#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:10:00 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181908 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/08/2240850.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240850 _cell_angle_alpha 89.620 _cell_angle_beta 89.260 _cell_angle_gamma 82.730 _cell_length_a 9.7060 _cell_length_b 10.6430 _cell_length_c 25.0730 _exptl_crystal_F_000 1180.00 _reflns_d_resolution_high 0.7093 _cod_data_source_file zs2332Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' u3348 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 269.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7829.93 8696.64 59.89 o 3 0 0 3995.18 4187.39 22.19 o 4 0 0 3066.68 2609.01 20.56 o 5 0 0 9237.89 9032.21 100.06 o 6 0 0 1.99 6.97 7.76 o 7 0 0 1428.55 1544.78 33.52 o 8 0 0 1320.52 1378.08 35.00 o 9 0 0 2576.32 2472.71 83.60 o 10 0 0 77.47 51.14 24.57 o 11 0 0 181.07 247.69 43.13 o 12 0 0 5.65 9.31 40.44 o -12 1 0 840.36 953.60 64.24 o -11 1 0 3078.10 3642.96 94.58 o -10 1 0 6703.37 7320.72 120.08 o -9 1 0 2623.45 2513.34 69.20 o -8 1 0 27.28 31.52 14.50 o -7 1 0 7609.78 7693.98 107.93 o -6 1 0 10067.35 10115.44 147.23 o -5 1 0 3016.76 3374.56 43.15 o -4 1 0 10295.85 11548.29 96.47 o -3 1 0 6212.86 6943.63 76.70 o -2 1 0 1628.41 2135.65 27.76 o -1 1 0 3028.83 3539.23 110.60 o 2 1 0 496.23 529.96 7.69 o 3 1 0 8725.25 9713.97 39.30 o 4 1 0 11951.29 11658.39 91.71 o 5 1 0 38.34 92.83 11.59 o 6 1 0 68.02 54.09 9.01 o 7 1 0 1863.75 1883.38 44.55 o 8 1 0 558.52 513.24 26.03 o 9 1 0 1.74 11.64 21.18 o 10 1 0 24.91 9.67 24.43 o 11 1 0 1151.50 1036.54 40.22 o 12 1 0 1665.30 1840.51 75.10 o -12 2 0 344.16 420.11 52.36 o -11 2 0 172.86 211.46 44.22 o -10 2 0 75.71 28.65 38.53 o -9 2 0 135.53 100.87 34.95 o -8 2 0 4.17 22.97 16.41 o -7 2 0 1891.84 1896.18 33.80 o -6 2 0 940.46 850.45 27.96 o -5 2 0 363.12 366.76 24.74 o -4 2 0 2.00 23.80 9.80 o -3 2 0 9885.28 10805.75 78.47 o -2 2 0 20832.26 15706.85 388.95 o -1 2 0 1189.88 1442.55 15.63 o 0 2 0 30208.86 34807.39 110.91 o 1 2 0 7299.02 7693.65 94.62 o 2 2 0 7541.49 7547.58 86.16 o 3 2 0 3915.03 3710.99 20.60 o 4 2 0 3063.28 2912.74 33.01 o 5 2 0 15579.99 15959.29 97.24 o 6 2 0 6005.99 5648.03 122.91 o 7 2 0 1377.90 1211.32 30.92 o 8 2 0 2993.47 3132.62 51.90 o 9 2 0 758.14 735.02 31.00 o 10 2 0 597.52 614.91 32.00 o 11 2 0 97.63 140.83 27.12 o 12 2 0 889.21 1002.21 44.00 o -11 3 0 23.58 11.61 