#------------------------------------------------------------------------------ #$Date: 2015-05-30 05:48:58 +0300 (Sat, 30 May 2015) $ #$Revision: 137551 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/07/2240790.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2240790 loop_ _publ_author_name 'Akhazzane, Mohamed' 'Al Houari, Ghali' 'El Yazidi, Mohamed' 'Saadi, Mohamed' 'El Ammari, Lahcen' _publ_section_title ; Crystal structure of (E)-4-ethyl-2-(4-methoxybenzylidene)-3,4-dihydronaphthalen-1(2H)-one ; _journal_coeditor_code HB7434 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o432 _journal_paper_doi 10.1107/S205698901501004X _journal_volume 71 _journal_year 2015 _chemical_formula_iupac 'C20 H20 O2' _chemical_formula_moiety 'C20 H20 O2' _chemical_formula_sum 'C20 H20 O2' _chemical_formula_weight 292.36 _chemical_melting_point 383 _chemical_name_systematic ; (E)-4-Ethyl-2-(4-methoxybenzylidene)-3,4-dihydronaphthalen-1(2H)-\ one ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 110.721(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.0411(13) _cell_length_b 8.9698(9) _cell_length_c 15.5832(18) _cell_measurement_reflns_used 4068 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 28.697 _cell_measurement_theta_min 2.666 _cell_volume 1574.2(3) _computing_cell_refinement ; SAINT (Bruker, 2009) ; _computing_data_collection ; APEX2 (Bruker, 2009) ; _computing_data_reduction ; SAINT (Bruker, 2009) ; _computing_molecular_graphics ; ORTEPIII (Burnett & Johnson, 1996) and ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; PLATON (Spek, 2009) and publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2013 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS2013 (Sheldrick, 2008) ; _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker X8 APEX CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0459 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 25378 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.697 _diffrn_reflns_theta_min 2.666 _exptl_absorpt_coefficient_mu 0.078 _exptl_absorpt_correction_type none _exptl_crystal_colour Colourless _exptl_crystal_density_diffrn 1.234 _exptl_crystal_description needles _exptl_crystal_F_000 624 _exptl_crystal_size_max 0.38 _exptl_crystal_size_mid 0.16 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.160 _refine_diff_density_min -0.150 _refine_ls_extinction_coef 0.0088(16) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL2013 (Sheldrick, 2015) ; _refine_ls_goodness_of_fit_ref 1.008 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 200 _refine_ls_number_reflns 4068 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.008 _refine_ls_R_factor_all 0.0843 _refine_ls_R_factor_gt 0.0462 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0546P)^2^+0.2497P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1090 _refine_ls_wR_factor_ref 0.1292 _reflns_number_gt 2552 _reflns_number_total 4068 _reflns_threshold_expression I>2\s(I) _cod_data_source_file hb7434sup1.cif _cod_data_source_block I _cod_database_code 2240790 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; 1 0 0 -3.30 0.10 1 0 0 -3.30 0.10 1 0 0 -3.50 0.10 1 0 0 -3.40 0.10 -1 0 0 -3.20 0.10 -1 0 0 -3.40 0.10 -1 0 0 -3.50 0.10 -1 0 0 -3.40 0.10 2 0 0 2236.78 73.39 -2 0 0 2361.96 73.79 -2 0 0 2336.87 73.89 -2 0 0 2222.78 73.29 2 0 0 2228.58 73.79 2 0 0 2163.08 73.29 2 0 0 2185.88 73.89 3 0 0 1140.79 38.30 3 0 0 1128.59 38.40 -3 0 0 1183.68 38.50 3 0 0 1176.98 38.30 -3 0 0 1141.29 38.30 3 0 0 1197.18 38.30 -3 0 0 1236.48 38.30 -4 0 0 177.88 6.30 4 0 0 168.58 6.30 4 0 0 168.08 6.30 4 0 0 168.78 6.40 4 0 0 181.48 6.30 5 0 0 624.94 21.50 5 0 0 640.64 21.50 5 0 0 646.54 21.70 5 0 0 643.94 21.50 6 0 0 412.66 13.80 6 0 0 388.86 13.70 6 0 0 363.66 13.90 6 0 0 403.06 13.80 7 0 0 1.40 0.90 7 0 0 1.90 1.10 -7 0 0 1.00 0.60 7 0 0 0.60 1.20 7 0 0 4.80 1.40 8 0 0 79.89 4.10 8 0 0 78.39 4.40 -8 0 0 79.49 3.70 8 0 0 85.79 4.10 8 0 0 77.69 4.00 9 0 0 5.20 1.60 9 0 0 5.80 1.70 9 0 0 6.20 1.50 -9 0 0 5.70 1.30 9 0 0 5.30 1.90 9 0 0 5.90 1.00 10 0 0 0.60 0.80 10 0 0 0.20 1.40 10 0 0 -1.00 1.60 10 0 0 -1.20 1.40 11 0 0 1.80 1.90 11 0 0 1.20 1.80 11 0 0 2.20 1.50 12 0 0 -0.90 2.00 12 0 0 2.90 1.70 12 0 0 0.50 1.50 13 0 0 28.80 3.50 13 0 0 28.50 3.40 13 0 0 29.70 4.10 14 0 0 10.30 2.60 14 0 0 7.90 2.30 14 0 0 4.00 2.90 15 0 0 9.80 2.70 15 0 0 8.30 2.70 15 0 0 12.50 3.70 16 0 0 1.00 2.50 16 0 0 2.10 3.40 16 0 0 1.30 2.20 0 -1 0 -3.10 0.10 0 -1 0 -3.00 0.10 0 -1 0 -3.30 0.10 0 1 0 -2.70 0.20 -1 -1 0 147.29 4.70 -1 -1 0 126.89 4.70 -1 -1 0 117.99 4.70 -1 -1 0 138.89 4.60 1 1 0 139.19 4.60 1 1 0 163.98 4.70 1 1 0 121.49 4.70 -2 -1 0 543.95 18.00 2 -1 0 521.55 17.70 2 -1 0 529.25 17.70 2 -1 0 521.75 17.90 -2 -1 0 525.15 17.90 -2 -1 0 563.34 17.90 -2 -1 0 573.04 17.80 2 -1 0 564.24 17.80 2 -1 0 517.45 17.80 -2 -1 0 543.55 17.90 -2 1 0 561.54 17.90 2 1 0 538.95 17.90 2 1 0 529.15 17.90 2 1 0 543.85 18.00 -2 1 0 543.45 17.60 2 1 0 533.35 17.90 -2 1 0 549.54 17.60 2 1 0 532.95 17.80 2 1 0 541.65 17.90 -3 -1 0 76.29 3.20 -3 -1 0 76.19 3.10 -3 -1 0 81.99 3.20 3 -1 0 74.99 3.00 -3 -1 0 71.59 3.10 3 -1 0 71.99 2.80 3 -1 0 71.49 2.90 3 -1 0 74.59 3.20 -3 1 0 76.69 2.80 3 1 0 75.99 3.10 -3 1 0 82.69 3.00 3 1 0 72.79 3.10 3 1 0 77.39 3.20 -3 1 0 75.79 3.10 -3 1 0 74.49 2.80 3 1 0 74.39 2.90 3 1 0 75.59 3.10 -4 -1 0 235.68 8.50 4 -1 0 241.98 8.30 4 -1 0 232.48 8.20 -4 -1 0 254.77 8.50 4 -1 0 230.68 8.60 4 -1 0 247.28 8.40 -4 -1 0 240.68 8.50 4 1 0 228.78 8.60 4 1 0 232.58 8.50 4 1 0 243.08 8.50 4 1 0 234.48 8.10 -4 1 0 239.48 8.30 4 1 0 236.78 8.50 -4 1 0 232.38 8.10 5 -1 0 875.51 28.10 5 -1 0 815.82 28.20 5 -1 0 840.72 28.10 -5 -1 0 834.42 28.30 5 -1 0 830.82 28.40 5 1 0 845.52 28.50 5 1 0 852.11 27.90 5 1 0 839.02 28.40 5 1 0 840.62 28.30 -5 1 0 868.31 28.00 5 1 0 892.61 28.40 6 -1 0 1.50 0.90 6 -1 0 2.40 0.80 6 -1 0 2.10 0.80 6 -1 0 1.70 1.10 -6 -1 0 1.20 0.90 6 1 0 1.80 0.70 6 1 0 1.80 1.20 6 1 0 1.30 1.00 6 1 0 2.30 1.00 6 1 0 1.10 0.90 -6 1 0 3.40 0.80 7 -1 0 85.49 4.10 7 -1 0 100.89 4.10 7 -1 0 84.39 4.00 7 -1 0 78.09 4.30 -7 -1 0 93.19 4.10 7 1 0 93.19 4.30 7 1 0 90.39 4.20 7 1 0 89.99 3.60 7 1 0 85.49 4.40 7 1 0 90.29 4.20 -7 1 0 87.99 3.70 8 -1 0 13.30 1.70 8 -1 0 15.60 1.70 -8 -1 0 13.30 1.70 8 -1 0 14.90 2.10 8 -1 0 14.00 2.20 -8 1 0 16.30 1.60 8 1 0 11.00 1.80 8 1 0 16.10 1.40 8 1 0 18.50 2.10 8 1 0 15.90 2.30 8 1 0 13.90 2.00 9 -1 0 0.00 1.00 9 -1 0 -0.50 1.50 9 -1 0 -0.70 1.40 -9 -1 0 -1.70 0.90 9 -1 0 -0.70 1.10 9 1 0 -1.20 1.30 9 1 0 0.30 0.80 -9 1 0 -0.80 0.80 9 1 0 -0.10 1.40 9 1 0 -0.20 1.30 9 1 0 -0.80 1.20 10 -1 0 4.20 1.60 10 -1 0 2.00 1.70 10 -1 0 6.00 1.80 10 1 0 5.70 1.70 10 1 0 6.20 1.90 10 1 0 5.00 1.00 10 1 0 2.80 1.60 11 -1 0 0.40 1.80 11 -1 0 0.30 1.30 11 -1 0 2.20 1.60 11 1 0 0.60 1.50 11 1 0 -0.80 1.80 11 1 0 2.00 1.70 12 -1 0 2.50 1.50 12 -1 0 1.80 2.00 12 -1 0 6.20 2.40 12 1 0 3.40 2.30 12 1 0 -1.30 1.40 12 1 0 1.70 1.90 13 -1 0 2.50 1.90 13 -1 0 3.70 2.10 13 -1 0 8.00 2.70 13 1 0 3.60 2.00 13 1 0 5.20 2.10 13 1 0 9.70 2.90 14 -1 0 1.20 1.80 14 -1 0 0.70 1.80 14 -1 0 1.60 2.80 14 -1 0 -0.20 1.90 14 1 0 2.70 2.20 14 1 0 -0.10 1.80 14 1 0 0.60 2.50 15 -1 0 -0.60 3.00 15 -1 0 9.70 2.60 15 -1 0 4.20 2.50 15 1 0 3.80 2.40 15 1 0 5.30 2.70 15 1 0 6.40 3.20 16 -1 0 0.20 2.10 16 -1 0 5.20 3.50 16 1 0 1.90 2.50 16 1 0 0.60 3.10 16 1 0 -1.10 2.10 0 -2 0 2081.79 66.79 0 -2 0 2015.50 66.99 0 -2 0 1944.71 66.89 0 -2 0 2175.48 66.69 0 2 0 2042.40 66.69 -1 -2 0 0.80 0.70 -1 -2 0 2.00 0.80 -1 -2 0 0.80 0.40 -1 -2 0 0.30 0.60 1 -2 0 0.90 0.70 -1 -2 0 0.10 0.60 -1 2 0 0.60 0.20 1 2 0 0.00 0.30 1 2 0 1.30 0.50 1 2 0 0.60 0.40 1 2 0 0.80 0.70 -1 2 0 0.20 0.70 1 2 0 -0.10 0.70 -2 -2 0 167.08 6.00 -2 -2 0 168.88 6.20 -2 -2 0 179.18 6.30 -2 -2 0 178.88 6.20 -2 -2 0 171.48 6.20 2 -2 0 176.78 6.20 -2 -2 0 171.78 6.20 2 2 0 178.78 6.00 2 2 0 176.28 6.20 2 2 0 167.08 6.10 2 2 0 168.98 6.10 -2 2 0 164.38 6.10 2 2 0 163.68 6.10 -3 -2 0 111.29 4.00 3 -2 0 110.89 3.60 3 -2 0 111.49 4.00 -3 -2 0 98.59 4.10 -3 -2 0 96.19 4.10 -3 -2 0 111.99 4.40 3 -2 0 96.99 3.60 3 -2 0 96.79 4.10 3 -2 0 102.09 4.00 3 2 0 103.89 4.00 3 2 0 102.59 4.00 3 2 0 109.69 4.20 3 2 0 103.09 4.20 3 2 0 95.49 4.10 3 2 0 100.69 4.10 4 -2 0 389.76 13.30 4 -2 0 381.56 13.70 4 -2 0 391.86 13.90 4 -2 0 418.76 13.60 -4 -2 0 418.46 13.60 -4 -2 0 400.36 13.80 -4 -2 0 383.46 13.80 4 -2 0 407.16 13.30 -4 2 0 399.66 13.00 4 2 0 427.86 13.80 4 2 0 384.36 13.80 4 2 0 402.96 13.60 4 2 0 393.76 13.80 4 2 0 403.26 13.90 4 2 0 390.76 13.80 5 -2 0 0.10 0.50 5 -2 0 0.60 0.90 5 -2 0 1.20 0.90 -5 -2 0 0.10 0.80 5 -2 0 0.30 0.50 5 -2 0 -0.10 0.60 5 2 0 0.80 0.80 5 2 0 -0.90 1.00 5 2 0 0.20 1.00 -5 2 0 0.30 0.40 5 2 0 0.30 0.70 5 2 0 0.60 0.80 6 -2 0 42.10 2.50 6 -2 0 40.00 2.70 -6 -2 0 41.70 2.60 6 -2 0 41.30 2.20 6 -2 0 40.00 2.20 6 2 0 40.20 2.70 6 2 0 45.90 2.70 6 2 0 42.20 2.20 6 2 0 46.20 2.70 6 2 0 43.90 2.90 -7 -2 0 1.50 1.10 7 -2 0 0.20 