#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:11:09 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181909 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/09/2240902.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240902 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.2846 _cell_length_b 13.8914 _cell_length_c 19.5592 _exptl_crystal_F_000 752.00 _reflns_d_resolution_high 0.8007 _cod_data_source_file hg5449Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' chico' _shelx_refln_list_code 4 _shelx_f_calc_maximum 163.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7423.70 7153.96 24.27 o 4 0 0 266.70 265.03 7.41 o 6 0 0 317.50 335.59 4.57 o 1 1 0 1828.43 1815.83 8.43 o 2 1 0 776.68 686.81 5.39 o 3 1 0 0.39 7.21 0.98 o 4 1 0 642.55 662.34 8.30 o 5 1 0 254.32 244.27 2.84 o 6 1 0 454.11 470.48 5.32 o 7 1 0 63.31 61.30 1.90 o 0 2 0 243.96 221.05 3.37 o 1 2 0 147.29 148.58 2.73 o 2 2 0 213.39 212.69 5.04 o 3 2 0 335.11 386.87 5.33 o 4 2 0 96.53 104.26 4.65 o 5 2 0 16.70 13.59 0.84 o 6 2 0 85.30 95.32 2.38 o 7 2 0 37.01 34.85 1.48 o 1 3 0 4.78 7.55 2.93 o 2 3 0 3.53 2.73 0.59 o 3 3 0 1312.49 1404.75 14.47 o 4 3 0 179.25 170.77 6.00 o 5 3 0 234.14 215.48 3.22 o 6 3 0 718.17 759.33 9.66 o 7 3 0 380.20 402.64 4.99 o 0 4 0 9663.17 7660.69 27.30 o 1 4 0 5988.98 5350.38 100.28 o 2 4 0 0.95 3.65 0.60 o 3 4 0 5228.13 5573.06 29.44 o 4 4 0 132.20 122.20 5.13 o 5 4 0 47.23 61.83 3.27 o 6 4 0 4614.18 4508.65 12.28 o 7 4 0 534.35 544.92 5.71 o 1 5 0 1793.13 1683.47 10.85 o 2 5 0 1125.86 1248.54 15.97 o 3 5 0 791.91 778.68 9.19 o 4 5 0 79.10 98.28 2.56 o 5 5 0 109.13 86.88 1.79 o 6 5 0 285.40 248.58 4.86 o 7 5 0 0.07 -0.03 0.30 o 0 6 0 969.84 916.49 11.55 o 1 6 0 195.81 194.74 5.83 o 2 6 0 109.94 105.77 3.12 o 3 6 0 7.23 8.80 1.05 o 4 6 0 8.72 8.15 0.49 o 5 6 0 53.13 44.15 2.13 o 6 6 0 0.97 0.48 0.46 o 7 6 0 5.15 4.02 0.50 o 1 7 0 475.16 464.68 6.56 o 2 7 0 261.50 290.59 7.85 o 3 7 0 1437.68 1468.95 13.29 o 4 7 0 327.63 333.58 5.52 o 5 7 0 118.42 128.83 3.66 o 6 7 0 3.05 3.42 0.66 o 7 7 0 4.61 4.21 0.47 o 0 8 0 4103.19 3978.27 28.54 o 1 8 0 541.36 560.44 7.59 o 2 8 0 499.70 494.01 8.58 o 3 8 0 471.25 464.75 5.57 o 4 8 0 64.22 71.21 2.68 o 5 8 0 