data_2240915 _cell_angle_alpha 85.403 _cell_angle_beta 73.421 _cell_angle_gamma 82.020 _cell_length_a 10.6663 _cell_length_b 14.3138 _cell_length_c 14.5728 _exptl_crystal_F_000 968.00 _reflns_d_resolution_high 0.8200 _cod_data_source_file wm5178Isup2.hkl _cod_data_source_block I _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 307.82 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 15929.14 13870.62 145.79 o 2 0 0 3814.69 3641.27 102.62 o 3 0 0 5136.85 5396.47 143.39 o 4 0 0 356.34 323.65 55.96 o 5 0 0 32.76 92.96 55.49 o 6 0 0 5.34 -18.23 42.14 o 7 0 0 108.67 77.95 39.41 o 8 0 0 400.10 370.32 40.21 o 9 0 0 387.88 400.48 61.94 o 10 0 0 51.52 194.26 43.33 o 11 0 0 463.98 511.81 31.82 o 12 0 0 287.94 242.26 30.22 o -12 1 0 70.44 109.99 38.74 o -11 1 0 24.99 -4.42 30.85 o -10 1 0 106.75 170.38 33.10 o -9 1 0 93.89 149.27 35.48 o -8 1 0 29.35 58.06 38.38 o -7 1 0 1359.40 1242.14 92.43 o -6 1 0 131.32 78.62 42.52 o -5 1 0 1458.47 1240.79 103.08 o -4 1 0 3.70 85.77 72.66 o -3 1 0 45.44 67.46 68.76 o -2 1 0 783.29 802.60 104.93 o -1 1 0 613.50 618.01 91.20 o 1 1 0 756.49 709.02 51.72 o 2 1 0 2034.72 1860.75 74.35 o 3 1 0 5424.77 4859.44 252.81 o 4 1 0 72.29 49.32 65.63 o 5 1 0 13.45 98.18 54.38 o 6 1 0 2976.04 2175.91 357.21 o 7 1 0 156.47 173.44 39.71 o 8 1 0 534.41 570.55 47.79 o 9 1 0 89.43 73.52 54.46 o 10 1 0 66.21 122.74 109.03 o 11 1 0 82.22 77.79 45.95 o 12 1 0 18.15 70.50 32.53 o -12 2 0 9.92 20.96 42.98 o -11 2 0 4.58 -18.72 31.20 o -10 2 0 32.88 41.87 32.61 o -9 2 0 1.10 -12.57 35.16 o -8 2 0 745.70 710.63 69.15 o -7 2 0 5.92 44.74 63.24 o -6 2 0 331.65 292.55 42.00 o -5 2 0 115.64 59.10 68.85 o -4 2 0 528.00 588.64 91.19 o -3 2 0 2418.86 2574.80 78.84 o -2 2 0 1079.67 977.11 85.62 o -1 2 0 5113.55 4629.08 488.90 o 0 2 0 183.30 239.34 59.34 o 1 2 0 87.40 239.49 59.45 o 2 2 0 506.28 473.99 80.28 o 3 2 0 630.30 569.59 53.71 o 4 2 0 1528.40 1556.33 56.91 o 5 2 0 4284.30 4428.21 74.54 o 6 2 0 742.76 735.00 44.27 o 7 2 0 32.27 26.56 40.06 o 8 2 0 198.86 248.13 39.25 o 9 2 0 177.49 219.22 36.84 o 10 2 0 1.89 -18.13 33.52 o 11 2 0 41.36 130.24 81.38 o 12 2 0 5.72 36.71 28.91 o -11 3 0 0.37 11.61 34.80 o -10 3 0 59.67 78.46 47.89 o -9 3 0 142.94 156.69 35.06 o -8 3 0 121.71 176.21 55.34 o -7 3 0 437.02 412.59 40.34 o -6 3 0 504.60 457.18 41.21 o -5 3 0 1320.44 