data_2240743 _cell_angle_alpha 90.000 _cell_angle_beta 105.833 _cell_angle_gamma 90.000 _cell_length_a 15.5991 _cell_length_b 7.4440 _cell_length_c 13.7920 _exptl_crystal_F_000 796.00 _reflns_d_resolution_high 0.7186 _cod_data_source_file sj5459Isup2.hkl _cod_data_source_block I _shelx_title ' s98 in C2/c (BLOCK ORANGE)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 94.89 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 0 0 1973.70 1769.84 29.52 o 10 0 0 6886.28 7229.46 87.25 o 12 0 0 1437.84 1616.15 21.09 o 14 0 0 93.48 156.98 4.61 o 16 0 0 724.72 915.03 11.53 o 18 0 0 106.74 114.79 2.31 o 20 0 0 155.97 140.74 2.79 o 1 1 0 264.18 422.82 4.09 o 3 1 0 315.35 399.69 3.45 o 5 1 0 5.26 4.54 0.25 o 7 1 0 24.34 32.94 0.95 o 9 1 0 3.29 2.17 0.64 o 11 1 0 17.51 25.64 0.78 o 13 1 0 45.27 48.13 0.97 o 15 1 0 74.94 78.40 1.33 o 17 1 0 8.31 6.65 0.63 o 19 1 0 3.14 1.43 0.67 o 2 2 0 266.37 345.54 4.89 o 4 2 0 7560.68 7208.02 229.42 o 6 2 0 696.43 416.55 4.34 o 8 2 0 180.99 143.43 1.65 o 10 2 0 130.61 92.50 1.22 o 12 2 0 123.56 185.52 2.98 o 14 2 0 44.19 61.99 1.12 o 16 2 0 267.38 342.89 5.07 o 18 2 0 57.40 71.98 2.29 o 20 2 0 76.99 69.05 1.41 o 1 3 0 88.36 28.12 0.42 o 3 3 0 177.61 222.25 2.38 o 5 3 0 1665.43 1414.32 12.73 o 7 3 0 75.49 67.02 0.94 o 9 3 0 1059.37 1048.21 9.32 o 11 3 0 0.04 0.62 0.40 o 13 3 0 3.14 1.58 0.44 o 15 3 0 7.85 10.10 0.65 o 17 3 0 8.50 6.74 0.66 o 19 3 0 0.02 0.67 0.69 o 2 4 0 5930.10 6171.10 80.21 o 6 4 0 3918.39 3784.63 30.54 o 8 4 0 751.34 822.26 7.50 o 10 4 0 67.32 36.41 0.68 o 12 4 0 260.01 329.01 3.21 o 14 4 0 355.12 357.05 3.74 o 16 4 0 378.58 392.05 3.96 o 18 4 0 114.20 137.17 2.22 o 1 5 0 540.54 537.10 5.78 o 3 5 0 499.68 443.53 6.01 o 5 5 0 2937.39 2932.58 28.99 o 7 5 0 74.09 90.33 1.48 o 9 5 0 1053.48 1006.29 8.88 o 11 5 0 58.39 62.36 1.62 o 13 5 0 104.80 114.22 1.97 o 15 5 0 34.73 24.66 0.94 o 17 5 0 0.07 0.14 0.65 o 0 6 0 1691.59 1983.62 26.49 o 2 6 0 2680.17 2454.43 29.11 o 4 6 0 2981.99 3253.96 39.28 o 6 6 0 1558.38 1492.22 12.90 o 8 6 0 113.43 131.77 1.58 o 10 6 0 18.90 23.01 0.59 o 12 6 0 102.38 118.78 2.39 o 14 6 0 199.29 211.17 3.45 o 16 6 0 80.01 71.21 1.37 o 1 7 0 259.51 303.65 3.66 o 3 7 0 173.84 132.26 1.86 o 5 7 0 1184.17 1243.22 12.37 o 7 7 0 147.75 154.01 3.22 