 -6 7.22 14.21 9.50 o 2 8 -6 347.73 355.04 15.55 o 3 8 -6 24.26 16.12 10.55 o 4 8 -6 85.16 80.32 14.84 o 5 8 -6 25.41 0.11 22.20 o 1 9 -6 31.20 28.42 11.09 o 2 9 -6 172.61 162.96 10.09 o 3 9 -6 46.16 36.29 10.90 o 4 9 -6 216.71 219.32 18.00 o 5 9 -6 32.58 -16.26 24.61 o 0 10 -6 225.87 237.53 33.65 o 1 10 -6 106.90 92.71 13.28 o 2 10 -6 35.04 34.15 9.34 o 3 10 -6 55.17 46.41 11.83 o 4 10 -6 40.23 45.13 20.96 o 1 11 -6 40.10 26.75 13.47 o 2 11 -6 29.19 16.75 16.51 o 3 11 -6 155.36 164.34 19.25 o 4 11 -6 40.05 59.89 21.02 o 0 12 -6 64.85 52.63 19.67 o 1 12 -6 144.49 126.66 15.43 o 2 12 -6 33.18 22.20 20.24 o 3 12 -6 49.81 66.41 18.75 o 4 12 -6 23.83 9.45 22.23 o 1 13 -6 10.77 -9.45 14.34 o 2 13 -6 9.91 23.24 32.70 o 3 13 -6 167.36 169.56 20.37 o 0 14 -6 36.42 6.16 31.99 o 1 14 -6 312.35 316.96 24.25 o 2 14 -6 133.02 106.21 24.45 o 3 14 -6 98.50 50.16 20.17 o 1 15 -6 79.58 84.38 19.76 o 2 15 -6 172.65 129.54 25.88 o 3 15 -6 5.90 -6.14 37.56 o 0 16 -6 222.79 279.86 40.05 o 1 16 -6 16.09 -1.73 24.03 o 2 16 -6 5.35 -11.77 25.68 o 1 17 -6 11.03 -5.82 25.89 o 0 0 -5 1680.50 1683.99 46.94 o 2 0 -5 1163.97 1191.14 28.38 o 4 0 -5 331.81 323.65 14.79 o 6 0 -5 193.46 167.86 24.88 o 1 1 -5 66.49 61.80 3.68 o 2 1 -5 716.26 723.71 13.31 o 3 1 -5 306.06 312.95 8.72 o 4 1 -5 234.48 254.50 9.50 o 5 1 -5 140.21 111.12 14.06 o 6 1 -5 111.50 126.62 16.09 o 0 2 -5 620.83 619.28 14.16 o 1 2 -5 441.20 414.75 8.40 o 2 2 -5 263.33 291.12 8.21 o 3 2 -5 292.31 293.86 8.65 o 4 2 -5 42.75 39.25 7.27 o 5 2 -5 0.31 -10.91 13.30 o 6 2 -5 89.57 108.88 16.28 o 1 3 -5 200.77 195.59 5.73 o 2 3 -5 244.78 244.06 7.70 o 3 3 -5 559.63 587.07 12.80 o 4 3 -5 181.84 191.37 8.88 o 5 3 -5 333.58 363.62 17.39 o 6 3 -5 39.18 51.34 23.35 o 0 4 -5 224.47 211.93 8.57 o 1 4 -5 1238.34 1250.91 21.87 o 2 4 -5 84.67 84.64 4.72 o 3 4 -5 30.94 34.18 5.04 o 4 4 -5 27.23 27.44 7.86 o 5 4 -5 201.91 185.68 12.37 o 6 4 -5 7.94 13.11 15.63 o 1 5 -5 72.45 74.28 4.30 o 2 5 -5 259.71 235.91 7.96 o 3 5 -5 618.69 591.02 13.00 o 4 5 -5 42.23 35.65 8.09 o 5 5 -5 112.62 130.74 11.76 o 6 5 -5 5.75 -0.41 17.01 o 0 6 -5 170.58 150.12 9.24 o 1 6 -5 901.99 911.16 18.39 o 2 6 -5 139.08 132.71 5.94 o 3 6 -5 271.92 247.17 9.60 o 4 6 -5 30.27 30.52 9.15 o 5 6 -5 68.27 69.35 11.28 o 6 6 -5 82.61 82.51 19.34 o 1 7 -5 85.72 80.97 5.26 o 2 7 -5 425.33 401.20 11.29 o 3 7 -5 192.69 185.48 8.73 o 4 7 -5 408.60 374.77 15.72 o 5 7 -5 36.29 42.03 11.33 o 6 7 -5 141.04 126.44 17.16 o 0 8 -5 1227.19 1236.46 36.32 o 1 8 -5 66.26 56.51 5.54 o 2 8 -5 529.69 533.47 14.94 o 3 8 -5 12.99 4.25 6.51 o 4 8 -5 170.99 147.52 12.60 o 5 8 -5 66.79 63.08 11.86 o 6 8 -5 83.14 66.75 17.03 o 1 9 -5 7.06 6.52 7.52 o 2 9 -5 252.56 251.82 12.94 o 3 9 -5 213.05 187.62 9.02 o 4 9 -5 491.92 466.53 20.25 o 5 9 -5 39.07 39.12 11.81 o 6 9 -5 114.26 118.88 27.33 o 0 10 -5 332.23 331.48 21.12 o 1 10 -5 350.60 336.39 15.78 o 2 10 -5 109.40 116.64 8.38 o 3 10 -5 81.46 