1328.28 77.06 o -4 3 0 3224.96 3184.56 131.73 o -3 3 0 459.66 464.32 84.74 o -2 3 0 5.67 -14.64 75.58 o -1 3 0 2.22 14.08 68.53 o 0 3 0 663.25 689.43 69.85 o 1 3 0 3052.31 3192.26 227.02 o 2 3 0 10685.71 9633.12 1493.60 o 3 3 0 189.59 164.16 51.09 o 4 3 0 2530.89 2671.62 58.41 o 5 3 0 299.41 286.26 53.67 o 6 3 0 3557.69 3327.16 238.58 o 7 3 0 303.63 339.74 44.22 o 8 3 0 608.34 558.16 39.04 o 9 3 0 708.13 671.88 37.75 o 10 3 0 303.60 284.71 33.22 o 11 3 0 113.58 40.92 31.92 o 12 3 0 5.75 36.56 65.61 o -11 4 0 130.52 100.97 30.44 o -10 4 0 188.14 226.40 36.95 o -9 4 0 240.40 196.00 35.17 o -8 4 0 40.92 109.51 41.24 o -7 4 0 760.42 727.10 170.67 o -6 4 0 2.41 -1.23 38.39 o -5 4 0 635.44 626.45 60.23 o -4 4 0 536.96 581.72 72.44 o -3 4 0 8.15 -18.76 73.97 o -2 4 0 699.37 583.32 129.75 o -1 4 0 2894.14 2395.43 172.37 o 0 4 0 68.37 64.78 47.50 o 1 4 0 1228.26 1180.54 125.45 o 2 4 0 901.96 815.97 44.63 o 3 4 0 292.25 379.76 52.64 o 4 4 0 90.90 124.76 55.04 o 5 4 0 4051.48 3993.72 53.23 o 6 4 0 40.69 28.37 41.40 o 7 4 0 18.60 -32.53 58.70 o 8 4 0 299.00 163.83 85.23 o 9 4 0 43.12 22.33 36.58 o 10 4 0 2.10 -35.99 47.13 o 11 4 0 10.27 31.89 49.78 o 12 4 0 5.60 -11.50 32.43 o -11 5 0 0.08 22.63 29.99 o -10 5 0 13.25 29.01 31.00 o -9 5 0 79.40 77.75 52.40 o -8 5 0 47.78 -18.41 36.21 o -7 5 0 180.51 211.17 38.75 o -6 5 0 108.68 113.28 40.78 o -5 5 0 1058.53 1093.89 58.03 o -4 5 0 534.27 399.77 64.92 o -3 5 0 65.75 23.29 68.76 o -2 5 0 541.30 537.63 64.00 o -1 5 0 841.59 684.47 79.30 o 0 5 0 35.83 46.81 44.07 o 1 5 0 294.77 217.39 47.68 o 2 5 0 967.52 764.85 76.94 o 3 5 0 3156.88 3151.99 66.33 o 4 5 0 11.57 -6.73 51.86 o 5 5 0 2350.46 2386.23 63.59 o 6 5 0 434.28 394.12 43.94 o 7 5 0 75.35 90.21 38.12 o 8 5 0 112.78 149.17 37.96 o 9 5 0 76.24 96.52 51.08 o 10 5 0 169.61 215.87 32.63 o 11 5 0 27.98 -14.08 30.69 o 12 5 0 3.93 39.95 46.68 o -11 6 0 57.69 84.19 29.66 o -10 6 0 234.73 200.64 58.17 o -9 6 0 49.43 69.66 41.81 o -8 6 0 335.52 371.08 47.64 o -7 6 0 524.04 585.08 39.48 o -6 6 0 199.86 108.21 39.86 o -5 6 0 452.85 504.53 56.19 o -4 6 0 232.74 293.69 87.07 o -3 6 0 139.49 130.39 51.01 o -2 6 0 620.47 444.42 77.58 o -1 6 0 4099.36 4458.75 285.32 o 0 6 0 7354.06 7589.83 111.66 o 1 6 0 1083.12 914.59 47.36 o 2 6 0 3273.91 3333.78 173.44 o 3 6 0 2502.66 2382.40 76.52 o 4 6 0 2433.01 