o 9 7 0 219.73 226.28 3.46 o 11 7 0 2.28 3.03 0.55 o 13 7 0 6.57 6.70 0.68 o 15 7 0 3.01 1.04 0.73 o 0 8 0 998.15 1117.55 20.68 o 2 8 0 1591.82 1464.19 15.00 o 4 8 0 596.38 611.50 7.65 o 6 8 0 468.56 528.72 6.18 o 8 8 0 256.38 226.24 2.95 o 10 8 0 239.56 291.13 3.56 o 12 8 0 195.17 202.52 2.87 o 1 9 0 2.89 0.39 0.75 o 3 9 0 60.12 66.61 1.26 o 5 9 0 351.66 324.17 3.97 o 7 9 0 110.14 121.00 3.26 o 9 9 0 137.34 137.12 2.15 o 0 10 0 119.19 134.47 3.48 o 2 10 0 123.03 88.93 2.77 o 4 10 0 9.17 4.76 1.16 o -21 1 1 118.10 139.37 2.05 o -19 1 1 87.50 83.22 1.52 o -17 1 1 327.27 266.74 3.13 o -15 1 1 475.36 620.93 6.37 o -13 1 1 305.03 205.05 2.36 o -11 1 1 8784.35 9621.54 95.82 o -9 1 1 8033.77 8286.17 100.15 o -5 1 1 5207.28 5280.30 68.15 o 5 1 1 18.62 60.13 1.00 o 7 1 1 227.68 327.54 5.37 o 9 1 1 2934.36 2802.06 41.18 o 11 1 1 1975.17 1916.03 19.26 o 13 1 1 241.07 389.74 4.06 o 15 1 1 376.05 338.22 3.61 o 17 1 1 435.99 438.77 4.45 o 19 1 1 88.64 108.79 1.68 o -20 2 1 19.00 15.27 1.62 o -18 2 1 1.66 0.95 0.77 o -16 2 1 17.69 18.24 0.75 o -14 2 1 17.61 10.56 0.55 o -12 2 1 368.76 333.17 3.41 o -10 2 1 876.13 928.37 10.24 o -8 2 1 231.30 245.11 2.45 o -6 2 1 1479.19 1356.46 11.42 o -4 2 1 30.71 50.33 0.66 o -2 2 1 867.43 680.86 20.62 o 2 2 1 489.96 560.30 4.82 o 4 2 1 372.54 315.00 6.82 o 6 2 1 93.21 89.36 1.38 o 8 2 1 147.14 143.87 1.69 o 10 2 1 5.99 1.68 0.54 o 12 2 1 47.10 53.13 0.97 o 14 2 1 75.20 81.49 1.29 o 16 2 1 1.34 1.57 0.67 o 18 2 1 10.56 10.92 0.79 o 20 2 1 11.14 8.57 0.90 o -19 3 1 25.05 24.62 0.99 o -17 3 1 101.30 99.87 1.62 o -15 3 1 220.37 231.75 2.77 o -13 3 1 248.89 220.65 2.43 o -11 3 1 2338.72 2451.16 20.37 o -9 3 1 2287.13 2065.15 17.81 o -5 3 1 5698.18 6034.85 101.31 o -1 3 1 427.70 669.10 8.26 o 1 3 1 1519.85 993.52 8.45 o 3 3 1 67.29 43.03 0.59 o 5 3 1 2327.77 2314.07 32.29 o 7 3 1 20.14 7.30 0.50 o 9 3 1 1465.17 1721.73 14.46 o 11 3 1 698.97 604.13 9.33 o 13 3 1 867.45 1038.88 9.48 o 15 3 1 728.52 743.58 9.91 o 17 3 1 237.41 208.00 2.48 o 19 3 1 61.71 68.09 1.40 o -18 4 1 2.30 0.89 0.67 o -16 4 1 29.03 38.85 0.93 o -14 4 1 5.04 7.77 0.53 o -12 4 1 186.99 178.72 2.76 o -10 4 1 15.42 23.89 0.67 o -8 4 1 84.01 66.91 1.09 o -6 4 1 2551.71 2404.21 30.66 o -4 4 1 142.25 193.83 3.67 o -2 4 1 2586.60 