405.74 411.61 6.50 o 6 8 0 91.23 101.41 2.84 o 1 9 0 90.81 94.84 3.31 o 2 9 0 39.32 51.28 3.84 o 3 9 0 383.71 368.81 5.81 o 4 9 0 150.65 141.49 3.82 o 5 9 0 101.14 98.81 3.13 o 6 9 0 26.29 24.56 1.33 o 0 10 0 84.10 85.12 4.56 o 1 10 0 4.20 6.80 1.35 o 2 10 0 448.33 413.92 6.15 o 3 10 0 375.04 379.21 6.19 o 4 10 0 21.38 21.26 1.53 o 5 10 0 220.05 234.62 4.64 o 6 10 0 13.88 16.65 0.98 o 1 11 0 114.85 107.70 1.86 o 2 11 0 252.56 246.92 4.74 o 3 11 0 32.78 34.26 1.90 o 4 11 0 59.00 63.33 2.53 o 5 11 0 101.98 105.66 2.85 o 6 11 0 1.11 0.70 0.23 o 0 12 0 1127.62 1113.17 9.20 o 1 12 0 38.46 38.53 1.21 o 2 12 0 26.51 30.42 1.66 o 3 12 0 747.28 790.01 8.52 o 4 12 0 14.10 12.72 1.08 o 5 12 0 7.47 10.35 0.79 o 1 13 0 46.65 52.36 4.74 o 2 13 0 61.67 64.46 2.25 o 3 13 0 422.31 431.82 5.68 o 4 13 0 28.33 31.24 0.98 o 5 13 0 56.90 59.07 1.37 o 0 14 0 184.75 182.89 3.50 o 1 14 0 5.46 4.77 0.43 o 2 14 0 54.62 54.30 1.33 o 3 14 0 0.29 0.79 0.34 o 4 14 0 210.64 198.16 1.91 o 1 15 0 244.40 253.12 3.71 o 2 15 0 3.77 3.15 0.32 o 3 15 0 80.18 82.30 1.40 o 0 16 0 282.08 263.33 3.83 o 1 16 0 9.31 10.31 0.62 o 2 16 0 3.11 3.86 0.92 o 1 17 0 51.23 48.69 1.28 o 1 0 1 5644.97 4833.68 117.90 o 2 0 1 69.29 97.60 3.16 o 3 0 1 1381.17 1384.28 9.86 o 4 0 1 968.22 1037.97 13.25 o 5 0 1 34.70 31.51 1.34 o 6 0 1 9.51 10.18 0.87 o 7 0 1 248.09 255.98 3.87 o -7 1 1 69.16 73.48 1.64 o -6 1 1 147.02 151.48 3.24 o -5 1 1 104.15 104.76 2.47 o -4 1 1 175.49 194.50 6.41 o -3 1 1 171.32 181.44 3.63 o -2 1 1 2798.09 2721.76 18.12 o -1 1 1 2939.25 2674.51 23.78 o 0 1 1 1227.40 1104.20 5.63 o 1 1 1 2946.53 2650.30 10.42 o 2 1 1 2801.39 2807.54 10.79 o 3 1 1 168.55 179.37 3.54 o 4 1 1 176.23 192.04 4.47 o 5 1 1 103.82 102.43 2.39 o 6 1 1 145.97 150.00 3.13 o 7 1 1 71.61 76.08 1.34 o -7 2 1 95.55 96.12 1.51 o -6 2 1 21.01 23.61 1.29 o -5 2 1 0.89 0.61 0.21 o -4 2 1 155.11 168.45 6.03 o -3 2 1 350.37 391.32 7.71 o -2 2 1 6.77 8.83 0.97 o -1 2 1 126.33 128.06 2.68 o 0 2 1 131.07 111.40 1.14 o 1 2 1 124.84 132.76 1.73 o 2 2 1 7.26 8.48 0.63 o 3 2 1 346.65 390.51 5.27 o 4 2 1 155.50 166.47 4.18 o 5 2 1 1.00 0.73 0.29 o 6 2 1 20.95 23.00 0.94 o 7 2 1 95.73 99.64 2.39 o -7 3 1 33.19 33.50 0.89 o -6 3 1 165.04 157.70 