data_2240762 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.5276 _cell_length_b 12.7878 _cell_length_c 28.2850 _exptl_crystal_F_000 2356.34 _reflns_d_resolution_high 0.7470 _cod_data_source_file gk26311sup2.hkl _cod_data_source_block 1 _shelx_title ' k13_51 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 440.43 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 99960.83 116331.95 2709.24 o 4 0 0 21452.95 21394.22 816.10 o 6 0 0 23405.47 23721.13 973.48 o 8 0 0 5026.32 5039.94 472.95 o 10 0 0 19816.42 19334.70 1006.06 o 12 0 0 5322.96 4435.24 558.86 o 14 0 0 1199.45 1146.67 337.43 o 1 1 0 7301.82 7351.75 157.71 o 2 1 0 38153.44 40077.77 726.25 o 3 1 0 75098.05 81419.01 1660.88 o 4 1 0 34792.60 35417.66 796.69 o 5 1 0 507.63 1329.53 105.96 o 6 1 0 28242.33 29611.54 728.69 o 7 1 0 63851.90 62779.91 1409.66 o 8 1 0 5031.20 5123.04 342.09 o 9 1 0 2631.15 2585.02 260.37 o 10 1 0 6158.70 5638.38 407.57 o 11 1 0 11510.91 10762.61 540.69 o 12 1 0 18.98 56.88 109.71 o 13 1 0 3009.97 2952.58 324.51 o 14 1 0 1021.13 946.41 197.01 o 15 1 0 49.32 95.85 130.79 o 0 2 0 12323.92 12652.72 323.06 o 1 2 0 16673.15 17375.12 377.58 o 2 2 0 36919.61 38720.71 760.23 o 3 2 0 5327.94 5989.19 206.68 o 4 2 0 87635.48 91625.07 1760.30 o 5 2 0 1712.20 2130.84 152.29 o 6 2 0 9369.13 9554.46 322.28 o 7 2 0 13745.64 13870.75 434.15 o 8 2 0 934.36 1192.09 124.60 o 9 2 0 2878.21 3134.29 280.91 o 10 2 0 643.80 1259.60 201.23 o 11 2 0 2255.72 2170.57 261.31 o 12 2 0 3346.46 2972.80 321.36 o 13 2 0 81.05 127.94 116.36 o 14 2 0 7345.06 6360.05 504.14 o 15 2 0 2957.35 2861.77 367.41 o 1 3 0 21317.92 21824.75 447.74 o 2 3 0 112.37 141.04 32.47 o 3 3 0 20604.91 19134.87 431.03 o 4 3 0 3271.26 3560.82 145.84 o 5 3 0 49888.18 52834.50 1086.70 o 6 3 0 2361.88 2396.97 133.88 o 7 3 0 7278.14 7732.07 303.47 o 8 3 0 13.55 170.17 70.61 o 9 3 0 131.18 357.24 119.87 o 10 3 0 7.55 50.20 93.39 o 11 3 0 3399.39 3290.96 322.12 o 12 3 0 3146.00 3246.59 364.02 o 13 3 0 498.95 605.52 187.41 o 14 3 0 4846.72 4353.54 413.77 o 15 3 0 249.04 338.61 152.08 o 0 4 0 10514.06 10794.57 445.18 o 1 4 0 114976.10 116934.14 2516.30 o 2 4 0 678.18 869.69 66.80 o 3 4 0 29833.47 30851.54 655.74 o 4 4 0 52761.05 51732.22 1056.13 o 5 4 0 651.03 902.60 91.83 o 6 4 0 26673.64 25228.33 605.97 o 7 4 0 1298.26 1696.58 119.35 o 8 4 0 221.13 367.06 86.75 o 9 4 0 6291.60 6141.50 405.74 o 10 4 0 851.49 859.12 167.85 o 11 4 0 11919.63 11808.83 565.75 o 12 4 0 8848.76 8382.92 544.51 o 13 4 0 7158.00 6828.91 502.37 o 14 4 0 9440.70 8518.06 577.72 o 15 4 0 0.70 -124.62 197.27 o 1 5 0 51446.70 52286.45 1102.06 o 2 5 0 496.72 2173.55 101.41 o 3 5 0 115212.43 117618.63 2383.09 o 4 5 0 5695.23 6015.12 206.81 o 5 5 0 2511.59 3384.33 179.05 o 6 5 0 21.46 704.84 92.69 o 7 5 0 37639.38 