2006.98 21.49 o 0 4 1 101.42 146.26 1.50 o 2 4 1 1038.74 832.89 11.31 o 4 4 1 104.89 135.93 1.45 o 6 4 1 8.61 4.92 0.28 o 8 4 1 1204.74 1187.12 10.70 o 10 4 1 15.13 16.25 0.51 o 12 4 1 213.65 239.67 2.71 o 14 4 1 4.20 7.72 0.61 o 16 4 1 12.00 10.42 0.75 o 18 4 1 7.29 5.26 0.82 o -17 5 1 78.66 90.89 2.14 o -15 5 1 427.60 413.88 4.00 o -13 5 1 592.91 640.33 6.17 o -11 5 1 827.23 829.61 7.62 o -9 5 1 1981.24 1980.01 18.51 o -7 5 1 4716.44 5152.16 52.92 o -5 5 1 6722.06 6621.94 69.97 o -3 5 1 5890.90 6614.68 93.81 o -1 5 1 297.53 188.33 2.25 o 1 5 1 632.31 731.73 8.25 o 3 5 1 1154.65 1072.52 9.74 o 5 5 1 1640.15 1751.85 14.97 o 7 5 1 709.91 644.01 8.23 o 9 5 1 254.11 359.06 3.49 o 11 5 1 494.97 469.25 4.41 o 13 5 1 935.22 995.84 8.92 o 15 5 1 527.38 542.28 5.34 o 17 5 1 170.25 150.20 2.08 o -16 6 1 47.34 52.31 1.15 o -14 6 1 18.48 15.71 0.65 o -12 6 1 10.15 14.78 0.85 o -10 6 1 35.35 29.53 0.64 o -8 6 1 116.21 139.41 1.66 o -6 6 1 791.82 831.14 9.28 o -4 6 1 250.01 222.27 2.89 o -2 6 1 4284.63 4603.11 46.36 o 0 6 1 657.70 506.31 5.34 o 2 6 1 2040.54 2332.26 22.90 o 4 6 1 28.69 12.97 0.40 o 6 6 1 24.34 15.03 0.46 o 8 6 1 282.07 282.47 2.82 o 10 6 1 23.22 28.33 0.76 o 12 6 1 92.06 94.35 1.35 o 14 6 1 2.62 3.56 0.60 o 16 6 1 7.80 7.19 0.75 o -15 7 1 144.95 141.96 1.88 o -13 7 1 317.71 345.99 4.99 o -11 7 1 242.01 225.70 2.44 o -9 7 1 394.72 431.92 4.76 o -7 7 1 591.90 551.35 5.77 o -5 7 1 1262.51 1227.92 12.37 o -3 7 1 714.19 776.55 10.05 o -1 7 1 198.67 144.52 2.13 o 1 7 1 8.10 2.83 0.26 o 3 7 1 73.37 68.55 1.11 o 5 7 1 8.79 11.70 0.93 o 7 7 1 83.49 78.40 1.18 o 9 7 1 32.02 32.96 0.73 o 11 7 1 95.62 99.40 1.35 o 13 7 1 144.63 135.63 2.12 o 15 7 1 70.60 60.99 1.61 o -12 8 1 105.70 115.63 2.54 o -10 8 1 70.45 70.84 1.36 o -8 8 1 56.58 52.71 1.16 o -6 8 1 0.82 1.90 0.58 o -4 8 1 3.90 5.31 0.48 o -2 8 1 980.79 949.21 10.70 o 0 8 1 173.57 168.36 2.66 o 2 8 1 134.20 135.20 2.65 o 4 8 1 20.31 22.69 0.68 o 6 8 1 59.88 50.56 1.05 o 8 8 1 78.01 80.09 1.40 o 10 8 1 11.26 12.01 0.57 o 12 8 1 56.79 54.40 1.17 o -9 9 1 316.06 345.36 4.76 o -7 9 1 263.12 208.19 2.82 o -5 9 1 548.10 571.01 6.46 o -3 9 1 576.06 578.88 6.26 o -1 9 1 1036.73 946.46 13.91 o 1 9 1 537.33 641.03 8.98 o 3 9 1 497.10 491.45 7.11 o 5 9 1 230.52 243.52 3.22 o 