#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:07:28 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181906 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/06/2240613.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240613 _cell_angle_alpha 90.000 _cell_angle_beta 99.843 _cell_angle_gamma 90.000 _cell_length_a 5.0441 _cell_length_b 18.2374 _cell_length_c 8.8653 _exptl_crystal_F_000 384.00 _reflns_d_resolution_high 0.8553 _cod_data_source_file hb7400Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2014_november_suchetan_ca2l_0m_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 85.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 61.21 65.17 3.30 o 4 0 0 192.89 181.05 7.65 o 2 1 0 7.27 11.42 0.84 o 3 1 0 110.09 98.53 2.79 o 4 1 0 371.35 376.91 10.79 o 5 1 0 47.18 50.51 1.65 o 1 2 0 2393.99 2624.61 91.56 o 2 2 0 318.71 329.01 11.19 o 3 2 0 11.25 10.01 0.55 o 4 2 0 36.30 33.48 1.32 o 5 2 0 311.33 318.17 8.24 o 1 3 0 7291.10 5453.46 300.74 o 2 3 0 899.93 943.03 31.44 o 3 3 0 186.05 161.54 3.97 o 4 3 0 19.94 21.46 0.98 o 5 3 0 45.94 49.01 1.83 o 0 4 0 43.14 42.82 2.61 o 1 4 0 779.46 849.25 23.42 o 2 4 0 2449.77 2375.18 76.18 o 3 4 0 368.48 361.17 7.83 o 4 4 0 759.71 756.40 24.47 o 5 4 0 109.46 114.25 4.18 o 1 5 0 464.14 538.72 14.67 o 2 5 0 1013.83 993.62 32.52 o 3 5 0 72.17 75.53 2.14 o 4 5 0 16.62 15.96 1.77 o 5 5 0 33.69 35.70 1.64 o 0 6 0 1218.33 1151.75 37.42 o 1 6 0 512.70 560.06 16.18 o 2 6 0 811.93 774.39 22.25 o 3 6 0 128.61 126.01 2.88 o 4 6 0 1082.46 925.79 56.78 o 5 6 0 37.92 40.03 1.74 o 1 7 0 62.22 48.45 2.12 o 2 7 0 58.34 47.98 1.52 o 3 7 0 474.62 437.71 9.37 o 4 7 0 614.14 604.33 27.90 o 5 7 0 165.09 179.31 5.31 o 0 8 0 510.91 489.88 16.68 o 1 8 0 89.18 88.04 3.42 o 2 8 0 21.16 18.04 0.58 o 3 8 0 8.27 12.06 0.50 o 4 8 0 281.61 284.93 8.37 o 5 8 0 70.67 67.65 2.57 o 1 9 0 87.33 73.03 1.87 o 2 9 0 386.45 380.24 7.27 o 3 9 0 1422.10 1417.21 29.74 o 4 9 0 98.53 96.48 3.15 o 5 9 0 162.12 161.52 5.54 o 0 10 0 1004.45 902.90 20.74 o 1 10 0 3.91 2.28 0.21 o 2 10 0 764.71 699.97 13.87 o 3 10 0 58.78 57.01 1.62 o 4 10 0 92.39 95.41 3.60 o 5 10 0 3.49 3.92 0.44 o 1 11 0 144.69 118.68 2.30 o 2 11 0 9.06 8.85 0.45 o 3 11 0 0.97 1.99 