32.99 o -10 3 0 268.45 306.04 43.56 o -9 3 0 1521.96 1601.42 60.63 o -8 3 0 116.30 155.83 31.84 o -7 3 0 318.84 307.91 28.59 o -6 3 0 4298.41 4356.96 64.55 o -5 3 0 5062.81 5310.00 76.56 o -4 3 0 220.56 106.73 9.66 o -3 3 0 3705.07 4335.86 27.75 o -2 3 0 1335.69 1143.02 33.55 o -1 3 0 6450.63 5633.18 356.98 o 0 3 0 10881.74 12120.09 131.61 o 1 3 0 16537.58 18120.12 133.28 o 2 3 0 14392.89 14072.02 85.07 o 3 3 0 38189.77 43024.33 82.02 o 4 3 0 6997.46 6676.87 38.88 o 5 3 0 990.38 1046.41 15.61 o 6 3 0 5504.45 5276.17 56.32 o 7 3 0 3222.11 3102.01 59.24 o 8 3 0 914.33 896.75 30.47 o 9 3 0 19.86 39.24 20.42 o 10 3 0 1345.63 1298.91 40.49 o 11 3 0 397.75 391.49 32.91 o 12 3 0 6.24 17.13 27.04 o -11 4 0 270.38 236.24 41.79 o -10 4 0 19.85 38.28 37.93 o -9 4 0 110.06 132.75 37.12 o -8 4 0 8373.53 8768.87 119.97 o -7 4 0 6138.67 6247.00 239.15 o -6 4 0 631.55 569.73 21.96 o -5 4 0 375.22 339.21 14.72 o -4 4 0 12370.14 13400.52 167.90 o -3 4 0 2964.27 2846.16 31.44 o -2 4 0 519.55 622.15 16.24 o -1 4 0 11216.49 11475.31 111.81 o 0 4 0 3944.88 3771.54 36.29 o 1 4 0 123.91 164.50 11.73 o 2 4 0 3150.17 3723.75 26.33 o 3 4 0 43.53 68.76 7.79 o 4 4 0 0.07 8.72 7.83 o 5 4 0 3993.46 3835.47 51.94 o 6 4 0 10302.67 10578.00 58.05 o 7 4 0 7125.28 7145.85 43.16 o 8 4 0 142.60 119.52 20.59 o 9 4 0 1725.20 1730.57 41.45 o 10 4 0 2572.61 2611.63 52.03 o 11 4 0 1213.93 1397.96 85.98 o 12 4 0 52.71 66.39 36.59 o -11 5 0 292.14 284.42 45.98 o -10 5 0 276.21 307.77 46.18 o -9 5 0 71.63 65.91 37.33 o -8 5 0 323.21 216.36 36.49 o -7 5 0 1.14 13.93 16.57 o -6 5 0 301.84 264.62 19.93 o -5 5 0 555.95 570.26 16.23 o -4 5 0 3481.15 3511.39 39.84 o -3 5 0 309.12 261.52 14.84 o -2 5 0 562.36 508.24 21.79 o -1 5 0 22204.30 23826.24 151.95 o 0 5 0 35717.16 41571.25 417.99 o 1 5 0 3483.99 3385.34 26.87 o 2 5 0 909.90 933.25 28.89 o 3 5 0 15927.69 16101.27 140.71 o 4 5 0 5127.61 4856.66 32.06 o 5 5 0 4683.90 4729.79 32.59 o 6 5 0 339.91 274.04 12.74 o 7 5 0 2248.88 2415.39 31.97 o 8 5 0 4536.85 4632.22 54.42 o 9 5 0 2506.88 2679.78 49.34 o 10 5 0 475.30 411.10 49.21 o 11 5 0 735.04 623.63 132.31 o 12 5 0 808.39 815.65 39.50 o -10 6 0 1749.99 1329.64 62.74 o -9 6 0 762.37 695.63 51.38 o -8 6 0 485.21 526.52 45.86 o -7 6 0 3666.85 3964.82 82.51 o -6 6 0 5033.95 5159.55 105.54 o -5 6 0 2673.06 2844.58 36.87 o -4 6 0 326.90 375.50 30.86 o -3 6 0 3243.46 3379.87 39.17 o -2 6 0 6456.51 6648.69 50.60 o -1 6 0 1961.92 