64.54 8.10 o 4 10 -5 32.50 34.58 10.65 o 5 10 -5 80.64 37.35 16.73 o 6 10 -5 41.90 47.46 23.22 o 1 11 -5 72.81 66.96 12.21 o 2 11 -5 62.42 67.42 14.55 o 3 11 -5 222.70 224.51 15.58 o 4 11 -5 42.92 28.41 12.78 o 5 11 -5 126.69 119.29 28.56 o 0 12 -5 113.41 147.14 13.15 o 1 12 -5 653.21 656.46 35.00 o 2 12 -5 25.10 39.05 16.23 o 3 12 -5 122.87 112.42 12.23 o 4 12 -5 23.07 19.45 13.41 o 5 12 -5 140.81 130.45 21.88 o 1 13 -5 197.11 220.20 19.93 o 2 13 -5 59.22 59.41 17.54 o 3 13 -5 425.49 431.62 23.33 o 4 13 -5 62.41 76.82 14.64 o 5 13 -5 122.50 118.58 22.34 o 0 14 -5 436.78 433.17 45.97 o 1 14 -5 80.15 94.69 18.25 o 2 14 -5 240.75 224.39 20.78 o 3 14 -5 46.78 53.14 12.81 o 4 14 -5 30.76 15.84 19.38 o 5 14 -5 24.42 24.00 23.47 o 1 15 -5 115.82 117.00 19.74 o 2 15 -5 65.52 58.15 19.16 o 3 15 -5 152.26 130.65 22.99 o 4 15 -5 155.94 144.43 27.04 o 0 16 -5 995.02 1016.82 67.54 o 1 16 -5 60.80 32.56 19.57 o 2 16 -5 273.13 290.01 24.91 o 3 16 -5 53.03 88.45 42.77 o 4 16 -5 45.17 75.14 26.60 o 1 17 -5 118.02 102.40 21.73 o 2 17 -5 177.30 199.75 23.58 o 3 17 -5 48.14 48.86 22.66 o 4 17 -5 176.97 206.17 31.13 o 0 18 -5 45.67 72.04 31.99 o 1 18 -5 84.41 77.74 33.18 o 2 18 -5 16.39 -22.31 22.31 o 3 18 -5 87.80 85.21 23.90 o 1 19 -5 40.51 25.24 25.36 o 2 19 -5 97.66 90.37 25.42 o 0 20 -5 54.43 31.04 36.73 o 1 20 -5 234.03 239.34 28.97 o 2 20 -5 7.49 35.37 26.05 o 0 0 -4 6039.37 6173.47 165.73 o 2 0 -4 2035.82 2141.18 48.09 o 4 0 -4 488.38 525.16 17.10 o 6 0 -4 181.01 161.36 20.17 o 1 1 -4 72.92 76.31 3.00 o 2 1 -4 1223.60 1256.44 21.38 o 3 1 -4 179.20 187.05 5.50 o 4 1 -4 2056.01 2088.18 39.36 o 5 1 -4 100.85 117.43 11.22 o 6 1 -4 115.37 135.06 17.31 o 7 1 -4 10.46 8.85 19.43 o 0 2 -4 999.90 1069.76 21.58 o 1 2 -4 922.20 902.35 14.75 o 2 2 -4 356.71 385.83 8.35 o 3 2 -4 660.54 655.00 11.95 o 4 2 -4 362.21 367.38 10.07 o 5 2 -4 131.30 127.48 10.04 o 6 2 -4 111.41 131.27 14.18 o 7 2 -4 84.92 83.45 16.66 o 1 3 -4 185.04 189.12 5.44 o 2 3 -4 158.78 161.77 5.39 o 3 3 -4 1322.53 1304.98 21.05 o 4 3 -4 44.53 40.07 4.63 o 5 3 -4 113.29 123.49 11.09 o 6 3 -4 25.05 53.33 14.54 o 7 3 -4 66.65 75.85 16.69 o 0 4 -4 192.28 207.37 7.25 o 1 4 -4 1650.58 1647.01 28.08 o 2 4 -4 14.41 9.31 3.06 o 3 4 -4 305.69 311.26 7.59 o 4 4 -4 48.38 42.78 4.87 o 5 4 -4 182.81 178.75 9.21 o 6 4 -4 1.78 20.43 13.33 o 7 4 -4 84.91 67.24 17.48 o 1 5 -4 1161.65 1172.44 23.98 o 2 5 -4 93.24 90.88 3.82 o 3 5 -4 1087.13 1104.90 18.68 o 4 5 -4 208.72 207.16 8.16 o 5 5 -4 608.43 621.22 20.01 o 6 5 -4 44.74 36.04 13.16 o 7 5 -4 76.43 90.39 17.29 o 0 6 -4 3266.77 3353.15 92.36 o 1 6 -4 1402.50 1407.06 27.66 o 2 6 -4 710.29 682.74 14.08 o 3 6 -4 85.15 97.26 4.51 o 4 6 -4 16.31 12.48 5.22 o 5 6 -4 154.47 141.46 9.02 o 6 6 -4 43.12 28.05 10.72 o 7 6 -4 44.43 41.47 17.27 o 1 7 -4 15.76 14.07 3.49 o 2 7 -4 831.33 781.35 17.48 o 3 7 -4 155.58 146.45 6.51 o 4 7 -4 625.20 602.72 15.89 o 5 7 -4 257.61 235.89 12.01 