1.00 7 -2 0 0.30 1.20 7 -2 0 -0.20 0.80 7 -2 0 0.20 0.80 7 2 0 -0.20 0.70 7 2 0 0.40 1.10 7 2 0 0.50 1.20 7 2 0 0.10 1.30 8 -2 0 -2.10 1.30 8 -2 0 0.00 0.90 8 -2 0 1.00 1.30 -8 -2 0 1.40 1.10 8 -2 0 0.10 1.00 8 2 0 2.40 1.50 8 2 0 1.30 1.30 8 2 0 -0.30 0.80 8 2 0 0.30 1.60 -9 -2 0 9.30 1.70 9 -2 0 8.30 2.00 9 -2 0 6.90 1.60 9 -2 0 8.80 2.10 9 -2 0 8.60 1.50 9 2 0 7.50 1.90 9 2 0 5.90 1.80 9 2 0 8.70 1.30 9 2 0 7.50 2.20 10 -2 0 7.50 2.00 10 -2 0 3.00 1.30 10 -2 0 4.60 1.70 10 2 0 2.50 1.70 10 2 0 5.40 2.10 10 2 0 4.10 1.00 10 2 0 3.00 1.70 11 -2 0 -0.50 1.20 11 -2 0 4.20 1.90 11 -2 0 -0.50 1.70 11 2 0 0.30 1.60 11 2 0 0.60 1.60 11 2 0 3.70 1.90 12 -2 0 16.60 2.80 12 -2 0 14.60 3.10 12 -2 0 9.80 2.10 12 2 0 13.10 2.50 12 2 0 16.50 2.70 12 2 0 9.40 2.70 13 -2 0 15.30 2.80 13 -2 0 17.30 2.70 13 -2 0 12.30 2.50 13 -2 0 13.70 3.20 13 2 0 20.00 3.00 13 2 0 17.20 3.40 13 2 0 12.50 2.70 14 -2 0 -0.10 2.60 14 -2 0 -1.70 1.70 14 -2 0 1.70 1.90 14 2 0 0.00 1.80 14 2 0 -1.30 1.80 14 2 0 2.60 2.70 15 -2 0 -6.10 2.40 15 -2 0 -1.90 1.60 15 2 0 -2.70 1.90 15 2 0 -3.10 2.80 15 2 0 -3.40 2.00 16 -2 0 1.20 2.10 16 -2 0 -2.70 3.00 16 2 0 3.10 3.20 16 2 0 -0.30 2.40 16 2 0 -0.80 3.10 0 -3 0 -0.20 0.40 0 -3 0 0.20 0.40 0 -3 0 0.50 0.50 0 3 0 0.70 0.80 -1 -3 0 706.63 23.40 -1 -3 0 735.13 23.60 -1 -3 0 686.63 23.40 1 -3 0 676.43 23.00 -1 -3 0 702.13 23.20 1 3 0 694.03 23.70 -1 3 0 720.33 23.70 1 3 0 726.43 23.40 -1 3 0 725.43 23.10 1 3 0 715.53 23.20 -2 -3 0 125.39 4.70 -2 -3 0 118.29 4.30 -2 -3 0 114.49 4.60 2 3 0 119.09 4.70 -2 3 0 121.89 4.70 2 3 0 119.59 4.30 2 3 0 121.69 4.70 3 -3 0 281.37 9.20 -3 -3 0 272.47 10.00 -3 -3 0 276.17 9.70 3 -3 0 278.97 9.20 3 -3 0 277.97 9.20 -3 -3 0 283.77 10.00 3 3 0 286.07 10.00 3 3 0 286.67 10.00 3 3 0 293.17 9.70 3 3 0 287.17 10.10 -3 3 0 287.07 10.00 -4 -3 0 244.98 8.90 4 -3 0 232.38 8.10 -4 -3 0 242.28 8.80 4 -3 0 244.48 8.80 4 -3 0 238.28 8.90 4 -3 0 242.68 8.10 4 3 0 237.98 8.70 4 3 0 247.68 8.60 4 3 0 239.28 8.90 4 3 0 244.58 8.80 -5 -3 0 2.80 1.10 -5 -3 0 3.90 1.10 5 -3 0 4.40 0.70 5 -3 0 3.60 1.10 5 -3 0 3.30 1.10 5 -3 0 4.10 0.70 5 3 0 3.70 0.90 5 3 0 3.10 1.30 5 3 0 6.40 1.20 5 3 0 3.90 1.40 -6 -3 0 7.20 1.40 6 -3 0 6.00 1.50 6 -3 0 6.90 0.90 6 -3 0 7.40 1.40 6 -3 0 6.90 0.90 6 3 0 10.00 1.50 6 3 0 11.00 1.80 6 3 0 5.40 1.10 6 3 0 6.00 1.50 -7 -3 0 87.19 4.30 7 -3 0 73.69 3.60 7 -3 0 86.79 4.10 7 -3 0 83.79 3.70 7 -3 0 85.69 4.50 7 3 0 78.49 4.50 7 3 0 91.59 4.50 7 3 0 83.69 3.80 7 3 0 82.19 4.30 8 -3 0 18.90 2.50 8 -3 0 18.10 2.20 8 -3 0 18.60 1.80 8 -3 0 13.00 1.60 -8 -3 0 16.40 2.20 8 3 0 17.30 2.60 8 3 0 19.70 1.90 8 3 0 17.80 2.30 8 3 0 14.60 2.30 -9 -3 0 1.40 1.30 9 -3 0 4.60 1.60 9 -3 0 0.60 1.00 9 -3 0 1.90 1.10 9 -3 0 1.70 1.70 9 3 0 -0.90 1.80 9 3 0 0.40 1.60 9 3 0 1.70 1.10 9 3 0 3.50 1.60 10 -3 0 2.30 1.60 -10 -3 0 5.30 1.60 10 -3 0 0.80 1.80 10 -3 0 3.30 1.30 10 3 0 1.30 1.50 10 3 0 3.50 1.20 10 3 0 2.20 1.90 10 3 0 1.90 2.10 11 -3 0 -2.10 0.90 11 -3 0 3.10 2.00 11 -3 0 1.10 2.00 11 3 0 0.20 1.90 11 3 0 -0.50 1.40 11 3 0 -1.50 2.00 12 -3 0 1.10 2.00 12 -3 0 1.50 2.30 12 -3 0 -0.10 1.40 12 -3 0 0.00 1.40 12 3 0 -1.80 2.10 12 3 0 1.80 1.70 12 3 0 0.70 1.80 13 -3 0 16.50 3.00 13 -3 0 16.90 2.70 13 -3 0 22.50 4.00 13 3 0 27.80 3.60 13 3 0 21.90 3.80 13 3 0 27.40 3.60 14 -3 0 13.70 3.50 14 -3 0 13.30 2.60 14 3 0 10.90 3.40 14 3 0 19.90 3.20 14 3 0 13.30 3.00 15 -3 0 2.80 3.20 15 -3 0 -1.40 1.70 15 3 0 -5.20 2.10 15 3 0 4.70 3.20 0 -4 0 2.10 0.60 0 -4 0 1.90 0.50 0 -4 0 1.40 0.60 0 4 0 2.60 0.90 0 4 0 2.60 0.60 1 -4 0 105.49 3.90 -1 -4 0 104.49 4.20 -1 -4 0 115.09 4.30 -1 -4 0 109.89 4.10 -1 4 0 117.59 4.00 1 4 0 105.19 4.60 -1 4 0 117.89 4.70 -2 -4 0 30.60 1.90 2 -4 0 27.80 1.10 -2 -4 0 28.40 1.90 -2 -4 0 27.90 1.50 -2 4 0 26.80 2.00 2 4 0 26.30 1.90 2 4 0 24.70 2.00 2 4 0 31.60 1.50 2 4 0 26.60 1.60 -3 -4 0 174.98 6.50 -3 -4 0 165.38 6.00 -3 -4 0 169.98 6.40 3 4 0 154.78 6.50 3 4 0 164.38 6.50 -3 4 0 162.08 6.50 3 4 0 171.18 6.00 4 -4 0 35.60 1.40 -4 -4 0 33.30 2.30 4 -4 0 37.80 2.40 -4 -4 0 37.30 2.40 4 -4 0 35.20 1.40 4 4 0 37.70 2.30 4 4 0 38.10 2.50 -4 4 0 37.50 2.40 4 4 0 37.40 2.00 4 4 0 39.00 2.50 5 -4 0 5.70 1.40 5 -4 0 6.10 1.40 -5 -4 0 5.60 1.30 5 -4 0 7.70 0.60 -5 -4 0 8.10 1.40 5 -4 0 6.20 0.70 5 -4 0 7.00 0.70 5 -4 0 7.80 0.60 5 4 0 10.40 1.80 5 4 0 7.60 1.30 5 4 0 5.90 1.20 6 -4 0 71.89 3.00 -6 -4 0 74.09 3.90 6 -4 0 71.59 3.80 6 -4 0 71.19 3.00 6 -4 0 70.79 3.90 6 4 0 72.69 3.80 6 4 0 71.59 4.10 6 4 0 74.09 3.70 -7 -4 0 43.10 3.20 7 -4 0 49.60 2.50 7 -4 0 59.29 3.50 7 -4 0 48.20 3.50 7 -4 0 49.70 2.60 7 4 0 58.09 3.40 7 4 0 51.49 3.70 7 4 0 51.59 3.10 8 -4 0 54.49 3.50 8 -4 0 46.20 3.60 8 -4 0 46.50 2.70 8 -4 0 47.40 2.70 -8 -4 0 54.99 3.60 8 4 0 50.89 3.10 8 4 0 54.19 3.60 8 4 0 46.50 4.00 9 -4 0 7.10 1.30 9 -4 0 6.30 2.00 9 -4 0 4.40 2.00 9 -4 0 8.40 1.40 9 -4 0 8.70 1.40 -9 -4 0 8.50 1.90 9 4 0 7.10 1.50 9 4 0 9.50 2.30 9 4 0 8.60 1.90 10 -4 0 -0.50 1.00 10 -4 0 -1.10 0.90 -10 -4 0 -1.70 1.40 10 -4 0 -1.90 1.60 10 -4 0 -0.20 1.70 10 4 0 -2.50 1.70 10 4 0 0.00 1.60 10 4 0 -1.60 1.00 11 -4 0 0.20 2.00 11 -4 0 -0.40 1.90 11 -4 0 0.10 1.20 11 4 0 -2.00 1.90 11 4 0 -1.40 1.30 12 -4 0 6.30 1.70 12 -4 0 10.40 2.50 12 -4 0 6.20 2.50 12 4 0 6.90 2.20 12 4 0 10.30 2.90 13 -4 0 2.30 2.70 13 -4 0 1.30 1.50 13 -4 0 8.90 3.10 13 4 0 3.20 2.70 14 -4 0 4.70 3.10 14 -4 0 4.10 1.90 14 4 0 13.00 3.50 15 -4 0 2.20 1.80 15 -4 0 -0.70 3.10 15 4 0 4.60 3.10 15 4 0 0.10 2.70 0 -5 0 -0.20 0.60 0 -5 0 -0.10 0.50 0 -5 0 -0.40 0.50 0 5 0 -0.10 0.60 0 5 0 -0.30 1.00 -1 -5 0 41.80 2.20 1 -5 0 41.40 1.90 1 -5 0 41.80 2.20 -1 -5 0 39.00 1.90 1 -5 0 41.00 1.90 -1 -5 0 37.50 2.20 1 5 0 33.50 2.50 -1 5 0 35.20 2.60 -1 5 0 40.10 1.80 2 -5 0 4.30 0.50 -2 -5 0 2.60 1.00 -2 -5 0 1.90 0.90 -2 -5 0 3.50 0.70 2 5 0 2.80 1.20 -2 5 0 2.30 1.20 -2 5 0 4.50 0.40 2 5 0 5.20 0.70 -3 -5 0 81.99 3.40 -3 -5 0 83.69 3.90 -3 -5 0 88.59 4.00 3 -5 0 78.69 2.80 3 5 0 92.69 3.80 3 5 0 82.29 4.10 -3 5 0 78.69 4.10 3 5 0 77.69 4.00 3 5 0 87.69 3.30 -4 -5 0 28.40 2.40 -4 -5 0 30.60 2.50 4 -5 0 24.40 1.00 4 5 0 28.80 1.70 4 5 0 25.30 2.50 -4 5 0 25.90 2.40 4 5 0 26.90 2.40 5 -5 0 5.50 0.60 5 -5 0 6.10 0.60 -5 -5 0 5.30 1.50 5 -5 0 5.70 1.60 -5 -5 0 8.80 1.50 5 5 0 6.80 1.60 5 5 0 6.30 1.30 5 5 0 8.10 1.70 6 -5 0 36.10 1.80 6 -5 0 39.50 3.00 6 -5 0 39.80 2.90 -6 -5 0 40.50 3.10 6 -5 0 36.10 1.80 6 5 0 39.00 2.70 6 5 0 35.30 2.70 6 5 0 38.20 3.30 7 -5 0 50.49 3.60 7 -5 0 57.39 3.60 7 -5 0 48.90 2.50 -7 -5 0 55.19 3.70 7 -5 0 49.20 2.00 7 -5 0 53.89 2.50 7 5 0 50.19 3.80 7 5 0 50.69 3.20 7 5 0 53.69 3.70 8 -5 0 34.60 2.20 -8 -5 0 30.40 3.00 8 -5 0 40.10 3.50 8 -5 0 35.60 2.20 8 -5 0 32.70 3.40 8 5 0 36.20 2.80 8 5 0 37.30 3.60 8 5 0 37.10 3.30 9 -5 0 13.20 1.60 9 -5 0 19.00 1.80 9 -5 0 16.40 2.60 9 -5 0 17.20 2.70 -9 -5 0 18.60 2.60 9 5 0 19.10 2.20 9 5 0 19.40 2.60 9 5 0 16.50 2.80 -10 -5 0 29.30 3.20 10 -5 0 32.70 3.50 10 -5 0 26.50 2.40 10 -5 0 27.50 3.50 10 5 0 30.10 2.80 10 5 0 31.10 3.70 11 -5 0 6.50 1.60 11 -5 0 6.80 2.20 11 -5 0 7.20 2.70 11 5 0 8.60 2.60 12 -5 0 -1.70 1.90 12 -5 0 0.80 1.30 12 -5 0 -0.30 2.20 12 5 0 -0.10 2.20 13 -5 0 0.60 1.50 13 -5 0 -0.20 2.50 13 5 0 0.80 2.60 14 -5 0 -3.10 2.50 14 -5 0 -1.10 1.40 14 5 0 0.30 2.60 14 5 0 4.60 3.00 15 -5 0 1.40 1.70 15 -5 0 -1.10 3.10 15 5 0 0.40 2.70 15 5 0 -7.30 2.30 0 -6 0 112.49 4.60 0 -6 0 114.39 4.50 0 -6 0 122.09 4.60 0 6 0 111.99 4.50 0 6 0 104.49 5.30 -1 -6 0 5.10 1.10 -1 -6 0 5.30 0.90 1 -6 0 5.90 0.90 -1 -6 0 4.50 1.10 1 -6 0 4.40 0.90 1 -6 0 6.10 1.10 -1 6 0 3.70 1.50 1 6 0 5.70 1.60 -1 6 0 6.90 0.90 1 6 0 7.40 1.30 -2 -6 0 50.99 2.80 -2 -6 0 48.70 2.90 -2 -6 0 48.20 2.30 2 -6 0 46.40 2.10 2 -6 0 47.20 2.10 2 -6 0 46.60 2.80 2 6 0 48.10 3.30 -2 6 0 47.10 3.20 -2 6 0 49.90 1.90 -3 -6 0 46.70 2.90 3 -6 0 47.90 2.00 -3 -6 0 49.20 2.40 -3 -6 0 51.09 3.00 -3 6 0 48.90 3.30 3 6 0 46.80 3.20 3 6 0 49.20 2.20 4 -6 0 37.70 1.50 -4 -6 0 38.90 2.80 -4 -6 0 39.10 2.90 -4 6 0 38.30 3.00 4 6 0 44.30 2.60 4 6 0 41.50 3.10 4 6 0 38.70 2.00 4 6 0 37.20 2.90 -5 -6 0 34.80 3.00 5 -6 0 30.70 2.90 -5 -6 0 29.50 2.70 5 -6 0 29.40 1.30 5 6 0 32.80 2.20 5 6 0 27.50 2.90 5 6 0 28.60 2.80 6 -6 0 11.70 2.20 6 -6 0 10.90 2.10 -6 -6 0 6.80 2.00 6 -6 0 8.20 0.80 6 6 0 10.90 2.00 6 6 0 10.60 1.80 6 6 0 9.10 2.20 7 -6 0 1.20 0.70 7 -6 0 4.10 1.80 -7 -6 0 2.00 1.60 7 -6 0 5.70 2.00 7 6 0 2.00 1.60 7 6 0 2.50 1.80 -8 -6 0 4.60 1.80 8 -6 0 6.90 2.20 8 -6 0 4.80 1.00 8 -6 0 6.20 2.10 8 6 0 7.30 2.20 8 6 0 7.10 1.70 9 -6 0 0.40 1.70 -9 -6 0 5.40 2.10 9 -6 0 5.20 2.10 9 -6 0 4.60 1.00 9 6 0 7.80 2.30 9 6 0 4.60 1.70 10 -6 0 -1.20 0.80 10 -6 0 1.70 2.30 -10 -6 0 0.60 1.60 10 -6 0 0.40 1.90 10 6 0 1.10 2.30 10 6 0 1.00 1.40 11 -6 0 -0.10 1.80 11 -6 0 2.60 2.40 11 -6 0 -2.00 1.00 11 6 0 -3.20 2.00 12 -6 0 0.20 2.50 12 -6 0 -0.60 2.20 12 -6 0 -1.40 1.10 12 6 0 0.30 2.40 13 -6 0 2.30 3.10 13 -6 0 1.30 1.40 13 6 0 0.30 2.70 13 6 0 2.80 2.70 14 -6 0 1.50 1.50 14 -6 0 -3.10 2.70 14 