38237.34 876.40 o 8 5 0 166.49 286.44 87.04 o 9 5 0 9620.80 9342.47 402.75 o 10 5 0 11.79 349.32 140.12 o 11 5 0 794.07 820.75 167.34 o 12 5 0 444.05 824.77 167.26 o 13 5 0 567.19 455.74 143.64 o 14 5 0 147.14 169.37 136.45 o 0 6 0 54373.41 54316.59 1528.57 o 1 6 0 14913.78 14732.11 355.10 o 2 6 0 46.51 178.02 38.05 o 3 6 0 24253.17 23700.36 545.44 o 4 6 0 28768.81 28687.57 654.86 o 5 6 0 4388.84 4094.17 195.00 o 6 6 0 4233.71 4648.66 219.48 o 7 6 0 12.89 53.81 58.70 o 8 6 0 21911.21 20925.27 633.15 o 9 6 0 2077.55 3068.70 242.99 o 10 6 0 27229.77 26050.18 868.55 o 11 6 0 3535.76 3719.27 337.76 o 12 6 0 192.08 226.30 114.88 o 13 6 0 9632.01 9685.95 640.67 o 14 6 0 2979.75 2866.09 359.54 o 1 7 0 6686.58 6798.88 240.58 o 2 7 0 6212.73 6164.76 200.46 o 3 7 0 23263.62 23328.41 549.17 o 4 7 0 242.46 588.70 78.47 o 5 7 0 124.99 346.57 73.83 o 6 7 0 1595.49 1821.65 152.37 o 7 7 0 6622.22 5980.50 268.25 o 8 7 0 186.19 378.29 101.30 o 9 7 0 482.95 605.49 113.44 o 10 7 0 163.49 315.23 103.60 o 11 7 0 4633.50 4120.07 352.42 o 12 7 0 390.88 272.00 162.77 o 13 7 0 1532.81 1427.52 309.27 o 14 7 0 380.16 355.90 204.94 o 0 8 0 21819.40 22450.48 737.42 o 1 8 0 38765.30 36950.84 1034.42 o 2 8 0 6488.08 6393.33 264.18 o 3 8 0 12786.33 12629.63 351.30 o 4 8 0 1274.72 1488.57 113.11 o 5 8 0 9420.99 9178.17 306.92 o 6 8 0 7716.33 7320.00 301.60 o 7 8 0 16058.83 14875.25 453.27 o 8 8 0 229.76 1860.44 213.56 o 9 8 0 3986.47 3722.96 320.64 o 10 8 0 370.74 811.84 213.09 o 11 8 0 1966.81 1452.28 283.65 o 12 8 0 1214.93 1723.46 335.48 o 13 8 0 587.49 804.88 258.60 o 1 9 0 14043.22 13492.44 447.55 o 2 9 0 5682.10 6011.32 273.29 o 3 9 0 10500.70 10360.43 365.28 o 4 9 0 12668.05 12738.57 430.86 o 5 9 0 219.65 289.03 91.11 o 6 9 0 1311.57 1601.24 177.07 o 7 9 0 7539.62 7757.94 363.18 o 8 9 0 6212.72 6324.75 418.11 o 9 9 0 1230.18 1117.78 204.56 o 10 9 0 9379.64 8944.12 716.14 o 11 9 0 357.53 346.86 191.23 o 12 9 0 1199.53 966.60 255.06 o 13 9 0 270.88 32.15 183.90 o 0 10 0 70134.14 65732.89 2313.28 o 1 10 0 11148.66 11278.53 439.24 o 2 10 0 22323.77 21526.10 684.88 o 3 10 0 17154.04 16572.09 576.26 o 4 10 0 16472.52 16862.99 536.08 o 5 10 0 1377.65 1564.04 168.03 o 6 10 0 5671.83 5484.28 322.43 o 7 10 0 2091.18 2336.28 240.70 o 8 10 0 2091.81 2418.01 295.20 o 9 10 0 1965.22 2711.67 317.48 o 10 10 0 12757.99 13145.12 794.56 o 11 10 0 1904.10 1750.40 316.40 o 12 10 0 860.54 1258.99 292.25 o 1 11 0 3677.22 3849.30 293.94 o 2 11 0 1313.62 1188.06 166.01 o 3 11 0 15140.72 14327.28 544.61 o 4 11 0 6002.96 5973.69 369.14 o 5 11 0 752.03 952.12 159.61 o 6 11 0 10902.83 10784.75 484.74 o 7 11 0 9978.21 9183.44 644.77 o 8 11 0 706.21 1223.09 253.88 o 9 11 0 389.53 312.39 143.69 o 10 11 0 593.87 628.00 210.23 o 11 11 0 5285.07 5240.71 573.81 o 0 12 0 