0.45 o 4 11 0 9.76 10.54 0.75 o 0 12 0 142.34 149.50 4.45 o 1 12 0 389.69 398.48 8.57 o 2 12 0 139.48 132.33 3.10 o 3 12 0 0.46 0.71 0.25 o 4 12 0 42.37 46.84 1.67 o 1 13 0 1077.89 1138.26 23.97 o 2 13 0 2.69 2.51 0.30 o 3 13 0 281.45 264.96 9.43 o 4 13 0 55.27 54.01 1.83 o 0 14 0 318.18 319.64 9.24 o 1 14 0 218.71 221.71 4.95 o 2 14 0 2.09 2.65 0.35 o 3 14 0 16.02 16.92 0.83 o 4 14 0 236.87 266.38 8.86 o 1 15 0 186.39 205.92 5.00 o 2 15 0 181.92 189.13 4.65 o 3 15 0 73.52 75.48 2.47 o 4 15 0 104.25 113.66 4.85 o 0 16 0 265.58 290.55 8.47 o 1 16 0 327.65 350.45 8.27 o 2 16 0 164.53 168.43 3.87 o 3 16 0 3.00 2.95 0.44 o 1 17 0 248.19 267.36 5.92 o 2 17 0 39.01 35.99 1.07 o 3 17 0 179.77 196.00 6.64 o 0 18 0 6.30 8.96 0.72 o 1 18 0 299.29 319.28 6.99 o 2 18 0 2.87 4.41 0.36 o 3 18 0 91.83 87.47 3.15 o 1 19 0 219.39 228.59 4.74 o 2 19 0 7.72 7.10 0.49 o 0 20 0 445.39 444.44 14.54 o 1 20 0 1.11 2.93 0.30 o -5 0 1 20.52 20.68 1.40 o -3 0 1 24.64 29.90 1.40 o -1 0 1 53.02 50.84 2.18 o 1 0 1 408.52 487.72 15.78 o 3 0 1 1994.28 1984.41 54.83 o 5 0 1 213.89 221.24 18.68 o -5 1 1 71.64 74.36 2.49 o -4 1 1 53.99 58.31 2.01 o -3 1 1 1760.18 1574.45 30.92 o -2 1 1 39.94 46.74 1.82 o -1 1 1 147.50 147.50 3.88 o 0 1 1 286.48 180.57 14.62 o 1 1 1 70.34 94.94 2.77 o 2 1 1 626.08 692.58 22.58 o 3 1 1 2145.59 1970.45 38.49 o 4 1 1 130.01 123.21 4.43 o 5 1 1 210.14 228.32 6.69 o -5 2 1 167.61 180.76 6.26 o -4 2 1 677.82 712.15 20.01 o -3 2 1 18.32 23.12 0.74 o -2 2 1 1328.46 1374.63 44.43 o -1 2 1 2814.82 3181.44 101.22 o 0 2 1 549.07 611.13 15.15 o 1 2 1 841.17 998.82 32.23 o 2 2 1 3121.32 3199.29 107.06 o 3 2 1 227.19 212.63 4.45 o 4 2 1 275.90 264.08 8.43 o 5 2 1 22.42 23.74 1.19 o -5 3 1 133.34 149.23 5.33 o -4 3 1 594.36 618.57 17.43 o -3 3 1 20.75 20.43 0.68 o -2 3 1 13.61 19.04 1.32 o 0 3 1 151.62 165.91 3.69 o 1 3 1 702.02 777.56 19.57 o 2 3 1 97.56 88.12 3.47 o 3 3 1 190.57 190.04 4.62 o 4 3 1 184.03 186.80 5.86 o 5 3 1 80.35 85.60 3.19 o -5 4 1 2.53 2.62 0.41 o -4 4 1 210.51 208.95 5.52 o -3 4 1 1.50 2.65 0.30 o -2 4 1 49.13 46.92 2.26 o -1 4 1 5999.98 6621.62 258.27 o 0 4 1 3467.64 3743.10 130.51 o 1 4 1 18.39 27.12 0.88 o 2 4 1 1089.90 1112.19 69.44 o 3 4 1 103.49 99.02 2.71 