o 6 7 -4 65.94 48.38 11.18 o 7 7 -4 7.19 9.13 17.42 o 0 8 -4 1284.33 1272.40 35.68 o 1 8 -4 107.18 115.07 5.81 o 2 8 -4 653.29 646.52 15.16 o 3 8 -4 8.02 12.22 5.33 o 4 8 -4 213.46 205.72 9.10 o 5 8 -4 4.11 0.06 8.17 o 6 8 -4 143.54 138.86 12.60 o 7 8 -4 22.06 18.77 17.93 o 1 9 -4 94.99 95.38 6.80 o 2 9 -4 627.97 607.72 15.24 o 3 9 -4 82.96 72.46 5.70 o 4 9 -4 350.24 342.90 13.64 o 5 9 -4 201.23 195.70 11.03 o 6 9 -4 145.03 167.85 13.44 o 7 9 -4 33.06 58.51 20.35 o 0 10 -4 988.62 999.17 33.11 o 1 10 -4 1072.92 1027.86 27.38 o 2 10 -4 342.22 322.10 10.42 o 3 10 -4 274.73 265.98 12.19 o 4 10 -4 88.39 93.50 9.38 o 5 10 -4 82.32 68.26 9.26 o 6 10 -4 88.85 90.75 15.83 o 1 11 -4 219.50 214.86 10.66 o 2 11 -4 385.32 383.33 12.72 o 3 11 -4 1022.02 976.79 30.72 o 4 11 -4 120.38 140.18 10.37 o 5 11 -4 275.18 286.82 14.12 o 6 11 -4 23.37 3.37 13.06 o 0 12 -4 56.34 61.47 9.38 o 1 12 -4 1024.40 1034.67 28.52 o 2 12 -4 68.51 59.59 6.86 o 3 12 -4 21.10 37.16 8.11 o 4 12 -4 0.97 -6.70 9.87 o 5 12 -4 107.82 81.06 12.29 o 6 12 -4 22.59 10.85 15.96 o 1 13 -4 196.80 208.10 14.00 o 2 13 -4 79.64 72.62 10.78 o 3 13 -4 438.96 429.10 18.16 o 4 13 -4 144.27 127.87 14.05 o 5 13 -4 181.34 172.77 16.00 o 6 13 -4 42.46 54.20 17.39 o 0 14 -4 890.64 859.48 54.98 o 1 14 -4 1042.63 1112.33 52.01 o 2 14 -4 107.67 124.52 20.50 o 3 14 -4 138.94 145.01 11.88 o 4 14 -4 143.03 154.41 16.40 o 5 14 -4 58.09 8.93 32.52 o 6 14 -4 69.01 87.11 23.20 o 1 15 -4 90.14 95.36 18.13 o 2 15 -4 544.05 568.12 33.31 o 3 15 -4 126.79 160.44 28.32 o 4 15 -4 395.80 379.49 27.06 o 5 15 -4 31.60 21.13 25.68 o 1 16 -4 189.94 158.41 30.81 o 2 16 -4 522.50 558.68 34.01 o 3 16 -4 26.71 26.02 17.53 o 4 16 -4 62.49 57.23 22.51 o 5 16 -4 27.24 6.65 52.49 o 1 17 -4 87.72 93.42 17.61 o 2 17 -4 170.02 180.91 20.07 o 3 17 -4 62.44 65.54 24.88 o 4 17 -4 282.81 307.56 27.31 o 5 17 -4 13.25 4.65 26.92 o 0 18 -4 672.01 756.63 57.82 o 1 18 -4 122.78 124.45 20.03 o 2 18 -4 212.20 248.28 57.82 o 3 18 -4 26.23 8.11 19.24 o 4 18 -4 28.49 -2.80 24.59 o 1 19 -4 78.96 67.78 20.41 o 2 19 -4 62.27 72.23 20.41 o 3 19 -4 230.49 238.65 24.48 o 4 19 -4 29.94 53.60 19.69 o 0 20 -4 132.51 105.69 33.18 o 1 20 -4 371.11 417.98 36.73 o 2 20 -4 11.69 -5.64 22.32 o 3 20 -4 86.61 119.88 23.16 o 1 21 -4 96.15 84.24 24.55 o 2 21 -4 28.63 28.59 38.98 o 3 21 -4 226.29 244.52 23.46 o 0 22 -4 142.33 159.24 37.20 o 1 22 -4 151.26 168.44 26.86 o 2 22 -4 121.17 144.49 34.83 o 1 23 -4 26.73 79.90 26.40 o 0 0 -3 1802.42 1831.03 50.74 o 2 0 -3 2771.34 2790.99 62.32 o 4 0 -3 85.63 127.49 13.78 o 6 0 -3 268.41 269.76 23.71 o 8 0 -3 64.77 33.20 57.23 o 1 1 -3 301.32 295.99 5.95 o 2 1 -3 577.94 590.45 10.21 o 3 1 -3 796.66 834.24 15.90 o 4 1 -3 1773.28 1791.48 32.25 o 5 1 -3 373.44 382.23 10.77 o 6 1 -3 205.69 225.53 12.35 o 7 1 -3 5.91 23.42 13.65 o 8 1 -3 61.22 68.26 22.92 o 0 2 -3 3579.43 3740.70 80.10 o 1 2 -3 2913.81 2998.26 49.86 o 2 2 -3 1119.50 1089.13 