1503.29 2380.22 344.05 o 1 12 0 1853.43 2134.06 225.20 o 2 12 0 5674.21 5483.78 371.37 o 3 12 0 1717.57 1744.82 207.94 o 4 12 0 28794.77 28309.28 899.40 o 5 12 0 7391.49 7513.80 524.08 o 6 12 0 18969.28 18293.69 772.52 o 7 12 0 2333.77 2147.15 329.01 o 8 12 0 290.29 463.75 179.15 o 9 12 0 1111.53 1152.08 252.69 o 10 12 0 345.21 94.13 165.26 o 1 13 0 177.21 257.75 88.30 o 2 13 0 675.79 1190.49 180.90 o 3 13 0 7401.43 6805.49 421.80 o 4 13 0 465.07 386.58 138.17 o 5 13 0 2778.59 2920.32 327.47 o 6 13 0 75.40 6.42 102.72 o 7 13 0 627.24 729.16 210.66 o 8 13 0 3118.65 2891.26 389.64 o 9 13 0 1364.87 1520.32 281.24 o 10 13 0 1340.87 2580.39 781.71 o 0 14 0 0.43 -11.17 105.60 o 1 14 0 7648.14 7084.45 435.42 o 2 14 0 3494.65 3138.09 296.92 o 3 14 0 5308.08 4571.65 416.18 o 4 14 0 6122.65 6183.15 495.42 o 5 14 0 1440.26 1391.11 235.92 o 6 14 0 5324.78 4978.66 507.51 o 7 14 0 3899.19 3690.46 446.09 o 8 14 0 176.07 200.50 144.21 o 1 15 0 2745.35 2898.26 383.70 o 2 15 0 264.50 726.03 167.04 o 3 15 0 10273.76 9462.33 637.85 o 4 15 0 806.20 579.17 160.22 o 5 15 0 448.15 312.19 129.94 o 6 15 0 679.93 708.46 191.08 o 7 15 0 2983.88 2976.39 404.57 o 0 16 0 9693.24 10114.89 1075.57 o 1 16 0 1122.60 825.11 201.89 o 2 16 0 1887.05 1846.45 267.24 o 3 16 0 1871.71 2301.70 303.26 o 4 16 0 1535.42 1517.40 243.10 o 5 16 0 1201.96 1497.11 252.57 o 1 17 0 2771.88 3166.88 423.04 o 1 0 1 952.28 970.75 38.69 o 2 0 1 4704.76 4828.26 110.08 o 3 0 1 47958.03 50380.51 913.84 o 4 0 1 1423.53 2113.37 106.73 o 5 0 1 84691.77 87798.12 1836.76 o 6 0 1 20674.25 22002.52 651.05 o 7 0 1 185.93 386.35 98.84 o 8 0 1 833.48 1410.87 181.51 o 9 0 1 32654.55 29634.02 914.26 o 10 0 1 162.61 545.86 138.71 o 11 0 1 7181.71 6971.42 477.51 o 12 0 1 2652.59 2840.88 313.45 o 13 0 1 2218.20 2301.28 300.19 o 14 0 1 2638.55 2238.63 296.41 o 15 0 1 2877.55 2985.22 347.82 o -15 1 1 368.52 482.49 162.41 o -14 1 1 37.91 101.32 125.57 o -13 1 1 51.89 135.41 113.08 o -12 1 1 10390.56 9357.57 583.11 o -11 1 1 2260.93 2343.96 276.40 o -10 1 1 15771.10 15555.19 617.51 o -9 1 1 1934.82 1952.82 230.23 o -8 1 1 38735.09 38284.05 1068.37 o -7 1 1 14045.81 14188.65 429.91 o -6 1 1 31396.56 31301.18 765.00 o -5 1 1 13881.44 13459.21 379.92 o -4 1 1 14263.61 14888.07 391.38 o -3 1 1 1458.23 1551.67 60.46 o -2 1 1 25789.20 28965.70 537.10 o -1 1 1 6106.59 5658.74 132.61 o 1 1 1 5983.29 5681.27 133.73 o 2 1 1 26548.44 29328.96 544.13 o 3 1 1 1317.62 1561.07 92.94 o 4 1 1 15476.83 15583.65 435.15 o 5 1 1 14440.13 14514.66 402.88 o 6 1 1 30349.36 30499.81 749.50 o 7 1 1 14308.15 14107.41 427.61 o 8 1 1 37415.86 36646.38 1036.98 o 9 1 1 1666.38 1816.93 221.80 o 10 1 1 15753.51 15501.62 613.58 o 11 1 1 2191.88 2337.66 273.83 o 12 1 1 10674.52 8925.03 568.81 o 13 1 1 31.70 75.24 114.14 