6 0 1.10 2.80 14 6 0 -2.60 2.60 0 -7 0 -0.20 0.80 0 -7 0 -0.50 0.90 0 -7 0 -0.90 0.80 0 7 0 -0.20 1.40 0 7 0 -0.70 0.80 1 -7 0 73.39 3.30 -1 -7 0 65.19 3.60 -1 -7 0 73.39 3.20 1 -7 0 78.49 3.60 -1 -7 0 74.39 3.70 1 -7 0 77.79 3.30 -1 7 0 70.79 4.30 -1 7 0 70.29 3.10 1 7 0 71.19 3.60 1 7 0 73.69 4.40 -2 -7 0 4.10 1.30 2 -7 0 6.10 0.90 2 -7 0 3.50 0.80 2 -7 0 5.10 1.30 -2 -7 0 3.80 0.90 -2 -7 0 3.80 1.40 2 7 0 2.50 1.30 -2 7 0 4.40 0.60 -2 7 0 1.10 1.60 2 7 0 8.70 2.00 3 -7 0 121.19 5.60 -3 -7 0 133.69 4.80 -3 -7 0 121.89 5.70 3 -7 0 125.99 4.60 3 -7 0 122.49 4.60 -3 -7 0 130.09 5.70 3 7 0 117.69 6.10 3 7 0 125.29 5.80 -3 7 0 130.79 6.20 -4 -7 0 90.39 4.80 4 -7 0 86.99 3.30 4 7 0 96.19 5.10 -4 7 0 93.89 5.00 5 -7 0 1.20 0.40 5 -7 0 1.00 1.50 -5 -7 0 0.30 1.30 -5 7 0 3.60 1.70 5 7 0 1.80 1.60 5 7 0 2.90 1.60 -6 -7 0 3.00 1.60 6 -7 0 2.20 0.50 6 -7 0 0.30 1.50 6 -7 0 -1.60 1.30 6 7 0 2.10 1.50 6 7 0 3.50 1.70 7 -7 0 -0.10 0.50 -7 -7 0 -1.60 1.40 7 -7 0 0.80 1.60 7 -7 0 -1.60 1.70 7 7 0 -1.50 1.60 7 7 0 0.60 1.50 8 -7 0 4.20 1.90 8 -7 0 6.70 2.10 8 -7 0 5.60 0.90 -8 -7 0 4.80 1.90 8 7 0 6.10 2.10 8 7 0 7.40 2.30 9 -7 0 1.30 1.80 9 -7 0 2.60 0.90 9 -7 0 2.40 2.10 -9 -7 0 4.60 1.90 9 7 0 0.30 2.00 9 7 0 3.40 1.80 -10 -7 0 0.90 1.80 10 -7 0 1.90 2.10 10 -7 0 1.50 0.90 10 -7 0 4.20 2.20 10 7 0 2.00 1.80 10 7 0 0.60 2.30 11 -7 0 1.80 2.20 11 -7 0 0.00 1.00 11 -7 0 -3.10 2.00 11 7 0 -1.20 2.10 11 7 0 -3.00 1.90 12 -7 0 0.20 1.20 12 -7 0 -5.40 1.90 12 7 0 0.30 2.80 12 7 0 3.00 2.50 13 -7 0 0.80 2.60 13 -7 0 -0.50 1.20 13 7 0 -0.60 2.70 13 7 0 -1.10 2.50 0 -8 0 6.30 1.20 0 -8 0 5.40 1.30 0 -8 0 3.20 1.00 0 8 0 3.20 1.80 0 8 0 3.10 1.10 -1 -8 0 2.60 0.90 -1 -8 0 1.60 1.10 1 -8 0 3.80 1.20 1 -8 0 1.30 1.00 -1 -8 0 5.00 1.30 1 -8 0 2.00 0.90 -1 8 0 1.30 1.30 1 8 0 2.40 1.70 1 8 0 1.70 1.10 -1 8 0 2.40 0.80 2 -8 0 24.00 1.70 2 -8 0 18.10 1.60 -2 -8 0 25.10 2.40 2 -8 0 23.30 2.20 2 8 0 21.20 2.80 -2 8 0 20.80 2.60 2 8 0 20.90 2.30 -3 -8 0 21.40 2.40 3 -8 0 19.30 2.20 3 -8 0 21.90 1.50 3 -8 0 21.50 1.50 -3 8 0 19.40 2.70 3 8 0 24.00 2.50 3 8 0 22.50 2.90 -4 -8 0 51.69 3.60 4 -8 0 51.89 2.30 4 -8 0 51.29 2.30 4 -8 0 55.49 3.60 4 8 0 51.39 4.00 4 8 0 51.49 3.50 -4 8 0 55.29 3.90 5 -8 0 0.40 0.50 -5 -8 0 0.40 1.50 -5 8 0 -0.20 1.60 5 8 0 -1.20 1.50 5 8 0 -1.10 1.30 6 -8 0 11.80 2.30 6 -8 0 10.50 0.80 -6 -8 0 7.60 2.10 6 8 0 11.80 2.40 6 8 0 15.90 2.60 7 -8 0 14.90 1.00 -7 -8 0 12.50 2.50 7 -8 0 12.20 2.50 7 -8 0 16.10 2.70 7 8 0 12.90 2.70 7 8 0 15.20 2.50 7 8 0 12.90 2.70 8 -8 0 8.80 2.40 8 -8 0 8.60 2.50 -8 -8 0 9.60 2.40 8 -8 0 12.00 1.00 8 8 0 16.10 2.70 8 8 0 14.20 3.00 8 8 0 11.30 2.80 9 -8 0 7.10 2.50 9 -8 0 5.00 0.90 -9 -8 0 5.40 2.20 9 -8 0 5.70 2.40 9 8 0 5.60 2.40 9 8 0 10.60 2.50 9 8 0 4.90 2.40 10 -8 0 -1.80 2.10 -10 -8 0 2.90 2.10 10 -8 0 0.50 0.80 10 -8 0 1.70 2.30 10 8 0 0.70 2.20 10 8 0 3.60 2.40 10 8 0 -1.60 1.80 11 -8 0 5.70 2.80 11 -8 0 8.30 2.60 11 -8 0 9.20 1.30 11 8 0 7.20 3.10 11 8 0 1.90 2.40 12 -8 0 -1.30 2.50 12 -8 0 3.40 1.20 12 8 0 2.00 2.80 12 8 0 -2.60 2.50 0 -9 0 1.70 1.20 0 9 0 -0.40 0.90 0 9 0 1.10 1.80 1 -9 0 62.99 3.30 -1 -9 0 60.49 3.60 1 -9 0 57.49 3.20 -1 9 0 51.79 4.20 1 9 0 57.79 3.40 1 9 0 52.89 4.30 -2 -9 0 -1.30 1.30 2 -9 0 0.00 1.10 2 -9 0 0.30 0.90 2 -9 0 0.50 0.90 2 9 0 0.40 1.70 2 9 0 2.20 1.30 -2 9 0 0.40 1.40 3 -9 0 16.40 1.50 3 -9 0 16.40 2.20 -3 -9 0 20.10 2.60 3 -9 0 19.90 1.60 -3 9 0 13.70 2.40 3 9 0 21.00 2.60 3 9 0 20.50 3.00 4 -9 0 -0.90 1.20 4 -9 0 0.10 0.60 -4 -9 0 0.20 1.50 4 -9 0 -0.50 0.70 -4 9 0 -1.50 1.60 4 9 0 -1.80 1.40 4 9 0 0.30 1.70 5 -9 0 4.00 0.70 -5 -9 0 5.00 1.90 5 -9 0 3.40 0.70 5 -9 0 2.00 1.60 5 9 0 2.70 2.00 5 9 0 4.20 1.90 6 -9 0 21.70 3.00 6 -9 0 20.50 1.00 -6 -9 0 19.70 2.90 6 -9 0 19.50 1.00 6 -9 0 21.90 2.90 6 9 0 20.30 3.20 6 9 0 19.10 2.90 7 -9 0 12.50 2.70 7 -9 0 15.50 2.80 -7 -9 0 15.10 2.80 7 9 0 15.70 2.80 7 9 0 6.80 2.30 8 -9 0 -0.10 1.90 8 -9 0 2.10 2.20 -8 -9 0 6.30 2.30 8 9 0 2.60 2.10 8 9 0 7.70 2.50 9 -9 0 -1.80 2.10 9 -9 0 0.40 0.50 9 -9 0 5.20 2.50 -9 -9 0 3.40 2.30 9 9 0 1.90 2.20 9 9 0 -0.30 2.00 9 9 0 -0.40 2.50 -10 -9 0 0.20 2.30 10 -9 0 1.50 2.60 10 -9 0 2.10 0.70 10 -9 0 -1.40 2.10 10 9 0 1.60 2.70 10 9 0 -3.40 1.70 10 9 0 0.80 2.40 11 -9 0 -0.10 0.70 11 -9 0 3.40 2.90 11 9 0 1.70 2.50 11 9 0 -3.50 2.10 0 -10 0 9.40 1.80 0 10 0 10.10 2.50 1 -10 0 1.60 1.20 -1 -10 0 1.20 1.40 1 10 0 -0.30 1.80 -1 10 0 2.70 2.00 2 -10 0 5.40 1.30 -2 -10 0 5.90 1.70 2 10 0 4.40 1.70 2 10 0 3.10 1.70 -2 10 0 4.60 2.10 3 -10 0 0.00 0.80 3 -10 0 -1.20 0.90 -3 -10 0 -0.10 1.50 3 10 0 1.10 1.40 3 10 0 -2.00 1.80 -3 10 0 0.40 1.80 -4 -10 0 -0.70 1.70 4 -10 0 0.10 0.70 4 -10 0 0.00 0.80 4 10 0 -2.20 1.30 4 10 0 -0.30 1.90 -4 10 0 0.00 1.80 -5 -10 0 3.70 2.00 5 -10 0 2.50 1.80 5 -10 0 1.00 0.60 5 -10 0 0.30 0.60 5 10 0 -0.40 2.00 5 10 0 -2.00 1.40 6 -10 0 2.00 1.90 6 -10 0 1.80 2.00 -6 -10 0 -0.20 2.10 6 10 0 0.40 2.00 6 10 0 -0.40 1.90 7 -10 0 12.80 3.10 7 -10 0 13.20 2.50 -7 -10 0 11.50 2.80 7 -10 0 11.00 2.60 7 10 0 6.10 2.50 7 10 0 10.80 2.80 8 -10 0 2.20 2.00 -8 -10 0 1.40 2.10 8 -10 0 4.50 2.30 8 -10 0 -1.20 2.10 8 10 0 -0.70 1.90 8 10 0 3.10 2.60 -9 -10 0 4.70 2.50 9 -10 0 0.60 2.30 9 -10 0 2.60 2.30 9 -10 0 5.10 2.60 9 10 0 -1.10 2.30 9 10 0 5.40 2.60 10 -10 0 0.30 2.40 10 -10 0 1.80 2.40 -10 -10 0 0.40 2.30 10 10 0 3.30 2.70 10 10 0 -2.10 1.80 0 -11 0 -0.50 1.40 0 11 0 0.30 2.10 -1 -11 0 0.30 1.50 1 -11 0 -0.20 1.30 1 11 0 -3.10 1.30 -1 11 0 1.50 2.00 2 -11 0 -0.50 1.20 -2 -11 0 3.00 1.80 2 11 0 1.80 2.10 -2 11 0 0.60 2.10 -3 -11 0 -0.30 1.80 3 -11 0 0.60 1.00 3 11 0 -1.10 2.20 -3 11 0 -4.60 1.70 -4 -11 0 1.10 2.10 4 -11 0 2.80 1.00 4 11 0 -1.00 2.10 -4 11 0 0.10 2.20 -5 -11 0 -0.10 2.10 5 -11 0 0.30 0.60 5 -11 0 5.00 2.10 5 -11 0 -0.90 0.60 5 11 0 -0.30 2.30 5 11 0 2.10 1.90 -6 -11 0 13.70 3.10 6 -11 0 10.40 2.80 6 11 0 6.10 2.70 6 11 0 9.60 2.50 -7 -11 0 -1.30 1.90 7 -11 0 0.70 2.10 7 -11 0 2.00 2.20 7 11 0 3.30 2.20 7 11 0 -0.40 2.30 -8 -11 0 1.00 2.50 8 -11 0 -1.40 1.90 8 -11 0 3.30 2.30 8 11 0 3.30 2.60 8 11 0 -1.70 2.10 0 -12 0 2.90 1.70 0 12 0 3.30 2.50 1 -12 0 -0.30 1.50 -1 -12 0 0.30 1.80 -1 12 0 2.20 2.40 1 12 0 -2.00 2.20 2 -12 0 -0.10 1.30 -2 -12 0 1.60 1.80 2 12 0 -1.60 2.30 -2 12 0 -0.10 2.30 3 -12 0 0.60 1.20 -3 -12 0 -0.20 2.10 3 12 0 3.90 2.70 -3 12 0 2.80 2.50 -4 -12 0 6.30 2.60 4 -12 0 4.10 1.20 4 12 0 5.30 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0.90 7 1 -3 1.50 1.30 7 1 -3 1.50 1.10 6 -1 -3 150.78 5.70 -6 -1 3 150.48 5.80 6 -1 -3 144.59 5.90 6 -1 -3 150.78 6.00 6 1 -3 142.69 5.80 6 1 -3 134.39 5.90 -6 1 3 144.39 5.50 6 1 -3 145.09 5.80 5 -1 -3 61.69 3.00 5 -1 -3 59.19 3.00 5 -1 -3 54.29 2.70 -5 -1 3 56.89 3.10 -5 -1 3 60.99 2.80 5 1 -3 60.29 2.90 5 1 -3 58.29 2.90 -5 1 3 63.29 2.60 5 1 -3 61.69 3.00 4 -1 -3 36.50 1.90 -4 -1 3 31.10 1.90 4 -1 -3 32.70 2.00 -4 -1 3 32.20 1.80 -4 -1 3 33.50 1.80 -4 -1 3 33.60 2.20 4 -1 -3 29.90 1.80 4 1 -3 31.80 2.00 -4 1 3 30.90 1.60 4 1 -3 34.90 1.90 4 1 -3 35.10 1.90 3 -1 -3 643.54 22.40 -3 -1 3 691.63 22.20 -3 -1 3 674.23 22.30 -3 -1 3 683.43 22.40 3 -1 -3 680.23 22.20 3 -1 -3 688.43 22.30 -3 -1 3 650.23 22.50 3 -1 -3 695.23 22.50 -3 1 3 682.83 22.40 3 1 -3 670.33 22.20 -3 1 3 656.23 22.40 3 1 -3 671.73 22.40 3 1 -3 685.83 22.50 3 1 -3 688.83 22.40 -3 1 3 623.34 22.10 -2 -1 3 439.36 15.50 -2 -1 3 456.65 15.10 2 -1 -3 467.65 15.30 2 -1 -3 452.25 15.40 -2 -1 3 451.25 15.40 2 -1 -3 480.25 15.40 -2 -1 3 469.15 15.50 2 -1 -3 464.95 15.40 -2 1 3 465.85 15.50 2 1 -3 458.65 15.10 2 1 -3 493.45 15.60 2 1 -3 471.15 15.50 -2 1 3 450.35 15.40 -2 1 3 449.76 15.40 2 1 -3 442.36 15.30 -2 1 3 454.95 15.30 1 -1 -3 35.50 1.60 1 -1 -3 33.00 1.70 -1 -1 3 34.30 1.60 -1 -1 3 35.40 1.70 -1 -1 3 35.00 1.90 1 -1 -3 34.90 1.70 1 -1 -3 34.50 1.70 -1 1 3 35.60 1.70 -1 1 3 38.20 1.70 1 1 -3 33.50 1.60 1 1 -3 31.90 1.70 -1 1 3 34.50 1.80 1 1 -3 35.20 1.90 0 -1 -3 2.30 0.70 0 -1 -3 1.70 0.70 0 -1 -3 0.70 0.50 0 -1 3 1.70 0.50 0 -1 3 0.60 0.60 0 -1 3 1.10 0.30 0 -1 -3 0.90 0.70 0 -1 3 1.40 0.80 0 -1 3 0.90 0.50 0 1 -3 0.40 0.70 0 1 3 0.70 0.80 0 1 -3 2.50 0.60 0 1 -3 1.20 0.30 0 1 3 0.70 0.60 0 1 3 1.40 0.50 0 1 -3 0.60 0.40 0 1 -3 0.60 0.60 0 1 -3 1.10 0.40 1 -1 3 1935.91 62.59 1 -1 3 1862.91 62.59 1 -1 3 1863.61 62.79 -1 -1 -3 1824.62 62.69 1 -1 3 1999.00 62.49 -1 -1 -3 1964.30 62.69 -1 -1 -3 1937.01 62.79 -1 -1 -3 1967.80 62.69 -1 -1 -3 1951.00 62.79 -1 1 -3 1893.01 62.69 -1 1 -3 1916.11 62.69 1 1 3 1905.81 62.69 -1 1 -3 1898.71 63.09 1 1 3 1902.91 62.69 1 1 3 1921.21 62.59 1 1 3 1907.31 62.79 -1 1 -3 2022.80 62.59 -1 1 -3 1976.00 62.49 2 -1 3 1029.80 33.00 -2 -1 -3 1013.90 33.30 -2 -1 -3 1044.50 33.00 -2 -1 -3 1004.60 33.20 2 -1 3 1014.00 33.00 -2 -1 -3 1055.09 32.80 2 -1 3 987.80 33.10 2 -1 3 985.20 32.70 -2 -1 -3 995.70 33.20 2 -1 3 994.90 33.10 -2 1 -3 1021.10 32.90 2 1 3 929.61 33.30 2 1 3 982.90 33.20 -2 1 -3 1003.80 32.80 2 1 3 999.70 33.30 -2 1 -3 1036.10 33.10 -2 1 -3 1036.30 33.10 -3 -1 -3 