18.42 o 3 2 -3 1475.80 1549.78 26.26 o 4 2 -3 404.15 384.17 9.71 o 5 2 -3 423.59 408.04 11.28 o 6 2 -3 22.10 34.94 9.41 o 7 2 -3 55.29 49.81 14.21 o 8 2 -3 33.17 49.08 17.91 o 1 3 -3 1045.18 1067.71 21.16 o 2 3 -3 1118.19 1154.26 19.34 o 3 3 -3 2843.49 2923.19 50.18 o 4 3 -3 206.22 210.14 7.81 o 5 3 -3 748.15 760.73 16.91 o 6 3 -3 20.39 31.17 9.46 o 7 3 -3 14.16 29.43 14.09 o 8 3 -3 1.37 -3.77 17.91 o 0 4 -3 504.16 546.92 14.01 o 1 4 -3 4407.67 4535.97 87.77 o 2 4 -3 328.88 319.05 7.03 o 3 4 -3 94.75 100.69 4.43 o 4 4 -3 101.22 107.74 5.03 o 5 4 -3 407.71 383.48 11.28 o 6 4 -3 52.87 41.93 10.09 o 7 4 -3 180.49 177.87 15.77 o 8 4 -3 1.05 -9.55 18.03 o 1 5 -3 1207.06 1263.45 25.33 o 2 5 -3 121.19 112.04 4.92 o 3 5 -3 2134.01 2133.61 38.50 o 4 5 -3 232.62 240.19 7.92 o 5 5 -3 288.95 294.77 10.09 o 6 5 -3 6.95 5.73 9.71 o 7 5 -3 60.39 45.64 14.54 o 8 5 -3 10.20 20.58 21.00 o 0 6 -3 2888.02 2999.32 103.72 o 1 6 -3 3394.08 3461.39 71.22 o 2 6 -3 188.67 172.58 6.60 o 3 6 -3 562.60 578.78 12.34 o 4 6 -3 172.11 181.58 6.81 o 5 6 -3 101.67 88.45 6.09 o 6 6 -3 72.80 85.89 8.82 o 7 6 -3 71.80 73.52 15.22 o 1 7 -3 145.70 163.61 6.11 o 2 7 -3 1244.58 1237.40 28.10 o 3 7 -3 327.29 321.43 8.74 o 4 7 -3 1358.38 1314.28 24.88 o 5 7 -3 137.03 136.84 7.40 o 6 7 -3 279.23 277.36 13.09 o 7 7 -3 14.98 23.54 16.28 o 0 8 -3 7589.41 7966.71 294.32 o 1 8 -3 112.94 121.08 5.30 o 2 8 -3 2037.77 1988.24 40.22 o 3 8 -3 257.78 250.75 7.92 o 4 8 -3 115.41 113.51 5.37 o 5 8 -3 61.23 72.13 6.93 o 6 8 -3 255.99 240.03 17.73 o 7 8 -3 10.35 -3.14 15.20 o 1 9 -3 67.28 63.68 5.09 o 2 9 -3 1492.56 1469.17 31.02 o 3 9 -3 223.43 229.87 8.69 o 4 9 -3 902.86 877.73 18.19 o 5 9 -3 91.80 94.34 9.91 o 6 9 -3 199.28 194.51 11.52 o 7 9 -3 37.34 34.29 15.88 o 0 10 -3 887.41 890.51 39.54 o 1 10 -3 417.09 423.70 13.39 o 2 10 -3 339.75 309.35 9.12 o 3 10 -3 73.66 72.12 5.37 o 4 10 -3 139.85 132.74 6.28 o 5 10 -3 37.40 33.47 7.02 o 6 10 -3 151.61 128.99 11.08 o 7 10 -3 141.33 150.80 17.74 o 1 11 -3 241.84 221.23 9.89 o 2 11 -3 448.92 445.71 12.53 o 3 11 -3 822.09 771.36 15.88 o 4 11 -3 100.10 96.10 6.54 o 5 11 -3 283.33 280.03 12.17 o 6 11 -3 9.75 -5.20 11.35 o 7 11 -3 64.10 69.98 17.19 o 0 12 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411.83 431.41 17.89 o 4 21 0 25.08 24.04 11.14 o 5 21 0 143.71 161.17 16.39 o 0 22 0 143.36 179.08 18.12 o 1 22 0 204.64 247.96 14.52 o 2 22 0 197.90 192.16 12.43 o 3 22 0 76.99 85.77 12.10 o 4 22 0 21.11 53.83 17.27 o 5 22 0 47.94 53.20 17.05 o 1 23 0 72.75 69.01 13.59 o 2 23 0 163.16 182.71 13.24 o 3 23 0 185.20 243.76 17.17 o 4 23 0 232.03 256.40 18.66 o 0 24 0 641.25 614.74 39.27 o 1 24 0 1.27 3.19 13.91 o 2 24 0 305.23 345.34 20.48 o 3 24 0 2.58 2.70 15.65 o 4 24 0 2.70 -17.05 17.05 o 1 25 0 1.45 -0.38 21.44 o 2 25 0 118.38 103.64 16.93 o 3 25 0 5.41 15.24 17.21 o 0 26 0 208.02 205.45 38.86 o 1 26 0 136.85 181.13 20.25 o 2 26 0 6.46 26.31 21.65 o 2 0 1 