3.87 o -5 3 1 241.56 225.76 4.03 o -4 3 1 18.44 17.61 2.08 o -3 3 1 953.81 1035.54 12.83 o -2 3 1 200.46 224.53 4.91 o -1 3 1 1370.43 1366.24 7.86 o 0 3 1 1733.02 1467.49 10.54 o 1 3 1 1372.39 1410.30 7.37 o 2 3 1 199.37 207.39 4.26 o 3 3 1 963.17 1055.20 12.23 o 4 3 1 18.16 17.09 1.90 o 5 3 1 240.06 229.95 3.55 o 6 3 1 164.95 153.90 4.31 o 7 3 1 32.08 30.77 1.36 o -7 4 1 281.95 274.49 6.86 o -6 4 1 204.90 197.67 4.31 o -5 4 1 243.56 249.11 2.67 o -4 4 1 115.31 118.27 5.17 o -3 4 1 1519.68 1571.33 16.10 o -2 4 1 28.07 29.07 1.79 o -1 4 1 425.74 371.68 4.65 o 0 4 1 264.39 269.18 9.46 o 1 4 1 430.97 373.93 5.53 o 2 4 1 28.26 25.07 1.33 o 3 4 1 1518.60 1598.36 15.40 o 4 4 1 116.16 122.99 5.00 o 5 4 1 244.48 252.54 3.46 o 6 4 1 205.76 200.70 4.19 o 7 4 1 279.92 280.42 4.00 o -7 5 1 41.98 34.71 1.43 o -6 5 1 127.97 122.44 3.39 o -5 5 1 342.45 330.67 7.61 o -4 5 1 174.55 197.05 7.64 o -3 5 1 22.27 22.91 12.39 o -2 5 1 372.73 401.44 7.91 o -1 5 1 1378.05 1324.85 6.65 o 0 5 1 1021.14 892.33 7.32 o 1 5 1 1377.99 1318.04 9.51 o 2 5 1 372.05 421.52 35.14 o 3 5 1 21.98 18.70 1.68 o 4 5 1 176.71 189.75 2.51 o 5 5 1 347.63 329.03 4.41 o 6 5 1 125.89 117.46 3.33 o 7 5 1 42.57 35.28 1.39 o -7 6 1 26.75 34.03 1.33 o -6 6 1 17.93 24.36 1.55 o -5 6 1 64.79 66.38 1.71 o -4 6 1 60.78 61.34 1.83 o -3 6 1 106.75 108.25 3.60 o -2 6 1 46.80 44.57 2.05 o -1 6 1 333.34 320.69 10.22 o 0 6 1 423.39 412.41 5.44 o 1 6 1 332.57 317.22 5.08 o 2 6 1 47.01 45.54 1.99 o 3 6 1 107.50 111.45 3.52 o 4 6 1 60.69 65.33 1.44 o 5 6 1 63.91 65.05 1.60 o 6 6 1 17.79 23.41 1.49 o 7 6 1 27.59 33.37 1.28 o -7 7 1 1.32 1.96 0.35 o -6 7 1 175.06 168.90 3.83 o -5 7 1 449.57 418.06 6.57 o -4 7 1 518.72 535.63 5.94 o -3 7 1 653.01 655.91 9.09 o -2 7 1 141.96 136.89 3.76 o -1 7 1 793.29 767.49 8.36 o 0 7 1 235.90 225.64 7.41 o 1 7 1 791.05 771.89 8.43 o 2 7 1 144.03 141.77 3.67 o 3 7 1 651.80 641.05 15.79 o 4 7 1 518.45 535.39 15.24 o 5 7 1 452.03 418.93 6.56 o 6 7 1 173.46 167.40 3.78 o 7 7 1 1.24 1.57 0.30 o -6 8 1 96.18 95.58 2.74 o -5 8 1 120.66 134.84 3.70 o -4 8 1 940.06 915.03 9.50 o -3 8 1 185.05 186.14 3.42 o -2 8 1 14.74 18.30 1.43 o -1 8 1 173.11 162.69 4.08 o 0 8 1 661.36 695.66 18.58 o 1 8 1 170.54 