183.48 6.30 -3 -1 -3 180.28 6.70 -3 -1 -3 184.78 6.10 3 -1 3 178.48 6.10 3 -1 3 183.98 6.50 3 -1 3 171.88 6.60 3 -1 3 174.68 6.40 3 -1 3 171.28 6.50 3 1 3 175.38 6.80 -3 1 -3 180.48 6.00 3 1 3 175.18 6.80 3 1 3 180.28 6.70 -3 1 -3 185.28 6.30 -3 1 -3 183.98 6.10 3 1 3 181.78 6.70 -4 -1 -3 49.00 2.50 4 -1 3 48.50 2.40 -4 -1 -3 49.30 2.30 4 -1 3 46.50 2.50 4 -1 3 45.20 2.10 4 -1 3 48.60 2.40 4 -1 3 45.80 2.60 4 1 3 47.70 2.60 -4 1 -3 49.30 2.00 -4 1 -3 50.19 2.20 4 1 3 45.60 2.70 4 1 3 46.30 2.70 4 1 3 49.50 2.60 5 -1 3 17.10 1.90 5 -1 3 22.20 1.40 5 -1 3 24.00 2.00 5 -1 3 18.10 1.70 -5 -1 -3 19.90 1.80 5 -1 3 17.10 1.60 5 1 3 22.50 2.00 5 1 3 19.10 2.10 -5 1 -3 20.40 1.30 5 1 3 17.50 1.60 -5 1 -3 19.20 1.40 5 1 3 20.20 1.90 5 1 3 20.90 2.10 6 -1 3 32.50 2.50 -6 -1 -3 34.90 2.30 6 -1 3 34.40 2.10 6 -1 3 30.40 2.70 6 -1 3 33.30 2.30 6 -1 3 36.70 2.30 6 1 3 33.80 2.90 6 1 3 37.80 2.80 -6 1 -3 37.70 2.10 6 1 3 31.90 2.50 -6 1 -3 35.30 2.00 6 1 3 32.90 2.20 6 1 3 37.10 2.50 7 -1 3 183.18 7.70 7 -1 3 187.48 7.20 7 -1 3 185.48 6.90 7 -1 3 177.98 7.20 -7 -1 -3 172.08 7.10 7 -1 3 180.68 7.40 7 1 3 172.98 7.00 7 1 3 193.58 7.50 7 1 3 186.98 7.70 7 1 3 169.98 7.40 -7 1 -3 172.58 6.80 7 1 3 174.08 7.70 8 -1 3 34.80 2.60 -8 -1 -3 40.80 2.70 8 -1 3 33.80 3.40 8 -1 3 39.60 2.80 8 -1 3 33.00 2.50 8 -1 3 37.40 2.90 8 1 3 28.50 2.90 8 1 3 34.90 3.40 8 1 3 34.10 2.60 8 1 3 39.10 3.50 -8 1 -3 34.90 2.30 9 -1 3 3.20 1.90 9 -1 3 7.70 1.80 9 -1 3 4.90 1.60 9 -1 3 8.60 1.70 9 1 3 8.30 1.90 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336.47 11.50 5 -2 3 0.30 0.50 5 -2 3 -0.10 0.70 -5 -2 -3 1.40 0.90 5 -2 3 -0.10 0.80 -5 -2 -3 -0.40 0.50 5 -2 3 -0.80 0.70 5 -2 3 0.50 1.10 5 -2 3 -0.70 0.60 5 2 3 2.00 1.30 5 2 3 0.10 0.90 5 2 3 0.10 0.60 5 2 3 1.20 0.80 5 2 3 0.80 1.10 6 -2 3 0.70 0.90 6 -2 3 0.60 1.00 -6 -2 -3 1.30 1.00 6 -2 3 0.50 0.50 6 -2 3 0.70 1.20 6 -2 3 0.10 0.80 6 -2 3 -1.20 0.80 6 2 3 0.10 0.60 6 2 3 2.00 1.40 6 2 3 0.20 1.10 6 2 3 0.30 1.40 7 -2 3 68.79 2.60 7 -2 3 68.59 3.50 7 -2 3 62.69 3.90 7 -2 3 69.59 3.30 -7 -2 -3 60.99 3.60 7 -2 3 64.99 3.50 7 -2 3 65.19 3.50 7 2 3 65.99 4.20 7 2 3 66.99 4.10 7 2 3 60.89 3.80 7 2 3 64.69 2.70 8 -2 3 258.27 10.30 -8 -2 -3 240.18 9.80 8 -2 3 238.08 9.60 8 -2 3 260.07 9.60 8 -2 3 248.38 9.70 8 -2 3 249.88 9.30 8 2 3 251.67 10.40 8 2 3 255.17 8.50 8 2 3 238.28 10.40 8 2 3 265.97 10.30 9 -2 3 70.99 4.00 9 -2 3 75.29 3.80 9 -2 3 71.09 4.10 9 -2 3 80.39 4.90 9 2 3 75.79 4.60 9 2 3 65.09 4.80 9 2 3 72.69 4.80 10 -2 3 5.00 1.70 10 -2 3 4.40 1.60 10 -2 3 2.00 2.00 10 -2 3 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12 -3 -3 13.00 2.70 12 -3 -3 9.60 2.00 12 3 -3 16.80 3.10 12 3 -3 13.40 2.50 12 3 -3 7.70 2.50 12 3 -3 10.20 1.90 11 -3 -3 20.50 2.90 11 -3 -3 17.20 2.80 11 -3 -3 15.10 2.10 11 3 -3 22.10 2.80 11 3 -3 15.80 2.80 11 3 -3 15.70 2.10 11 3 -3 17.70 2.90 -10 -3 3 12.30 2.00 10 -3 -3 13.90 2.00 10 -3 -3 14.50 2.40 10 -3 -3 11.60 2.10 10 3 -3 15.20 2.00 10 3 -3 12.70 2.50 10 3 -3 14.00 2.30 10 3 -3 12.60 2.40 9 -3 -3 20.70 2.10 9 -3 -3 20.10 2.70 -9 -3 3 21.30 2.40 9 -3 -3 20.90 2.70 9 3 -3 23.20 2.30 9 3 -3 21.70 2.60 9 3 -3 20.20 2.80 9 3 -3 20.40 2.60 8 -3 -3 4.50 1.70 8 -3 -3 3.50 1.70 -8 -3 3 5.70 1.50 8 -3 -3 3.10 1.10 8 3 -3 4.20 1.30 8 3 -3 4.10 1.50 8 3 -3 5.30 1.70 8 3 -3 5.00 1.50 7 -3 -3 161.48 6.80 -7 -3 3 156.68 6.50 7 -3 -3 160.28 6.10 7 -3 -3 156.68 6.70 7 3 -3 153.08 6.40 7 3 -3 153.48 6.60 7 3 -3 159.58 6.90 7 3 -3 161.58 6.70 6 -3 -3 -0.50 1.00 6 -3 -3 -0.70 0.60 6 -3 -3 0.70 1.20 -6 -3 3 0.30 1.00 -6 -3 3 0.90 1.10 6 3 -3 -0.80 1.20 6 3 -3 0.80 0.90 6 3 -3 0.80 1.00 6 3 -3 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7.70 1.00 5 -3 3 7.40 1.40 5 -3 3 10.90 1.30 -5 -3 -3 8.80 1.50 5 -3 3 9.70 1.20 5 3 3 7.60 1.70 5 3 3 8.20 1.20 5 3 3 5.80 1.40 5 3 3 9.10 1.80 6 -3 3 1.20 1.30 -6 -3 -3 0.70 1.20 6 -3 3 3.00 1.00 6 -3 3 1.00 0.90 6 -3 3 1.70 0.90 6 -3 3 1.70 1.10 6 3 3 0.70 0.80 6 3 3 0.80 1.50 6 3 3 1.90 1.60 6 3 3 0.20 1.10 7 -3 3 -1.60 1.40 7 -3 3 0.00 1.00 -7 -3 -3 1.20 1.20 7 -3 3 1.60 1.20 7 -3 3 -0.40 1.00 7 -3 3 1.10 1.00 7 3 3 0.90 1.70 7 3 3 0.60 1.30 7 3 3 1.20 1.60 7 3 3 0.10 0.80 -8 -3 -3 7.50 1.70 8 -3 3 2.40 1.20 8 -3 3 6.90 2.10 8 -3 3 5.20 1.50 8 -3 3 2.60 1.30 8 -3 3 5.60 1.30 8 3 3 8.60 1.90 8 3 3 3.70 2.10 8 3 3 2.40 1.90 8 3 3 3.50 1.00 9 -3 3 0.70 1.70 -9 -3 -3 0.90 1.40 9 -3 3 0.10 1.00 9 -3 3 1.50 1.30 9 -3 3 -0.20 1.20 9 3 3 0.90 2.00 9 3 3 -2.40 1.60 9 3 3 -1.60 1.20 10 -3 3 20.10 2.40 10 -3 3 25.10 3.30 10 -3 3 27.10 2.70 10 -3 3 28.00 2.70 10 3 3 25.20 3.60 10 3 3 30.40 3.30 10 3 3 19.50 3.20 11 -3 3 1.70 2.30 11 -3 3 5.00 1.60 11 -3 3 4.70 1.60 11 3 3 4.60 2.50 11 3 3 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2.70 6 4 -4 35.50 3.20 6 4 -4 35.60 2.50 -5 -4 4 4.50 1.20 -5 -4 4 2.90 1.20 5 -4 -4 5.30 0.90 5 -4 -4 2.50 0.80 -5 -4 4 5.10 1.20 5 -4 -4 4.00 1.50 5 4 -4 3.50 1.30 5 4 -4 4.80 1.10 5 4 -4 5.60 1.10 5 4 -4 3.90 1.50 -4 -4 4 3.10 1.00 4 -4 -4 3.90 0.80 4 -4 -4 2.50 1.30 -4 -4 4 2.20 0.90 4 -4 -4 3.00 0.80 -4 -4 4 3.30 1.10 4 4 -4 2.10 1.10 4 4 -4 2.10 1.20 4 4 -4 2.80 0.90 -3 -4 4 56.09 2.60 3 -4 -4 55.89 2.80 3 -4 -4 57.89 2.60 3 -4 -4 46.00 2.40 -3 -4 4 52.69 2.70 -3 -4 4 51.69 2.90 -3 4 4 52.59 2.50 3 4 -4 55.19 2.60 3 4 -4 55.49 3.10 3 4 -4 50.79 2.60 2 -4 -4 149.39 5.50 2 -4 -4 142.89 5.60 -2 -4 4 151.18 5.70 -2 -4 4 148.29 6.00 -2 -4 4 146.09 5.40 2 4 -4 153.58 5.50 2 4 -4 141.09 6.00 -2 4 4 150.88 5.70 -1 -4 4 12.20 1.50 -1 -4 4 14.50 1.20 -1 -4 4 13.60 1.20 1 -4 -4 12.90 1.00 1 -4 -4 15.50 1.40 -1 4 4 11.40 1.40 1 4 -4 11.00 1.50 1 4 -4 14.30 1.00 0 -4 4 143.39 6.20 0 -4 4 155.88 5.60 0 -4 -4 156.38 6.00 0 4 4 152.18 6.20 0 4 -4 150.38 6.20 0 4 -4 162.98 5.60 0 4 4 151.58 6.10 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3.00 5 2 8 40.30 3.80 6 -2 8 91.59 4.80 6 -2 8 88.19 5.60 6 -2 8 87.19 4.70 -6 -2 -8 89.49 5.00 6 2 8 81.59 4.70 6 2 8 84.19 5.40 6 2 8 91.09 5.30 7 -2 8 0.20 1.40 7 -2 8 2.70 1.90 7 -2 8 -0.10 1.70 7 2 8 -1.10 1.80 7 2 8 0.60 1.50 7 2 8 -0.50 1.70 8 -2 8 -3.10 1.50 8 -2 8 -3.10 1.40 8 2 8 0.10 1.90 8 2 8 -1.70 1.90 9 -2 8 3.40 2.00 9 -2 8 5.10 2.40 9 2 8 8.30 2.80 9 2 8 7.70 2.60 10 -2 8 2.60 2.20 10 -2 8 1.60 1.70 10 2 8 -2.70 2.10 10 2 8 -0.20 2.20 11 -2 8 17.80 3.40 11 2 8 10.00 3.40 11 2 8 16.80 3.70 12 -2 8 -3.40 2.80 12 2 8 -0.50 2.40 12 2 8 -0.90 3.00 16 -3 -8 0.80 2.70 16 -3 -8 6.30 3.50 16 -3 -8 3.50 2.30 16 3 -8 5.80 3.00 16 3 -8 3.20 2.70 15 -3 -8 1.60 2.70 15 -3 -8 8.70 3.10 15 -3 -8 4.60 2.10 15 3 -8 3.10 2.70 15 3 -8 -0.30 1.90 15 3 -8 2.10 2.40 14 -3 -8 0.10 1.60 14 -3 -8 2.10 2.60 14 -3 -8 5.40 2.70 14 3 -8 -3.70 1.60 14 3 -8 -0.30 1.80 14 3 -8 1.10 2.40 13 -3 -8 0.70 1.90 13 -3 -8 -0.40 1.50 13 -3 -8 -3.80 2.00 13 3 -8 2.50 1.80 13 3 -8 0.60 2.00 13 3 -8 -0.60 1.50 13 3 -8 -0.50 2.10 12 -3 -8 0.30 1.80 12 -3 -8 -3.20 1.20 12 -3 -8 0.90 2.10 12 3 -8 -0.20 1.50 12 3 -8 0.20 1.60 12 3 -8 2.40 2.10 12 3 -8 1.00 1.70 11 -3 -8 -1.30 1.80 11 -3 -8 -0.30 1.30 -11 -3 8 -0.60 1.30 11 -3 -8 2.30 1.90 11 3 -8 0.00 1.40 11 3 -8 2.30 1.50 11 3 -8 -1.20 1.30 11 3 -8 0.00 1.60 10 -3 -8 142.09 7.20 -10 -3 8 137.39 7.50 10 -3 -8 148.89 7.20 10 -3 -8 149.19 6.70 -10 -3 8 156.38 6.90 10 3 -8 139.19 7.20 10 3 -8 141.99 6.90 10 3 -8 149.69 6.60 10 3 -8 162.68 7.20 9 -3 -8 33.30 2.90 9 -3 -8 35.40 3.70 -9 -3 8 39.20 3.40 9 -3 -8 31.10 3.20 -9 -3 8 32.70 3.50 9 3 -8 33.40 3.20 9 3 -8 41.70 3.10 9 3 -8 37.00 3.60 9 3 -8 43.40 3.20 8 -3 -8 3.30 1.70 -8 -3 8 3.80 1.50 8 -3 -8 6.40 1.50 -8 -3 8 5.60 2.10 8 -3 -8 5.60 2.00 -8 3 8 6.10 1.30 8 3 -8 4.50 1.40 8 3 -8 5.20 1.50 8 3 -8 5.50 1.70 8 3 -8 5.80 1.90 7 -3 -8 12.80 1.70 -7 -3 8 11.00 2.30 7 -3 -8 11.20 2.00 7 3 -8 13.30 1.60 7 3 -8 15.50 2.10 7 3 -8 12.80 2.20 7 3 -8 13.80 1.90 -6 -3 8 2.70 1.70 6 -3 -8 1.80 1.20 -6 -3 8 3.20 1.20 6 -3 -8 2.70 1.60 6 3 -8 -0.10 1.40 6 3 -8 1.70 1.20 6 3 -8 1.50 1.00 -6 3 8 3.70 1.50 6 3 -8 2.80 0.90 5 -3 -8 9.10 1.50 -5 -3 8 12.10 1.70 5 -3 -8 11.20 1.90 -5 -3 8 8.50 1.90 5 3 -8 11.40 1.80 5 3 -8 8.10 1.00 -5 3 8 7.80 1.50 5 3 -8 9.50 1.60 5 3 -8 8.20 1.40 4 -3 -8 41.00 2.90 -4 -3 8 43.80 3.30 4 -3 -8 39.70 2.70 -4 -3 8 44.10 2.70 4 3 -8 38.70 2.70 4 3 -8 39.50 2.40 -4 3 8 37.00 2.60 4 3 -8 42.90 1.70 4 3 -8 45.70 2.80 -4 3 8 48.60 3.00 -3 -3 8 99.89 4.30 3 -3 -8 96.59 4.40 -3 -3 8 90.19 4.80 3 -3 -8 88.89 4.30 3 3 -8 91.39 4.30 3 3 -8 87.69 4.10 -3 3 8 92.39 4.20 3 3 -8 88.99 4.00 -3 3 8 94.19 4.50 -2 -3 8 114.39 5.50 2 -3 -8 123.09 5.10 2 -3 -8 118.69 5.00 -2 -3 8 110.09 4.80 -2 3 8 114.19 5.20 2 3 -8 108.99 4.70 -2 3 8 114.49 4.80 2 3 -8 116.99 4.70 2 3 -8 108.19 5.00 1 -3 -8 43.80 2.80 -1 -3 8 44.40 2.70 1 -3 -8 49.60 2.70 -1 -3 8 48.60 3.40 1 3 -8 47.80 2.80 -1 3 8 46.20 2.60 -1 3 8 51.19 3.10 1 3 -8 46.80 2.40 0 -3 8 16.00 1.40 0 -3 8 10.10 1.80 0 -3 8 10.60 0.70 0 -3 8 11.50 1.40 0 -3 8 9.10 1.50 0 -3 -8 11.30 1.70 0 3 -8 10.50 1.60 0 3 -8 13.80 1.30 0 3 8 8.80 1.20 0 3 8 12.00 