4478.19 4766.36 165.27 o 4 0 1 10.03 54.53 6.19 o 6 0 1 19.04 33.74 11.60 o 8 0 1 104.43 89.68 22.85 o 1 1 1 6139.81 6391.23 135.53 o 2 1 1 4968.21 5300.97 112.34 o 3 1 1 230.91 221.61 6.25 o 4 1 1 1704.48 1619.44 38.23 o 5 1 1 235.08 247.55 10.36 o 6 1 1 471.08 481.19 15.67 o 7 1 1 10.48 21.94 12.45 o 8 1 1 3.96 6.23 17.30 o 0 2 1 6473.06 6816.32 222.32 o 1 2 1 21165.30 22767.71 454.62 o 2 2 1 3007.02 2959.40 58.61 o 3 2 1 530.70 502.49 12.40 o 4 2 1 87.20 101.39 7.64 o 5 2 1 387.29 410.39 12.14 o 6 2 1 179.77 199.20 9.50 o 7 2 1 173.75 164.64 12.31 o 8 2 1 25.80 36.48 17.08 o 1 3 1 5375.69 5648.06 119.96 o 2 3 1 282.54 258.30 11.02 o 3 3 1 5200.36 5422.92 104.15 o 4 3 1 805.53 779.56 15.68 o 5 3 1 1303.26 1282.64 27.87 o 6 3 1 25.50 22.82 6.36 o 7 3 1 132.71 147.17 12.12 o 8 3 1 7.06 1.21 14.54 o 0 4 1 63.33 54.59 6.64 o 1 4 1 5977.68 5972.69 112.17 o 2 4 1 496.26 485.80 10.64 o 3 4 1 611.85 579.19 15.19 o 4 4 1 56.87 67.53 3.88 o 5 4 1 478.20 466.17 11.77 o 6 4 1 234.75 219.11 9.56 o 7 4 1 397.23 383.21 20.26 o 8 4 1 25.91 9.90 14.83 o 1 5 1 717.17 718.35 15.93 o 2 5 1 263.69 275.30 8.18 o 3 5 1 7477.13 7679.46 159.72 o 4 5 1 84.71 85.04 4.21 o 5 5 1 1032.41 1014.49 24.23 o 6 5 1 150.51 152.08 8.11 o 7 5 1 12.80 15.29 9.11 o 8 5 1 29.20 29.81 16.53 o 0 6 1 2799.63 2795.05 106.65 o 1 6 1 10377.28 10522.13 216.59 o 2 6 1 744.39 713.68 16.89 o 3 6 1 618.24 573.60 12.82 o 4 6 1 94.86 108.71 4.89 o 5 6 1 54.39 62.36 4.89 o 6 6 1 329.46 341.38 12.92 o 7 6 1 29.57 12.21 9.48 o 8 6 1 38.17 38.25 14.98 o 1 7 1 294.39 285.09 7.77 o 2 7 1 2572.40 2507.65 49.21 o 3 7 1 893.14 827.82 17.44 o 4 7 1 2448.46 2395.06 46.41 o 5 7 1 59.86 63.65 5.16 o 6 7 1 134.53 137.22 8.01 o 7 7 1 34.39 23.57 9.73 o 8 7 1 13.06 -16.58 17.13 o 0 8 1 18209.10 19218.14 724.70 o 1 8 1 363.88 383.79 9.46 o 2 8 1 5354.00 5427.14 100.91 o 3 8 1 444.51 465.26 10.90 o 4 8 1 129.01 127.06 5.69 o 5 8 1 152.10 152.92 8.64 o 6 8 1 247.99 232.25 10.53 o 7 8 1 4.36 6.51 9.99 o 8 8 1 67.21 34.66 25.18 o 1 9 1 158.69 151.84 4.69 o 2 9 1 2576.28 2537.37 46.21 o 3 9 1 663.26 683.97 15.77 o 4 9 1 2032.11 1987.66 41.17 o 5 9 1 241.71 244.90 10.80 o 6 9 1 107.16 120.59 8.14 o 7 9 1 96.39 88.89 17.19 o 8 9 1 8.24 -10.82 18.85 o 0 10 1 1814.84 1818.88 78.75 o 1 10 1 682.98 602.44 14.18 o 2 10 1 998.18 959.85 19.76 o 3 10 1 5.90 9.84 3.27 o 4 10 1 272.24 289.22 9.34 o 5 10 1 58.41 60.27 5.80 o 6 10 1 260.76 284.17 13.11 o 7 10 1 32.70 39.08 17.82 o 8 10 1 42.98 34.60 25.19 o 1 11 1 628.12 669.73 15.73 o 2 11 1 242.99 214.87 6.98 o 3 11 1 1770.76 1737.61 33.87 o 4 11 1 359.29 353.46 11.03 o 5 11 1 406.22 437.45 14.86 o 6 11 1 83.79 104.56 10.48 o 7 11 1 19.84 17.28 12.64 o 8 11 1 11.40 22.49 28.15 o 0 12 1 192.65 245.57 13.95 o 1 12 1 3745.00 3665.17 74.82 o 2 12 1 72.71 69.50 4.14 o 3 12 1 1075.72 1084.63 22.09 o 4 12 1 30.25 28.83 5.43 o 5 12 1 23.86 29.94 7.19 o 6 12 1 75.00 79.61 11.83 o 7 12 1 