7 9 1 498.56 565.92 5.96 o 9 9 1 421.60 391.07 4.75 o -4 10 1 143.95 167.18 2.48 o -2 10 1 472.34 416.75 5.92 o 0 10 1 182.86 221.05 3.75 o 2 10 1 41.67 32.80 1.40 o 4 10 1 6.97 15.53 1.13 o -20 0 2 50.96 58.76 1.79 o -18 0 2 389.79 403.29 6.53 o -16 0 2 593.96 505.07 10.20 o -14 0 2 736.35 987.53 13.35 o -12 0 2 1967.51 1843.61 26.18 o -10 0 2 2543.94 2545.83 64.16 o -8 0 2 53.03 68.49 1.27 o -6 0 2 3785.58 2639.28 29.93 o 12 0 2 984.51 854.26 21.56 o 14 0 2 781.94 944.78 12.18 o 16 0 2 594.40 560.51 7.65 o 18 0 2 154.00 137.82 2.74 o 20 0 2 174.06 194.93 3.30 o -21 1 2 3.47 4.44 0.80 o -19 1 2 0.64 1.54 0.64 o -17 1 2 34.36 28.07 0.83 o -15 1 2 83.01 75.53 1.30 o -13 1 2 287.05 259.70 2.78 o -11 1 2 0.01 2.16 0.43 o -9 1 2 185.12 183.73 2.84 o -7 1 2 4679.43 4878.47 63.92 o -3 1 2 2129.10 1836.23 16.61 o -1 1 2 289.75 437.32 6.79 o 1 1 2 31.20 68.53 1.04 o 5 1 2 2494.89 2445.34 21.90 o 7 1 2 336.98 357.53 5.06 o 9 1 2 47.29 30.67 0.69 o 11 1 2 10.07 31.25 1.12 o 13 1 2 91.55 75.79 1.23 o 15 1 2 65.49 60.93 1.11 o 17 1 2 0.08 0.39 0.59 o 19 1 2 1.35 0.14 0.74 o -20 2 2 96.32 91.42 1.64 o -18 2 2 332.97 343.36 5.12 o -16 2 2 702.77 664.10 6.89 o -14 2 2 693.77 806.04 7.90 o -12 2 2 1432.87 1492.52 12.75 o -10 2 2 2463.19 2571.66 21.52 o -8 2 2 9.73 12.27 0.49 o -6 2 2 3044.63 2335.07 19.85 o -2 2 2 1659.42 724.63 6.30 o 0 2 2 9.29 32.21 0.91 o 2 2 2 436.84 649.01 7.66 o 4 2 2 5844.98 4919.38 72.21 o 6 2 2 5769.43 6012.59 90.51 o 8 2 2 1225.62 1169.33 19.50 o 10 2 2 5040.29 5608.84 72.63 o 12 2 2 214.93 134.77 1.70 o 14 2 2 314.47 379.23 4.03 o 16 2 2 190.23 202.12 3.57 o 18 2 2 14.14 8.86 0.71 o -19 3 2 28.41 36.55 0.97 o -17 3 2 1.75 1.60 0.60 o -15 3 2 12.66 11.94 0.56 o -13 3 2 94.64 74.52 1.11 o -11 3 2 553.00 460.86 4.14 o -9 3 2 58.63 45.72 0.76 o -7 3 2 36.38 45.08 0.73 o -5 3 2 1864.12 1524.95 12.98 o -3 3 2 1307.58 982.10 11.89 o 1 3 2 5487.30 5152.82 80.74 o 3 3 2 13.23 6.89 0.28 o 5 3 2 489.93 372.22 3.73 o 7 3 2 39.77 41.39 0.66 o 9 3 2 779.75 849.92 7.35 o 11 3 2 5.66 0.20 0.45 o 13 3 2 41.20 31.07 0.78 o 15 3 2 21.59 20.40 0.87 o 17 3 2 11.25 7.73 0.72 o 19 3 2 0.06 0.74 0.93 o -18 4 2 299.97 310.34 3.25 o -16 4 2 626.68 649.68 6.38 o -14 4 2 1225.76 1206.48 10.89 o -12 4 2 1555.21 1758.79 15.17 