1.90 1 -3 8 24.10 1.50 -1 -3 -8 26.20 2.40 1 -3 8 23.50 2.60 1 -3 8 28.30 2.10 1 -3 8 29.90 1.60 1 -3 8 28.40 2.10 1 3 8 25.10 2.70 -1 3 -8 25.30 1.60 -1 3 -8 23.10 2.10 1 3 8 28.50 2.00 2 -3 8 -0.40 1.00 2 -3 8 -1.10 0.80 2 -3 8 -0.40 1.30 -2 -3 -8 -2.20 1.00 2 -3 8 -1.10 1.00 2 -3 8 0.40 0.50 2 3 8 -2.30 1.30 2 3 8 0.40 1.40 2 3 8 0.60 0.90 -2 3 -8 -0.80 0.90 3 -3 8 35.40 2.50 3 -3 8 39.60 2.60 3 -3 8 34.60 3.30 -3 -3 -8 38.10 2.90 3 -3 8 39.40 2.50 3 3 8 35.90 2.60 3 3 8 36.10 3.30 3 3 8 36.10 3.40 -3 3 -8 38.60 2.30 4 -3 8 31.00 2.50 -4 -3 -8 34.10 3.10 4 -3 8 30.60 3.30 4 -3 8 34.20 2.60 4 -3 8 27.30 2.40 4 3 8 31.50 3.30 4 3 8 31.50 2.60 -4 3 -8 34.30 2.00 4 3 8 34.40 3.30 5 -3 8 -0.40 1.10 5 -3 8 1.30 1.50 5 -3 8 0.80 1.70 -5 -3 -8 2.80 1.50 5 -3 8 -0.70 1.10 -5 3 -8 1.70 0.80 5 3 8 1.30 1.80 5 3 8 1.40 1.80 5 3 8 3.40 1.30 -6 -3 -8 50.99 3.60 6 -3 8 49.60 4.10 6 -3 8 52.19 3.60 6 -3 8 44.10 3.10 6 3 8 48.70 4.40 6 3 8 49.20 3.40 6 3 8 47.50 4.40 7 -3 8 5.90 2.10 7 -3 8 5.70 1.80 7 -3 8 4.80 2.30 7 3 8 8.00 2.50 7 3 8 7.80 1.80 7 3 8 11.10 2.80 8 -3 8 1.90 2.00 8 -3 8 0.70 1.50 8 -3 8 0.90 1.80 8 3 8 1.70 2.40 8 3 8 0.80 2.00 8 3 8 0.40 1.50 9 -3 8 14.00 3.20 9 -3 8 20.00 3.10 9 -3 8 20.60 2.80 9 3 8 19.90 3.50 9 3 8 26.90 3.80 9 3 8 17.50 2.70 10 -3 8 10.00 3.10 10 -3 8 13.80 3.40 10 3 8 12.40 3.10 10 3 8 6.20 2.90 10 3 8 15.40 2.80 11 -3 8 1.20 2.50 11 -3 8 -1.90 2.20 11 3 8 -4.00 2.30 11 3 8 -0.20 1.90 11 3 8 2.70 3.10 12 -3 8 2.70 3.00 12 -3 8 -1.80 2.40 12 3 8 1.20 2.60 12 3 8 0.50 2.80 16 -4 -8 4.80 3.30 16 -4 -8 1.70 2.80 16 -4 -8 -1.80 1.70 16 4 -8 0.00 2.70 16 4 -8 4.30 2.80 15 -4 -8 1.90 2.80 15 -4 -8 3.00 1.90 15 -4 -8 1.30 2.70 15 4 -8 4.50 2.80 15 4 -8 4.00 2.20 15 4 -8 6.80 2.90 14 -4 -8 -3.80 2.00 14 -4 -8 1.60 2.50 14 -4 -8 -0.60 1.60 14 4 -8 1.00 2.00 14 4 -8 4.70 2.20 14 4 -8 8.30 2.90 13 -4 -8 2.00 2.10 13 -4 -8 2.00 2.40 13 -4 -8 0.60 1.60 13 4 -8 4.50 1.90 13 4 -8 1.40 2.30 13 4 -8 3.00 2.10 12 -4 -8 6.30 2.30 12 -4 -8 3.40 1.60 12 -4 -8 5.90 2.50 12 4 -8 6.40 2.10 12 4 -8 3.00 1.80 12 4 -8 8.70 2.70 11 -4 -8 7.50 2.30 11 -4 -8 6.60 1.80 -11 -4 8 7.20 2.50 -11 -4 8 3.70 1.70 11 -4 -8 4.60 2.30 11 4 -8 4.10 2.20 11 4 -8 7.20 2.00 11 4 -8 4.70 2.10 -10 -4 8 1.30 1.50 10 -4 -8 2.30 1.30 10 -4 -8 3.60 2.20 -10 -4 8 5.50 2.20 10 -4 -8 5.00 2.00 10 4 -8 2.20 1.70 10 4 -8 2.50 1.60 10 4 -8 2.50 1.60 10 4 -8 1.90 2.00 -9 -4 8 41.30 4.10 9 -4 -8 59.59 4.30 9 -4 -8 47.10 3.30 9 -4 -8 44.50 4.00 -9 -4 8 54.79 3.60 9 4 -8 52.39 3.30 9 4 -8 63.09 3.80 9 4 -8 49.80 3.80 9 4 -8 50.79 4.10 8 -4 -8 0.40 1.90 -8 -4 8 -1.00 1.80 8 -4 -8 0.80 1.20 -8 -4 8 -0.40 1.30 8 4 -8 0.30 1.80 8 4 -8 1.40 1.20 8 4 -8 0.40 1.30 8 4 -8 2.30 1.40 7 -4 -8 2.70 1.80 7 -4 -8 2.20 1.10 -7 -4 8 1.90 1.80 -7 -4 8 4.10 1.40 7 4 -8 1.50 1.30 7 4 -8 -0.20 1.00 7 4 -8 -0.20 1.60 7 4 -8 2.50 1.20 -6 -4 8 83.09 4.20 6 -4 -8 68.59 3.80 6 -4 -8 67.99 4.10 -6 -4 8 71.89 4.60 6 4 -8 77.69 4.40 6 4 -8 70.89 4.30 6 4 -8 76.49 3.90 6 4 -8 76.59 3.40 -5 -4 8 2.60 1.70 -5 -4 8 1.10 0.60 5 -4 -8 1.90 1.60 -5 -4 8 2.40 1.20 5 -4 -8 0.70 1.00 5 4 -8 2.80 1.50 5 4 -8 1.90 0.70 -5 4 8 1.10 1.10 5 4 -8 0.10 0.30 5 4 -8 1.10 1.20 -4 -4 8 1.00 1.10 -4 -4 8 2.90 1.60 4 -4 -8 2.20 1.10 -4 -4 8 1.90 0.50 4 -4 -8 4.60 1.60 -4 4 8 0.70 1.10 4 4 -8 2.60 1.00 4 4 -8 2.50 1.40 4 4 -8 2.40 1.50 -4 4 8 0.10 1.10 3 -4 -8 141.99 6.00 -3 -4 8 147.59 6.60 3 -4 -8 131.59 6.00 -3 -4 8 148.39 5.90 3 4 -8 134.99 5.60 -3 4 8 136.89 5.60 3 4 -8 134.89 6.10 -3 4 8 137.09 6.00 3 4 -8 136.19 5.90 -2 -4 8 112.89 4.80 -2 -4 8 110.49 5.40 2 -4 -8 101.59 4.90 2 -4 -8 105.19 5.00 2 4 -8 106.89 5.10 2 4 -8 111.69 4.50 -2 4 8 107.59 4.50 -2 4 8 115.89 5.20 -1 -4 8 55.59 3.00 -1 -4 8 60.09 3.90 1 -4 -8 56.49 3.40 1 -4 -8 61.19 2.80 1 4 -8 61.09 3.40 -1 4 8 57.49 3.50 1 4 -8 58.19 2.70 -1 4 8 55.99 2.80 0 -4 -8 8.00 1.60 0 -4 8 5.30 1.20 0 -4 8 6.80 0.50 0 -4 8 3.10 1.50 0 4 8 8.80 1.80 0 4 -8 6.20 1.40 0 4 8 4.40 0.90 -1 -4 -8 72.99 4.00 1 -4 8 66.89 4.30 1 -4 8 68.29 2.80 1 -4 8 65.89 3.30 1 4 8 63.89 4.10 1 4 8 69.39 3.10 -1 4 -8 70.59 3.60 2 -4 8 1.70 1.50 -2 -4 -8 4.10 1.50 2 -4 8 3.50 0.90 2 -4 8 1.50 1.10 2 -4 8 3.20 1.00 2 -4 8 1.20 1.10 2 4 8 2.50 0.90 2 4 8 1.00 1.20 -2 4 -8 2.30 1.20 3 -4 8 1.20 1.00 3 -4 8 2.00 1.10 -3 -4 -8 0.40 1.40 3 -4 8 2.40 1.20 3 -4 8 1.60 0.70 3 -4 8 1.30 1.60 3 4 8 -1.50 1.60 -3 4 -8 1.30 1.00 3 4 8 3.00 1.00 3 4 8 -0.10 1.80 4 -4 8 0.90 0.70 4 -4 8 -1.10 1.50 4 -4 8 -0.50 1.00 -4 -4 -8 -1.30 1.30 4 -4 8 0.10 1.20 4 -4 8 0.90 1.10 4 4 8 -0.60 1.70 -4 4 -8 0.10 0.90 4 4 8 -1.00 1.70 4 4 8 0.40 0.90 -5 -4 -8 41.00 3.50 5 -4 8 32.50 2.50 5 -4 8 31.90 2.80 5 -4 8 35.30 2.70 5 -4 8 31.20 3.50 5 4 8 36.50 3.80 5 4 8 36.50 3.70 5 4 8 34.20 2.60 -5 4 -8 34.40 2.20 6 -4 8 -0.70 1.40 6 -4 8 -0.30 1.10 6 -4 8 -0.40 1.70 -6 -4 -8 0.70 1.40 6 4 8 -1.90 1.80 6 4 8 -0.40 1.00 6 4 8 2.50 2.00 7 -4 8 17.60 2.60 7 -4 8 23.90 3.40 7 -4 8 24.60 2.50 7 4 8 23.60 3.50 7 4 8 23.60 2.50 7 4 8 20.90 3.40 8 -4 8 14.60 3.00 8 -4 8 18.50 3.00 8 4 8 13.30 2.20 8 4 8 17.80 3.40 8 4 8 19.40 3.40 9 -4 8 15.00 3.10 9 -4 8 15.50 3.00 9 4 8 20.00 3.90 9 4 8 16.30 3.40 10 -4 8 7.40 3.00 10 -4 8 14.20 3.00 10 4 8 16.60 3.60 10 4 8 19.80 3.90 11 -4 8 -0.40 2.40 11 -4 8 -3.50 2.20 11 4 8 2.10 3.00 11 4 8 -3.00 2.60 12 -4 8 2.60 2.80 12 -4 8 -2.20 2.50 12 4 8 2.20 2.90 12 4 8 -0.20 2.70 16 -5 -8 -0.60 2.90 16 -5 -8 0.50 1.80 16 -5 -8 1.70 3.00 16 5 -8 2.50 2.90 16 5 -8 4.50 3.00 15 -5 -8 0.70 2.90 15 -5 -8 1.80 1.90 15 -5 -8 2.60 2.80 15 5 -8 0.70 1.90 15 5 -8 3.50 2.90 15 5 -8 6.10 2.70 14 -5 -8 7.20 2.10 14 -5 -8 8.20 2.90 14 -5 -8 1.90 2.70 14 5 -8 8.20 2.80 14 5 -8 8.00 2.70 14 5 -8 7.90 3.00 13 -5 -8 -3.10 2.20 13 -5 -8 0.10 2.30 13 -5 -8 0.30 1.50 13 5 -8 0.80 2.30 13 5 -8 3.60 2.00 13 5 -8 3.70 2.00 12 -5 -8 5.60 2.60 12 -5 -8 4.30 1.70 12 -5 -8 6.70 2.40 12 5 -8 8.10 2.30 12 5 -8 2.40 1.90 12 5 -8 4.20 2.40 11 -5 -8 1.20 1.40 -11 -5 8 4.90 2.40 -11 -5 8 -1.60 1.40 11 -5 -8 0.00 1.80 11 -5 -8 -1.60 2.10 11 5 -8 -0.80 1.60 11 5 -8 0.60 2.00 11 5 -8 0.60 1.60 10 -5 -8 0.10 1.60 10 -5 -8 -0.90 1.40 -10 -5 8 -0.90 1.30 -10 -5 8 -2.00 2.00 10 -5 -8 0.40 1.30 10 5 -8 2.80 1.90 10 5 -8 3.30 2.10 10 5 -8 0.20 1.40 9 -5 -8 32.00 2.80 -9 -5 8 37.10 3.30 -9 -5 8 28.90 3.40 9 -5 -8 31.70 3.50 9 5 -8 30.50 3.60 9 5 -8 26.30 2.60 9 5 -8 28.70 3.30 8 -5 -8 38.90 3.90 8 -5 -8 29.70 2.70 -8 -5 8 33.10 3.40 -8 -5 8 30.60 3.00 8 5 -8 35.90 3.70 8 5 -8 34.40 2.50 8 5 -8 40.70 3.70 7 -5 -8 118.99 5.50 -7 -5 8 114.09 5.70 -7 -5 8 106.59 6.20 7 -5 -8 118.29 6.20 7 5 -8 122.59 6.20 7 5 -8 123.59 5.10 7 5 -8 136.89 5.80 7 5 -8 110.09 6.00 6 -5 -8 16.50 2.00 -6 -5 8 18.90 2.70 6 -5 -8 18.50 2.70 6 5 -8 20.60 2.80 6 5 -8 12.30 2.30 6 5 -8 17.10 1.60 -5 -5 8 1.10 0.80 5 -5 -8 0.60 1.10 -5 -5 8 -0.10 1.60 -5 -5 8 0.60 1.10 5 -5 -8 1.10 1.40 5 5 -8 0.70 1.20 5 5 -8 0.70 1.00 -5 5 8 0.90 1.20 5 5 -8 1.40 1.60 4 -5 -8 1.30 1.60 -4 -5 8 1.80 1.60 -4 -5 8 3.70 1.40 4 -5 -8 2.60 1.20 -4 -5 8 1.10 0.60 -4 5 8 1.00 1.30 4 5 -8 0.90 1.60 4 5 -8 2.60 0.90 3 -5 -8 -1.20 1.40 3 -5 -8 0.10 1.00 -3 -5 8 0.60 0.30 -3 -5 8 -0.80 1.40 -3 -5 8 0.50 1.10 -3 5 8 -0.40 1.30 3 5 -8 1.60 0.80 3 5 -8 2.20 1.20 2 -5 -8 -0.90 1.10 -2 -5 8 0.10 0.90 -2 -5 8 1.00 1.50 2 -5 -8 0.30 0.70 2 5 -8 -1.20 1.30 -2 5 8 0.20 1.30 -1 -5 8 1.50 1.50 1 -5 -8 -1.10 1.10 -1 -5 8 1.60 0.90 1 -5 -8 0.90 0.60 -1 5 8 2.50 1.50 -1 5 8 -0.40 0.60 1 5 -8 -0.10 1.00 0 -5 8 0.40 0.50 0 -5 8 0.70 1.00 0 -5 8 1.40 1.50 0 -5 8 0.50 0.50 0 -5 -8 -1.10 1.20 0 5 -8 -0.50 1.20 0 5 8 1.70 1.50 0 5 8 -0.70 0.60 1 -5 8 35.00 1.90 -1 -5 -8 35.40 3.10 1 -5 8 29.90 3.20 1 -5 8 33.30 2.30 -1 5 -8 31.20 2.80 1 5 8 35.30 1.70 1 5 8 35.00 3.30 2 -5 8 71.89 4.70 2 -5 8 64.49 3.30 -2 -5 -8 60.39 3.90 2 -5 8 69.89 3.10 2 5 8 61.19 2.70 2 5 8 70.99 4.40 -2 5 -8 56.49 3.60 3 -5 8 2.10 1.10 3 -5 8 1.20 1.10 -3 -5 -8 3.30 1.60 3 -5 8 1.90 1.70 -3 5 -8 1.60 1.10 3 5 8 2.30 0.80 3 5 8 1.60 1.70 4 -5 8 32.60 2.80 -4 -5 -8 34.50 3.30 4 -5 8 32.00 2.50 4 -5 8 33.70 3.60 4 -5 8 34.40 2.40 4 -5 8 28.50 2.10 4 5 8 32.90 2.10 4 5 8 31.00 3.50 4 5 8 26.80 3.40 -4 5 -8 26.10 2.40 5 -5 8 12.10 2.30 5 -5 8 11.10 2.60 -5 -5 -8 18.50 2.60 5 -5 8 12.70 2.00 -5 5 -8 14.50 1.80 5 5 8 13.50 2.70 5 5 8 13.80 1.60 5 5 8 17.80 3.00 6 -5 8 38.00 3.30 -6 -5 -8 39.10 3.70 6 -5 8 36.80 4.10 6 5 8 40.90 4.40 6 5 8 37.50 4.20 7 -5 8 55.79 4.10 7 -5 8 39.30 4.50 7 5 8 52.49 5.00 7 5 8 53.09 5.00 8 -5 8 9.50 2.50 8 -5 8 7.30 2.60 8 5 8 11.30 2.90 8 5 8 11.70 3.00 9 -5 8 6.00 2.60 9 -5 8 3.30 2.20 9 5 8 3.10 2.60 9 5 8 4.40 2.70 10 -5 8 -2.80 2.30 10 -5 8 2.80 2.40 10 5 8 1.70 2.80 10 5 8 1.50 2.70 11 -5 8 -0.20 2.60 11 -5 8 4.30 2.70 11 5 8 3.20 3.00 11 5 8 3.70 3.00 15 -6 -8 -2.90 2.70 15 -6 -8 1.60 1.90 15 -6 -8 2.10 2.70 15 6 -8 3.20 2.40 15 6 -8 -2.70 1.80 15 6 -8 2.20 2.60 14 -6 -8 -4.60 2.50 14 -6 -8 2.50 2.60 14 -6 -8 2.50 1.80 14 6 -8 -1.10 2.00 14 6 -8 5.20 3.00 14 6 -8 0.30 2.00 