165.45 4.13 o 2 8 1 14.96 19.64 2.53 o 3 8 1 186.85 184.46 3.58 o 4 8 1 942.11 927.98 9.65 o 5 8 1 120.73 131.23 3.68 o 6 8 1 95.39 93.51 2.73 o -6 9 1 58.59 60.58 2.04 o -5 9 1 13.35 13.40 1.19 o -4 9 1 757.09 769.42 8.77 o -3 9 1 1563.41 1503.94 14.37 o -2 9 1 73.70 75.56 4.17 o -1 9 1 128.88 130.62 3.85 o 0 9 1 187.53 220.53 7.25 o 1 9 1 130.31 134.46 5.92 o 2 9 1 73.53 86.81 5.23 o 3 9 1 1557.11 1491.51 53.88 o 4 9 1 763.50 771.68 9.05 o 5 9 1 13.18 13.32 1.21 o 6 9 1 58.65 59.91 2.05 o -6 10 1 35.06 34.34 1.38 o -5 10 1 17.78 18.35 1.33 o -4 10 1 23.47 22.43 1.55 o -3 10 1 287.51 273.26 3.50 o -2 10 1 62.45 60.47 5.02 o -1 10 1 22.06 18.36 0.90 o 0 10 1 133.32 130.46 4.54 o 1 10 1 22.51 20.86 1.50 o 2 10 1 62.54 60.74 4.12 o 3 10 1 286.63 276.08 5.38 o 4 10 1 23.16 23.16 1.61 o 5 10 1 18.07 20.18 1.41 o 6 10 1 34.07 33.18 1.35 o -6 11 1 23.69 25.06 0.91 o -5 11 1 110.44 116.90 2.96 o -4 11 1 110.39 104.69 3.19 o -3 11 1 91.91 101.95 2.16 o -2 11 1 1190.74 1178.26 27.28 o -1 11 1 85.54 83.01 1.74 o 0 11 1 417.56 388.37 5.49 o 1 11 1 85.30 84.03 2.30 o 2 11 1 1194.49 1215.68 10.64 o 3 11 1 92.62 96.51 3.21 o 4 11 1 111.38 106.63 3.30 o 5 11 1 110.46 114.69 2.96 o 6 11 1 23.66 25.30 0.93 o -5 12 1 439.43 444.49 4.80 o -4 12 1 107.91 111.61 2.97 o -3 12 1 496.11 491.62 12.10 o -2 12 1 455.40 446.93 4.21 o -1 12 1 10.19 9.26 0.89 o 0 12 1 29.80 33.33 0.92 o 1 12 1 10.15 8.61 0.88 o 2 12 1 458.91 458.64 6.43 o 3 12 1 493.56 489.19 6.79 o 4 12 1 107.66 107.13 3.01 o 5 12 1 438.42 425.49 15.74 o -5 13 1 143.58 122.01 1.86 o -4 13 1 111.92 114.11 1.86 o -3 13 1 621.22 617.71 4.58 o -2 13 1 263.99 282.64 4.52 o -1 13 1 153.76 149.83 3.39 o 0 13 1 37.81 38.27 1.21 o 1 13 1 154.15 152.29 3.40 o 2 13 1 263.70 283.33 4.82 o 3 13 1 625.85 628.61 6.95 o 4 13 1 112.90 115.19 2.67 o 5 13 1 143.07 131.00 2.08 o -4 14 1 1.80 2.02 0.22 o -3 14 1 67.05 70.02 1.86 o -2 14 1 131.73 134.06 3.12 o -1 14 1 26.12 29.18 1.00 o 0 14 1 226.96 218.47 2.68 o 1 14 1 26.51 28.77 1.01 o 2 14 1 134.86 132.91 2.05 o 3 14 1 65.63 68.41 1.98 o 4 14 1 1.62 1.98 0.24 o -3 15 1 21.64 22.05 0.71 o -2 15 1 63.75 63.54 1.27 o -1 15 1 16.06 13.98 0.61 o 0 15 1 57.55 62.37 1.91 o 1 15 1 15.93 14.64 0.96 