o 4 4 1 57.73 53.21 1.69 o 5 4 1 100.70 102.95 4.59 o -5 5 1 210.59 212.75 7.32 o -4 5 1 743.42 698.10 22.66 o -3 5 1 673.72 587.46 21.39 o -2 5 1 631.77 615.69 20.56 o -1 5 1 205.16 210.32 6.43 o 0 5 1 1070.44 1188.18 23.51 o 1 5 1 5196.38 5493.66 129.34 o 2 5 1 203.43 200.10 9.11 o 3 5 1 709.21 656.85 15.04 o 4 5 1 0.09 0.89 0.30 o 5 5 1 81.49 78.76 3.70 o -5 6 1 62.43 66.08 2.57 o -4 6 1 12.52 15.69 0.87 o -3 6 1 36.15 40.69 2.53 o -2 6 1 2582.95 2527.71 62.87 o -1 6 1 42.62 43.67 1.86 o 0 6 1 2686.09 2709.66 61.40 o 1 6 1 365.99 421.69 10.97 o 2 6 1 12.87 11.76 0.46 o 3 6 1 524.03 468.29 10.01 o 4 6 1 53.59 54.49 1.72 o 5 6 1 42.73 45.85 1.91 o -5 7 1 18.16 17.61 0.99 o -4 7 1 420.02 410.02 13.61 o -3 7 1 75.51 79.41 3.00 o -2 7 1 10.84 9.38 0.53 o -1 7 1 4190.25 4318.11 119.57 o 0 7 1 118.17 114.96 3.54 o 1 7 1 368.95 369.45 9.95 o 2 7 1 208.45 220.54 3.96 o 3 7 1 1.11 4.69 0.38 o 4 7 1 14.76 14.26 0.87 o 5 7 1 47.76 48.78 1.99 o -5 8 1 18.02 16.85 0.94 o -4 8 1 45.65 48.44 3.06 o -3 8 1 252.55 257.98 7.51 o -2 8 1 1685.93 1510.59 29.68 o -1 8 1 428.26 434.69 13.05 o 0 8 1 2363.65 2260.52 56.48 o 1 8 1 415.73 426.00 12.80 o 2 8 1 385.51 329.98 6.04 o 3 8 1 399.55 389.85 8.42 o 4 8 1 117.75 122.44 5.56 o 5 8 1 33.64 30.41 1.15 o -5 9 1 72.46 66.13 2.51 o -4 9 1 4.64 4.73 0.49 o -3 9 1 744.81 729.94 18.30 o -2 9 1 639.35 579.61 12.30 o -1 9 1 1337.95 1191.51 22.32 o 0 9 1 294.94 281.84 6.49 o 1 9 1 1396.35 1279.26 25.33 o 2 9 1 691.21 651.05 11.53 o 3 9 1 8.16 9.96 0.75 o 4 9 1 66.05 72.07 2.43 o 5 9 1 95.65 100.89 4.33 o -5 10 1 24.28 23.34 1.08 o -4 10 1 0.75 0.77 0.26 o -3 10 1 436.96 445.98 11.34 o -2 10 1 0.26 2.40 0.48 o -1 10 1 2.15 5.48 0.52 o 0 10 1 1759.69 1700.41 30.04 o 1 10 1 350.78 331.56 6.35 o 2 10 1 63.18 79.94 1.85 o 3 10 1 734.63 742.05 15.77 o 4 10 1 86.57 82.08 3.17 o 5 10 1 15.53 13.06 1.47 o -5 11 1 168.16 166.52 6.90 o -4 11 1 2.22 2.59 0.44 o -3 11 1 658.20 598.57 16.82 o -2 11 1 341.18 325.51 7.64 o -1 11 1 554.62 515.93 10.34 o 0 11 1 232.52 230.95 4.14 o 1 11 1 640.34 593.77 11.17 o 2 11 1 932.10 967.84 19.09 o 3 11 1 32.84 37.39 1.21 o 4 11 1 15.56 17.20 0.85 o -4 12 1 301.11 290.40 8.37 o -3 12 1 401.80 372.66 15.05 o -2 12 1 1041.50 