2372.26 50.33 o 5 6 0 1258.37 1360.96 52.56 o 6 6 0 1869.75 1245.94 147.63 o 7 6 0 29.73 20.45 48.05 o 8 6 0 7.62 32.78 51.71 o 9 6 0 146.43 164.18 34.92 o 10 6 0 46.58 59.52 33.27 o 11 6 0 108.64 129.07 31.30 o 12 6 0 27.87 80.48 32.74 o -10 7 0 92.44 87.73 30.86 o -9 7 0 13.94 41.56 31.67 o -8 7 0 45.42 73.66 35.04 o -7 7 0 232.65 192.66 46.02 o -6 7 0 162.48 145.37 44.03 o -5 7 0 961.09 806.09 125.58 o -4 7 0 693.13 585.12 46.67 o -3 7 0 3110.99 2875.73 118.55 o -2 7 0 1565.66 1446.84 52.77 o -1 7 0 4109.22 4332.79 243.11 o 0 7 0 2580.10 2561.19 131.70 o 1 7 0 981.92 951.86 82.67 o 2 7 0 56.85 62.39 39.96 o 3 7 0 0.08 44.28 45.09 o 4 7 0 1200.90 989.82 140.09 o 5 7 0 183.84 126.22 42.26 o 6 7 0 165.95 151.51 38.83 o 7 7 0 785.51 759.81 39.46 o 8 7 0 500.65 526.42 38.88 o 9 7 0 217.10 172.16 63.03 o 10 7 0 143.55 140.62 48.41 o 11 7 0 267.86 290.18 57.00 o -10 8 0 1.55 8.77 34.85 o -9 8 0 67.07 78.20 37.81 o -8 8 0 22.58 56.90 33.48 o -7 8 0 3.88 9.21 35.13 o -6 8 0 522.01 481.56 34.22 o -5 8 0 10.73 -16.55 34.20 o -4 8 0 41.99 45.55 38.85 o -3 8 0 19.69 19.07 40.87 o -2 8 0 570.92 497.73 48.13 o -1 8 0 127.82 96.59 37.17 o 0 8 0 411.88 480.73 38.92 o 1 8 0 12.83 -2.07 38.65 o 2 8 0 2692.27 2450.08 367.23 o 3 8 0 3508.92 3072.22 193.81 o 4 8 0 31.42 55.39 38.77 o 5 8 0 2381.73 2105.58 196.44 o 6 8 0 837.83 906.39 39.38 o 7 8 0 207.49 202.61 36.66 o 8 8 0 5.67 -20.26 34.53 o 9 8 0 17.80 29.60 40.01 o 10 8 0 4.95 18.05 41.66 o 11 8 0 32.79 28.72 39.44 o -9 9 0 24.67 13.88 32.13 o -8 9 0 180.77 121.81 28.95 o -7 9 0 181.43 146.45 29.85 o -6 9 0 162.32 137.89 36.47 o -5 9 0 1.56 25.64 34.06 o -4 9 0 979.98 878.00 206.60 o -3 9 0 1786.30 1433.15 267.01 o -2 9 0 513.42 429.90 41.46 o -1 9 0 1347.40 1278.72 236.98 o 0 9 0 354.81 352.24 34.89 o 1 9 0 279.09 294.24 34.91 o 2 9 0 776.01 745.40 34.10 o 3 9 0 14.45 2.17 37.44 o 4 9 0 408.53 421.55 40.19 o 5 9 0 0.40 51.93 38.41 o 6 9 0 212.17 206.93 41.27 o 7 9 0 33.37 133.36 36.10 o 8 9 0 901.26 907.66 47.07 o 9 9 0 572.59 524.51 33.53 o 10 9 0 298.18 397.05 35.00 o 11 9 0 81.72 133.51 35.15 o -9 10 0 38.62 -2.62 40.55 o -8 10 0 3.29 9.11 40.44 o -7 10 0 87.00 53.13 41.16 o -6 10 0 34.88 48.44 44.72 o -5 10 0 302.60 177.10 53.45 o -4 10 0 195.79 230.51 66.84 o -3 10 0 4.01 12.98 42.28 o -2 10 0 1.34 -18.30 42.67 o -1 10 0 