o -10 4 2 2078.46 2088.82 17.44 o -8 4 2 1049.32 1020.13 9.14 o -6 4 2 2694.65 2952.67 42.85 o -4 4 2 1.06 6.35 0.36 o -2 4 2 940.81 865.45 8.63 o 0 4 2 338.74 299.77 2.79 o 2 4 2 3024.11 3013.74 35.12 o 4 4 2 7061.39 7205.06 130.90 o 6 4 2 4753.02 5148.91 42.43 o 8 4 2 1356.82 1131.94 10.08 o 10 4 2 1529.55 1842.84 16.05 o 12 4 2 562.18 476.51 4.74 o 14 4 2 533.60 533.72 5.22 o 16 4 2 129.90 151.68 2.37 o 18 4 2 24.55 16.27 0.84 o -17 5 2 1.18 0.51 0.64 o -15 5 2 1.96 0.03 0.53 o -13 5 2 217.56 218.49 2.57 o -11 5 2 22.48 32.58 0.73 o -9 5 2 659.50 608.97 5.94 o -7 5 2 8.66 12.16 0.37 o -5 5 2 289.47 256.04 3.03 o -3 5 2 744.91 729.84 8.78 o -1 5 2 449.98 470.29 7.43 o 1 5 2 2667.38 2791.63 26.31 o 3 5 2 141.02 101.08 1.21 o 5 5 2 1207.71 1304.49 12.18 o 7 5 2 10.39 10.16 0.65 o 9 5 2 33.66 37.23 0.71 o 11 5 2 99.20 114.11 1.93 o 13 5 2 99.53 100.97 1.41 o 15 5 2 53.06 49.09 1.14 o 17 5 2 1.61 0.99 0.75 o -16 6 2 109.40 116.11 1.57 o -14 6 2 401.88 369.50 3.67 o -12 6 2 321.05 390.57 3.96 o -10 6 2 197.67 165.20 1.91 o -8 6 2 209.96 220.23 2.47 o -6 6 2 117.73 175.00 2.31 o -4 6 2 238.18 187.70 2.35 o -2 6 2 53.37 96.66 1.68 o 0 6 2 47.99 42.49 1.07 o 2 6 2 829.07 883.19 7.82 o 4 6 2 2228.75 2249.65 20.71 o 6 6 2 1749.46 1916.97 16.90 o 8 6 2 1162.42 1069.04 9.64 o 10 6 2 486.46 569.09 5.60 o 12 6 2 457.56 469.64 4.49 o 14 6 2 293.62 262.52 3.06 o 16 6 2 91.32 109.00 1.63 o -15 7 2 45.44 47.62 1.05 o -13 7 2 58.66 56.75 1.03 o -11 7 2 132.65 142.25 1.81 o -9 7 2 362.96 344.99 4.31 o -7 7 2 19.03 21.44 0.71 o -5 7 2 17.97 16.90 0.59 o -3 7 2 268.46 305.35 3.40 o -1 7 2 0.02 1.78 0.38 o 1 7 2 1627.80 1750.04 22.55 o 3 7 2 451.48 350.73 5.46 o 5 7 2 1067.98 1190.67 10.49 o 7 7 2 58.29 49.91 0.85 o 9 7 2 16.84 15.61 0.59 o 11 7 2 19.34 17.41 0.70 o 13 7 2 3.22 4.60 0.73 o -12 8 2 333.66 342.98 3.88 o -10 8 2 248.01 221.94 2.87 o -8 8 2 275.82 312.34 3.58 o -6 8 2 266.29 260.99 3.23 o -4 8 2 633.61 637.11 6.95 o -2 8 2 305.11 335.58 4.22 o 0 8 2 598.31 594.53 6.54 o 2 8 2 266.94 268.32 5.91 o 4 8 2 680.68 682.12 7.74 o 6 8 2 647.46 640.35 8.37 o 8 8 2 650.67 648.80 7.03 o 10 8 2 328.49 319.51 3.23 o 12 8 2 172.76 184.34 2.27 o -9 9 2 221.45 222.04 2.89 o -7 9 2 109.71 119.11 2.13 o -5 9 2 36.52 30.47 1.05 o -3 9 2 