o 2 15 1 64.31 63.96 2.41 o 3 15 1 20.75 20.40 0.84 o -2 16 1 0.64 0.90 0.31 o -1 16 1 370.82 372.51 4.86 o 0 16 1 227.16 216.39 2.18 o 1 16 1 371.61 361.42 2.65 o 2 16 1 0.75 1.29 0.28 o -1 17 1 166.09 153.78 2.21 o 1 17 1 168.29 155.23 2.27 o 0 0 2 2521.96 2200.58 7.30 o 1 0 2 4149.57 3800.38 9.08 o 2 0 2 465.28 470.35 4.50 o 3 0 2 2.89 10.54 6.44 o 4 0 2 5.24 12.02 1.60 o 5 0 2 170.35 176.22 3.26 o 6 0 2 20.12 21.54 1.27 o 7 0 2 96.71 99.34 1.58 o -7 1 2 569.16 583.25 5.50 o -6 1 2 72.50 71.40 2.32 o -5 1 2 37.34 39.02 1.56 o -4 1 2 42.91 48.16 3.27 o -3 1 2 1179.16 1319.51 49.18 o -2 1 2 1291.17 1302.45 7.73 o -1 1 2 1016.95 942.57 7.27 o 0 1 2 1303.23 1178.70 7.88 o 1 1 2 1011.06 1002.30 9.36 o 2 1 2 1296.68 1286.57 7.35 o 3 1 2 1168.26 1292.31 9.38 o 4 1 2 41.57 49.46 2.28 o 5 1 2 37.01 36.50 1.50 o 6 1 2 72.18 70.58 1.62 o 7 1 2 569.76 567.99 4.79 o -7 2 2 18.21 18.91 0.71 o -6 2 2 93.32 87.00 2.55 o -5 2 2 223.29 238.89 3.85 o -4 2 2 746.77 790.30 13.31 o -3 2 2 1182.99 1285.76 14.19 o -2 2 2 887.74 915.30 9.85 o -1 2 2 2419.26 2305.96 12.03 o 0 2 2 1370.33 1282.29 5.55 o 1 2 2 2421.72 2354.09 13.73 o 2 2 2 892.38 873.67 6.05 o 3 2 2 1184.21 1296.08 20.00 o 4 2 2 741.44 771.57 8.94 o 5 2 2 222.68 226.15 2.84 o 6 2 2 92.70 88.60 1.82 o 7 2 2 18.62 19.83 0.67 o -7 3 2 111.66 102.06 1.71 o -6 3 2 784.57 768.45 7.49 o -5 3 2 26.58 25.41 1.30 o -4 3 2 296.97 282.81 8.09 o -3 3 2 1244.79 1374.17 15.02 o -2 3 2 533.56 559.44 8.10 o -1 3 2 1854.47 1763.78 8.84 o 0 3 2 6214.27 5043.23 16.16 o 1 3 2 1855.70 1836.29 7.76 o 2 3 2 535.64 557.69 4.98 o 3 3 2 1255.76 1391.53 10.00 o 4 3 2 294.29 279.84 7.31 o 5 3 2 27.27 26.53 0.94 o 6 3 2 789.88 790.18 5.37 o 7 3 2 111.11 101.18 2.32 o -7 4 2 83.70 91.05 1.46 o -6 4 2 265.44 280.99 5.29 o -5 4 2 43.37 43.84 1.71 o -4 4 2 0.25 0.48 0.60 o -3 4 2 224.26 244.99 6.58 o -2 4 2 357.10 401.06 5.49 o -1 4 2 1599.94 1493.32 7.34 o 0 4 2 108.94 134.12 3.43 o 1 4 2 1594.96 1538.48 18.76 o 2 4 2 359.57 405.41 8.78 o 3 4 2 222.38 241.26 5.74 o 4 4 2 0.24 1.32 0.60 o 5 4 2 43.71 45.81 1.34 o 6 4 2 262.03 269.92 6.18 o 7 4 2 82.96 87.81 2.15 o -7 5 2 51.41 49.74 1.37 o -6 5 2 206.12 190.42 3.40 o -5 5 2 398.38 361.04 4.03 o -4 5 