13 -6 -8 3.30 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59.19 4.10 0 -4 9 63.29 3.30 0 4 -9 55.39 3.40 0 4 9 61.19 3.10 0 4 9 61.49 4.00 -1 -4 -9 4.60 1.60 1 -4 9 6.20 0.90 1 -4 9 3.00 1.70 1 -4 9 6.10 1.10 1 -4 9 7.90 1.50 -1 4 -9 6.80 1.50 1 4 9 9.20 1.30 1 4 9 6.90 2.00 -2 -4 -9 1.90 1.40 2 -4 9 0.00 1.00 2 -4 9 -0.20 1.60 2 -4 9 1.50 1.10 2 -4 9 1.10 0.90 -2 4 -9 -0.90 1.00 2 4 9 -1.00 1.60 2 4 9 -1.10 0.90 3 -4 9 0.90 1.10 -3 -4 -9 1.70 1.40 3 -4 9 0.00 1.70 3 -4 9 1.50 1.10 3 -4 9 4.20 1.30 3 4 9 1.30 1.80 3 4 9 1.50 1.00 -3 4 -9 2.60 1.10 3 4 9 2.30 1.80 4 -4 9 20.10 2.90 4 -4 9 21.30 2.20 4 -4 9 19.60 2.20 -4 -4 -9 23.10 2.70 4 4 9 21.60 3.00 4 4 9 20.20 2.00 -4 4 -9 19.90 1.90 4 4 9 21.70 3.00 -5 -4 -9 91.39 5.30 5 -4 9 95.49 4.80 5 -4 9 98.99 6.20 5 -4 9 94.39 4.70 5 4 9 99.29 4.80 5 4 9 96.99 5.80 -5 4 -9 93.99 4.20 5 4 9 104.59 6.00 6 -4 9 2.80 1.30 6 -4 9 7.30 2.40 6 -4 9 4.40 1.70 6 4 9 3.80 2.20 6 4 9 4.80 1.40 6 4 9 5.40 2.30 7 -4 9 4.90 2.30 7 -4 9 5.00 2.00 7 4 9 4.40 1.60 7 4 9 3.60 2.30 7 4 9 5.50 2.50 8 -4 9 10.60 2.80 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1.30 5 -5 -10 0.50 1.70 -5 -5 10 2.00 1.90 5 5 -10 3.80 1.70 5 5 -10 2.20 1.70 -5 5 10 1.90 1.50 4 -5 -10 88.59 4.60 4 -5 -10 82.49 4.90 -4 -5 10 91.09 5.50 4 5 -10 77.19 4.80 -4 5 10 95.39 4.40 -4 5 10 90.69 4.90 -3 -5 10 6.80 2.30 3 -5 -10 13.20 2.00 3 -5 -10 10.60 2.20 -3 5 10 10.70 2.10 -3 5 10 10.30 1.60 3 5 -10 12.40 2.20 2 -5 -10 168.98 7.30 -2 -5 10 170.18 7.00 -2 -5 10 161.88 7.90 2 -5 -10 165.88 7.30 2 5 -10 152.18 7.20 -2 5 10 169.68 6.50 -2 5 10 166.98 7.50 -1 -5 10 48.80 3.10 1 -5 -10 38.00 3.10 1 -5 -10 46.20 3.40 -1 -5 10 42.80 3.90 1 5 -10 39.30 3.20 -1 5 10 41.10 3.70 -1 5 10 44.90 2.60 0 -5 10 -0.40 1.10 0 -5 10 1.20 1.70 0 -5 -10 3.10 1.60 0 5 10 0.80 1.50 0 5 10 1.00 0.90 0 5 -10 0.50 1.40 -1 -5 -10 2.70 1.60 1 -5 10 5.00 2.00 1 -5 10 7.50 1.70 1 5 10 6.10 1.10 -1 5 -10 5.60 1.60 1 5 10 5.70 2.00 -2 -5 -10 2.40 1.60 2 -5 10 -1.50 1.50 -2 5 -10 -0.50 1.00 2 5 10 -2.20 1.50 2 5 10 0.00 0.90 3 -5 10 21.70 3.20 -3 -5 -10 26.20 3.00 3 5 10 21.70 3.20 -3 5 -10 23.80 2.30 -4 -5 -10 24.10 3.00 4 -5 10 23.50 3.40 4 -5 10 27.80 2.50 4 5 10 23.10 3.40 -4 5 -10 22.50 2.20 -5 -5 -10 1.70 1.70 5 -5 10 1.30 1.90 5 5 10 3.60 2.20 5 5 10 1.00 2.10 6 -5 10 -2.20 1.80 6 5 10 1.60 2.30 6 5 10 3.00 2.30 7 -5 10 4.90 2.50 7 5 10 4.80 2.70 7 5 10 6.40 2.70 8 -5 10 4.50 2.70 8 5 10 6.30 3.00 8 5 10 8.00 3.30 9 -5 10 10.70 3.40 9 5 10 7.20 3.20 9 5 10 12.90 3.70 10 -5 10 0.60 2.60 10 5 10 -0.90 2.40 10 5 10 3.60 3.30 15 -6 -10 2.40 1.90 15 -6 -10 -1.20 2.60 15 -6 -10 -0.30 2.80 15 6 -10 7.20 2.80 15 6 -10 8.80 3.30 14 -6 -10 10.30 3.70 14 -6 -10 6.90 2.20 14 -6 -10 8.20 3.30 14 6 -10 5.50 2.50 14 6 -10 5.30 3.00 13 -6 -10 2.50 2.50 13 -6 -10 0.20 2.50 13 -6 -10 4.10 1.90 13 6 -10 4.10 2.30 13 6 -10 2.00 2.10 12 -6 -10 -0.60 2.10 -12 -6 10 1.50 2.60 12 -6 -10 1.80 2.80 12 -6 -10 -0.50 1.40 12 6 -10 1.00 2.00 12 6 -10 4.40 2.50 11 -6 -10 1.10 2.40 -11 -6 10 -1.00 2.10 -11 -6 10 1.10 1.70 11 -6 -10 2.30 1.50 11 -6 -10 -0.30 1.80 11 6 -10 1.30 2.00 11 6 -10 2.30 2.20 -10 -6 10 0.70 1.60 10 -6 -10 0.80 1.60 -10 -6 10 0.50 2.10 10 -6 -10 -2.30 2.10 10 6 -10 1.70 2.20 10 6 -10 -0.70 1.80 -9 -6 10 1.70 1.60 9 -6 -10 3.20 1.70 -9 -6 10 4.80 2.60 9 -6 -10 0.30 2.10 9 6 -10 4.30 2.10 9 6 -10 3.70 1.70 -8 -6 10 56.19 4.00 8 -6 -10 57.59 4.60 8 -6 -10 54.39 3.70 -8 -6 10 63.99 5.20 8 6 -10 50.19 4.00 8 6 -10 52.79 4.10 7 -6 -10 0.20 1.50 -7 -6 10 2.60 2.00 -7 -6 10 1.10 1.50 7 -6 -10 0.60 1.40 7 6 -10 1.70 1.90 6 -6 -10 29.40 3.50 6 -6 -10 26.80 2.80 -6 -6 10 19.90 3.00 6 6 -10 28.70 3.20 5 -6 -10 13.50 2.60 5 -6 -10 7.10 1.70 -5 -6 10 9.20 2.30 5 6 -10 10.50 2.10 -5 6 10 14.20 2.20 4 -6 -10 8.70 2.20 4 -6 -10 7.30 1.80 -4 -6 10 7.00 2.30 -4 6 10 6.00 1.70 4 6 -10 9.90 2.10 -3 -6 10 0.00 1.80 3 -6 -10 1.30 1.60 3 -6 -10 -0.70 1.20 -3 6 10 0.20 1.40 3 6 -10 -1.20 1.00 2 -6 -10 3.80 1.60 -2 -6 10 6.40 2.10 2 -6 -10 3.60 1.70 -2 6 10 6.30 1.80 2 6 -10 5.20 1.80 -1 -6 10 23.90 3.10 1 -6 -10 29.80 3.10 1 6 -10 27.50 3.00 -1 6 10 25.60 3.00 0 -6 -10 -2.40 1.20 0 -6 10 -2.30 1.60 0 6 -10 0.60 1.30 0 6 10 0.50 1.50 -1 -6 -10 12.00 2.30 1 -6 10 16.30 2.70 -1 6 -10 14.10 2.30 1 6 10 16.60 2.70 -2 -6 -10 2.30 1.70 2 -6 10 5.50 2.10 2 6 10 4.20 2.00 -2 6 -10 3.10 1.30 3 -6 10 2.10 2.00 -3 -6 -10 4.70 1.90 3 6 10 1.90 2.00 -3 6 -10 3.10 1.40 -4 -6 -10 16.50 2.70 4 -6 10 12.30 2.80 -4 6 -10 8.40 1.70 4 6 10 11.00 2.80 5 -6 10 4.00 2.50 -5 -6 -10 4.70 2.00 5 6 10 7.20 2.80 6 -6 10 7.90 2.70 6 6 10 4.80 2.70 6 6 10 8.20 2.90 7 -6 10 4.60 2.50 7 6 10 5.80 2.70 7 6 10 -2.20 2.40 8 -6 10 0.30 2.50 8 6 10 -1.80 2.30 8 6 10 2.30 3.00 9 -6 10 -0.50 2.70 9 6 10 4.00 3.00 9 6 10 -1.00 2.50 14 -7 -10 3.00 2.70 14 -7 -10 2.10 1.70 14 -7 -10 1.90 3.20 14 7 -10 -4.20 2.20 13 -7 -10 2.30 2.80 13 -7 -10 0.70 1.70 13 -7 -10 -2.50 2.80 13 7 -10 1.90 2.40 -12 -7 10 3.00 2.70 12 -7 -10 -1.90 2.20 12 -7 -10 0.00 1.70 12 -7 -10 -2.40 2.60 12 7 -10 0.70 2.10 11 -7 -10 2.70 1.60 -11 -7 10 -0.20 2.40 11 -7 -10 3.40 2.80 -11 -7 10 1.70 1.80 11 -7 -10 1.10 2.20 11 7 -10 1.30 2.20 10 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1.90 0 7 -10 4.30 1.70 -1 -7 -10 10.60 2.40 1 -7 10 6.10 2.40 1 7 10 4.90 2.10 -1 7 -10 6.90 1.80 -2 -7 -10 2.40 2.00 2 -7 10 2.10 2.00 2 7 10 2.60 2.10 -2 7 -10 1.70 1.50 -3 -7 -10 1.90 1.80 3 -7 10 -0.10 1.90 -3 7 -10 0.80 1.50 3 7 10 2.10 2.00 -4 -7 -10 -1.30 1.50 4 -7 10 1.00 2.10 -4 7 -10 0.00 1.40 4 7 10 -2.20 1.80 5 -7 10 1.30 2.40 -5 -7 -10 0.80 1.90 5 7 10 1.60 2.10 6 -7 10 9.40 3.00 6 7 10 8.00 3.00 7 -7 10 6.00 2.90 7 7 10 8.50 3.10 8 -7 10 1.10 2.60 8 7 10 -2.50 2.60 9 -7 10 -0.90 2.70 13 -8 -10 -1.60 2.10 13 -8 -10 1.00 3.00 13 -8 -10 2.90 1.90 13 8 -10 1.40 2.40 12 -8 -10 2.70 2.40 12 -8 -10 -1.60 2.70 -12 -8 10 2.70 2.60 12 -8 -10 -0.80 1.70 12 8 -10 2.60 2.20 11 -8 -10 -0.20 1.50 11 -8 -10 -1.40 2.00 -11 -8 10 -1.80 2.40 11 -8 -10 -2.20 2.30 -11 -8 10 2.70 2.30 11 8 -10 0.60 2.20 10 -8 -10 -1.90 2.20 -10 -8 10 -2.10 1.60 -10 -8 10 4.70 2.70 10 -8 -10 0.50 1.60 10 8 -10 2.70 2.20 -9 -8 10 -1.70 2.00 -9 -8 10 2.80 1.80 9 -8 -10 -1.30 2.30 9 -8 -10 2.00 1.60 9 8 -10 2.00 1.70 8 -8 -10 1.90 2.30 8 -8 -10 2.60 1.60 -8 -8 10 -2.10 1.90 -8 -8 10 -1.80 1.70 8 8 -10 2.40 2.10 7 -8 -10 2.40 1.90 7 -8 -10 0.60 1.40 -7 -8 10 1.80 2.00 -7 -8 10 1.20 1.50 7 8 -10 1.20 1.80 6 -8 -10 -0.80 1.40 6 -8 -10 -1.90 1.80 -6 -8 10 -1.00 1.30 -6 -8 10 -0.40 2.00 6 8 -10 -1.70 1.70 5 -8 -10 0.10 2.00 5 -8 -10 2.50 1.70 -5 -8 10 1.10 1.50 -5 -8 10 -0.30 1.90 -5 8 10 -1.10 1.30 5 8 -10 0.60 1.80 4 -8 -10 0.10 1.50 -4 -8 10 -3.10 1.60 4 -8 -10 1.20 1.90 -4 8 10 -0.80 1.50 4 8 -10 -0.40 1.70 -3 -8 10 3.00 2.20 3 -8 -10 0.60 1.70 3 -8 -10 4.70 2.20 -3 8 10 5.40 1.90 3 8 -10 3.00 1.90 2 -8 -10 21.60 2.90 -2 -8 10 19.70 3.10 2 8 -10 26.10 3.30 -2 8 10 22.30 2.90 1 -8 -10 4.40 2.00 -1 -8 10 2.80 2.40 1 8 -10 1.20 1.70 -1 8 10 5.20 2.00 0 -8 -10 1.30 1.90 0 -8 10 1.70 2.10 0 8 10 4.10 1.90 0 8 -10 1.00 1.50 -1 -8 -10 3.00 1.90 1 -8 10 1.30 2.00 1 8 10 0.20 1.70 -1 8 -10 1.20 1.50 2 -8 10 7.00 2.60 -2 -8 -10 6.90 2.30 -2 8 -10 0.50 1.60 2 8 10 4.20 2.20 -3 -8 -10 1.50 2.00 3 -8 10 3.40 2.60 3 8 10 2.90 2.20 -3 8 -10 3.80 1.80 -4 -8 -10 -2.30 1.70 4 -8 10 0.00 2.30 -4 8 -10 -1.30 1.50 4 8 10 2.00 2.30 -5 -8 -10 -0.90 2.30 5 -8 10 5.80 2.90 5 8 10 2.80 2.30 6 -8 10 2.30 2.80 6 8 10 0.70 2.40 7 -8 10 3.70 3.20 7 8 10 0.10 2.50 12 -9 -10 -0.50 2.40 12 -9 -10 -6.20 2.80 12 -9 -10 -0.10 1.80 12 9 -10 1.90 2.50 -11 -9 10 -0.30 2.10 11 -9 -10 -1.90 2.60 11 -9 -10 6.70 2.70 11 -9 -10 0.70 1.80 11 9 -10 0.40 2.30 -10 -9 10 3.10 2.20 10 -9 -10 4.20 3.10 10 -9 -10 1.10 1.80 10 9 -10 0.70 2.40 -9 -9 10 2.90 2.30 -9 -9 10 0.50 2.90 9 -9 -10 0.40 1.60 9 -9 -10 2.60 2.80 9 9 -10 -0.80 2.10 -8 -9 10 10.50 3.00 8 -9 -10 12.70 2.30 8 -9 -10 8.40 3.10 -8 -9 10 12.70 2.60 8 9 -10 12.30 3.00 7 -9 -10 10.40 2.20 -7 -9 10 6.70 2.20 -7 -9 10 9.60 2.60 7 -9 -10 15.90 3.30 7 9 -10 14.00 2.80 -6 -9 10 14.80 3.00 6 -9 -10 22.40 2.80 6 -9 -10 22.10 3.70 -6 -9 10 21.20 3.00 6 9 -10 20.70 3.60 -5 -9 10 3.20 1.80 5 -9 -10 7.60 2.50 5 -9 -10 3.70 1.90 -5 -9 10 5.40 2.40 5 9 -10 5.90 2.40 4 -9 -10 27.70 3.20 -4 -9 10 22.30 3.40 -4 -9 10 21.00 2.70 4 -9 -10 20.30 3.50 4 9 -10 22.50 3.40 -4 9 10 22.50 2.90 3 -9 -10 20.00 3.30 -3 -9 10 15.30 3.10 3 -9 -10 17.80 2.70 -3 9 10 19.20 2.70 3 9 -10 19.50 3.10 -2 -9 10 22.60 3.40 2 -9 -10 19.20 3.00 2 9 -10 21.60 3.10 -2 9 10 18.90 2.80 1 -9 -10 1.40 1.80 -1 -9 10 -2.10 1.90 -1 9 10 0.40 1.50 1 9 -10 1.20 1.80 0 -9 10 3.10 2.60 0 -9 -10 8.20 2.30 0 9 10 4.60 2.30 0 9 -10 1.80 1.80 1 -9 10 3.70 2.70 -1 -9 -10 0.40 1.80 1 9 10 -1.90 1.90 -1 9 -10 0.30 1.60 2 -9 10 4.30 2.80 -2 -9 -10 -0.30 1.90 -2 9 -10 0.60 1.60 2 9 10 3.10 2.40 3 -9 10 4.70 2.60 -3 -9 -10 0.40 2.10 3 9 10 3.30 2.30 -3 9 -10 2.00 2.00 -4 -9 -10 0.40 2.10 4 -9 10 0.00 2.30 -4 