2009.61 65.60 o 0 6 0 122.63 124.79 12.93 o 1 6 0 663.48 672.22 24.07 o 2 6 0 1224.66 1233.32 19.64 o 3 6 0 18.72 13.03 10.32 o 4 6 0 1071.58 941.16 26.78 o 5 6 0 2418.03 2439.88 30.49 o 6 6 0 417.57 393.85 14.37 o 7 6 0 235.71 263.10 14.61 o 8 6 0 243.39 194.46 18.14 o 9 6 0 35.72 21.48 16.41 o 10 6 0 188.84 206.01 42.82 o 11 6 0 374.27 365.61 46.35 o 12 6 0 885.01 925.11 59.79 o -10 7 0 30.00 87.98 39.62 o -9 7 0 317.72 220.32 39.86 o -8 7 0 242.53 254.59 39.55 o -7 7 0 1.96 15.97 31.36 o -6 7 0 413.53 438.90 24.80 o -5 7 0 3174.44 3238.36 38.37 o -4 7 0 886.29 890.32 20.86 o -3 7 0 565.86 572.89 16.66 o 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407.13 361.31 46.75 o -5 9 0 2861.23 2868.01 69.50 o -4 9 0 3899.54 4269.08 80.38 o -3 9 0 3439.78 3702.00 74.55 o -2 9 0 3031.95 2843.94 65.40 o -1 9 0 2966.86 2992.81 66.56 o 0 9 0 2758.87 2765.11 63.77 o 1 9 0 719.23 614.45 40.05 o 2 9 0 2755.69 2884.87 67.09 o 3 9 0 989.46 1047.61 46.57 o 4 9 0 471.79 491.80 36.85 o 5 9 0 26.14 15.08 27.67 o 6 9 0 1745.12 1718.45 41.95 o 7 9 0 731.74 751.80 32.83 o 8 9 0 179.12 165.34 23.79 o 9 9 0 169.28 132.83 32.95 o 10 9 0 102.78 115.61 34.53 o -5 10 0 27.75 46.09 26.56 o -4 10 0 689.41 750.29 44.27 o -3 10 0 2.26 -7.05 28.61 o -2 10 0 1220.97 1214.43 50.79 o -1 10 0 327.92 314.71 35.66 o 0 10 0 1263.36 1381.78 51.79 o 1 10 0 1084.83 1122.74 49.65 o 2 10 0 1410.61 1388.34 52.80 o 3 10 0 5028.51 5097.60 92.63 o 4 10 0 446.03 525.03 41.79 o 5 10 0 2813.77 3005.50 78.26 o 6 10 0 292.77 325.50 40.48 o 7 10 0 305.29 342.89 42.07 o 8 10 0 2265.57 2488.47 76.97 o 9 10 0 1143.15 945.92 53.53 o 10 10 0 43.16 70.58 38.58 o -5 11 0 438.55 452.57 43.19 o 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0 177.47 202.27 42.86 o 5 13 0 402.89 398.73 50.15 o -5 -13 1 2772.14 2983.04 90.38 o -4 -13 1 165.95 156.79 45.03 o -3 -13 1 35.65 47.48 41.20 o -2 -13 1 956.97 959.73 60.28 o -1 -13 1 3658.13 2726.41 81.80 o 0 -13 1 1210.20 753.21 49.43 o 1 -13 1 89.53 53.76 30.75 o 2 -13 1 991.56 1151.35 61.37 o 3 -13 1 561.40 556.92 50.85 o -8 -12 1 99.07 122.86 43.27 o -7 -12 1 695.60 805.85 57.29 o -6 -12 1 102.18 124.79 40.05 o -5 -12 1 31.91 46.91 35.15 o -4 -12 1 1314.91 1250.47 61.59 o -3 -12 1 521.35 524.81 49.35 o -2 -12 1 49.65 77.41 38.67 o -1 -12 1 63.85 67.32 37.08 o 0 -12 1 33.36 -2.90 35.86 o 1 -12 1 84.46 86.87 38.97 o 2 -12 1 2084.08 2173.94 73.14 o 3 -12 1 1938.82 1425.21 61.45 o 