1045.12 23.81 o -1 12 1 3.03 12.70 0.50 o 0 12 1 230.30 230.80 4.74 o 1 12 1 113.33 127.30 2.75 o 2 12 1 1225.66 1264.76 24.93 o 3 12 1 0.92 1.55 0.34 o 4 12 1 23.78 22.57 1.04 o -4 13 1 22.22 25.15 1.22 o -3 13 1 36.31 28.67 1.78 o -2 13 1 120.56 120.61 3.18 o -1 13 1 0.67 0.98 0.21 o 0 13 1 347.42 349.38 7.07 o 1 13 1 33.46 38.45 1.02 o 2 13 1 635.06 639.81 12.76 o 3 13 1 38.45 39.86 1.24 o 4 13 1 152.29 149.66 4.45 o -4 14 1 157.88 152.59 5.27 o -3 14 1 78.40 79.40 5.15 o -2 14 1 620.40 609.13 19.93 o -1 14 1 0.01 1.21 0.23 o 0 14 1 92.27 89.24 2.03 o 1 14 1 105.73 108.59 2.43 o 2 14 1 231.76 236.61 5.68 o 3 14 1 2.56 3.44 0.35 o 4 14 1 112.34 111.84 5.30 o -4 15 1 0.70 1.38 0.29 o -3 15 1 451.60 475.69 15.61 o -2 15 1 19.98 20.19 1.05 o -1 15 1 267.57 279.25 6.16 o 0 15 1 95.90 96.61 2.07 o 1 15 1 722.64 762.18 16.18 o 2 15 1 243.13 247.66 6.29 o 3 15 1 268.08 285.10 8.23 o -3 16 1 23.73 23.11 1.15 o -2 16 1 45.72 45.25 1.53 o -1 16 1 2.50 4.74 0.57 o 0 16 1 254.41 275.11 6.05 o 1 16 1 2.94 4.36 0.35 o 2 16 1 61.53 66.90 1.86 o 3 16 1 26.00 32.21 1.22 o -3 17 1 133.30 144.65 5.01 o -2 17 1 204.66 203.90 5.47 o -1 17 1 129.48 132.22 3.38 o 0 17 1 3.87 6.27 0.47 o 1 17 1 62.12 63.63 1.65 o 2 17 1 1.08 2.41 0.30 o 3 17 1 38.76 37.44 1.55 o -3 18 1 5.49 5.20 0.46 o -2 18 1 420.94 433.16 12.31 o -1 18 1 25.61 28.08 0.97 o 0 18 1 451.75 479.24 11.16 o 1 18 1 51.48 56.76 1.40 o 2 18 1 268.89 278.13 6.55 o -2 19 1 8.28 7.61 0.59 o -1 19 1 25.71 30.13 0.92 o 0 19 1 63.35 64.95 2.00 o 1 19 1 6.53 6.39 0.47 o 2 19 1 8.25 9.55 0.55 o -1 20 1 3.17 4.58 0.37 o 0 20 1 159.75 147.02 3.97 o 1 20 1 209.43 196.00 6.64 o 0 21 1 16.02 18.30 1.20 o -4 0 2 119.34 117.16 10.53 o -2 0 2 4927.82 5325.40 208.02 o 4 0 2 103.40 108.21 4.73 o -5 1 2 490.85 541.60 21.76 o -4 1 2 0.05 0.35 0.22 o -3 1 2 353.26 297.68 6.48 o -2 1 2 518.04 550.13 18.24 o -1 1 2 38.97 57.91 2.03 o 1 1 2 1556.08 1730.58 47.88 o 2 1 2 259.69 276.89 16.59 o 3 1 2 308.96 304.12 6.56 o 4 1 2 218.97 189.97 4.25 o 5 1 2 0.30 1.29 0.54 o -5 2 2 3.24 4.40 0.61 o -4 2 2 56.96 60.07 1.85 o -3 2 2 75.48 75.31 1.84 o -2 2 2 55.29 66.74 2.88 o -1 2 2 536.76 710.40 16.04 o 0 2 2 1011.94 1260.10 40.29 o 1 2 2 703.17 835.34 27.17 