9 -10 -0.60 1.80 4 9 10 0.90 2.30 -5 -9 -10 -3.30 2.20 5 -9 10 2.70 2.60 5 9 10 -1.40 2.20 6 -9 10 -3.80 2.20 6 9 10 0.80 2.50 10 -10 -10 0.60 1.90 10 -10 -10 0.00 3.20 -10 -10 10 0.40 2.20 10 10 -10 -1.40 2.20 9 -10 -10 -1.50 2.80 9 -10 -10 1.10 1.70 -9 -10 10 -1.40 1.80 9 10 -10 3.60 2.50 8 -10 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3.10 5 4 -11 42.10 3.70 -5 4 11 46.50 3.40 4 -4 -11 9.00 2.00 4 -4 -11 6.90 2.00 -4 -4 11 6.00 2.20 -4 4 11 8.10 1.70 -4 4 11 8.20 2.00 4 4 -11 8.20 1.70 4 4 -11 6.70 1.90 4 4 -11 7.30 1.70 3 -4 -11 8.70 1.90 -3 -4 11 11.90 2.50 3 -4 -11 13.60 2.10 -3 4 11 11.30 2.30 -3 4 11 11.40 1.80 3 4 -11 13.30 2.20 3 4 -11 15.00 2.00 -2 -4 11 66.79 4.80 2 -4 -11 63.49 3.80 2 -4 -11 67.09 4.00 2 4 -11 59.49 3.90 -2 4 11 69.09 3.60 -2 4 11 59.39 4.10 -1 -4 11 281.67 12.20 1 -4 -11 307.87 11.70 1 -4 -11 299.97 11.30 1 4 -11 292.67 11.40 -1 4 11 309.27 11.10 -1 4 11 302.07 12.00 0 -4 11 30.10 3.40 0 -4 -11 35.60 2.60 0 -4 -11 35.60 3.20 0 4 -11 34.80 2.70 0 4 11 33.50 2.60 0 4 11 31.30 3.30 1 -4 11 5.70 2.00 -1 -4 -11 8.30 1.90 1 -4 11 7.00 1.60 -1 -4 -11 5.70 1.40 1 4 11 8.10 1.50 1 4 11 6.80 2.20 -1 4 -11 5.10 1.50 2 -4 11 2.50 1.80 2 -4 11 -2.10 1.10 -2 -4 -11 3.60 1.60 2 4 11 -1.70 1.00 -2 4 -11 0.30 1.00 2 4 11 -1.10 1.50 3 -4 11 5.20 2.20 -3 -4 -11 13.80 2.30 3 -4 11 11.90 2.00 3 4 11 9.60 1.70 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-5 11 -3.40 1.90 11 -5 -11 -0.20 1.40 -11 -5 11 2.80 1.70 11 5 -11 1.30 1.90 11 5 -11 1.20 1.70 11 5 -11 -1.60 1.30 -10 -5 11 -0.70 1.50 10 -5 -11 0.90 1.60 10 -5 -11 1.20 2.20 -10 -5 11 1.20 2.30 10 -5 -11 0.60 1.70 10 5 -11 2.90 1.90 10 5 -11 -0.30 1.20 10 5 -11 2.70 2.20 -9 -5 11 1.10 1.50 -9 -5 11 3.30 2.30 9 -5 -11 2.30 1.50 9 -5 -11 -0.20 2.10 9 5 -11 0.50 1.80 9 5 -11 -0.40 1.80 9 5 -11 0.00 1.00 -8 -5 11 106.69 6.30 8 -5 -11 94.69 5.80 8 -5 -11 98.19 5.30 8 5 -11 100.39 5.80 8 5 -11 93.29 5.60 7 -5 -11 23.90 2.70 -7 -5 11 27.90 3.50 7 -5 -11 27.20 3.40 7 5 -11 27.10 3.20 7 5 -11 22.90 2.90 -6 -5 11 44.40 4.20 6 -5 -11 50.49 4.00 6 -5 -11 48.80 3.50 6 5 -11 47.90 4.10 6 5 -11 53.69 3.80 -6 5 11 52.69 3.60 5 -5 -11 1.60 1.40 5 -5 -11 1.40 1.50 -5 -5 11 4.10 2.00 5 5 -11 5.20 1.70 -5 5 11 3.30 1.70 5 5 -11 2.80 1.50 -4 -5 11 8.20 2.30 4 -5 -11 8.50 1.80 4 -5 -11 8.50 2.10 4 5 -11 8.80 2.10 -4 5 11 8.10 2.10 -4 5 11 7.50 1.60 3 -5 -11 9.90 2.00 3 -5 -11 8.00 2.00 -3 -5 11 6.90 2.30 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-0.10 2.90 -1 3 20 0.00 2.60 0 -3 20 3.10 3.40 0 3 20 11.90 3.60 1 -3 20 1.70 3.30 1 3 20 -3.70 2.30 11 -4 -20 -3.40 2.50 -11 -4 20 2.50 3.30 11 4 -20 0.70 2.20 11 4 -20 -1.10 2.30 -11 4 20 6.20 2.70 -10 -4 20 -0.80 3.20 10 -4 -20 -2.40 2.40 10 4 -20 0.40 2.00 -10 4 20 -2.70 2.40 10 4 -20 -0.80 2.20 -9 -4 20 2.90 3.30 9 -4 -20 7.50 3.10 -9 4 20 8.70 2.90 9 4 -20 3.70 2.60 -8 -4 20 -0.70 3.00 8 -4 -20 -5.20 2.30 -8 4 20 -2.50 2.20 8 4 -20 -2.90 1.90 7 -4 -20 -5.20 2.10 -7 -4 20 -2.40 2.70 7 4 -20 0.30 1.80 -7 4 20 2.60 3.30 -6 -4 20 -1.00 2.90 6 4 -20 4.50 2.20 -5 -4 20 -2.50 2.70 5 4 -20 -0.40 1.80 -5 4 20 0.60 2.30 -4 -4 20 1.20 3.10 4 4 -20 -1.40 1.80 -4 4 20 -3.90 2.20 -3 -4 20 -3.70 2.70 3 4 -20 -2.30 1.40 -3 4 20 -0.70 2.30 -2 -4 20 5.90 3.40 -2 4 20 -1.90 2.40 -1 -4 20 -0.50 3.20 -1 4 20 -1.80 2.50 0 -4 20 -5.70 2.80 0 4 20 2.60 2.80 9 -5 -20 -2.60 2.50 -9 -5 20 -3.30 3.10 9 5 -20 2.60 2.60 8 -5 -20 -0.60 2.50 -8 -5 20 -3.80 3.00 8 5 -20 1.50 2.20 7 -5 -20 -1.00 2.60 -7 -5 20 0.60 3.30 7 5 -20 3.10 2.10 -6 -5 20 -3.40 2.90 6 -5 -20 -5.20 2.20 -6 5 20 -3.50 2.00 6 5 -20 1.10 1.80 -5 -5 20 -1.40 3.00 -5 5 20 0.60 2.60 5 5 -20 6.70 2.40 -4 -5 20 3.30 3.50 4 5 -20 2.60 2.00 -4 5 20 5.00 2.90 -3 -5 20 -1.80 3.20 3 5 -20 0.70 1.90 -3 5 20 -1.30 2.50 -2 -5 20 1.30 3.30 -2 5 20 -2.30 2.50 -6 -6 20 0.00 3.20 6 -6 -20 -5.70 2.50 6 6 -20 -2.30 1.60 -6 6 20 2.20 2.30 -5 -6 20 -2.30 3.30 -5 6 20 5.40 2.80 5 6 -20 -0.60 1.90 -11 0 21 0.70 3.50 11 0 -21 0.50 2.80 10 0 -21 -0.10 2.20 -10 0 21 1.20 2.90 9 0 -21 1.30 2.30 -9 0 21 1.10 3.00 -8 0 21 3.50 3.20 -7 0 21 -1.80 2.60 -6 0 21 -2.70 2.90 -5 0 21 0.70 2.90 -4 0 21 -3.00 2.60 -3 0 21 -1.60 2.20 -3 0 21 -1.20 3.00 -2 0 21 -5.70 2.40 -2 0 21 3.70 2.90 -1 0 21 2.10 2.60 -1 0 21 -5.10 2.40 0 0 21 -0.50 2.90 0 0 21 -5.60 2.70 11 -1 -21 3.90 2.80 -11 -1 21 2.00 3.20 -11 1 21 0.50 3.10 11 1 -21 -1.10 2.20 10 -1 -21 3.90 2.60 -10 -1 21 4.00 3.70 10 1 -21 3.90 2.40 -10 1 21 5.80 3.30 9 -1 -21 6.60 2.80 -9 -1 21 0.60 3.10 -9 1 21 6.80 3.30 -8 -1 21 3.00 3.20 -8 1 21 -1.30 2.70 -7 -1 21 0.80 3.00 -7 1 21 -1.20 2.80 -6 -1 21 1.20 3.10 -6 1 21 -3.90 3.00 -5 -1 21 5.20 3.20 -5 1 21 5.80 3.50 -4 -1 21 -2.20 2.70 -4 1 21 0.50 3.10 -3 -1 21 -0.20 2.90 3 1 -21 -5.10 1.50 -3 1 21 -5.10 2.40 -3 1 21 1.10 2.50 -2 -1 21 -0.90 2.70 -2 1 21 2.30 2.80 -2 1 21 2.00 3.00 -1 -1 21 -1.60 2.30 -1 -1 21 -3.90 2.80 -1 1 21 -3.40 2.90 -1 1 21 2.90 2.80 0 -1 21 -3.90 3.20 0 -1 21 -0.10 2.90 0 1 21 -5.70 2.30 0 1 21 -0.10 2.50 11 -2 -21 5.50 3.00 -11 -2 21 -0.60 3.20 11 2 -21 1.90 2.40 -11 2 21 7.90 3.70 10 -2 -21 27.40 4.20 -10 -2 21 30.50 5.30 10 2 -21 36.10 4.20 -10 2 21 26.50 4.60 9 -2 -21 27.10 4.00 -9 -2 21 25.00 4.70 -9 2 21 33.70 4.90 -8 -2 21 3.20 3.40 -8 2 21 4.50 3.30 -7 -2 21 1.90 3.20 -7 2 21 -1.20 2.80 -6 -2 21 -2.10 2.90 6 2 -21 -4.20 1.90 -6 2 21 -1.20 2.80 -5 -2 21 -1.80 2.90 -5 2 21 0.00 2.90 5 2 -21 -1.30 2.00 -4 -2 21 8.60 3.90 4 2 -21 7.20 2.40 -4 2 21 7.40 3.30 -4 2 21 9.10 3.30 -3 -2 21 3.00 3.20 3 2 -21 0.20 1.70 -3 2 21 -1.20 2.50 -3 2 21 2.20 3.00 -2 -2 21 -2.30 2.80 -2 2 21 -7.90 2.40 -2 2 21 -0.60 2.60 -1 -2 21 -1.60 3.20 -1 2 21 0.60 2.70 10 -3 -21 0.60 3.00 -10 -3 21 0.80 3.30 -10 3 21 -1.30 2.50 10 3 -21 0.50 2.40 9 -3 -21 0.50 2.30 -9 -3 21 4.50 3.50 -9 3 21 -1.00 2.70 9 3 -21 0.90 2.40 -8 -3 21 3.10 3.40 8 -3 -21 3.50 2.80 -8 3 21 0.80 2.90 8 3 -21 -0.80 2.20 -7 -3 21 -1.00 3.20 7 3 -21 5.90 2.50 -7 3 21 8.60 3.20 -6 -3 21 -8.60 2.40 -6 3 21 -2.90 2.40 6 3 -21 -3.50 2.00 -5 -3 21 4.70 3.30 -5 3 21 1.60 2.60 -5 3 21 2.10 2.50 5 3 -21 -1.00 1.80 -4 -3 21 -5.90 2.60 4 3 -21 2.80 2.20 -4 3 21 1.20 2.80 -3 -3 21 1.10 3.10 3 3 -21 3.40 2.10 -3 3 21 0.20 2.70 -2 -3 21 -7.80 3.00 -2 3 21 0.90 2.90 -1 -3 21 -0.90 3.10 -9 -4 21 2.10 3.60 9 -4 -21 -0.20 2.80 9 4 -21 2.30 2.50 8 -4 -21 1.00 2.70 -8 -4 21 -1.50 3.10 8 4 -21 4.00 2.40 -7 -4 21 -4.30 3.00 7 4 -21 -0.20 2.00 -6 -4 21 -0.10 3.50 6 4 -21 -3.10 2.00 -5 -4 21 1.80 3.30 5 4 -21 0.10 1.80 -5 4 21 -0.30 2.70 -4 -4 21 -6.00 3.20 4 4 -21 1.40 1.70 -4 4 21 1.80 3.00 -3 -4 21 0.80 3.30 -3 4 21 -1.80 2.50 -9 0 22 30.70 5.00 -8 0 22 -1.90 2.90 -7 0 22 -1.00 3.30 -6 0 22 -0.10 3.00 -5 0 22 -2.30 2.80 -4 0 22 6.70 3.40 -3 0 22 -4.60 3.10 -9 -1 22 7.10 4.10 -9 1 22 -1.40 2.90 -8 -1 22 -2.90 3.20 -8 1 22 -4.30 2.70 -7 -1 22 9.00 3.60 -7 1 22 4.60 3.20 -6 -1 22 -0.20 3.10 -6 1 22 1.90 3.30 -5 -1 22 6.60 3.60 -5 1 22 1.90 2.90 -4 -1 22 9.00 3.70 -4 1 22 1.50 3.40 -3 -1 22 0.40 2.90 -3 1 22 -5.50 2.30 -3 1 22 3.10 3.00 -8 -2 22 -4.40 2.70 -8 2 22 -0.60 2.60 8 2 -22 -6.00 2.00 -7 -2 22 -3.00 2.90 -7 2 22 -1.50 2.60 7 2 -22 -3.40 2.10 -6 -2 22 0.20 3.20 -6 2 22 -5.70 2.70 6 2 -22 -1.60 2.10 -5 -2 22 0.80 3.10 5 2 -22 -2.90 2.10 -5 2 22 -3.40 2.70 -4 -2 22 -5.30 2.60 4 2 -22 -1.50 1.90 -4 2 22 -0.70 3.00 -4 2 22 -0.90 2.50 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 15163 _shelx_res_file ; TITL EL15_D568_DRX3_AK6_a.res in P2(1)/c CELL 0.71073 12.0411 8.9698 15.5832 90.000 110.721 90.000 ZERR 4.00 0.0013 0.0009 0.0018 0.000 0.003 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H O UNIT 80 80 8 MERG 2 OMIT 1 0 0 SHEL 50 0.74 FMAP 2 PLAN 10 ACTA BOND $H L.S. 10 TEMP 23.00 WGHT 0.054600 0.249700 EXTI 0.008762 FVAR 0.57332 C1 1 0.646528 0.607085 0.838265 11.00000 0.05195 0.04087 = 0.03524 0.00045 0.00615 -0.00275 C2 1 0.522925 0.641223 0.830299 11.00000 0.05537 0.03492 = 0.03279 -0.00142 0.01378 -0.00293 C3 1 0.490256 0.629278 0.907610 11.00000 0.07051 0.04867 = 0.03536 -0.00130 0.01674 -0.00505 AFIX 43 H3 2 0.546769 0.601668 0.963569 11.00000 -1.20000 AFIX 0 C4 1 0.376070 0.657691 0.902118 11.00000 0.08123 0.06623 = 0.04709 -0.00302 0.03557 -0.00059 AFIX 43 H4 2 0.355190 0.648613 0.953913 11.00000 -1.20000 AFIX 0 C5 1 0.292050 0.699946 0.819099 11.00000 0.06410 0.07212 = 0.05776 -0.00216 0.03110 0.00813 AFIX 43 H5 2 0.214446 0.719141 0.815029 11.00000 -1.20000 AFIX 0 C6 1 0.323213 0.713664 0.742299 11.00000 0.05404 0.05785 = 0.04285 0.00001 0.01793 0.00754 AFIX 43 H6 2 0.266152 0.742884 0.686974 11.00000 -1.20000 AFIX 0 C7 1 0.437930 0.684712 0.746086 11.00000 0.05111 0.03466 = 0.03542 -0.00279 0.01496 0.00021 C8 1 0.472604 0.697548 0.662329 11.00000 0.04753 0.04266 = 0.03244 0.00517 0.01188 0.00815 AFIX 13 H8 2 0.420547 0.771739 0.621343 11.00000 -1.20000 AFIX 0 C9 1 0.600290 0.753345 0.689389 11.00000 0.05152 0.04637 = 0.04215 0.00802 0.01698 0.00261 AFIX 23 H9A 2 0.623094 0.754158 0.635601 11.00000 -1.20000 