49.75 62.14 17.96 o 1 13 1 573.83 536.82 12.69 o 2 13 1 126.79 125.13 5.59 o 3 13 1 1047.22 1042.25 22.67 o 4 13 1 468.05 471.08 12.79 o 5 13 1 674.00 671.57 16.95 o 6 13 1 25.15 38.98 12.36 o 7 13 1 6.19 15.71 19.96 o 0 14 1 2207.15 2215.65 86.29 o 1 14 1 2021.81 1949.50 40.22 o 2 14 1 1522.24 1450.66 30.55 o 3 14 1 10.37 7.97 4.68 o 4 14 1 88.24 95.70 5.96 o 5 14 1 386.19 387.66 15.42 o 6 14 1 131.74 121.30 12.14 o 7 14 1 113.55 140.86 20.56 o 1 15 1 430.09 434.80 11.42 o 2 15 1 1991.92 2002.67 41.90 o 3 15 1 469.72 463.77 12.24 o 4 15 1 1528.39 1525.69 31.95 o 5 15 1 19.59 33.39 8.52 o 6 15 1 157.94 188.63 13.41 o 7 15 1 18.30 25.73 20.59 o 0 16 1 3226.77 3104.10 119.55 o 1 16 1 186.14 191.24 8.06 o 2 16 1 1044.45 1038.91 22.44 o 3 16 1 45.28 47.33 5.78 o 4 16 1 5.12 4.18 6.84 o 5 16 1 10.54 11.27 9.22 o 6 16 1 35.75 47.72 13.50 o 7 16 1 10.76 55.77 21.87 o 1 17 1 38.28 38.14 5.28 o 2 17 1 1052.18 1028.07 22.17 o 3 17 1 96.75 92.84 7.17 o 4 17 1 417.29 410.76 17.57 o 5 17 1 22.63 12.45 9.89 o 6 17 1 90.34 97.06 15.78 o 0 18 1 1223.28 1202.82 50.34 o 1 18 1 944.75 964.42 21.59 o 2 18 1 155.79 160.54 8.66 o 3 18 1 211.48 210.61 10.11 o 4 18 1 90.70 86.75 10.76 o 5 18 1 62.77 22.47 9.90 o 6 18 1 120.33 100.47 20.11 o 1 19 1 321.33 310.65 12.63 o 2 19 1 17.60 23.74 7.06 o 3 19 1 595.11 572.16 18.86 o 4 19 1 115.00 108.08 10.65 o 5 19 1 164.02 192.62 15.47 o 6 19 1 3.01 -15.24 16.61 o 0 20 1 2.53 3.02 11.94 o 1 20 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2459.12 69.96 o 4 1 2 2236.64 2272.27 55.95 o 5 1 2 192.95 203.31 11.13 o 6 1 2 197.96 255.79 13.89 o 7 1 2 107.06 107.86 19.43 o 8 1 2 3.85 2.43 23.11 o 0 2 2 3189.46 3345.34 98.69 o 1 2 2 5940.03 6202.38 129.33 o 3 2 2 321.08 377.99 15.95 o 4 2 2 217.82 236.33 9.35 o 5 2 2 55.83 62.05 6.79 o 6 2 2 635.47 596.09 17.30 o 7 2 2 59.83 79.11 14.95 o 8 2 2 40.02 22.48 23.93 o 1 3 2 194.47 192.43 5.05 o 2 3 2 2236.67 2305.40 67.36 o 3 3 2 2156.53 1986.85 53.16 o 4 3 2 513.88 493.86 14.15 o 5 3 2 1176.46 1143.86 30.77 o 6 3 2 39.60 50.00 8.52 o 7 3 2 20.24 25.97 10.88 o 8 3 2 10.84 12.02 24.04 o 0 4 2 943.47 904.68 29.92 o 1 4 2 5696.90 5751.57 134.07 o 2 4 2 1373.64 1351.44 30.57 o 3 4 2 651.72 604.29 13.83 o 4 4 2 9.40 11.57 4.62 o 5 4 2 287.32 297.20 12.55 o 6 4 2 206.24 211.64 12.78 o 7 4 2 77.61 83.20 15.63 o 8 4 2 2.77 -0.42 24.86 o 1 5 2 1075.48 1031.26 25.36 o 2 5 2 664.63 659.49 14.28 o 3 5 2 2017.00 2022.96 42.18 o 4 5 2 238.43 239.76 9.56 o 5 5 2 823.76 808.96 21.57 o 6 5 2 101.17 96.27 8.69 o 7 5 2 21.59 30.02 26.88 o 8 5 2 2.61 10.18 24.38 o 0 6 2 3857.18 3775.17 118.52 o 1 6 2 2112.04 2137.42 52.71 o 2 6 2 4083.53 4156.38 83.86 o 3 6 2 148.58 139.57 6.58 o 4 6 2 74.63 78.72 5.21 o 5 6 2 159.33 149.52 8.24 o 6 6 2 113.43 122.84 9.18 o 7 6 2 165.24 140.30 17.86 o 8 6 2 21.66 48.97 39.22 o 1 7 2 637.43 663.03 17.16 o 2 7 2 3917.80 4001.38 82.54 o 3 7 2 320.87 310.27 8.37 o 4 7 2 1564.56 