o 14 1 1 51.07 73.60 118.85 o 15 1 1 451.41 396.26 166.04 o -15 2 1 531.43 457.54 190.15 o -14 2 1 1137.72 1360.09 249.53 o -13 2 1 737.70 802.72 187.17 o -12 2 1 3725.28 3370.89 345.50 o -11 2 1 1647.35 1970.53 254.41 o -10 2 1 8764.05 8287.71 504.01 o -9 2 1 7024.00 6589.94 418.94 o -8 2 1 2159.88 2149.41 155.54 o -7 2 1 7115.70 6930.58 277.82 o -6 2 1 2529.98 2868.04 177.56 o -5 2 1 10343.19 11104.56 339.85 o -4 2 1 19649.73 19721.62 450.47 o -3 2 1 69551.09 73181.17 1494.97 o -2 2 1 56715.17 58981.25 1196.79 o -1 2 1 6347.56 7141.17 167.89 o 0 2 1 1501.60 1221.05 55.40 o 1 2 1 7022.65 7695.02 166.20 o 2 2 1 58858.72 60145.48 1145.68 o 3 2 1 66756.05 69841.80 1271.64 o 4 2 1 20108.33 20621.98 466.86 o 5 2 1 9881.40 10666.76 329.70 o 6 2 1 2298.35 2718.37 170.41 o 7 2 1 7079.54 7129.63 286.87 o 8 2 1 1983.11 1942.38 150.40 o 9 2 1 7024.46 6864.70 425.96 o 10 2 1 8510.78 8540.21 470.92 o 11 2 1 1500.54 2088.45 257.10 o 12 2 1 3910.21 3573.83 354.76 o 13 2 1 775.20 905.25 200.55 o 14 2 1 1187.27 1180.50 212.59 o 15 2 1 574.18 599.38 186.69 o -15 3 1 2105.89 2045.82 316.13 o -14 3 1 3052.02 3517.69 373.02 o -13 3 1 2988.97 3038.97 364.58 o -12 3 1 3262.46 2886.70 347.73 o -11 3 1 5061.49 4711.52 422.26 o -10 3 1 94.90 244.66 115.42 o -9 3 1 14044.74 14008.44 606.82 o -8 3 1 7704.24 7677.81 344.34 o -7 3 1 26698.85 26664.45 758.56 o -6 3 1 43959.66 43981.34 1001.02 o -5 3 1 15076.41 14726.27 399.83 o 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842.91 o -4 4 1 156.83 223.67 49.37 o -3 4 1 16226.31 15870.42 401.50 o -2 4 1 1322.46 1725.68 88.15 o -1 4 1 7584.83 7317.68 234.06 o 0 4 1 139.88 335.65 29.05 o 1 4 1 6962.18 6502.94 177.95 o 2 4 1 1194.69 1625.36 88.72 o 3 4 1 15912.88 15443.19 370.95 o 4 4 1 223.00 253.10 52.47 o 5 4 1 37486.52 39285.46 847.16 o 6 4 1 11974.29 12103.15 347.92 o 7 4 1 9312.08 10234.24 314.55 o 8 4 1 4971.53 5134.90 287.23 o 9 4 1 23119.95 23332.41 775.92 o 10 4 1 507.67 451.84 124.65 o 11 4 1 4683.48 5104.46 397.97 o 12 4 1 1650.16 2048.76 255.78 o 13 4 1 2444.11 2673.82 304.17 o 14 4 1 769.84 714.82 173.23 o 15 4 1 963.42 1263.82 585.49 o -14 5 1 450.25 506.22 193.16 o -13 5 1 2015.86 2139.15 304.37 o -12 5 1 10924.78 10545.26 576.45 o -11 5 1 8138.92 8072.52 495.25 o -10 5 1 11101.01 10004.13 511.44 o -9 5 1 19642.42 19096.44 644.84 o -8 5 1 11232.56 11029.60 411.37 o -7 5 1 13537.41 13707.41 407.95 o -6 5 1 21113.64 20669.04 530.70 o -5 5 1 13272.22 13520.04 376.35 o -4 5 1 10198.38 10651.47 304.21 o -3 5 1 15702.55 16835.44 405.94 o -2 5 1 48528.24 48619.79 972.81 o -1 5 1 1986.54 2388.48 138.22 o 0 5 1 24904.37 24881.43 528.08 o 1 5 1 1800.86 2114.18 98.34 o 2 5 1 49167.16 47730.14 961.97 o 3 5 1 16243.01 17147.11 412.88 o 4 5 1 10349.20 10849.18 306.70 o 5 5 1 13813.74 