22.55 24.24 33.03 o 0 10 0 213.64 185.74 32.98 o 1 10 0 114.91 139.39 33.30 o 2 10 0 690.52 608.10 42.17 o 3 10 0 1534.15 1498.62 160.14 o 4 10 0 1055.61 992.85 75.39 o 5 10 0 547.32 560.61 39.06 o 6 10 0 66.79 74.61 35.63 o 7 10 0 93.25 135.60 34.45 o 8 10 0 0.72 -27.71 42.20 o 9 10 0 4.08 105.09 46.36 o 10 10 0 160.88 148.91 30.15 o -8 11 0 0.10 6.97 39.49 o -7 11 0 13.48 -0.75 46.76 o -6 11 0 0.81 2.76 42.40 o -5 11 0 652.76 673.51 46.98 o -4 11 0 96.97 99.88 45.00 o -3 11 0 425.26 350.78 74.38 o -2 11 0 2036.89 1746.07 406.15 o -1 11 0 45.80 48.16 32.90 o 0 11 0 176.77 146.62 33.96 o 1 11 0 9.22 -39.54 39.54 o 2 11 0 17.28 60.74 37.55 o 3 11 0 211.54 256.86 39.93 o 4 11 0 152.02 205.26 45.79 o 5 11 0 0.23 -5.04 35.96 o 6 11 0 115.22 188.22 38.70 o 7 11 0 5.49 -17.99 33.23 o 8 11 0 19.97 33.15 49.58 o 9 11 0 59.53 41.09 32.96 o 10 11 0 1.42 -29.74 29.74 o -7 12 0 22.87 27.41 38.92 o -6 12 0 91.94 80.81 41.53 o -5 12 0 455.63 362.41 42.85 o -4 12 0 724.15 602.71 333.57 o -3 12 0 0.25 -16.91 67.65 o -2 12 0 298.50 285.86 52.90 o -1 12 0 298.29 299.65 47.25 o 0 12 0 128.47 150.94 40.48 o 1 12 0 494.91 439.12 41.05 o 2 12 0 1491.84 1472.91 216.39 o 3 12 0 2625.65 2514.74 44.72 o 4 12 0 1215.14 1233.09 116.95 o 5 12 0 310.57 426.12 150.65 o 6 12 0 257.39 286.13 37.96 o 7 12 0 2.87 -28.77 33.47 o 8 12 0 204.98 215.38 37.70 o 9 12 0 10.33 34.20 45.89 o 10 12 0 1.74 -2.00 41.02 o -7 13 0 102.43 61.35 39.04 o -6 13 0 6.37 9.62 38.25 o -5 13 0 0.61 3.06 37.70 o -4 13 0 53.82 14.67 45.32 o -3 13 0 102.08 91.35 48.75 o -2 13 0 238.42 96.16 55.35 o -1 13 0 225.40 177.54 61.26 o 0 13 0 3.04 17.12 38.28 o 1 13 0 1083.50 1196.17 43.13 o 2 13 0 145.98 178.85 37.54 o 3 13 0 26.86 64.06 36.14 o 4 13 0 107.06 135.04 35.86 o 5 13 0 5.62 44.25 58.65 o 6 13 0 0.20 -43.92 57.39 o 7 13 0 0.57 -27.61 31.40 o 8 13 0 13.81 -29.93 29.93 o 9 13 0 67.48 47.10 56.20 o -6 14 0 129.67 134.84 37.49 o -5 14 0 7.90 -0.08 37.39 o -1 14 0 130.82 146.96 66.01 o 0 14 0 57.58 50.05 41.69 o 1 14 0 197.21 195.05 39.06 o 2 14 0 791.77 778.98 39.89 o 3 14 0 292.35 334.64 36.37 o 4 14 0 125.90 122.40 34.77 o 5 14 0 134.60 94.46 37.77 o 6 14 0 64.21 66.98 33.47 o 7 14 0 470.66 396.90 39.92 o 8 14 0 417.81 385.25 31.40 o 0 15 0 458.47 438.85 106.98 o 1 15 0 166.85 142.19 37.99 o 2 15 0 71.07 110.65 36.42 o 3 15 0 