1564.43 36.05 o 5 7 2 71.97 65.12 7.20 o 6 7 2 417.31 395.24 17.62 o 7 7 2 23.84 16.65 16.74 o 8 7 2 6.84 26.37 25.77 o 0 8 2 5956.62 5629.07 176.12 o 1 8 2 36.07 43.39 3.10 o 2 8 2 2594.95 2496.60 54.93 o 3 8 2 82.50 89.16 4.77 o 4 8 2 151.42 163.00 7.42 o 5 8 2 39.44 55.51 7.26 o 6 8 2 172.14 187.69 11.06 o 7 8 2 2.48 -3.24 14.20 o 8 8 2 79.36 44.87 32.82 o 1 9 2 116.95 108.38 5.25 o 2 9 2 1615.07 1540.77 35.08 o 3 9 2 189.72 185.00 7.19 o 4 9 2 1578.32 1573.26 35.37 o 5 9 2 164.61 179.36 8.95 o 6 9 2 117.97 136.13 11.75 o 7 9 2 13.67 7.73 15.17 o 8 9 2 28.64 10.51 20.62 o 0 10 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27.70 8.73 o 6 14 2 21.38 23.85 11.81 o 7 14 2 37.90 44.94 20.51 o 1 15 2 219.29 224.64 10.69 o 2 15 2 273.82 264.69 10.85 o 3 15 2 84.44 95.61 9.26 o 4 15 2 658.47 692.59 20.43 o 5 15 2 84.43 83.38 11.38 o 6 15 2 86.11 107.15 14.85 o 7 15 2 26.97 10.56 25.98 o 0 16 2 2641.18 2687.40 104.81 o 1 16 2 215.13 197.75 9.23 o 2 16 2 292.48 287.17 12.48 o 3 16 2 122.28 122.82 8.57 o 4 16 2 28.27 32.27 10.16 o 5 16 2 72.56 80.26 11.84 o 6 16 2 184.88 183.90 20.70 o 1 17 2 208.21 200.50 10.08 o 2 17 2 463.10 457.00 16.12 o 3 17 2 293.21 288.73 14.79 o 4 17 2 619.42 689.58 26.24 o 5 17 2 126.51 142.99 14.44 o 6 17 2 46.52 39.67 16.18 o 0 18 2 930.15 933.86 31.99 o 1 18 2 349.83 339.45 13.25 o 2 18 2 526.06 547.83 18.72 o 3 18 2 87.41 95.11 9.81 o 4 18 2 75.65 55.25 17.68 o 5 18 2 111.60 110.85 14.89 o 6 18 2 49.29 71.79 19.75 o 1 19 2 189.89 194.10 10.30 o 2 19 2 403.18 414.10 17.98 o 3 19 2 608.24 616.68 21.80 o 4 19 2 101.54 99.83 13.94 o 5 19 2 102.97 126.02 15.91 o 0 20 2 15.29 30.20 15.83 o 1 20 2 1195.69 1190.55 37.98 o 2 20 2 47.49 37.39 9.96 o 3 20 2 210.36 231.92 13.29 o 4 20 2 33.58 32.61 12.06 o 5 20 2 73.61 67.67 17.35 o 1 21 2 169.60 185.63 16.81 o 2 21 2 35.16 20.92 10.73 o 3 21 2 275.49 298.27 16.01 o 4 21 2 108.02 105.46 16.08 o 5 21 2 160.17 162.97 19.24 o 0 22 2 308.85 334.01 29.15 o 1 22 2 243.16 274.91 20.19 o 2 22 2 127.47 132.54 18.21 o 3 22 2 17.09 10.92 13.86 o 4 22 2 20.76 5.91 16.83 o 1 23 2 13.13 17.88 15.56 o 2 23 2 172.06 164.63 19.94 o 3 23 2 81.10 73.31 15.88 o 4 23 2 233.67 220.02 27.61 o 0 24 2 530.16 605.77 43.71 o 1 24 2 30.16 28.14 21.55 o 2 24 2 229.48 224.14 21.91 o 3 24 2 42.21 27.76 17.30 o 1 25 2 12.54 23.09 24.56 o 2 25 2 174.65 160.46 23.51 o 0 26 2 29.92 75.24 28.13 o 0 0 3 2018.17 2040.75 101.18 o 2 0 3 3079.75 3081.50 153.08 o 4 0 3 110.80 111.85 16.11 o 6 0 3 269.40 295.97 37.68 o 8 0 3 69.99 72.04 36.97 o 1 1 3 289.17 301.71 12.52 o 2 1 3 482.60 504.64 17.17 o 3 1 3 933.26 960.17 25.37 o 4 1 3 1569.40 1573.64 55.91 o 5 1 3 344.86 347.98 19.83 o 6 1 3 204.11 216.46 19.59 o 7 1 3 9.57 -8.97 19.69 o 8 1 3 57.75 -1.34 26.06 o 0 2 3 3339.14 3414.12 138.74 o 1 2 3 2767.61 2796.84 70.45 o 2 2 3 992.16 973.70 23.83 o 3 2 3 1314.45 1367.50 41.52 o 4 2 3 376.74 364.19 20.23 o 5 2 3 422.53 