o 2 2 2 0.99 1.00 0.67 o 3 2 2 279.89 242.77 5.73 o 4 2 2 1.32 1.70 0.38 o 5 2 2 1.74 3.91 0.57 o -5 3 2 632.38 678.74 27.08 o -4 3 2 6.66 8.73 0.55 o -3 3 2 441.27 401.11 9.33 o -2 3 2 958.28 1048.86 34.16 o 0 3 2 20.22 37.78 1.20 o 1 3 2 170.68 193.56 6.41 o 2 3 2 839.85 877.90 45.07 o 3 3 2 379.47 335.23 7.81 o 4 3 2 72.19 67.94 3.14 o 5 3 2 36.74 43.46 1.81 o -5 4 2 635.55 672.78 21.97 o -4 4 2 606.35 605.72 19.75 o -3 4 2 75.18 81.28 2.57 o -2 4 2 458.30 521.84 17.52 o -1 4 2 3768.85 4124.26 92.82 o 0 4 2 485.58 553.23 11.88 o 1 4 2 3.07 7.56 0.86 o 2 4 2 136.05 107.74 2.70 o 3 4 2 252.46 238.72 5.66 o 4 4 2 70.11 72.14 2.12 o 5 4 2 35.35 37.82 1.98 o -5 5 2 31.72 29.74 1.24 o -4 5 2 99.81 117.13 4.26 o -3 5 2 87.13 99.39 5.09 o -2 5 2 671.60 700.71 22.27 o -1 5 2 24.81 36.54 1.62 o 0 5 2 1636.94 1949.21 38.26 o 1 5 2 1634.28 2039.01 92.56 o 2 5 2 187.75 167.88 3.66 o 3 5 2 11.54 14.30 0.60 o 4 5 2 607.94 587.88 19.12 o 5 5 2 41.32 44.25 2.24 o -5 6 2 21.58 17.49 1.01 o -4 6 2 745.81 772.20 25.07 o -3 6 2 84.30 102.58 6.97 o -2 6 2 1643.12 1474.63 31.19 o -1 6 2 468.33 524.79 15.20 o 0 6 2 216.09 227.44 5.65 o 1 6 2 58.54 57.12 3.22 o 2 6 2 1269.38 1138.95 19.10 o 3 6 2 0.98 3.56 0.32 o 4 6 2 58.07 63.98 1.67 o 5 6 2 269.79 270.08 11.02 o -5 7 2 231.21 224.86 7.61 o -4 7 2 88.25 92.36 2.80 o -3 7 2 1015.25 983.07 24.50 o -2 7 2 94.54 88.08 2.01 o -1 7 2 480.82 446.68 13.21 o 0 7 2 570.41 579.30 17.20 o 1 7 2 1503.87 1449.57 57.77 o 2 7 2 88.57 82.91 1.67 o 3 7 2 371.32 372.30 8.05 o 4 7 2 26.46 25.80 1.20 o 5 7 2 86.11 89.05 3.17 o -5 8 2 116.54 120.16 4.26 o -4 8 2 309.40 309.09 10.04 o -3 8 2 134.87 144.09 5.36 o -2 8 2 171.96 188.22 3.96 o -1 8 2 2.34 3.89 0.56 o 0 8 2 440.98 425.89 10.33 o 1 8 2 1071.68 973.19 20.63 o 2 8 2 203.31 214.61 4.76 o 3 8 2 1.60 3.75 0.60 o 4 8 2 0.33 6.55 0.49 o 5 8 2 417.66 413.27 16.44 o -5 9 2 80.25 76.12 2.59 o -4 9 2 2.17 3.24 0.40 o -3 9 2 608.75 587.61 16.77 o -2 9 2 9.47 11.49 0.51 o -1 9 2 48.58 63.54 1.47 o 0 9 2 15.16 13.98 0.52 o 1 9 2 398.24 351.18 6.56 o 2 9 2 298.37 279.31 5.70 o 3 9 2 682.00 672.16 14.34 o 4 9 2 544.40 580.97 16.43 o -5 10 2 4.15 3.62 0.71 o -4 10 2 77.25 76.97 2.55 o -3 10 2 10.91 13.35 0.67 o -2 