2 63.20 64.04 3.99 o -3 5 2 970.52 1059.40 10.99 o -2 5 2 845.20 895.28 8.79 o -1 5 2 2089.47 1989.36 15.57 o 0 5 2 551.86 496.25 16.58 o 1 5 2 2085.16 2015.91 20.84 o 2 5 2 844.72 944.16 8.17 o 3 5 2 977.06 1091.00 38.92 o 4 5 2 63.77 61.92 1.27 o 5 5 2 401.54 356.56 3.72 o 6 5 2 206.76 187.94 2.57 o 7 5 2 51.66 48.74 1.57 o -7 6 2 23.45 25.13 1.41 o -6 6 2 211.66 223.55 4.52 o -5 6 2 297.57 286.96 3.60 o -4 6 2 207.37 197.56 3.63 o -3 6 2 580.40 645.62 13.20 o -2 6 2 434.39 468.59 6.69 o -1 6 2 1689.73 1645.32 6.94 o 0 6 2 880.31 865.55 19.16 o 1 6 2 1694.81 1722.55 19.93 o 2 6 2 433.83 488.46 7.08 o 3 6 2 575.65 643.66 16.54 o 4 6 2 204.38 201.27 2.65 o 5 6 2 297.06 281.36 3.35 o 6 6 2 213.16 216.98 4.36 o 7 6 2 24.24 27.98 1.13 o -7 7 2 2.11 2.46 0.38 o -6 7 2 154.38 150.35 3.60 o -5 7 2 82.89 76.50 1.88 o -4 7 2 187.69 200.24 4.64 o -3 7 2 242.52 256.16 7.55 o -2 7 2 801.30 753.30 8.78 o -1 7 2 1230.10 1163.51 10.05 o 0 7 2 47.14 39.44 2.52 o 1 7 2 1230.81 1197.73 17.44 o 2 7 2 805.21 775.59 15.99 o 3 7 2 239.68 239.74 9.97 o 4 7 2 186.21 199.36 3.98 o 5 7 2 82.97 76.84 2.83 o 6 7 2 151.09 141.44 3.46 o 7 7 2 2.17 2.71 0.31 o -6 8 2 4.07 3.55 0.62 o -5 8 2 132.67 116.37 2.67 o -4 8 2 202.18 185.72 4.90 o -3 8 2 515.24 524.14 4.73 o -2 8 2 509.04 503.76 7.30 o -1 8 2 487.09 472.85 6.84 o 0 8 2 4.07 5.03 0.75 o 1 8 2 484.95 487.24 11.44 o 2 8 2 512.79 511.00 13.24 o 3 8 2 515.85 517.63 6.08 o 4 8 2 203.07 189.61 4.43 o 5 8 2 130.87 116.35 3.47 o 6 8 2 4.19 3.89 0.64 o -6 9 2 131.98 149.84 3.16 o -5 9 2 82.14 82.42 1.82 o -4 9 2 23.25 24.11 1.08 o -3 9 2 804.01 798.02 5.83 o -2 9 2 508.29 471.06 10.25 o -1 9 2 466.25 453.36 7.05 o 0 9 2 644.32 688.04 8.62 o 1 9 2 464.55 456.04 11.35 o 2 9 2 509.04 482.57 9.15 o 3 9 2 797.19 794.72 24.79 o 4 9 2 23.90 25.65 1.71 o 5 9 2 82.01 86.06 2.95 o 6 9 2 131.57 148.87 3.16 o -6 10 2 26.73 28.78 1.22 o -5 10 2 50.74 52.93 2.16 o -4 10 2 191.80 194.49 2.97 o -3 10 2 1972.14 1890.22 9.27 o -2 10 2 1162.50 1126.51 13.90 o -1 10 2 206.58 191.31 3.25 o 0 10 2 0.69 2.18 2.08 o 1 10 2 204.70 191.31 3.44 o 2 10 2 1161.13 1155.41 27.29 o 3 10 2 1977.83 1947.31 14.37 o 4 10 2 196.58 206.41 4.74 o 5 10 2 53.30 58.80 2.36 o 6 10 2 