410.96 20.57 o 6 2 3 14.73 17.18 10.66 o 7 2 3 48.96 50.17 20.99 o 8 2 3 26.36 53.30 26.80 o 1 3 3 1086.94 1099.24 26.83 o 2 3 3 1156.77 1156.89 26.26 o 3 3 3 2897.14 2946.39 79.38 o 4 3 3 272.22 273.40 11.87 o 5 3 3 874.10 894.85 39.53 o 6 3 3 16.75 20.65 10.63 o 7 3 3 12.87 27.74 19.75 o 8 3 3 2.11 14.48 26.71 o 0 4 3 486.14 530.08 18.69 o 1 4 3 4717.71 4735.66 93.86 o 2 4 3 343.48 339.47 10.43 o 3 4 3 142.25 149.02 7.67 o 4 4 3 111.80 125.02 7.82 o 5 4 3 496.87 481.42 17.84 o 6 4 3 47.43 60.73 11.08 o 7 4 3 200.06 209.01 23.20 o 8 4 3 0.68 36.10 26.96 o 1 5 3 1119.75 1153.97 25.32 o 2 5 3 140.93 122.94 6.12 o 3 5 3 2113.02 2071.33 51.74 o 4 5 3 224.91 232.09 12.51 o 5 5 3 290.19 273.95 13.43 o 6 5 3 1.75 -12.58 12.58 o 7 5 3 53.89 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534.55 21.47 o 4 5 5 27.13 19.62 10.20 o 5 5 5 104.71 127.56 20.46 o 6 5 5 2.35 -0.36 22.84 o 0 6 5 209.93 174.78 15.88 o 1 6 5 881.82 903.12 28.24 o 2 6 5 109.38 109.58 8.30 o 3 6 5 234.84 226.18 13.46 o 4 6 5 28.09 25.35 10.61 o 5 6 5 51.68 24.40 12.04 o 6 6 5 76.20 50.74 31.55 o 1 7 5 74.14 73.60 9.01 o 2 7 5 449.36 455.43 16.85 o 3 7 5 158.27 173.42 11.16 o 4 7 5 425.04 413.90 23.87 o 5 7 5 43.45 39.68 12.50 o 6 7 5 137.74 143.93 25.40 o 0 8 5 1272.29 1289.39 43.09 o 1 8 5 81.60 74.65 7.44 o 2 8 5 545.24 562.82 20.29 o 3 8 5 17.84 20.61 9.41 o 4 8 5 162.07 140.62 12.21 o 5 8 5 60.05 62.56 15.88 o 6 8 5 88.49 79.60 39.05 o 1 9 5 2.75 3.14 7.27 o 2 9 5 281.59 281.29 14.67 o 3 9 5 195.25 173.61 11.76 o 4 9 5 483.89 496.34 21.90 o 5 9 5 38.59 31.03 16.31 o 6 9 5 133.05 169.25 26.92 o 0 10 5 356.91 367.49 20.48 o 1 10 5 295.02 273.87 13.83 o 2 10 5 137.70 145.84 9.68 o 3 10 5 73.47 68.25 10.82 o 4 10 5 42.64 46.11 11.84 o 5 10 5 83.85 68.90 19.73 o 6 10 5 46.52 40.29 20.17 o 1 11 5 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5 66.75 52.92 17.14 o 2 18 5 18.14 16.15 16.17 o 3 18 5 92.10 100.32 18.84 o 1 19 5 32.29 21.95 17.51 o 2 19 5 91.58 83.55 18.16 o 0 20 5 52.23 98.00 26.30 o 1 20 5 238.28 236.37 19.88 o 2 20 5 4.91 7.38 18.27 o 4 0 6 28.52 49.76 28.20 o 1 1 6 31.25 43.84 16.82 o 2 1 6 397.55 426.06 32.70 o 4 1 6 152.51 146.40 21.28 o 5 1 6 16.56 43.76 23.88 o 0 2 6 239.37 270.85 31.04 o 1 2 6 624.73 679.85 44.79 o 2 2 6 17.18 41.23 17.54 o 4 2 6 49.86 42.25 19.85 o 5 2 6 82.56 86.44 25.38 o 1 3 6 166.60 184.92 15.91 o 2 3 6 41.72 52.61 18.48 o 4 3 6 61.13 62.56 27.96 o 5 3 6 161.90 212.35 25.89 o 0 4 6 32.27 29.62 18.72 o 1 4 6 327.90 368.55 41.11 o 2 4 6 145.07 165.22 16.06 o 3 4 6 61.90 19.43 18.25 o 4 4 6 2.82 13.03 26.78 o 5 4 6 56.48 60.78 24.59 o 1 5 6 29.17 33.40 29.86 o 2 5 6 58.49 66.12 14.79 o 3 5 6 328.94 322.80 37.91 o 4 5 6 9.24 -8.09 15.73 o 5 5 6 121.74 102.88 25.37 o 0 6 6 255.43 258.29 26.78 o 1 6 6 95.23 125.70 15.75 o 2 6 6 224.28 240.46 18.56 o 3 6 6 52.23 52.23 17.63 o 4 6 6 27.89 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