10 2 797.68 769.64 17.61 o -1 10 2 14.86 14.51 0.53 o 0 10 2 1456.74 1417.96 28.09 o 1 10 2 247.84 254.87 5.34 o 2 10 2 192.90 206.77 4.32 o 3 10 2 151.76 148.93 3.23 o 4 10 2 739.49 779.59 21.85 o -5 11 2 40.75 45.96 3.26 o -4 11 2 11.30 12.60 0.71 o -3 11 2 22.39 20.58 0.98 o -2 11 2 144.12 141.31 3.52 o -1 11 2 577.86 558.88 11.98 o 0 11 2 13.15 12.43 0.59 o 1 11 2 0.63 3.96 0.30 o 2 11 2 30.82 40.86 1.09 o 3 11 2 623.04 661.44 14.13 o 4 11 2 32.89 33.74 1.29 o -4 12 2 12.21 14.17 0.87 o -3 12 2 5.39 6.01 0.70 o -2 12 2 117.70 120.90 3.08 o -1 12 2 14.84 15.07 0.62 o 0 12 2 368.86 385.36 8.99 o 1 12 2 48.14 56.76 1.48 o 2 12 2 655.78 672.92 14.36 o 3 12 2 339.53 365.51 8.63 o 4 12 2 48.29 45.09 1.59 o -4 13 2 5.96 5.99 0.56 o -3 13 2 3.71 6.52 0.57 o -2 13 2 1.34 3.42 0.36 o -1 13 2 1085.66 1118.86 25.49 o 0 13 2 301.30 327.84 7.73 o 1 13 2 923.82 948.19 20.05 o 2 13 2 84.84 93.28 2.31 o 3 13 2 113.50 121.99 3.13 o 4 13 2 41.81 38.81 1.37 o -4 14 2 154.67 152.28 5.25 o -3 14 2 86.90 79.20 2.63 o -2 14 2 463.50 428.46 16.87 o -1 14 2 157.70 156.80 4.27 o 0 14 2 8.92 11.21 0.78 o 1 14 2 21.98 19.97 0.77 o 2 14 2 8.33 10.80 0.58 o 3 14 2 98.50 104.88 2.50 o -4 15 2 9.98 11.55 0.68 o -3 15 2 1.72 3.20 0.45 o -2 15 2 21.25 17.91 0.74 o -1 15 2 10.40 11.02 1.02 o 0 15 2 35.56 38.83 1.43 o 1 15 2 146.94 140.48 3.27 o 2 15 2 64.84 70.63 1.82 o 3 15 2 18.57 18.65 0.66 o -3 16 2 0.59 1.14 0.29 o -2 16 2 286.44 287.82 6.86 o -1 16 2 76.58 72.34 2.14 o 0 16 2 985.04 1001.56 25.09 o 1 16 2 16.53 16.35 0.79 o 2 16 2 245.27 245.27 5.44 o 3 16 2 39.15 36.13 1.33 o -3 17 2 111.39 114.94 4.05 o -2 17 2 31.51 27.23 0.96 o -1 17 2 178.30 180.02 4.44 o 0 17 2 320.00 330.87 8.58 o 1 17 2 73.40 79.83 2.19 o 2 17 2 154.30 166.29 4.48 o 3 17 2 58.95 64.21 4.46 o -3 18 2 27.85 31.58 2.13 o -2 18 2 0.74 1.33 0.27 o -1 18 2 0.10 1.10 0.27 o 0 18 2 19.62 24.89 1.00 o 1 18 2 588.26 672.82 18.97 o 2 18 2 8.54 8.23 0.57 o -2 19 2 75.89 67.49 1.95 o -1 19 2 45.13 47.28 1.50 o 0 19 2 115.42 115.00 3.21 o 1 19 2 233.68 241.24 7.04 o 2 19 2 2.25 3.03 0.48 o -1 20 2 4.13 4.14 0.41 o 0 20 2 139.28 143.26 3.85 o 1 20 2 28.16 29.23 1.31 o -5 0 3 177.55 210.15 12.66 o -3 0 3 544.37 542.55 17.88 o -1 0 3 