65.18 94.44 35.86 o 4 15 0 28.95 32.88 33.45 o 5 15 0 116.76 154.61 33.06 o 6 15 0 35.42 32.33 36.17 o 7 15 0 7.35 1.80 32.65 o 0 16 0 0.07 -8.95 60.84 o 1 16 0 37.48 14.54 35.39 o 2 16 0 54.73 66.48 35.77 o 3 16 0 142.41 134.12 34.83 o 4 16 0 98.34 25.30 34.16 o 5 16 0 37.48 -15.10 32.95 o 6 16 0 10.35 37.87 32.07 o 0 17 0 43.92 49.59 64.04 o 1 17 0 143.56 151.72 64.04 o 2 17 0 118.55 101.23 36.11 o 3 17 0 7.34 44.42 35.42 o 4 17 0 27.92 72.41 45.36 o -3 -17 1 41.07 20.51 38.19 o -2 -17 1 24.10 -14.57 36.06 o -1 -17 1 13.43 15.02 38.52 o 0 -17 1 26.89 17.68 35.02 o -5 -16 1 110.77 140.31 32.96 o -4 -16 1 8.06 13.13 37.79 o -3 -16 1 3.73 16.67 36.51 o -2 -16 1 4.12 0.91 34.62 o -1 -16 1 59.22 79.87 35.00 o 0 -16 1 42.11 57.04 34.64 o 1 -16 1 1.14 1.12 59.53 o -7 -15 1 168.00 101.91 39.08 o -6 -15 1 321.51 337.43 32.83 o -5 -15 1 340.86 355.76 53.94 o -4 -15 1 136.05 142.38 33.46 o -3 -15 1 205.63 271.11 43.18 o -2 -15 1 1.40 0.69 35.36 o -1 -15 1 23.04 38.27 36.16 o 0 -15 1 111.86 132.69 36.02 o 1 -15 1 1.03 24.43 34.18 o 2 -15 1 21.53 30.49 46.43 o 3 -15 1 7.52 6.69 47.14 o 4 -15 1 123.39 44.69 37.89 o 5 -15 1 407.44 179.51 90.43 o -8 -14 1 7.78 30.67 60.10 o -7 -14 1 76.52 43.71 32.05 o -6 -14 1 6.79 47.08 31.83 o -5 -14 1 70.08 61.38 33.37 o -4 -14 1 4.77 24.26 37.34 o -3 -14 1 5.92 47.14 35.28 o -2 -14 1 329.26 280.47 44.10 o -1 -14 1 756.64 813.52 45.57 o 0 -14 1 758.52 738.23 114.69 o 1 -14 1 78.06 73.56 36.96 o 2 -14 1 225.93 223.24 43.76 o 3 -14 1 236.04 217.21 41.93 o 4 -14 1 8.94 -0.94 36.96 o 5 -14 1 4.89 16.06 37.42 o 6 -14 1 0.46 0.34 38.77 o -9 -13 1 49.18 94.78 29.06 o -8 -13 1 0.88 44.62 32.45 o -7 -13 1 19.84 61.06 39.00 o -6 -13 1 235.37 199.79 41.71 o -5 -13 1 51.92 128.70 63.54 o -4 -13 1 422.73 417.48 34.85 o -3 -13 1 536.17 560.16 39.58 o -2 -13 1 189.58 229.29 37.30 o -1 -13 1 436.27 417.07 61.62 o 0 -13 1 11.42 33.17 37.36 o 1 -13 1 147.59 129.25 37.17 o 2 -13 1 155.57 138.53 42.31 o 3 -13 1 540.82 540.71 44.68 o 4 -13 1 338.68 311.78 41.60 o 5 -13 1 353.71 219.04 60.34 o 6 -13 1 107.48 43.43 39.10 o 7 -13 1 82.41 57.49 40.25 o -9 -12 1 128.07 85.61 29.36 o -8 -12 1 26.07 121.43 29.83 o -7 -12 1 69.98 76.88 53.46 o -6 -12 1 92.13 142.20 32.14 o -5 -12 1 12.53 110.46 60.96 o -4 -12 1 315.96 313.86 67.38 o -3 -12 1 92.15 51.25 35.80 o -2 -12 1 