0.09 1.04 0.53 o -1 9 2 1.14 3.76 0.98 o 1 9 2 312.22 273.73 4.15 o 3 9 2 151.61 160.65 5.91 o 5 9 2 118.27 114.13 1.92 o 7 9 2 3.89 1.77 0.71 o 9 9 2 44.36 43.96 2.30 o -4 10 2 279.71 291.21 3.58 o -2 10 2 183.50 209.02 5.46 o 0 10 2 314.92 319.54 4.63 o 2 10 2 117.94 125.28 4.08 o 4 10 2 95.91 88.34 2.37 o -21 1 3 113.62 107.65 1.79 o -19 1 3 79.82 88.53 1.46 o -17 1 3 680.33 763.67 7.27 o -15 1 3 115.38 98.28 1.43 o -13 1 3 274.84 385.55 4.37 o -11 1 3 127.83 105.55 1.48 o -9 1 3 649.48 506.94 5.14 o -7 1 3 2124.03 2802.82 27.60 o -3 1 3 2214.36 2582.88 24.05 o 5 1 3 7680.95 6860.82 93.10 o 7 1 3 2212.89 1771.89 14.81 o 9 1 3 626.41 718.79 9.82 o 11 1 3 473.12 490.31 5.68 o 13 1 3 1.00 1.30 0.54 o 15 1 3 338.81 379.58 4.09 o 17 1 3 33.81 44.27 1.02 o 19 1 3 65.21 64.63 1.33 o -20 2 3 1.26 1.77 0.68 o -18 2 3 6.72 5.45 0.63 o -16 2 3 205.93 198.13 2.99 o -14 2 3 90.61 116.46 1.53 o -12 2 3 28.54 35.87 0.71 o -10 2 3 1121.09 1019.15 8.92 o -8 2 3 81.60 86.66 1.09 o -6 2 3 24.35 67.46 0.87 o -4 2 3 434.85 345.38 3.33 o 0 2 3 4471.21 4027.36 124.78 o 2 2 3 228.73 173.16 1.89 o 4 2 3 3551.82 3344.83 29.89 o 6 2 3 2.69 4.33 0.37 o 8 2 3 118.40 88.42 1.17 o 10 2 3 268.68 356.63 3.80 o 12 2 3 30.68 55.27 0.96 o 14 2 3 43.39 30.90 1.36 o 16 2 3 1.70 1.58 0.59 o 18 2 3 3.30 0.75 0.74 o -19 3 3 96.88 104.74 1.57 o -17 3 3 149.82 175.33 2.10 o -15 3 3 60.75 80.81 1.47 o -13 3 3 24.73 16.25 0.57 o -11 3 3 11.22 17.60 0.53 o -9 3 3 535.90 497.72 4.61 o -7 3 3 109.12 95.78 1.12 o -5 3 3 7686.68 6884.42 193.76 o -3 3 3 1699.50 1782.30 15.22 o 3 3 3 9004.73 9293.61 207.41 o 5 3 3 3565.65 3703.48 33.19 o 7 3 3 1818.42 1718.73 14.92 o 9 3 3 194.45 153.25 3.15 o 11 3 3 683.27 811.41 8.93 o 13 3 3 205.10 205.53 3.24 o 15 3 3 286.76 288.81 3.24 o 17 3 3 77.43 99.49 1.98 o -18 4 3 11.97 14.39 0.80 o -16 4 3 1.65 2.43 0.59 o -14 4 3 1.86 6.20 0.48 o -12 4 3 100.50 123.35 1.51 o -10 4 3 1839.96 1720.94 14.07 o -8 4 3 39.83 50.17 0.74 o -6 4 3 2898.99 2740.01 23.25 o -4 4 3 4.87 2.26 0.17 o -2 4 3 3292.12 3116.50 28.77 o 0 4 3 966.85 1138.85 10.17 o 2 4 3 507.01 568.37 4.98 o 4 4 3 1656.19 1559.67 13.48 o 6 4 3 43.87 32.58 0.57 o 8 4 3 396.86 489.28 4.86 o 10 4 3 65.11 90.25 1.28 o 12 4 3 130.44 146.99 2.06 o 14 4 3 18.13 10.71 0.65 