27.25 28.99 1.23 o -5 11 2 67.58 65.91 2.18 o -4 11 2 103.08 100.21 3.41 o -3 11 2 369.41 372.11 4.14 o -2 11 2 1933.51 1863.43 28.04 o -1 11 2 68.53 66.18 1.55 o 0 11 2 478.38 500.37 5.57 o 1 11 2 67.86 65.12 4.87 o 2 11 2 1938.79 1906.82 74.60 o 3 11 2 372.31 375.86 6.29 o 4 11 2 104.13 104.65 3.26 o 5 11 2 67.93 69.82 2.30 o 6 11 2 105.72 119.80 1.94 o -5 12 2 28.52 32.94 1.27 o -4 12 2 61.16 56.50 1.46 o -3 12 2 119.67 116.08 2.21 o -2 12 2 455.66 469.11 5.35 o -1 12 2 93.11 92.19 2.74 o 0 12 2 50.58 50.70 1.75 o 1 12 2 93.62 92.80 2.82 o 2 12 2 453.56 478.67 6.65 o 3 12 2 118.72 114.90 3.31 o 4 12 2 60.87 55.55 2.18 o 5 12 2 29.61 34.25 1.96 o -4 13 2 252.00 249.77 2.81 o -3 13 2 911.16 921.09 5.61 o -2 13 2 452.91 454.66 5.81 o -1 13 2 165.48 172.21 3.72 o 0 13 2 409.48 385.61 3.87 o 1 13 2 166.08 172.37 3.74 o 2 13 2 452.43 457.10 6.21 o 3 13 2 908.74 929.58 8.55 o 4 13 2 251.18 247.74 3.93 o 5 13 2 235.08 236.48 2.78 o -4 14 2 218.02 196.74 2.59 o -3 14 2 300.27 291.03 3.06 o -2 14 2 241.66 242.49 4.28 o -1 14 2 218.91 226.27 2.71 o 0 14 2 134.10 137.71 2.15 o 1 14 2 217.78 230.09 2.88 o 2 14 2 241.60 245.66 4.09 o 3 14 2 295.74 281.08 4.06 o 4 14 2 216.31 201.45 9.71 o -3 15 2 145.66 140.68 3.45 o -2 15 2 58.42 56.93 1.41 o -1 15 2 379.61 376.23 4.56 o 0 15 2 29.47 26.56 1.30 o 1 15 2 380.25 370.41 5.93 o 2 15 2 58.42 56.71 1.48 o 3 15 2 147.21 142.31 6.47 o -2 16 2 87.55 82.49 5.75 o -1 16 2 25.16 26.97 0.88 o 0 16 2 14.40 12.74 0.56 o 1 16 2 25.75 27.55 1.09 o 2 16 2 87.59 85.78 1.73 o 1 0 3 0.19 1.30 0.36 o 2 0 3 271.76 271.38 5.24 o 3 0 3 2.20 3.31 0.78 o 4 0 3 62.96 61.28 3.70 o 5 0 3 309.53 320.32 4.50 o 6 0 3 68.80 68.09 1.63 o 7 0 3 29.94 30.86 1.20 o -7 1 3 1.34 1.79 0.29 o -6 1 3 164.56 169.27 3.67 o -5 1 3 325.34 336.03 4.66 o -4 1 3 91.45 109.52 4.95 o -3 1 3 529.29 551.98 9.34 o -2 1 3 1093.59 1100.92 10.73 o -1 1 3 4577.24 4004.78 103.64 o 0 1 3 3406.58 3101.95 56.47 o 1 1 3 4565.06 4268.00 9.08 o 2 1 3 1099.43 1100.88 14.12 o 3 1 3 526.05 546.24 7.03 o 4 1 3 89.58 104.84 3.30 o 5 1 3 325.38 324.60 4.49 o 6 1 3 164.28 172.25 2.50 o 7 1 3 1.23 1.65 0.35 o -7 2 3 85.43 84.15 1.50 o -6 2 3 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