13711.79 377.31 o 6 5 1 22047.16 21278.18 538.50 o 7 5 1 12918.59 12834.16 383.76 o 8 5 1 10872.21 10553.73 396.35 o 9 5 1 19904.16 18818.04 672.32 o 10 5 1 11691.26 11249.10 502.16 o 11 5 1 8356.20 8855.00 528.71 o 12 5 1 11072.98 11468.43 591.90 o 13 5 1 1997.35 2216.66 277.12 o 14 5 1 457.25 517.42 160.66 o -14 6 1 1070.15 1350.81 241.89 o -13 6 1 4416.34 4223.49 426.45 o -12 6 1 0.73 -4.26 104.68 o -11 6 1 3584.07 3714.85 339.78 o -10 6 1 1579.33 1641.20 215.24 o -9 6 1 5551.11 5966.90 338.60 o -8 6 1 2420.60 2563.50 221.62 o -7 6 1 4589.73 4673.24 243.62 o -6 6 1 829.58 1416.12 132.39 o -5 6 1 42025.30 41006.04 901.09 o -4 6 1 14990.55 14458.88 384.74 o -3 6 1 11750.68 11253.29 306.18 o -2 6 1 14640.28 15057.24 366.18 o -1 6 1 64614.79 63143.39 1458.05 o 0 6 1 1201.29 1453.01 94.62 o 1 6 1 63834.44 62410.25 1231.34 o 2 6 1 13591.42 13904.97 349.96 o 3 6 1 11833.41 11678.33 317.19 o 4 6 1 14289.52 14210.48 380.73 o 5 6 1 42790.64 42389.77 924.89 o 6 6 1 691.31 1377.57 129.34 o 7 6 1 4399.15 4402.87 231.56 o 8 6 1 2478.04 2470.40 211.55 o 9 6 1 5121.94 5598.78 327.00 o 10 6 1 1519.25 1523.08 211.23 o 11 6 1 3661.51 3650.61 335.31 o 12 6 1 2.43 21.99 98.29 o 13 6 1 4409.81 4529.71 436.86 o 14 6 1 1197.13 929.03 216.12 o -14 7 1 771.72 977.86 279.95 o -13 7 1 3091.11 2633.70 397.73 o -12 7 1 2752.79 2645.75 390.32 o -11 7 1 1511.34 1487.76 240.87 o -10 7 1 1457.03 1850.64 220.90 o -9 7 1 9500.94 9441.83 413.05 o -8 7 1 12974.05 11997.06 466.34 o -7 7 1 21159.59 19988.49 548.80 o -6 7 1 17160.61 17922.80 493.96 o -5 7 1 17901.38 17474.81 467.51 o -4 7 1 11719.08 12099.12 346.02 o -3 7 1 11511.81 10560.66 300.42 o -2 7 1 3236.36 3218.57 176.46 o -1 7 1 5312.53 5840.41 269.27 o 0 7 1 48470.75 49665.79 1102.50 o 1 7 1 5270.32 6338.20 200.93 o 2 7 1 3953.75 3871.69 161.64 o 3 7 1 10975.93 10471.88 302.69 o 4 7 1 11185.70 11245.45 331.15 o 5 7 1 18088.39 18187.55 481.83 o 6 7 1 17283.95 17686.23 488.18 o 7 7 1 21467.17 20673.32 560.60 o 8 7 1 12479.28 12258.63 444.43 o 9 7 1 9895.40 9450.07 412.84 o 10 7 1 1557.79 2019.18 228.84 o 11 7 1 1494.55 1604.20 215.40 o 12 7 1 2779.05 2768.44 320.34 o 13 7 1 3075.83 2846.77 409.23 o 14 7 1 720.24 765.67 231.36 o -13 8 1 359.15 480.09 219.46 o -12 8 1 2245.13 2489.12 388.33 o -11 8 1 862.32 1026.70 258.33 o -10 8 1 670.62 767.70 212.26 o -9 8 1 200.89 149.55 90.99 o -8 8 1 2825.06 3000.91 275.61 o -7 8 1 4829.32 5051.90 299.93 o -6 8 1 2523.68 3003.18 191.58 o -5 8 1 3514.98 3578.15 196.28 o -4 8 1 10875.17 11104.87 331.67 o -3 8 1 13976.39 13573.71 368.01 o -2 8 1 5937.78 6014.55 243.30 o -1 8 1 4573.19 4145.15 222.71 o 0 8 1 3588.19 3617.97 186.51 o 1 8 1 4668.22 4295.87 210.62 o 2 8 1 6473.07 6339.83 213.81 o 3 8 1 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