o 16 4 3 11.85 16.35 0.80 o 18 4 3 0.92 -0.48 0.73 o -17 5 3 81.29 80.89 1.29 o -15 5 3 105.52 139.83 1.82 o -13 5 3 163.46 111.10 1.57 o -11 5 3 161.87 228.21 2.45 o -9 5 3 237.84 226.90 2.44 o -7 5 3 232.62 206.00 2.14 o -5 5 3 2146.16 2320.87 22.85 o -3 5 3 3091.38 2880.41 28.56 o -1 5 3 6135.43 6558.23 92.63 o 1 5 3 5403.61 5672.16 64.68 o 3 5 3 4345.44 4468.22 37.83 o 5 5 3 2225.29 2127.52 18.07 o 7 5 3 805.94 980.26 9.19 o 9 5 3 322.30 234.31 2.52 o 11 5 3 225.10 287.67 3.09 o 13 5 3 231.62 245.41 2.63 o 15 5 3 147.13 122.32 1.98 o 17 5 3 54.86 67.15 1.43 o -16 6 3 3.22 4.53 0.64 o -14 6 3 0.02 0.48 0.56 o -12 6 3 39.70 39.54 0.80 o -10 6 3 118.17 111.15 1.39 o -8 6 3 161.43 187.92 2.70 o -6 6 3 1383.07 1349.78 13.07 o -4 6 3 53.59 38.80 0.78 o -2 6 3 146.66 180.03 2.19 o 0 6 3 786.42 876.33 7.58 o 2 6 3 110.29 64.60 0.90 o 4 6 3 1178.21 1426.00 12.85 o 6 6 3 435.62 383.05 3.90 o 8 6 3 1042.88 1146.89 10.78 o 10 6 3 237.31 247.47 2.76 o 12 6 3 94.03 89.78 2.07 o 14 6 3 4.86 4.30 0.69 o -15 7 3 275.43 306.22 5.45 o -13 7 3 294.50 254.88 2.68 o -11 7 3 252.69 328.94 6.77 o -9 7 3 237.11 222.01 2.90 o -7 7 3 439.51 456.68 5.75 o -5 7 3 1065.62 1177.98 12.59 o -3 7 3 2303.73 2235.85 21.46 o -1 7 3 1489.23 1502.25 17.53 o 1 7 3 1824.05 1936.87 26.81 o 3 7 3 839.34 807.70 9.12 o 5 7 3 910.65 873.61 8.57 o 7 7 3 414.79 491.24 4.66 o 9 7 3 147.91 140.79 1.65 o 11 7 3 51.79 57.09 1.05 o 13 7 3 35.65 43.90 1.31 o -12 8 3 0.35 -0.19 0.83 o -10 8 3 107.95 107.13 2.93 o -8 8 3 394.54 421.92 4.81 o -6 8 3 1619.25 1596.59 17.05 o -4 8 3 1031.56 1041.45 10.24 o -2 8 3 447.98 434.73 4.69 o 0 8 3 10.75 11.86 0.58 o 2 8 3 134.54 138.96 1.70 o 4 8 3 4.73 6.06 0.40 o 6 8 3 1.05 0.73 0.47 o 8 8 3 127.97 127.98 1.54 o 10 8 3 5.82 5.63 0.64 o -9 9 3 33.78 28.82 1.20 o -7 9 3 142.63 164.19 2.43 o -5 9 3 159.49 159.29 3.89 o -3 9 3 320.71 288.34 3.62 o -1 9 3 222.87 227.33 3.69 o 1 9 3 387.14 358.92 5.11 o 3 9 3 158.92 143.97 3.16 o 5 9 3 350.63 362.83 4.23 o 7 9 3 225.44 218.90 2.89 o -4 10 3 145.03 155.56 3.29 o -2 10 3 43.64 32.65 1.42 o 0 10 3 0.36 -0.41 0.90 o 2 10 3 45.57 53.71 2.04 o -20 0 4 14.70 11.85 1.03 o -18 0 4 85.03 92.47 1.89 o -16 0 4 882.55 875.94 11.96 o -14 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