223.05 258.49 7.46 o 3 0 3 447.27 454.57 16.13 o 5 0 3 1026.13 1023.85 57.02 o -5 1 3 115.01 129.18 5.77 o -4 1 3 23.55 22.62 1.03 o -3 1 3 1017.38 966.48 22.02 o -2 1 3 32.89 37.02 1.91 o -1 1 3 375.56 432.44 9.28 o 0 1 3 1150.06 1541.64 49.21 o 1 1 3 1880.34 1905.62 74.86 o 2 1 3 192.12 181.60 3.75 o 3 1 3 6.48 7.36 0.43 o 4 1 3 6.33 13.17 1.23 o 5 1 3 32.29 31.67 1.76 o -5 2 3 280.35 300.83 12.44 o -4 2 3 515.86 504.54 16.06 o -3 2 3 406.34 396.87 10.16 o -2 2 3 1167.74 1170.60 38.08 o -1 2 3 3.88 8.21 0.40 o 0 2 3 2417.84 2980.89 95.00 o 1 2 3 109.18 128.66 5.63 o 2 2 3 2052.95 1975.82 38.51 o 3 2 3 391.54 404.95 8.70 o 4 2 3 63.34 58.00 1.78 o 5 2 3 33.47 38.66 1.95 o -5 3 3 25.18 29.07 1.81 o -4 3 3 1.18 2.87 0.42 o -3 3 3 338.86 355.49 10.53 o -2 3 3 6.64 7.74 0.83 o -1 3 3 72.97 75.46 2.54 o 0 3 3 536.39 617.21 20.13 o 1 3 3 485.31 563.58 26.03 o 2 3 3 1683.78 1579.72 27.62 o 3 3 3 91.33 95.47 2.28 o 4 3 3 553.99 517.09 14.06 o 5 3 3 2.38 2.73 0.44 o -5 4 3 78.13 80.42 2.76 o -4 4 3 169.71 184.40 6.44 o -3 4 3 67.64 66.28 2.54 o -2 4 3 1313.20 1280.68 29.21 o -1 4 3 895.69 928.63 23.97 o 0 4 3 493.56 605.54 19.88 o 1 4 3 9.68 12.41 1.09 o 2 4 3 509.27 448.99 8.47 o 3 4 3 168.62 156.54 3.85 o 4 4 3 14.73 15.76 0.82 o 5 4 3 43.03 40.42 3.63 o -5 5 3 29.20 32.89 1.60 o -4 5 3 13.89 16.49 0.85 o -3 5 3 249.94 241.21 7.50 o -2 5 3 697.28 690.27 14.87 o -1 5 3 1033.67 1026.32 35.60 o 0 5 3 65.31 92.69 2.78 o 1 5 3 1164.89 1199.76 47.62 o 2 5 3 0.67 1.64 0.20 o 3 5 3 76.87 77.05 2.29 o 4 5 3 6.08 5.67 0.44 o 5 5 3 32.81 34.79 5.19 o -5 6 3 32.40 31.75 1.30 o -4 6 3 102.25 102.22 2.94 o -3 6 3 224.67 218.13 5.70 o -2 6 3 2535.71 2316.52 42.83 o -1 6 3 126.07 129.70 3.60 o 0 6 3 486.83 527.66 15.29 o 1 6 3 1384.25 1295.71 29.47 o 2 6 3 183.16 198.20 4.39 o 3 6 3 610.43 582.76 16.49 o 4 6 3 619.41 646.88 14.87 o 5 6 3 36.51 38.90 3.53 o -5 7 3 50.25 45.42 2.08 o -4 7 3 10.69 13.00 0.68 o -3 7 3 1.33 2.97 0.38 o -2 7 3 3716.07 3437.79 67.02 o -1 7 3 1774.81 1725.21 39.45 o 0 7 3 94.28 116.59 2.94 o 1 7 3 1350.29 1324.41 24.59 o 2 7 3 638.75 610.32 16.08 o 3 7 3 172.45 163.92 4.91 o 4 7 3 52.48 54.90 1.72 o -5 8 3 0.36 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