72.10 114.34 41.70 o -1 -12 1 36.55 43.27 39.54 o 0 -12 1 437.99 470.64 44.62 o 1 -12 1 4.53 21.38 38.39 o 2 -12 1 5.66 -3.07 51.31 o 3 -12 1 131.60 103.00 49.21 o 4 -12 1 364.65 331.50 65.10 o 5 -12 1 421.63 393.54 50.50 o 6 -12 1 11.27 30.54 41.62 o 7 -12 1 157.41 151.59 40.25 o 8 -12 1 3.26 35.25 38.14 o -10 -11 1 30.62 -1.94 31.61 o -9 -11 1 4.51 -10.67 29.53 o -8 -11 1 148.15 198.25 38.88 o -7 -11 1 75.82 123.92 32.05 o -6 -11 1 1.33 -19.64 72.29 o -5 -11 1 321.00 364.86 36.33 o -4 -11 1 154.02 152.52 37.24 o -3 -11 1 14.79 -7.33 37.58 o -2 -11 1 106.34 155.30 37.42 o -1 -11 1 31.07 77.26 38.64 o 0 -11 1 512.01 549.08 41.80 o 1 -11 1 51.85 53.92 38.84 o 2 -11 1 17.75 13.22 71.26 o 3 -11 1 378.41 385.49 55.88 o 4 -11 1 260.08 237.28 54.08 o 5 -11 1 5.23 38.62 51.99 o 6 -11 1 11.73 46.33 41.24 o 7 -11 1 25.77 7.38 38.98 o 8 -11 1 3.81 12.85 45.32 o -10 -10 1 42.33 58.63 43.75 o -9 -10 1 140.11 99.10 30.15 o -8 -10 1 1148.77 1245.18 106.12 o -7 -10 1 655.04 584.70 105.87 o -6 -10 1 404.30 405.08 35.76 o -5 -10 1 226.54 244.61 43.67 o -4 -10 1 116.18 112.83 81.16 o -3 -10 1 205.52 221.98 42.28 o -2 -10 1 1063.54 983.32 40.17 o -1 -10 1 6.44 10.83 41.33 o 0 -10 1 1352.85 1374.68 226.52 o 1 -10 1 4.34 0.29 38.01 o 2 -10 1 45.65 41.94 48.17 o 3 -10 1 11.14 6.38 48.11 o 4 -10 1 188.91 247.86 48.91 o 5 -10 1 164.08 132.64 48.16 o 6 -10 1 34.55 72.71 44.72 o 7 -10 1 0.62 10.33 41.33 o 8 -10 1 19.36 25.27 39.61 o 9 -10 1 35.13 55.06 39.47 o -11 -9 1 9.80 12.04 29.31 o -10 -9 1 0.08 10.47 40.32 o -9 -9 1 93.98 121.22 44.05 o -8 -9 1 6.71 95.30 32.96 o -7 -9 1 353.29 376.53 34.93 o -6 -9 1 1300.19 1336.20 39.04 o -5 -9 1 1846.66 1740.66 40.44 o -4 -9 1 461.54 455.31 42.45 o -3 -9 1 63.36 54.39 46.14 o -2 -9 1 27.80 85.31 38.03 o -1 -9 1 753.21 783.54 41.08 o 0 -9 1 731.73 787.95 43.98 o 1 -9 1 73.13 39.35 51.37 o 2 -9 1 51.86 60.15 47.02 o 3 -9 1 310.93 391.49 48.79 o 4 -9 1 492.62 543.79 51.44 o 5 -9 1 271.68 215.98 51.51 o 6 -9 1 366.08 392.85 64.20 o 7 -9 1 9.14 -26.71 43.91 o 8 -9 1 44.69 79.59 45.24 o 9 -9 1 21.90 -8.55 33.88 o -11 -8 1 55.19 36.69 28.64 o -10 -8 1 261.36 290.14 30.26 o -9 -8 1 288.55 330.61 42.86 o -8 -8 1 664.30 605.24 44.87 o -7 -8 1 142.48 191.96 56.95 o -6 -8 1 528.91 551.80 41.53 o -5 -8 1 516.32 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