4 -12 1 520.87 443.85 45.77 o -9 -11 1 151.34 174.16 41.40 o -8 -11 1 2133.96 2176.89 77.59 o -7 -11 1 994.14 1085.95 59.57 o -6 -11 1 224.21 193.32 37.71 o -5 -11 1 1722.16 1623.40 64.27 o -4 -11 1 3193.96 3335.71 84.49 o -3 -11 1 3469.19 3527.00 84.97 o -2 -11 1 621.72 583.68 46.69 o -1 -11 1 3461.88 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377.33 42.79 o -9 -7 1 820.77 708.23 186.79 o -8 -7 1 6993.12 7696.14 64.37 o -7 -7 1 5477.29 5668.66 93.31 o -6 -7 1 652.92 670.91 23.74 o -5 -7 1 1.61 2.48 10.05 o -4 -7 1 4946.57 4843.13 143.84 o -3 -7 1 5727.00 5559.12 57.14 o -2 -7 1 185.12 162.09 11.22 o -1 -7 1 50.70 53.43 8.95 o 0 -7 1 100.30 60.59 8.96 o 1 -7 1 477.63 485.77 13.71 o 2 -7 1 587.84 546.18 25.49 o 3 -7 1 533.45 527.39 16.36 o 4 -7 1 514.57 482.64 22.05 o 5 -7 1 354.75 351.06 22.67 o 6 -7 1 2691.78 2904.38 47.68 o 7 -7 1 2787.84 3042.93 76.51 o 8 -7 1 300.33 331.83 41.79 o 9 -7 1 48.91 69.15 40.50 o 10 -7 1 809.79 873.36 57.98 o -12 -6 1 529.36 537.29 52.12 o -11 -6 1 2.05 55.16 41.42 o -10 -6 1 351.50 353.26 28.68 o -9 -6 1 84.13 64.84 16.17 o -8 -6 1 375.29 432.92 20.49 o -7 -6 1 2.72 5.46 11.84 o -6 -6 1 14.22 12.71 10.24 o -5 -6 1 404.23 392.16 26.09 o -4 -6 1 4445.53 4412.00 72.97 o -3 -6 1 2314.98 2190.49 43.70 o -2 -6 1 31.73 32.66 8.83 o -1 -6 1 2766.71 2623.21 89.06 o 0 -6 1 15193.82 15705.85 86.03 o 1 -6 1 9524.84 9761.13 103.12 o 2 -6 1 1047.59 1062.45 24.06 o 3 -6 1 233.29 222.01 20.14 o 4 -6 1 5156.76 5491.01 53.29 o 5 -6 1 6256.77 6267.10 59.82 o 6 -6 1 666.76 681.61 66.26 o 7 -6 1 1675.41 1678.41 37.86 o 8 -6 1 5814.89 6011.86 107.07 o 9 -6 1 3202.94 3428.20 88.97 o 10 -6 1 367.62 289.82 41.05 o -12 -5 1 389.07 309.56 31.55 o -11 -5 1 1229.62 1181.76 228.25 o -10 -5 1 3935.45 4097.75 76.24 o -9 -5 1 5426.34 5563.00 54.53 o -8 -5 1 98.59 102.27 15.89 o -7 -5 1 2660.41 2598.19 54.39 o -6 -5 1 4945.03 5012.48 37.46 o -5 -5 1 1694.97 1644.45 20.61 o -4 -5 1 363.26 387.47 11.67 o -3 -5 1 11068.76 11126.39 111.27 o -2 -5 1 12013.27 12567.28 109.29 o -1 -5 1 8880.52 9056.09 118.16 o 0 -5 1 1608.79 1814.84 25.99 o 1 -5 1 2045.94 2238.94 27.60 o 2 -5 1 1720.64 1628.41 25.37 o 3 -5 1 238.80 272.92 15.28 o 4 -5 1 1602.55 1683.61 37.52 o 5 -5 1 4223.66 4413.24 47.02 o 6 -5 1 929.07 956.82 27.51 o 7 -5 1 45.67 36.82 17.75 o 8 -5 1 34.75 46.78 32.27 o 9 -5 1 289.09 316.51 42.52 o 10 -5 1 259.98 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