H9B 2 0.604729 0.854882 0.711781 11.00000 -1.20000 AFIX 0 C10 1 0.686183 0.657230 0.762521 11.00000 0.04614 0.04067 = 0.03766 -0.00047 0.00863 -0.00430 C11 1 0.792686 0.609798 0.764593 11.00000 0.04503 0.04772 = 0.04352 0.00204 0.00428 -0.00321 AFIX 43 H11 2 0.831520 0.547888 0.813992 11.00000 -1.20000 AFIX 0 C12 1 0.859113 0.637031 0.703936 11.00000 0.03670 0.04945 = 0.04606 -0.00184 0.00601 -0.00510 C13 1 0.844234 0.758549 0.645321 11.00000 0.04234 0.04439 = 0.06631 0.00180 0.01509 -0.00167 AFIX 43 H13 2 0.788421 0.831033 0.643986 11.00000 -1.20000 AFIX 0 C14 1 0.910240 0.774453 0.588966 11.00000 0.04433 0.05025 = 0.05919 0.00685 0.01188 -0.00531 AFIX 43 H14 2 0.897772 0.856081 0.549881 11.00000 -1.20000 AFIX 0 C15 1 0.994425 0.669182 0.590865 11.00000 0.04132 0.06110 = 0.05069 -0.00334 0.01096 -0.00441 C16 1 1.013638 0.549146 0.650501 11.00000 0.05196 0.06735 = 0.07396 0.01172 0.02268 0.01574 AFIX 43 H16 2 1.071513 0.478824 0.653144 11.00000 -1.20000 AFIX 0 C17 1 0.947207 0.534365 0.705502 11.00000 0.04895 0.06370 = 0.06174 0.01672 0.01200 0.00962 AFIX 43 H17 2 0.961162 0.453377 0.745188 11.00000 -1.20000 AFIX 0 C18 1 0.457300 0.550306 0.609352 11.00000 0.05502 0.05581 = 0.03960 -0.00568 0.01385 0.00726 AFIX 23 H18A 2 0.489430 0.562744 0.560829 11.00000 -1.20000 H18B 2 0.504242 0.474428 0.650753 11.00000 -1.20000 AFIX 0 C19 1 0.331441 0.494397 0.567232 11.00000 0.06348 0.06834 = 0.06140 -0.01727 0.00420 0.00165 AFIX 33 H19A 2 0.330336 0.405183 0.532907 11.00000 -1.50000 H19C 2 0.283290 0.569219 0.527062 11.00000 -1.50000 H19B 2 0.300594 0.473204 0.614917 11.00000 -1.50000 AFIX 0 O2 3 1.064140 0.672544 0.538348 11.00000 0.06422 0.08285 = 0.07170 0.00936 0.03200 0.00640 C20 1 1.052971 0.795022 0.478436 11.00000 0.08134 0.09450 = 0.07476 0.01655 0.03667 -0.00096 AFIX 33 H20A 2 1.107085 0.782849 0.446150 11.00000 -1.50000 H20B 2 1.071120 0.885680 0.513398 11.00000 -1.50000 H20C 2 0.973140 0.799516 0.435169 11.00000 -1.50000 AFIX 0 O1 3 0.712941 0.540134 0.905681 11.00000 0.06274 0.07451 = 0.04231 0.01659 0.00681 0.00789 HKLF 4 REM EL15_D568_DRX3_AK6_a.res in P2(1)/c REM R1 = 0.0462 for 2552 Fo > 4sig(Fo) and 0.0843 for all 4068 data REM 200 parameters refined using 0 restraints END WGHT 0.0546 0.2497 REM Highest difference peak 0.160, deepest hole -0.150, 1-sigma level 0.043 Q1 1 0.6670 0.6407 0.7940 11.00000 0.05 0.16 Q2 1 0.4999 0.6342 0.8635 11.00000 0.05 0.16 Q3 1 0.9186 0.6820 0.5640 11.00000 0.05 0.15 Q4 1 0.2390 0.5451 0.5519 11.00000 0.05 0.15 Q5 1 0.6473 0.6792 0.7237 11.00000 0.05 0.15 Q6 1 0.4965 0.6873 0.7982 11.00000 0.05 0.15 Q7 1 0.8168 0.6406 0.7280 11.00000 0.05 0.14 Q8 1 0.4382 0.6926 0.9044 11.00000 0.05 0.14 Q9 1 0.4633 0.6988 0.7094 11.00000 0.05 0.14 Q10 1 0.8791 0.5621 0.6814 11.00000 0.05 0.14 ; _shelx_res_checksum 48933 _shelxl_version_number .2013 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy C C1 0.64653(13) 0.60708(16) 0.83826(9) 0.0452(3) Uani d 1 C C2 0.52292(13) 0.64122(14) 0.83030(9) 0.0415(3) Uani d 1 C C3 0.49026(15) 0.62928(17) 0.90761(10) 0.0520(4) Uani d 1 H H3 0.5468 0.6017 0.9636 0.062 Uiso calc 1 C C4 0.37607(17) 0.65769(19) 0.90212(11) 0.0614(4) Uani d 1 H H4 0.3552 0.6486 0.9539 0.074 Uiso calc 1 C C5 0.29205(16) 0.6999(2) 0.81910(12) 0.0621(4) Uani d 1 H H5 0.2144 0.7191 0.8150 0.075 Uiso calc 1 C C6 0.32321(14) 0.71366(17) 0.74230(10) 0.0514(4) Uani d 1 H H6 0.2662 0.7429 0.6870 0.062 Uiso calc 1 C C7 0.43793(12) 0.68471(14) 0.74609(9) 0.0405(3) Uani d 1 C C8 0.47260(12) 0.69755(15) 0.66233(9) 0.0415(3) Uani d 1 H H8 0.4205 0.7717 0.6213 0.050 Uiso calc 1 C C9 0.60029(13) 0.75335(16) 0.68939(10) 0.0466(4) Uani d 1 H H9A 0.6231 0.7542 0.6356 0.056 Uiso calc 1 H H9B 0.6047 0.8549 0.7118 0.056 Uiso calc 1 C C10 0.68618(12) 0.65723(15) 0.76252(9) 0.0432(3) Uani d 1 C C11 0.79269(12) 0.60980(17) 0.76459(10) 0.0485(4) Uani d 1 H H11 0.8315 0.5479 0.8140 0.058 Uiso calc 1 C C12 0.85911(12) 0.63703(16) 0.70394(10) 0.0464(3) Uani d 1 C C13 0.84423(13) 0.75855(17) 0.64532(11) 0.0521(4) Uani d 1 H H13 0.7884 0.8310 0.6440 0.063 Uiso calc 1 C C14 0.91024(13) 0.77445(17) 0.58897(11) 0.0530(4) Uani d 1 H H14 0.8978 0.8561 0.5499 0.064 Uiso calc 1 C C15 0.99443(13) 0.66918(18) 0.59086(11) 0.0525(4) Uani d 1 C C16 1.01364(15) 0.5491(2) 0.65050(12) 0.0643(5) Uani d 1 H H16 1.0715 0.4788 0.6531 0.077 Uiso calc 1 C C17 0.94721(14) 0.53437(19) 0.70550(12) 0.0602(4) Uani d 1 H H17 0.9612 0.4534 0.7452 0.072 Uiso calc 1 C C18 0.45730(13) 0.55031(17) 0.60935(10) 0.0509(4) Uani d 1 H H18A 0.4894 0.5627 0.5608 0.061 Uiso calc 1 H H18B 0.5042 0.4744 0.6508 0.061 Uiso calc 1 C C19 0.33144(15) 0.4944(2) 0.56723(12) 0.0692(5) Uani d 1 H H19A 0.3303 0.4052 0.5329 0.104 Uiso calc 1 H H19C 0.2833 0.5692 0.5271 0.104 Uiso calc 1 H H19B 0.3006 0.4732 0.6149 0.104 Uiso calc 1 O O2 1.06414(11) 0.67254(15) 0.53835(9) 0.0708(4) Uani d 1 C C20 1.05297(19) 0.7950(2) 0.47844(14) 0.0811(6) Uani d 1 H H20A 1.1071 0.7828 0.4462 0.122 Uiso calc 1 H H20B 1.0711 0.8857 0.5134 0.122 Uiso calc 1 H H20C 0.9731 0.7995 0.4352 0.122 Uiso calc 1 O O1 0.71294(10) 0.54013(13) 0.90568(7) 0.0630(3) Uani d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0520(8) 0.0409(7) 0.0352(7) -0.0027(6) 0.0061(6) 0.0005(6) C2 0.0554(8) 0.0349(7) 0.0328(7) -0.0029(6) 0.0138(6) -0.0014(5) C3 0.0705(11) 0.0487(8) 0.0354(7) -0.0050(7) 0.0167(7) -0.0013(6) C4 0.0812(12) 0.0662(11) 0.0471(9) -0.0006(9) 0.0356(9) -0.0030(8) C5 0.0641(10) 0.0721(11) 0.0578(10) 0.0081(8) 0.0311(9) -0.0022(9) C6 0.0540(9) 0.0578(9) 0.0428(8) 0.0075(7) 0.0179(7) 0.0000(7) C7 0.0511(8) 0.0347(7) 0.0354(7) 0.0002(6) 0.0150(6) -0.0028(6) C8 0.0475(8) 0.0427(7) 0.0324(7) 0.0081(6) 0.0119(6) 0.0052(6) C9 0.0515(8) 0.0464(8) 0.0421(8) 0.0026(6) 0.0170(7) 0.0080(6) C10 0.0461(8) 0.0407(7) 0.0377(7) -0.0043(6) 0.0086(6) -0.0005(6) C11 0.0450(8) 0.0477(8) 0.0435(8) -0.0032(6) 0.0043(6) 0.0020(6) C12 0.0367(7) 0.0495(8) 0.0461(8) -0.0051(6) 0.0060(6) -0.0018(7) C13 0.0423(8) 0.0444(8) 0.0663(10) -0.0017(6) 0.0151(7) 0.0018(7) C14 0.0443(8) 0.0502(9) 0.0592(9) -0.0053(7) 0.0119(7) 0.0068(7) C15 0.0413(8) 0.0611(9) 0.0507(9) -0.0044(7) 0.0110(7) -0.0033(7) C16 0.0520(10) 0.0674(11) 0.0740(11) 0.0157(8) 0.0227(9) 0.0117(9) C17 0.0490(9) 0.0637(10) 0.0617(10) 0.0096(7) 0.0120(8) 0.0167(8) C18 0.0550(9) 0.0558(9) 0.0396(8) 0.0073(7) 0.0138(7) -0.0057(7) C19 0.0635(11) 0.0683(11) 0.0614(10) 0.0017(9) 0.0042(9) -0.0173(9) O2 0.0642(7) 0.0829(9) 0.0717(8) 0.0064(6) 0.0320(6) 0.0094(7) C20 0.0813(14) 0.0945(15) 0.0748(13) -0.0010(11) 0.0367(11) 0.0165(11) O1 0.0627(7) 0.0745(8) 0.0423(6) 0.0079(6) 0.0068(5) 0.0166(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O1 C1 C2 120.23(13) O1 C1 C10 122.05(14) C2 C1 C10 117.72(12) C3 C2 C7 119.51(14) C3 C2 C1 119.53(13) C7 C2 C1 120.95(12) C4 C3 C2 120.93(14) C4 C3 H3 119.5 C2 C3 H3 119.5 C3 C4 C5 119.65(15) C3 C4 H4 120.2 C5 C4 H4 120.2 C6 C5 C4 120.12(16) C6 C5 H5 119.9 C4 C5 H5 119.9 C5 C6 C7 121.25(15) C5 C6 H6 119.4 C7 C6 H6 119.4 C6 C7 C2 118.54(13) C6 C7 C8 121.70(12) C2 C7 C8 119.76(13) C7 C8 C9 110.23(11) C7 C8 C18 112.49(12) C9 C8 C18 110.38(11) C7 C8 H8 107.9 C9 C8 H8 107.9 C18 C8 H8 107.9 C10 C9 C8 112.04(11) C10 C9 H9A 109.2 C8 C9 H9A 109.2 C10 C9 H9B 109.2 C8 C9 H9B 109.2 H9A C9 H9B 107.9 C11 C10 C1 117.18(13) C11 C10 C9 126.41(13) C1 C10 C9 116.38(12) C10 C11 C12 132.10(14) C10 C11 H11 114.0 C12 C11 H11 114.0 C13 C12 C17 116.60(14) C13 C12 C11 125.69(14) C17 C12 C11 117.70(14) C14 C13 C12 121.82(15) C14 C13 H13 119.1 C12 C13 H13 119.1 C15 C14 C13 119.92(15) C15 C14 H14 120.0 C13 C14 H14 120.0 O2 C15 C14 125.17(15) O2 C15 C16 115.27(15) C14 C15 C16 119.56(15) C17 C16 C15 119.89(15) C17 C16 H16 120.1 C15 C16 H16 120.1 C16 C17 C12 122.17(15) C16 C17 H17 118.9 C12 C17 H17 118.9 C19 C18 C8 115.56(13) C19 C18 H18A 108.4 C8 C18 H18A 108.4 C19 C18 H18B 108.4 C8 C18 H18B 108.4 H18A C18 H18B 107.5 C18 C19 H19A 109.5 C18 C19 H19C 109.5 H19A C19 H19C 109.5 C18 C19 H19B 109.5 H19A C19 H19B 109.5 H19C C19 H19B 109.5 C15 O2 C20 118.51(14) O2 C20 H20A 109.5 O2 C20 H20B 109.5 H20A C20 H20B 109.5 O2 C20 H20C 109.5 H20A C20 H20C 109.5 H20B C20 H20C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance C1 O1 1.2285(16) C1 C2 1.481(2) C1 C10 1.491(2) C2 C3 1.3975(19) C2 C7 1.4040(19) C3 C4 1.371(2) C3 H3 0.9300 C4 C5 1.384(2) C4 H4 0.9300 C5 C6 1.381(2) C5 H5 0.9300 C6 C7 1.386(2) C6 H6 0.9300 C7 C8 1.5089(18) C8 C9 1.528(2) C8 C18 1.5337(19) C8 H8 0.9800 C9 C10 1.5092(19) C9 H9A 0.9700 C9 H9B 0.9700 C10 C11 1.341(2) C11 C12 1.459(2) C11 H11 0.9300 C12 C13 1.392(2) C12 C17 1.398(2) C13 C14 1.385(2) C13 H13 0.9300 C14 C15 1.378(2) C14 H14 0.9300 C15 O2 1.3644(19) C15 C16 1.387(2) C16 C17 1.370(2) C16 H16 0.9300 C17 H17 0.9300 C18 C19 1.508(2) C18 H18A 0.9700 C18 H18B 0.9700 C19 H19A 0.9600 C19 H19C 0.9600 C19 H19B 0.9600 O2 C20 1.417(2) C20 H20A 0.9600 C20 H20B 0.9600 C20 H20C 0.9600 _cod_database_fobs_code 2240790